#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:20 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180896 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103677.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103677_Fobs loop_ _publ_author_name 'Yasui, Masanori' 'Ishikawa, Yoshimitsu' 'Akiyama, Naoya' 'Ishida, Takayuki' 'Nogami, Takashi' 'Iwasaki, Fujiko' _publ_section_title ; Dipyrimidine--copper(II) dinitrate complexes showing magnetic interactions ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 288 _journal_page_last 295 _journal_volume 57 _journal_year 2001 _space_group_IT_number 29 _symmetry_space_group_name_Hall 'P 2c -2ac' _symmetry_space_group_name_H-M 'P c a 21' _exptl_crystal_F_000 700.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file oa00341asup2.hkl _cod_data_source_block 1a #BEGIN Tags that were not found in dictionaries: _shelx_title 'Cu(II)(NO3)2(pm)3 (1a)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 162.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -18 775.54 975.19 24.85 o 2 0 -18 13.07 10.12 2.53 o 0 1 -18 42.42 46.46 4.00 o 1 1 -18 153.63 151.14 11.30 o 2 1 -18 9.61 6.56 4.89 o 3 1 -18 134.92 143.89 11.08 o 0 2 -18 193.18 223.59 12.03 o 1 2 -18 52.97 62.21 5.41 o 2 2 -18 1.58 2.80 1.93 o 2 0 -17 619.21 722.33 20.97 o 4 0 -17 36.75 41.22 3.89 o 1 1 -17 484.46 526.90 17.89 o 2 1 -17 81.24 90.63 8.31 o 3 1 -17 206.69 267.89 13.14 o 4 1 -17 34.66 39.01 3.73 o 5 1 -17 148.29 158.62 11.04 o 1 2 -17 70.62 74.93 5.37 o 2 2 -17 71.16 85.87 5.93 o 3 2 -17 52.82 79.13 7.72 o 4 2 -17 34.12 39.22 3.80 o 1 3 -17 21.11 24.35 2.41 o 2 3 -17 236.82 264.77 13.25 o 3 3 -17 111.63 134.37 9.97 o 4 3 -17 13.88 13.48 2.47 o 1 4 -17 202.88 224.98 12.78 o 2 4 -17 0.29 0.59 4.70 o 0 0 -16 1749.63 2009.76 32.59 o 2 0 -16 3.16 3.12 4.19 o 4 0 -16 1005.03 1048.20 24.71 o 6 0 -16 0.24 -2.52 3.88 o 0 1 -16 71.45 82.24 7.42 o 1 1 -16 480.93 514.39 17.00 o 2 1 -16 17.35 19.30 2.24 o 3 1 -16 323.62 333.37 14.16 o 4 1 -16 112.95 115.90 9.15 o 5 1 -16 212.11 207.48 11.97 o 6 1 -16 9.36 6.58 4.65 o 0 2 -16 336.67 348.84 14.08 o 1 2 -16 22.33 22.73 2.25 o 2 2 -16 14.26 16.07 2.20 o 3 2 -16 142.01 163.66 10.38 o 4 2 -16 343.81 367.60 15.30 o 5 2 -16 38.58 49.24 4.91 o 6 2 -16 24.91 25.14 2.51 o 0 3 -16 164.36 177.16 10.36 o 1 3 -16 64.92 67.70 5.00 o 2 3 -16 48.30 46.76 4.54 o 3 3 -16 20.09 20.76 2.29 o 4 3 -16 303.98 323.73 14.60 o 5 3 -16 6.01 9.44 2.09 o 0 4 -16 32.29 29.06 2.79 o 1 4 -16 20.96 19.70 2.41 o 2 4 -16 9.59 10.89 2.10 o 3 4 -16 109.34 119.25 9.36 o 4 4 -16 14.08 14.48 2.34 o 0 5 -16 265.75 291.32 13.78 o 1 5 -16 11.87 13.05 2.17 o 2 5 -16 32.29 36.71 3.16 o 3 5 -16 2.44 -1.87 4.67 o 2 0 -15 672.78 782.71 19.82 o 4 0 -15 128.43 131.73 8.99 o 6 0 -15 330.40 347.03 14.68 o 1 1 -15 390.13 419.77 14.76 o 2 1 -15 115.47 117.02 8.37 o 3 1 -15 147.49 168.71 10.19 o 4 1 -15 150.21 157.46 9.82 o 5 1 -15 452.52 471.14 16.59 o 6 1 -15 71.13 81.41 7.67 o 7 1 -15 87.12 99.06 8.60 o 1 2 -15 111.34 107.89 7.99 o 2 2 -15 237.23 245.80 11.52 o 3 2 -15 338.63 332.14 13.65 o 4 2 -15 36.77 44.38 3.69 o 5 2 -15 68.06 89.03 7.85 o 6 2 -15 223.34 244.97 12.47 o 7 2 -15 56.39 54.77 5.17 o 1 3 -15 214.63 213.01 10.95 o 2 3 -15 544.05 585.52 17.76 o 3 3 -15 204.59 216.05 11.31 o 4 3 -15 9.51 10.50 2.13 o 5 3 -15 26.65 29.55 2.88 o 6 3 -15 214.28 223.25 12.40 o 1 4 -15 579.54 591.86 18.07 o 2 4 -15 118.30 124.70 8.78 o 3 4 -15 212.77 202.67 11.61 o 4 4 -15 27.73 29.23 2.65 o 5 4 -15 242.23 265.10 13.50 o 6 4 -15 27.71 26.71 2.60 o 1 5 -15 17.73 15.41 2.26 o 2 5 -15 581.81 562.59 18.40 o 3 5 -15 10.57 8.59 2.10 o 4 5 -15 28.32 29.68 2.95 o 5 5 -15 22.40 23.21 2.50 o 1 6 -15 158.03 142.67 10.11 o 2 6 -15 61.29 54.60 4.96 o 3 6 -15 97.40 93.89 8.39 o 0 0 -14 765.88 812.56 18.81 o 2 0 -14 211.73 231.98 10.67 o 4 0 -14 301.11 318.66 12.72 o 6 0 -14 166.79 148.07 9.46 o 8 0 -14 336.27 364.08 14.99 o 0 1 -14 60.52 68.35 5.72 o 1 1 -14 460.98 494.73 15.04 o 2 1 -14 1.32 1.01 3.63 o 3 1 -14 586.45 615.96 17.19 o 4 1 -14 28.31 28.75 2.51 o 5 1 -14 333.12 341.15 13.62 o 6 1 -14 19.88 19.25 2.14 o 7 1 -14 369.44 403.74 15.33 o 8 1 -14 61.43 65.78 5.46 o 0 2 -14 1588.64 1724.77 27.97 o 1 2 -14 124.49 121.36 8.01 o 2 2 -14 2.99 -2.15 3.72 o 3 2 -14 116.37 124.10 8.60 o 4 2 -14 571.39 558.69 17.08 o 5 2 -14 140.71 142.07 9.24 o 6 2 -14 70.82 73.28 7.25 o 7 2 -14 118.34 121.49 8.81 o 8 2 -14 261.31 255.11 12.94 o 0 3 -14 814.30 829.40 19.67 o 1 3 -14 125.05 132.26 8.65 o 2 3 -14 64.09 64.25 4.76 o 3 3 -14 273.54 281.61 12.27 o 4 3 -14 570.02 593.44 17.93 o 5 3 -14 108.53 114.90 8.55 o 6 3 -14 67.64 63.67 4.96 o 7 3 -14 128.49 118.99 9.26 o 0 4 -14 37.47 38.11 3.74 o 1 4 -14 517.29 501.39 16.07 o 2 4 -14 19.55 19.18 2.23 o 3 4 -14 691.31 716.96 19.78 o 4 4 -14 13.88 17.39 2.15 o 5 4 -14 111.48 120.57 9.32 o 6 4 -14 1.06 0.42 4.03 o 7 4 -14 174.03 167.46 11.17 o 0 5 -14 1002.91 1005.63 22.88 o 1 5 -14 28.25 27.87 2.63 o 2 5 -14 1.38 -0.69 3.64 o 3 5 -14 54.55 47.44 3.67 o 4 5 -14 608.30 573.11 18.44 o 5 5 -14 0.87 -0.46 3.52 o 6 5 -14 7.60 5.55 5.18 o 0 6 -14 366.11 368.84 14.49 o 1 6 -14 168.45 157.14 9.79 o 2 6 -14 17.24 19.04 2.18 o 3 6 -14 181.08 176.15 10.70 o 4 6 -14 122.42 104.07 9.04 o 0 7 -14 168.13 155.08 10.33 o 1 7 -14 108.07 92.59 8.76 o 2 7 -14 17.83 17.01 2.28 o 2 0 -13 899.07 967.20 20.04 o 4 0 -13 100.38 107.02 7.47 o 6 0 -13 566.48 599.92 17.10 o 8 0 -13 57.15 62.28 4.92 o 1 1 -13 171.10 174.62 8.90 o 2 1 -13 379.34 399.66 13.20 o 3 1 -13 350.67 358.00 12.71 o 4 1 -13 52.36 55.63 4.14 o 5 1 -13 571.35 597.46 17.03 o 6 1 -13 199.82 165.80 9.67 o 7 1 -13 145.03 145.40 9.41 o 8 1 -13 16.15 15.25 2.13 o 9 1 -13 272.96 292.38 13.49 o 1 2 -13 440.54 455.81 14.22 o 2 2 -13 1270.18 1301.78 23.63 o 3 2 -13 134.50 127.95 8.13 o 4 2 -13 13.92 13.44 1.96 o 5 2 -13 177.40 162.84 9.50 o 6 2 -13 311.60 274.64 12.42 o 7 2 -13 222.57 213.35 11.19 o 8 2 -13 36.98 45.44 4.46 o 9 2 -13 76.58 87.62 8.18 o 1 3 -13 235.22 238.44 10.53 o 2 3 -13 904.97 868.62 19.81 o 3 3 -13 32.09 31.01 2.88 o 4 3 -13 0.52 0.23 3.70 o 5 3 -13 225.15 210.29 10.86 o 6 3 -13 494.09 487.68 16.35 o 7 3 -13 15.46 5.77 4.42 o 8 3 -13 51.53 54.94 4.72 o 1 4 -13 840.20 793.80 19.26 o 2 4 -13 113.47 129.30 8.55 o 3 4 -13 636.22 679.73 18.63 o 4 4 -13 9.07 8.37 1.89 o 5 4 -13 526.35 542.40 17.56 o 6 4 -13 64.86 52.47 4.59 o 7 4 -13 253.29 241.67 12.53 o 8 4 -13 67.40 72.13 5.29 o 1 5 -13 65.01 59.03 4.52 o 2 5 -13 1549.52 1415.65 26.46 o 3 5 -13 47.24 43.75 4.14 o 4 5 -13 21.50 13.46 2.22 o 5 5 -13 4.86 4.30 2.88 o 6 5 -13 469.08 429.19 17.16 o 7 5 -13 12.04 13.06 2.07 o 1 6 -13 372.68 357.40 13.89 o 2 6 -13 161.88 145.51 9.46 o 3 6 -13 190.30 178.87 10.19 o 4 6 -13 58.03 55.61 4.95 o 5 6 -13 211.86 205.78 11.76 o 6 6 -13 77.44 74.24 5.87 o 1 7 -13 81.25 78.73 7.36 o 2 7 -13 191.78 158.24 10.18 o 3 7 -13 63.81 52.48 4.93 o 4 7 -13 38.88 32.30 2.97 o 0 0 -12 509.83 496.39 13.42 o 2 0 -12 101.73 100.12 6.65 o 4 0 -12 1214.89 1181.29 21.71 o 6 0 -12 430.62 408.62 13.85 o 8 0 -12 1204.63 1239.68 25.15 o 0 1 -12 920.03 934.52 18.39 o 1 1 -12 638.71 691.47 15.84 o 2 1 -12 73.35 72.43 5.98 o 3 1 -12 1104.30 1116.99 20.99 o 4 1 -12 277.32 259.90 10.60 o 5 1 -12 303.55 300.19 11.58 o 6 1 -12 43.47 47.61 4.11 o 7 1 -12 705.24 694.91 18.42 o 8 1 -12 224.12 222.02 11.17 o 9 1 -12 238.08 271.36 12.81 o 0 2 -12 646.76 734.57 16.50 o 1 2 -12 1605.76 1622.50 24.76 o 2 2 -12 20.63 23.53 2.16 o 3 2 -12 240.48 232.37 10.11 o 4 2 -12 355.59 363.68 12.83 o 5 2 -12 653.38 614.67 16.59 o 6 2 -12 20.45 16.54 2.12 o 7 2 -12 323.19 321.83 12.97 o 8 2 -12 313.07 343.04 13.69 o 9 2 -12 33.15 34.17 3.02 o 0 3 -12 1745.61 1745.86 25.74 o 1 3 -12 71.77 58.83 5.81 o 2 3 -12 192.89 188.26 9.06 o 3 3 -12 120.49 132.87 8.09 o 4 3 -12 292.49 287.56 11.85 o 5 3 -12 94.76 103.94 7.58 o 6 3 -12 5.72 7.27 1.78 o 7 3 -12 114.87 97.19 7.79 o 8 3 -12 176.96 169.14 10.33 o 9 3 -12 1.01 -3.66 3.66 o 0 4 -12 53.53 56.77 5.44 o 1 4 -12 1086.01 1057.02 21.00 o 2 4 -12 86.84 81.82 6.86 o 3 4 -12 950.37 915.49 20.44 o 4 4 -12 96.19 92.16 7.22 o 5 4 -12 123.97 114.47 8.54 o 6 4 -12 27.91 30.74 2.97 o 7 4 -12 210.24 210.20 11.17 o 8 4 -12 5.07 4.22 1.74 o 0 5 -12 983.97 991.50 20.69 o 1 5 -12 146.77 145.91 8.39 o 2 5 -12 41.51 35.09 3.08 o 3 5 -12 42.25 35.26 3.14 o 4 5 -12 979.49 897.43 21.45 o 5 5 -12 96.56 80.20 7.84 o 6 5 -12 37.74 32.44 2.85 o 7 5 -12 78.15 82.14 7.85 o 8 5 -12 262.32 291.89 13.90 o 0 6 -12 173.00 186.05 9.69 o 1 6 -12 233.22 244.34 11.14 o 2 6 -12 44.55 40.24 3.29 o 3 6 -12 405.42 383.83 14.13 o 4 6 -12 179.62 149.00 9.30 o 5 6 -12 268.16 235.49 12.21 o 6 6 -12 2.47 3.62 3.86 o 7 6 -12 191.83 212.86 12.77 o 0 7 -12 476.86 478.03 15.91 o 1 7 -12 80.23 82.39 7.52 o 2 7 -12 0.30 2.81 3.56 o 3 7 -12 317.03 279.63 12.64 o 4 7 -12 258.58 219.19 11.85 o 5 7 -12 31.82 30.51 2.81 o 0 8 -12 507.78 503.82 16.94 o 1 8 -12 28.51 29.52 2.82 o 2 8 -12 2.02 6.01 4.14 o 3 8 -12 70.29 62.96 5.22 o 2 0 -11 3315.72 3166.00 32.60 o 4 0 -11 195.72 185.31 8.84 o 6 0 -11 2540.96 2358.10 30.88 o 8 0 -11 46.90 44.10 4.37 o 10 0 -11 441.67 473.84 16.71 o 1 1 -11 909.62 926.21 17.56 o 2 1 -11 689.43 709.12 15.77 o 3 1 -11 968.16 974.75 18.62 o 4 1 -11 79.36 72.41 5.71 o 5 1 -11 406.92 373.65 12.26 o 6 1 -11 571.53 574.42 15.48 o 7 1 -11 201.00 202.48 9.91 o 8 1 -11 26.92 24.91 2.34 o 9 1 -11 428.22 437.85 15.33 o 10 1 -11 9.88 3.83 4.03 o 1 2 -11 710.34 711.85 15.61 o 2 2 -11 1698.39 1745.82 24.77 o 3 2 -11 506.35 532.41 14.29 o 4 2 -11 2.19 -1.47 3.43 o 5 2 -11 517.76 505.96 14.51 o 6 2 -11 622.16 602.42 16.08 o 7 2 -11 292.32 283.35 11.78 o 8 2 -11 58.54 60.01 4.44 o 9 2 -11 64.65 62.16 4.79 o 10 2 -11 213.71 227.34 12.11 o 1 3 -11 450.90 464.34 13.07 o 2 3 -11 1151.80 1150.52 20.79 o 3 3 -11 47.47 47.40 3.62 o 4 3 -11 104.22 118.02 7.69 o 5 3 -11 218.64 194.93 9.66 o 6 3 -11 486.85 509.87 15.41 o 7 3 -11 4.96 -1.81 3.74 o 8 3 -11 74.13 68.20 6.44 o 9 3 -11 201.47 178.38 10.54 o 1 4 -11 342.49 336.70 11.43 o 2 4 -11 18.06 20.37 1.85 o 3 4 -11 714.37 654.72 16.71 o 4 4 -11 68.95 72.95 6.68 o 5 4 -11 596.64 577.88 16.95 o 6 4 -11 103.83 99.34 7.74 o 7 4 -11 352.24 359.58 13.77 o 8 4 -11 11.88 4.17 3.93 o 9 4 -11 273.30 264.92 12.82 o 1 5 -11 17.66 16.82 1.74 o 2 5 -11 781.43 744.13 17.62 o 3 5 -11 154.80 143.14 8.39 o 4 5 -11 498.42 422.86 14.37 o 5 5 -11 11.21 8.05 1.99 o 6 5 -11 657.82 604.38 18.71 o 7 5 -11 4.44 7.34 1.75 o 8 5 -11 78.66 83.14 7.62 o 1 6 -11 449.71 403.50 13.52 o 2 6 -11 310.75 248.89 10.85 o 3 6 -11 309.76 306.42 12.36 o 4 6 -11 17.45 14.66 1.98 o 5 6 -11 308.02 261.35 12.54 o 6 6 -11 137.28 113.85 8.90 o 7 6 -11 71.74 81.89 8.13 o 1 7 -11 277.75 279.43 11.96 o 2 7 -11 574.09 539.97 16.49 o 3 7 -11 176.82 183.32 10.09 o 4 7 -11 20.55 19.78 2.21 o 5 7 -11 117.35 101.57 8.06 o 6 7 -11 134.00 100.98 8.29 o 1 8 -11 208.58 193.76 10.67 o 2 8 -11 665.92 613.12 18.43 o 3 8 -11 142.60 115.04 8.68 o 4 8 -11 21.71 21.84 2.45 o 0 0 -10 2493.02 2412.68 26.27 o 2 0 -10 808.18 860.04 15.99 o 4 0 -10 3001.87 2830.48 30.37 o 6 0 -10 381.91 371.28 12.21 o 8 0 -10 580.64 563.85 15.93 o 10 0 -10 26.15 34.16 3.13 o 0 1 -10 87.81 88.47 5.52 o 1 1 -10 1223.03 1199.02 18.84 o 2 1 -10 452.77 479.27 12.23 o 3 1 -10 1377.50 1311.09 20.40 o 4 1 -10 309.47 307.19 10.40 o 5 1 -10 407.38 371.70 11.76 o 6 1 -10 150.52 142.69 7.74 o 7 1 -10 439.83 435.55 13.50 o 8 1 -10 114.62 125.23 8.20 o 9 1 -10 50.54 47.04 4.20 o 10 1 -10 54.96 45.58 4.33 o 0 2 -10 2081.80 2177.90 25.41 o 1 2 -10 386.81 417.00 11.48 o 2 2 -10 16.55 19.25 1.90 o 3 2 -10 1724.16 1732.25 24.19 o 4 2 -10 1896.20 1893.42 25.91 o 5 2 -10 115.97 104.28 6.99 o 6 2 -10 4.14 4.22 3.34 o 7 2 -10 687.65 702.70 17.14 o 8 2 -10 391.04 398.53 13.78 o 9 2 -10 28.37 34.09 2.98 o 10 2 -10 33.44 34.34 3.19 o 0 3 -10 1653.73 1639.44 22.54 o 1 3 -10 403.49 409.37 11.59 o 2 3 -10 123.65 128.73 7.05 o 3 3 -10 289.42 278.22 10.29 o 4 3 -10 967.64 976.19 19.45 o 5 3 -10 4.36 0.61 3.18 o 6 3 -10 60.48 66.05 5.97 o 7 3 -10 349.42 330.91 12.33 o 8 3 -10 513.47 522.55 15.93 o 9 3 -10 64.05 56.30 4.49 o 10 3 -10 70.76 77.60 7.64 o 0 4 -10 35.31 38.00 3.05 o 1 4 -10 1641.37 1625.05 23.45 o 2 4 -10 117.13 123.25 7.00 o 3 4 -10 1051.23 973.87 19.30 o 4 4 -10 12.35 14.19 1.76 o 5 4 -10 1622.38 1530.60 26.21 o 6 4 -10 132.05 124.27 8.40 o 7 4 -10 957.23 966.75 21.44 o 8 4 -10 53.16 56.77 4.66 o 9 4 -10 134.51 138.94 9.05 o 0 5 -10 906.63 936.18 18.34 o 1 5 -10 138.04 133.67 7.36 o 2 5 -10 134.39 141.86 7.62 o 3 5 -10 364.96 337.28 11.90 o 4 5 -10 1079.15 940.09 20.27 o 5 5 -10 16.44 15.70 1.88 o 6 5 -10 145.88 155.44 9.59 o 7 5 -10 15.80 16.92 2.11 o 8 5 -10 700.58 724.76 19.76 o 9 5 -10 18.13 19.88 2.18 o 0 6 -10 17.41 17.42 1.73 o 1 6 -10 606.97 555.97 15.08 o 2 6 -10 12.57 10.72 1.64 o 3 6 -10 232.04 211.80 10.15 o 4 6 -10 250.98 254.06 11.07 o 5 6 -10 196.96 176.94 9.73 o 6 6 -10 28.56 26.70 2.38 o 7 6 -10 323.72 351.79 14.39 o 8 6 -10 103.96 110.48 8.69 o 0 7 -10 1050.19 1035.67 21.46 o 1 7 -10 201.36 194.77 9.63 o 2 7 -10 10.34 10.70 1.78 o 3 7 -10 355.35 343.65 13.01 o 4 7 -10 425.05 416.97 14.55 o 5 7 -10 84.31 85.07 7.52 o 6 7 -10 83.57 78.91 5.29 o 7 7 -10 108.81 105.45 8.87 o 0 8 -10 631.70 650.44 18.07 o 1 8 -10 95.25 90.61 7.59 o 2 8 -10 26.31 22.63 2.27 o 3 8 -10 121.42 112.70 8.59 o 4 8 -10 286.30 272.20 12.43 o 5 8 -10 28.57 22.16 2.45 o 0 9 -10 5.32 -3.17 4.63 o 1 9 -10 283.97 257.43 12.59 o 2 9 -10 22.36 19.34 2.22 o 3 9 -10 208.21 181.99 10.70 o 2 0 -9 4145.16 3996.69 32.71 o 4 0 -9 627.06 593.61 13.21 o 6 0 -9 2644.62 2406.06 28.60 o 8 0 -9 50.70 46.49 3.82 o 10 0 -9 416.18 437.47 15.05 o 1 1 -9 2759.98 2802.48 27.20 o 2 1 -9 1012.28 1129.85 17.63 o 3 1 -9 1228.68 1217.41 18.65 o 4 1 -9 345.09 347.35 10.40 o 5 1 -9 647.51 596.32 13.89 o 6 1 -9 123.89 113.85 6.78 o 7 1 -9 678.96 648.70 15.70 o 8 1 -9 28.66 35.59 3.31 o 9 1 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584.57 562.66 14.01 o 3 5 -9 76.32 74.99 5.88 o 4 5 -9 45.15 34.42 2.80 o 5 5 -9 22.29 25.64 2.44 o 6 5 -9 1714.66 1695.19 28.36 o 7 5 -9 26.01 25.77 2.46 o 8 5 -9 33.69 34.27 3.17 o 9 5 -9 78.55 101.88 8.05 o 1 6 -9 242.95 252.50 10.00 o 2 6 -9 772.17 727.27 16.73 o 3 6 -9 227.00 213.15 9.66 o 4 6 -9 11.43 12.30 1.75 o 5 6 -9 451.67 392.24 13.71 o 6 6 -9 690.45 629.67 17.73 o 7 6 -9 113.35 123.09 8.47 o 8 6 -9 0.99 0.80 4.14 o 1 7 -9 495.52 494.82 14.70 o 2 7 -9 312.17 298.15 11.66 o 3 7 -9 516.48 456.40 14.53 o 4 7 -9 32.95 31.84 2.90 o 5 7 -9 233.33 226.43 10.83 o 6 7 -9 136.62 132.78 8.95 o 7 7 -9 173.64 173.77 11.12 o 1 8 -9 166.20 165.38 9.35 o 2 8 -9 1135.83 1077.00 22.85 o 3 8 -9 69.49 64.27 4.55 o 4 8 -9 0.92 3.26 2.56 o 5 8 -9 229.89 209.12 11.23 o 6 8 -9 364.79 346.43 14.43 o 1 9 -9 405.22 408.40 14.98 o 2 9 -9 9.49 3.74 4.87 o 3 9 -9 47.06 45.78 4.51 o 4 9 -9 6.71 5.92 2.00 o 0 0 -8 6197.78 6167.39 37.64 o 2 0 -8 82.42 86.07 4.92 o 4 0 -8 1907.33 1607.64 20.45 o 6 0 -8 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59.62 65.72 6.38 o 3 9 -5 507.94 491.10 15.91 o 4 9 -5 8.65 12.20 2.02 o 5 9 -5 608.53 629.47 18.91 o 6 9 -5 17.09 16.17 2.32 o 1 10 -5 57.03 65.09 6.33 o 2 10 -5 351.77 340.44 14.08 o 3 10 -5 0.58 1.65 3.28 o 4 10 -5 19.59 20.36 2.50 o 0 0 -4 3151.93 3347.54 19.39 o 2 0 -4 186.30 174.59 4.69 o 4 0 -4 10790.50 9539.65 41.60 o 6 0 -4 350.32 332.48 8.88 o 8 0 -4 2748.31 2561.64 28.24 o 10 0 -4 647.89 614.68 16.06 o 12 0 -4 377.95 358.85 14.24 o 0 1 -4 13589.51 14440.57 45.00 o 1 1 -4 3983.09 4121.38 23.12 o 2 1 -4 2577.96 2564.00 18.60 o 3 1 -4 7104.07 6342.37 31.37 o 4 1 -4 1519.33 1389.20 15.24 o 5 1 -4 2626.30 2317.93 21.41 o 6 1 -4 127.66 133.71 5.89 o 7 1 -4 1745.16 1589.92 20.80 o 8 1 -4 262.91 241.13 9.01 o 9 1 -4 1004.16 926.74 18.49 o 10 1 -4 121.32 119.56 7.54 o 11 1 -4 708.62 734.92 18.95 o 12 1 -4 157.20 175.80 10.16 o 0 2 -4 176.49 188.78 4.97 o 1 2 -4 1715.40 1752.34 15.29 o 2 2 -4 3261.71 3565.61 24.20 o 3 2 -4 1559.78 1527.73 15.69 o 4 2 -4 1783.02 1577.60 16.84 o 5 2 -4 2540.59 2359.01 22.29 o 6 2 -4 639.05 575.75 11.95 o 7 2 -4 830.41 768.64 14.81 o 8 2 -4 892.14 854.25 16.79 o 9 2 -4 24.04 21.46 2.03 o 10 2 -4 51.68 47.53 3.94 o 11 2 -4 280.09 280.26 12.04 o 12 2 -4 329.86 309.89 13.50 o 0 3 -4 7069.55 7185.89 34.03 o 1 3 -4 1946.96 2000.99 17.52 o 2 3 -4 233.32 305.37 7.16 o 3 3 -4 757.68 753.17 11.74 o 4 3 -4 3703.83 3756.86 28.43 o 5 3 -4 4.20 3.72 2.53 o 6 3 -4 430.24 423.32 10.92 o 7 3 -4 364.38 376.87 11.03 o 8 3 -4 859.05 890.14 17.74 o 9 3 -4 175.25 182.60 9.10 o 10 3 -4 84.92 84.12 7.14 o 11 3 -4 34.08 34.77 3.07 o 12 3 -4 371.85 399.84 15.57 o 0 4 -4 2694.07 2885.20 22.98 o 1 4 -4 4169.49 4262.23 28.46 o 2 4 -4 15.06 15.14 1.44 o 3 4 -4 1517.40 1485.17 18.03 o 4 4 -4 117.87 115.80 6.27 o 5 4 -4 1506.97 1545.73 21.26 o 6 4 -4 38.45 36.88 2.94 o 7 4 -4 492.32 539.19 13.89 o 8 4 -4 226.50 210.83 9.64 o 9 4 -4 59.43 65.27 6.02 o 10 4 -4 16.09 15.05 1.96 o 11 4 -4 391.85 425.76 15.26 o 0 5 -4 12702.84 13213.14 57.12 o 1 5 -4 167.84 173.44 6.67 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8.83 o 5 8 -3 7.81 11.57 1.85 o 6 8 -3 630.39 614.89 18.73 o 7 8 -3 22.61 25.42 2.57 o 8 8 -3 118.95 135.74 10.38 o 1 9 -3 656.12 678.75 17.40 o 2 9 -3 12.91 19.05 2.07 o 3 9 -3 264.55 265.57 11.87 o 4 9 -3 5.60 8.00 1.82 o 5 9 -3 560.50 589.03 18.09 o 6 9 -3 10.18 4.30 4.74 o 7 9 -3 154.74 146.11 10.68 o 1 10 -3 0.47 -3.88 3.88 o 2 10 -3 517.85 525.55 16.91 o 3 10 -3 1.72 0.95 4.22 o 4 10 -3 156.15 162.26 10.33 o 5 10 -3 106.72 104.42 8.88 o 0 0 -2 21782.22 23480.15 112.56 o 2 0 -2 14181.07 12380.95 36.27 o 4 0 -2 13314.02 12018.03 44.10 o 6 0 -2 1450.66 1367.49 16.95 o 8 0 -2 1643.30 1577.17 21.60 o 10 0 -2 372.41 366.70 12.51 o 12 0 -2 380.55 426.57 15.15 o 0 1 -2 1913.40 1940.85 11.17 o 1 1 -2 1730.55 1771.90 11.94 o 2 1 -2 1789.85 1547.33 11.66 o 3 1 -2 4497.76 3926.67 21.60 o 4 1 -2 49.60 44.07 2.86 o 5 1 -2 1838.70 1610.70 16.99 o 6 1 -2 44.06 44.68 3.62 o 7 1 -2 2263.43 2075.30 23.14 o 8 1 -2 9.22 13.81 1.49 o 9 1 -2 370.97 337.46 11.13 o 10 1 -2 89.50 84.43 6.53 o 11 1 -2 752.21 775.57 19.07 o 12 1 -2 62.56 63.65 4.78 o 0 2 -2 12362.77 13611.09 39.69 o 1 2 -2 16564.90 17954.25 48.72 o 2 2 -2 855.69 951.64 11.12 o 3 2 -2 493.93 467.15 8.19 o 4 2 -2 9095.23 8999.14 40.73 o 5 2 -2 1055.21 1077.70 14.63 o 6 2 -2 228.46 256.78 7.92 o 7 2 -2 326.63 335.43 9.74 o 8 2 -2 2229.43 2194.15 26.51 o 9 2 -2 469.17 453.63 13.27 o 10 2 -2 100.90 114.40 7.45 o 11 2 -2 300.85 306.54 12.56 o 12 2 -2 380.76 412.07 15.33 o 0 3 -2 6957.46 7351.47 31.59 o 1 3 -2 8183.71 8965.76 36.17 o 2 3 -2 3820.34 4034.49 25.06 o 3 3 -2 2596.11 2811.27 23.32 o 4 3 -2 5680.43 5760.01 35.35 o 5 3 -2 2212.40 2344.59 23.43 o 6 3 -2 302.02 295.16 9.14 o 7 3 -2 242.05 238.05 8.88 o 8 3 -2 1493.07 1555.78 23.20 o 9 3 -2 337.10 338.60 12.04 o 10 3 -2 132.87 152.27 8.52 o 11 3 -2 264.61 284.78 12.35 o 12 3 -2 219.29 227.50 12.03 o 0 4 -2 3228.75 3615.92 24.52 o 1 4 -2 3828.94 4138.01 26.80 o 2 4 -2 1087.05 1301.20 15.53 o 3 4 -2 2729.11 2778.98 24.75 o 4 4 -2 208.46 211.63 7.66 o 5 4 -2 1660.14 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3.51 o 1 1 -1 7174.83 7867.92 25.20 o 2 1 -1 1248.48 1233.20 10.08 o 3 1 -1 1955.67 1780.50 14.09 o 4 1 -1 1949.47 1961.35 16.75 o 5 1 -1 5721.11 5438.50 31.72 o 6 1 -1 102.58 96.85 4.85 o 7 1 -1 544.33 544.75 11.94 o 8 1 -1 51.33 59.82 4.71 o 9 1 -1 504.06 505.62 13.45 o 10 1 -1 448.73 422.74 13.10 o 11 1 -1 9.07 10.38 1.71 o 12 1 -1 2.97 0.63 3.74 o 1 2 -1 8267.83 9016.44 31.18 o 2 2 -1 1986.89 1959.34 15.59 o 3 2 -1 3882.63 4024.70 24.22 o 4 2 -1 329.97 354.78 7.73 o 5 2 -1 2387.94 2359.74 21.67 o 6 2 -1 1814.21 1668.02 19.75 o 7 2 -1 793.73 805.71 14.84 o 8 2 -1 18.23 27.65 2.69 o 9 2 -1 555.65 572.72 14.73 o 10 2 -1 587.74 617.78 16.32 o 11 2 -1 140.22 156.97 9.25 o 12 2 -1 121.09 128.11 8.86 o 1 3 -1 3126.67 3425.06 21.13 o 2 3 -1 5668.31 5739.59 30.31 o 3 3 -1 3519.53 3756.09 26.67 o 4 3 -1 99.13 105.60 5.01 o 5 3 -1 316.62 300.48 8.47 o 6 3 -1 3608.85 3565.75 30.94 o 7 3 -1 1083.86 1102.46 18.40 o 8 3 -1 3.77 5.64 1.45 o 9 3 -1 433.30 442.99 13.37 o 10 3 -1 700.95 736.64 18.31 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22.59 o 10 0 0 107.04 107.61 7.03 o 12 0 0 355.17 428.15 15.24 o 0 1 0 2461.81 2871.41 11.23 o 1 1 0 11663.49 12426.81 82.02 o 2 1 0 1535.16 1666.62 11.78 o 3 1 0 2879.84 2871.23 18.12 o 4 1 0 1317.48 1172.31 12.98 o 5 1 0 1997.21 1890.42 18.40 o 6 1 0 513.79 478.06 10.28 o 7 1 0 2062.66 2000.15 22.72 o 8 1 0 527.35 498.63 12.35 o 9 1 0 246.58 227.19 9.28 o 10 1 0 30.28 31.73 2.72 o 11 1 0 292.42 313.40 12.21 o 12 1 0 45.07 52.44 4.41 o 0 2 0 3173.70 3381.30 16.77 o 1 2 0 115.01 111.03 3.39 o 2 2 0 222.61 279.70 5.89 o 3 2 0 1438.98 1371.90 13.93 o 4 2 0 3575.58 3769.85 25.42 o 5 2 0 15.14 22.19 1.97 o 6 2 0 20.98 20.85 1.76 o 7 2 0 1416.16 1418.07 19.73 o 8 2 0 2496.38 2430.37 27.88 o 9 2 0 1232.98 1237.60 21.28 o 10 2 0 72.88 80.27 6.52 o 11 2 0 368.44 365.30 13.59 o 12 2 0 331.15 363.00 14.65 o 0 3 0 45.95 60.20 2.94 o 1 3 0 439.74 591.93 8.73 o 2 3 0 509.05 560.68 9.28 o 3 3 0 125.64 152.45 5.53 o 4 3 0 1088.76 1023.70 14.56 o 5 3 0 2228.14 2353.70 23.47 o 6 3 0 1748.57 1727.34 21.45 o 7 3 0 310.29 281.10 9.58 o 8 3 0 1747.55 1833.77 25.24 o 9 3 0 255.83 272.62 10.80 o 10 3 0 38.53 40.24 3.75 o 11 3 0 351.98 330.59 13.54 o 12 3 0 105.51 111.10 8.88 o 0 4 0 221.45 228.41 6.11 o 1 4 0 667.96 664.03 10.60 o 2 4 0 365.43 478.57 9.56 o 3 4 0 1994.03 2170.71 21.80 o 4 4 0 223.87 206.85 7.46 o 5 4 0 505.30 472.42 11.70 o 6 4 0 189.49 211.27 8.31 o 7 4 0 1077.15 1152.31 20.02 o 8 4 0 66.89 70.84 5.97 o 9 4 0 250.85 265.89 11.14 o 10 4 0 33.90 31.11 2.74 o 11 4 0 273.97 300.70 13.14 o 12 4 0 77.62 85.75 8.39 o 0 5 0 2106.09 2260.72 21.57 o 1 5 0 761.39 807.10 13.11 o 2 5 0 52.59 60.26 4.23 o 3 5 0 1742.78 1955.18 22.46 o 4 5 0 1308.01 1313.24 19.49 o 5 5 0 116.58 115.10 6.62 o 6 5 0 625.81 607.97 15.03 o 7 5 0 35.44 38.56 3.52 o 8 5 0 754.14 817.05 18.99 o 9 5 0 44.49 50.79 4.38 o 10 5 0 598.13 619.40 18.79 o 11 5 0 0.91 0.71 4.10 o 0 6 0 687.88 710.97 13.48 o 1 6 0 799.85 772.37 14.30 o 2 6 0 389.10 423.24 11.06 o 3 6 0 2946.13 3107.36 30.94 o 4 6 0 469.57 438.95 12.43 o 5 6 0 797.17 816.12 17.52 o 6 6 0 53.96 68.50 6.43 o 7 6 0 984.67 964.65 20.98 o 8 6 0 521.05 512.19 16.17 o 9 6 0 151.00 171.87 10.26 o 10 6 0 276.87 279.00 13.42 o 0 7 0 514.72 543.51 13.08 o 1 7 0 484.09 522.53 13.04 o 2 7 0 0.82 -0.12 3.27 o 3 7 0 203.13 197.40 8.89 o 4 7 0 1202.54 1247.89 22.23 o 5 7 0 448.08 447.24 14.21 o 6 7 0 1.27 -3.58 3.83 o 7 7 0 571.40 565.76 17.38 o 8 7 0 359.74 393.09 15.12 o 9 7 0 134.22 138.97 9.64 o 10 7 0 0.18 5.20 4.48 o 0 8 0 2824.49 2934.50 33.10 o 1 8 0 20.70 20.35 1.96 o 2 8 0 326.25 305.04 11.43 o 3 8 0 167.25 168.83 8.86 o 4 8 0 1631.97 1651.41 27.12 o 5 8 0 0.71 0.10 3.80 o 6 8 0 1.08 3.22 4.58 o 7 8 0 21.19 17.43 2.41 o 8 8 0 416.38 398.45 16.26 o 0 9 0 177.64 180.51 9.76 o 1 9 0 1754.24 1782.92 28.29 o 2 9 0 52.57 42.36 4.17 o 3 9 0 1139.32 1147.37 23.57 o 4 9 0 54.80 50.79 4.51 o 5 9 0 945.63 964.25 23.39 o 6 9 0 17.49 20.65 2.41 o 7 9 0 180.28 171.18 11.00 o 0 10 0 1091.25 1103.80 23.90 o 1 10 0 31.53 34.41 3.13 o 2 10 0 12.08 18.93 2.41 o 3 10 0 74.60 61.47 5.02 o 4 10 0 564.97 574.58 18.80 o 5 10 0 0.55 4.60 4.73 o 0 11 0 33.23 34.87 3.01 o 1 11 0 214.53 208.56 11.95 o