#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:20 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180896 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103680.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103680_Fobs loop_ _publ_author_name 'Yasui, Masanori' 'Ishikawa, Yoshimitsu' 'Akiyama, Naoya' 'Ishida, Takayuki' 'Nogami, Takashi' 'Iwasaki, Fujiko' _publ_section_title ; Dipyrimidine--copper(II) dinitrate complexes showing magnetic interactions ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 288 _journal_page_last 295 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _exptl_crystal_F_000 390.00 _reflns_d_resolution_high 0.7845 _cod_data_source_file oa00343sup5.hkl _cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title 'Cu(II)(H2O)2(NO3)2(pm)2 (3)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 140.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 19722.54 17134.15 103.96 o 4 0 0 1134.79 1045.58 13.47 o 6 0 0 1199.75 1261.37 18.57 o 8 0 0 213.92 247.52 10.32 o 1 1 0 1178.90 1097.15 9.03 o 2 1 0 1126.32 1048.22 10.43 o 3 1 0 1830.96 1724.60 16.52 o 4 1 0 351.00 357.85 7.60 o 5 1 0 522.37 510.88 10.31 o 6 1 0 4.69 3.96 3.56 o 7 1 0 275.43 287.98 9.92 o 8 1 0 6.01 8.33 1.97 o 0 2 0 5211.20 8532.20 66.37 o 1 2 0 291.61 274.33 3.78 o 2 2 0 572.33 511.65 7.08 o 3 2 0 93.33 96.81 3.81 o 4 2 0 988.00 947.48 12.98 o 5 2 0 0.26 0.75 2.73 o 6 2 0 840.68 925.26 15.78 o 7 2 0 8.86 6.48 1.86 o 8 2 0 65.63 101.35 7.08 o 1 3 0 6.95 27.35 1.63 o 2 3 0 3411.57 3510.33 26.24 o 3 3 0 1984.15 2012.42 19.37 o 4 3 0 85.87 89.57 4.49 o 5 3 0 389.20 404.23 9.46 o 6 3 0 64.68 63.51 5.00 o 7 3 0 112.23 119.65 7.25 o 8 3 0 0.57 4.56 1.88 o 0 4 0 4191.02 5079.95 33.78 o 1 4 0 2.16 3.92 0.63 o 2 4 0 240.17 170.34 4.13 o 3 4 0 105.72 97.82 3.88 o 4 4 0 10.40 6.39 1.24 o 5 4 0 221.63 237.37 7.71 o 6 4 0 166.99 182.89 7.70 o 7 4 0 65.59 69.74 6.03 o 8 4 0 89.65 104.21 7.38 o 1 5 0 11.07 8.75 0.81 o 2 5 0 593.33 612.23 8.46 o 3 5 0 2881.41 2792.32 24.49 o 4 5 0 8.12 8.86 1.11 o 5 5 0 569.96 626.43 12.56 o 6 5 0 32.55 35.53 3.44 o 7 5 0 132.87 140.92 7.65 o 0 6 0 1851.39 2238.96 19.00 o 1 6 0 80.57 77.86 3.46 o 2 6 0 1657.59 1452.94 15.02 o 3 6 0 2.39 0.33 2.25 o 4 6 0 730.55 737.04 12.33 o 5 6 0 1.63 4.05 3.39 o 6 6 0 176.95 207.35 8.63 o 7 6 0 0.88 1.56 4.03 o 1 7 0 447.28 449.82 8.08 o 2 7 0 211.36 216.79 5.72 o 3 7 0 2119.94 2014.63 20.55 o 4 7 0 10.40 6.84 1.37 o 5 7 0 471.79 494.23 11.66 o 6 7 0 68.87 67.33 5.89 o 7 7 0 67.05 92.03 7.05 o 0 8 0 2352.07 3029.16 25.91 o 1 8 0 789.49 984.25 12.66 o 2 8 0 2291.36 2388.94 22.74 o 3 8 0 168.67 171.61 6.00 o 4 8 0 995.49 930.27 14.40 o 5 8 0 30.97 30.06 2.60 o 6 8 0 199.78 160.68 7.37 o 7 8 0 8.55 10.29 2.23 o 1 9 0 1228.45 1530.49 17.29 o 2 9 0 18.27 -6.91 6.91 o 3 9 0 2691.79 2712.90 26.76 o 4 9 0 5.98 3.87 3.10 o 5 9 0 1116.17 1067.54 17.48 o 6 9 0 14.29 18.14 1.99 o 7 9 0 169.68 134.52 8.02 o 0 10 0 2694.30 3394.43 30.40 o 1 10 0 62.43 67.62 4.46 o 2 10 0 1205.37 1338.21 17.23 o 3 10 0 24.67 -9.45 9.45 o 4 10 0 141.43 130.69 6.37 o 5 10 0 66.42 70.18 6.96 o 6 10 0 106.54 109.31 6.97 o 1 11 0 2676.40 3486.04 32.36 o 2 11 0 71.68 94.66 5.24 o 3 11 0 652.09 596.60 13.47 o 4 11 0 17.46 5.89 3.96 o 5 11 0 340.96 325.69 10.33 o 6 11 0 2.56 -5.90 5.90 o 0 12 0 13.11 14.97 1.44 o 1 12 0 343.01 423.25 10.18 o 2 12 0 8.55 9.94 1.50 o 3 12 0 214.10 209.76 7.90 o 4 12 0 17.85 15.58 1.84 o 5 12 0 6.61 -8.09 8.09 o 6 12 0 104.92 104.38 7.18 o 1 13 0 23.04 24.37 2.31 o 2 13 0 156.86 176.96 7.34 o 3 13 0 91.27 93.67 5.92 o 4 13 0 9.49 9.66 1.76 o 5 13 0 284.33 285.34 10.57 o 0 14 0 1108.77 1424.98 20.91 o 1 14 0 12.10 12.14 1.80 o 2 14 0 427.29 538.71 13.01 o 3 14 0 13.84 13.04 1.84 o 4 14 0 54.74 49.82 3.72 o 5 14 0 9.72 13.73 2.02 o 1 15 0 643.78 810.34 16.23 o 2 15 0 10.66 7.35 1.93 o 3 15 0 120.97 140.98 7.62 o 4 15 0 16.38 17.01 2.15 o 0 16 0 520.38 654.46 15.29 o 1 16 0 0.33 -4.29 4.29 o 2 16 0 498.68 591.88 14.94 o 3 16 0 1.62 1.99 3.99 o 1 17 0 318.88 393.40 12.59 o 2 17 0 63.61 71.37 4.91 o -8 0 1 127.63 136.37 7.93 o -6 0 1 344.78 347.56 9.76 o -4 0 1 634.40 638.29 10.18 o -2 0 1 250.04 236.86 4.38 o 0 0 1 6835.50 6483.16 190.40 o 2 0 1 2714.66 2750.53 22.10 o 4 0 1 67.64 64.55 3.89 o 6 0 1 207.99 218.19 7.97 o -8 1 1 0.10 -4.03 4.03 o -7 1 1 648.62 728.80 15.45 o -6 1 1 54.41 57.73 4.83 o -5 1 1 754.36 805.36 13.11 o -4 1 1 51.50 53.55 3.68 o -3 1 1 19.94 10.14 0.97 o -2 1 1 2638.46 2559.60 19.26 o -1 1 1 4653.14 4632.53 29.58 o 0 1 1 1108.81 1251.33 183.01 o 1 1 1 5588.32 4613.30 30.68 o 2 1 1 17.50 20.89 1.52 o 3 1 1 1539.27 1472.00 15.89 o 4 1 1 122.02 118.01 4.97 o 5 1 1 512.53 501.73 10.59 o 6 1 1 8.95 11.13 1.75 o 7 1 1 76.22 89.34 6.56 o -8 2 1 9.09 13.17 2.12 o -7 2 1 39.82 47.67 3.97 o -6 2 1 301.79 464.89 11.07 o -5 2 1 1384.18 1505.41 18.92 o -4 2 1 5751.43 6277.58 46.82 o -3 2 1 4522.85 4493.43 33.31 o -2 2 1 5722.00 5561.92 37.08 o -1 2 1 3061.92 3162.99 21.65 o 0 2 1 2574.14 3300.90 208.59 o 1 2 1 3386.93 3533.99 24.80 o 2 2 1 1650.15 1425.03 13.78 o 3 2 1 559.41 581.60 9.52 o 4 2 1 472.60 472.67 9.43 o 5 2 1 12.22 12.78 1.49 o 6 2 1 650.93 657.07 13.54 o 7 2 1 0.70 4.37 3.79 o -8 3 1 0.04 6.12 4.24 o -7 3 1 815.81 942.00 17.96 o -6 3 1 23.94 19.96 1.96 o -5 3 1 1254.41 1324.26 17.80 o -4 3 1 260.72 268.94 6.72 o -3 3 1 799.19 614.42 8.57 o -2 3 1 916.61 837.05 9.10 o -1 3 1 2770.03 3410.36 24.31 o 0 3 1 3898.84 5098.92 24.01 o 1 3 1 2467.34 3094.05 23.35 o 2 3 1 396.18 401.93 6.65 o 3 3 1 2159.55 1971.24 19.68 o 4 3 1 8.88 7.98 1.29 o 5 3 1 711.72 726.30 13.19 o 6 3 1 206.42 216.00 8.07 o 7 3 1 66.82 69.04 5.83 o -8 4 1 91.24 111.71 7.61 o -7 4 1 8.00 9.91 1.98 o -6 4 1 87.48 110.44 6.29 o -5 4 1 138.75 149.62 6.11 o -4 4 1 818.63 712.47 10.73 o -3 4 1 0.13 0.82 1.63 o -2 4 1 1124.44 1163.41 12.24 o -1 4 1 28.32 36.41 2.18 o 0 4 1 1626.61 1991.58 102.78 o 1 4 1 1592.33 1971.35 17.41 o 2 4 1 2041.31 2247.84 20.18 o 3 4 1 285.67 254.79 6.20 o 4 4 1 430.57 422.75 9.55 o 5 4 1 10.62 11.79 1.57 o 6 4 1 360.92 352.60 10.58 o 7 4 1 0.47 -0.74 3.68 o -8 5 1 5.45 3.54 4.35 o -7 5 1 385.43 433.61 12.49 o -6 5 1 160.58 200.12 7.88 o -5 5 1 331.11 280.95 7.63 o -4 5 1 58.57 56.26 3.58 o -3 5 1 1483.34 1374.28 15.18 o -2 5 1 26.04 42.71 2.87 o -1 5 1 2593.19 2920.71 23.01 o 0 5 1 189.16 214.61 14.15 o 1 5 1 125.61 95.84 3.67 o 2 5 1 94.58 99.66 4.14 o 3 5 1 610.41 549.61 9.50 o 4 5 1 26.24 36.60 3.42 o 5 5 1 239.73 259.12 8.66 o 6 5 1 52.22 51.54 5.13 o 7 5 1 3.40 -0.11 4.05 o -8 6 1 135.19 166.58 9.07 o -7 6 1 7.41 12.84 1.95 o -6 6 1 130.45 124.51 6.23 o -5 6 1 57.93 54.03 4.05 o -4 6 1 2010.78 1728.70 19.24 o -3 6 1 211.60 240.77 6.39 o -2 6 1 4792.57 5409.89 39.83 o -1 6 1 1489.14 1978.08 17.94 o 0 6 1 536.99 670.72 57.41 o 1 6 1 754.53 1091.95 12.99 o 2 6 1 275.15 244.54 6.40 o 3 6 1 163.95 203.65 6.59 o 4 6 1 417.79 346.41 8.47 o 5 6 1 14.90 12.26 1.64 o 6 6 1 131.23 123.61 7.28 o 7 6 1 17.74 21.06 2.31 o -8 7 1 0.44 -2.87 4.63 o -7 7 1 177.51 175.92 8.40 o -6 7 1 158.54 160.73 6.95 o -5 7 1 124.60 105.01 5.31 o -4 7 1 237.64 238.61 7.35 o -3 7 1 431.12 422.50 8.67 o -2 7 1 2.69 -1.39 2.24 o -1 7 1 1243.37 1392.09 14.82 o 0 7 1 628.17 837.55 68.92 o 1 7 1 2031.83 2734.72 24.62 o 2 7 1 190.63 220.83 6.35 o 3 7 1 3046.60 3365.43 31.54 o 4 7 1 65.15 85.28 5.32 o 5 7 1 1049.84 910.53 15.67 o 6 7 1 15.35 15.19 2.00 o 7 7 1 135.14 138.54 8.46 o -7 8 1 0.26 -1.89 3.38 o -6 8 1 341.98 312.44 9.65 o -5 8 1 13.71 19.41 1.85 o -4 8 1 2081.18 2133.60 24.13 o -3 8 1 80.11 102.76 4.79 o -2 8 1 3631.32 4081.90 33.44 o -1 8 1 490.28 565.89 9.20 o 0 8 1 966.66 1143.53 85.57 o 1 8 1 145.65 204.30 6.11 o 2 8 1 638.83 683.42 11.62 o 3 8 1 46.39 44.57 4.42 o 4 8 1 732.66 793.12 14.73 o 5 8 1 98.41 97.92 6.90 o 6 8 1 189.22 155.69 7.61 o 7 8 1 16.35 10.18 2.60 o -7 9 1 74.73 69.41 5.86 o -6 9 1 7.53 1.21 3.70 o -5 9 1 265.10 254.84 8.93 o -4 9 1 304.71 311.91 8.91 o -3 9 1 1149.14 1175.28 16.05 o -2 9 1 37.79 38.04 3.67 o -1 9 1 1169.17 1241.53 15.17 o 0 9 1 65.92 74.81 5.19 o 1 9 1 762.91 947.06 13.69 o 2 9 1 45.27 48.11 4.23 o 3 9 1 957.93 1097.89 16.73 o 4 9 1 11.34 13.21 1.79 o 5 9 1 408.73 469.76 12.80 o 6 9 1 15.51 17.78 2.14 o -7 10 1 118.92 114.76 7.64 o -6 10 1 144.58 145.35 7.95 o -5 10 1 340.99 350.90 10.77 o -4 10 1 193.37 207.11 7.43 o -3 10 1 61.84 66.87 4.54 o -2 10 1 840.72 1004.76 14.48 o -1 10 1 142.70 165.70 5.79 o 0 10 1 1354.18 1674.13 92.49 o 1 10 1 61.83 85.59 4.88 o 2 10 1 613.46 659.78 12.34 o 3 10 1 0.10 -6.30 6.30 o 4 10 1 187.39 212.93 8.46 o 5 10 1 41.69 35.55 2.92 o 6 10 1 69.60 78.64 6.91 o -6 11 1 1.70 -5.76 5.76 o -5 11 1 219.07 193.70 8.24 o -4 11 1 30.66 -6.36 6.36 o -3 11 1 26.33 28.95 2.57 o -2 11 1 1048.25 1148.97 16.36 o -1 11 1 428.84 505.33 10.34 o 0 11 1 592.71 724.03 33.17 o 1 11 1 1732.86 2273.54 24.78 o 2 11 1 1.92 4.74 3.59 o 3 11 1 421.90 429.28 11.78 o 4 11 1 1.73 -5.74 5.74 o 5 11 1 61.27 65.12 4.61 o 6 11 1 0.01 -9.18 9.18 o -6 12 1 344.83 334.82 12.04 o -5 12 1 0.49 -6.15 6.15 o -4 12 1 687.46 674.60 14.04 o -3 12 1 3.22 2.00 3.37 o -2 12 1 909.23 1024.12 16.06 o -1 12 1 145.87 185.10 6.82 o 0 12 1 859.82 1078.83 48.15 o 1 12 1 10.17 8.70 1.55 o 2 12 1 421.63 501.83 11.73 o 3 12 1 133.10 117.02 7.59 o 4 12 1 271.18 281.42 10.17 o 5 12 1 3.18 -7.85 7.85 o -6 13 1 8.51 -5.43 5.43 o -5 13 1 549.79 515.19 13.76 o -4 13 1 6.26 8.21 1.77 o -3 13 1 579.60 617.63 13.38 o -2 13 1 3.32 3.11 1.56 o -1 13 1 385.64 441.57 10.95 o 0 13 1 3.99 2.04 2.14 o 1 13 1 608.12 767.24 14.61 o 2 13 1 54.41 62.58 5.44 o 3 13 1 305.01 326.09 10.52 o 4 13 1 24.07 25.78 2.52 o 5 13 1 182.18 218.05 10.16 o -5 14 1 0.11 -0.98 3.80 o -4 14 1 149.76 144.10 7.57 o -3 14 1 253.18 274.86 9.55 o -2 14 1 195.48 203.47 8.12 o -1 14 1 804.00 924.66 16.67 o 0 14 1 600.48 728.20 27.78 o 1 14 1 186.64 243.82 8.95 o 2 14 1 311.32 390.17 11.33 o 3 14 1 0.43 1.60 4.11 o 4 14 1 78.24 79.94 6.48 o -4 15 1 29.50 29.08 2.78 o -3 15 1 37.95 38.76 3.49 o -2 15 1 10.14 4.10 4.12 o -1 15 1 220.88 258.83 9.55 o 0 15 1 0.17 -8.72 11.53 o 1 15 1 684.90 797.36 16.27 o 2 15 1 12.15 14.57 1.91 o 3 15 1 153.59 155.30 8.13 o 4 15 1 0.69 -4.38 4.38 o -4 16 1 278.79 287.15 11.00 o -3 16 1 0.00 -2.67 3.87 o -2 16 1 526.38 559.77 14.47 o -1 16 1 42.77 41.71 3.81 o 0 16 1 329.87 384.99 8.47 o 1 16 1 27.07 39.42 3.75 o 2 16 1 93.53 109.57 7.30 o 3 16 1 4.55 7.19 2.02 o -2 17 1 6.39 6.52 4.59 o -1 17 1 263.90 318.67 11.63 o 0 17 1 34.89 35.83 8.30 o 1 17 1 253.55 295.05 11.05 o 2 17 1 0.00 -4.18 4.18 o -8 0 2 83.70 92.16 6.88 o -6 0 2 299.17 311.61 9.03 o -4 0 2 131.13 126.27 4.61 o -2 0 2 1731.55 1643.29 14.11 o 0 0 2 850.73 964.57 34.93 o 2 0 2 2052.45 1987.54 18.95 o 4 0 2 394.86 362.38 8.93 o 6 0 2 31.04 30.94 3.06 o -8 1 2 2.78 -1.39 4.03 o -7 1 2 127.88 155.15 7.52 o -6 1 2 218.50 232.94 7.97 o -5 1 2 1239.36 1344.33 17.19 o -4 1 2 516.02 562.02 9.44 o -3 1 2 487.74 362.39 6.30 o -2 1 2 8.54 8.44 0.76 o -1 1 2 6846.44 7899.77 50.04 o 0 1 2 7.82 5.04 1.38 o 1 1 2 15292.02 12697.75 79.57 o 2 1 2 40.85 44.82 2.96 o 3 1 2 1278.58 1299.66 16.05 o 4 1 2 4.07 7.29 1.42 o 5 1 2 538.17 532.80 12.22 o 6 1 2 5.14 7.79 1.75 o 7 1 2 309.29 331.17 11.64 o -8 2 2 60.77 88.46 6.63 o -7 2 2 68.80 76.66 5.89 o -6 2 2 160.66 175.45 7.01 o -5 2 2 2.32 5.00 1.24 o -4 2 2 1766.51 1691.53 17.65 o -3 2 2 776.05 758.00 9.53 o -2 2 2 1852.78 1779.51 15.27 o -1 2 2 465.81 459.86 6.05 o 0 2 2 339.02 386.39 4.04 o 1 2 2 176.42 166.37 4.17 o 2 2 2 639.15 535.45 8.39 o 3 2 2 0.94 2.55 1.06 o 4 2 2 780.90 778.72 13.56 o 5 2 2 39.38 37.15 3.25 o 6 2 2 133.92 150.48 7.67 o 7 2 2 10.40 11.10 2.06 o -8 3 2 10.88 9.08 2.22 o -7 3 2 459.31 541.41 13.20 o -6 3 2 19.08 24.56 2.27 o -5 3 2 1815.11 1823.19 20.50 o -4 3 2 834.62 825.23 11.34 o -3 3 2 901.26 685.73 9.23 o -2 3 2 948.61 938.14 10.21 o -1 3 2 1779.44 1749.72 15.10 o 0 3 2 243.32 261.82 14.80 o 1 3 2 2385.88 2370.71 19.89 o 2 3 2 132.34 132.11 4.26 o 3 3 2 96.84 73.93 3.95 o 4 3 2 225.28 226.93 7.46 o 5 3 2 149.13 157.30 7.32 o 6 3 2 34.94 37.81 3.50 o 7 3 2 69.29 69.81 6.98 o -8 4 2 570.08 645.96 16.04 o -7 4 2 5.01 4.28 4.10 o -6 4 2 1531.91 1543.30 20.51 o -5 4 2 0.05 -2.28 2.45 o -4 4 2 3963.21 3410.41 28.98 o -3 4 2 0.70 -0.86 1.81 o -2 4 2 6059.47 5615.61 39.36 o -1 4 2 1405.28 1453.67 14.06 o 0 4 2 1009.51 1243.88 59.23 o 1 4 2 123.02 159.31 4.42 o 2 4 2 1712.21 1493.47 15.97 o 3 4 2 365.14 369.48 8.04 o 4 4 2 664.22 577.58 11.33 o 5 4 2 0.02 2.66 3.51 o 6 4 2 22.29 19.82 2.07 o 7 4 2 0.14 -4.25 4.25 o -8 5 2 26.69 29.65 2.82 o -7 5 2 358.98 361.39 10.96 o -6 5 2 39.42 41.68 4.10 o -5 5 2 247.27 211.40 6.58 o -4 5 2 0.32 1.79 1.49 o -3 5 2 1618.44 1358.39 14.90 o -2 5 2 160.87 147.68 4.47 o -1 5 2 9597.13 10599.82 69.14 o 0 5 2 53.99 57.39 4.79 o 1 5 2 3380.15 3898.08 31.20 o 2 5 2 174.33 157.68 5.06 o 3 5 2 304.27 262.83 6.96 o 4 5 2 0.42 0.95 2.81 o 5 5 2 290.15 270.29 9.04 o 6 5 2 15.23 18.67 2.12 o 7 5 2 65.29 72.65 7.03 o -8 6 2 319.66 344.65 12.14 o -7 6 2 210.57 194.00 8.31 o -6 6 2 254.63 235.73 7.80 o -5 6 2 70.44 63.61 4.01 o -4 6 2 1066.47 927.42 13.15 o -3 6 2 3.96 0.82 2.13 o -2 6 2 4458.60 4709.21 36.19 o -1 6 2 619.80 809.34 10.86 o 0 6 2 708.78 859.99 69.86 o 1 6 2 17.50 28.00 2.17 o 2 6 2 411.55 396.33 8.53 o 3 6 2 23.70 24.40 2.30 o 4 6 2 889.07 768.05 13.49 o 5 6 2 1.45 -0.13 3.35 o 6 6 2 175.08 146.47 8.03 o -8 7 2 0.04 3.82 3.90 o -7 7 2 315.59 275.45 9.49 o -6 7 2 2.83 4.01 2.82 o -5 7 2 427.67 353.46 8.90 o -4 7 2 20.70 15.82 1.34 o -3 7 2 787.13 714.23 11.49 o -2 7 2 192.77 224.48 6.14 o -1 7 2 1904.21 1983.52 19.62 o 0 7 2 2.23 7.35 1.49 o 1 7 2 714.75 848.81 12.55 o 2 7 2 439.73 552.80 10.58 o 3 7 2 275.28 276.14 7.94 o 4 7 2 10.18 8.66 1.55 o 5 7 2 222.00 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