#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103690.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103690_Fobs loop_ _publ_author_name 'Cai, Jiwen' 'Chen, Cai-Hong' 'Liao, Cheng-Zhu' 'Feng, Xiao-Long' 'Chen, Xiao-Ming' _publ_section_title ; Solid-state structures of group 1 and group 2 metal 1,5-naphthalenedisulfonates: systematic investigation of lamellar three-dimensional networks constructed by metal arenedisulfonate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 520 _journal_page_last 530 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.304 _cell_angle_gamma 90.000 _cell_length_a 13.1955 _cell_length_b 6.6981 _cell_length_c 9.6616 _exptl_crystal_F_000 436.00 _reflns_d_resolution_high 0.7112 _[local]_cod_data_source_file bm00444sup5.hkl _[local]_cod_data_source_block 4 #BEGIN Tags that were not found in dictionaries: _shelx_title ' in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 102.21 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 1160.07 1322.45 8.91 o 4 0 0 4234.11 4268.62 25.37 o 5 0 0 2088.40 2355.99 15.33 o 6 0 0 1959.79 2118.01 14.52 o 7 0 0 0.10 0.81 0.38 o 8 0 0 3138.33 3320.89 22.04 o 9 0 0 318.84 369.72 5.17 o 10 0 0 22.96 23.39 1.50 o 11 0 0 475.32 450.92 6.28 o 12 0 0 374.45 378.08 6.06 o 13 0 0 110.16 108.93 3.48 o 14 0 0 168.58 172.70 4.50 o 15 0 0 89.96 85.03 3.22 o 16 0 0 929.60 972.61 12.24 o 17 0 0 221.94 238.04 5.98 o 18 0 0 173.82 174.47 5.41 o 2 1 0 10.29 9.36 0.51 o 3 1 0 736.38 784.80 24.01 o 4 1 0 27.07 33.95 1.16 o 5 1 0 1468.59 1675.22 19.37 o 6 1 0 2174.42 2403.94 15.91 o 7 1 0 1062.61 1085.36 6.87 o 8 1 0 236.16 270.52 2.27 o 9 1 0 36.22 33.42 0.87 o 10 1 0 110.42 117.81 1.65 o 11 1 0 1269.10 1285.59 6.70 o 12 1 0 112.43 116.53 2.15 o 13 1 0 6.08 7.21 1.04 o 14 1 0 4.82 5.69 1.72 o 15 1 0 6.74 5.45 0.85 o 16 1 0 0.03 0.16 0.72 o 17 1 0 26.83 26.92 1.90 o 18 1 0 30.23 31.55 1.99 o 0 2 0 1712.87 1530.52 7.15 o 1 2 0 831.49 888.97 3.28 o 2 2 0 4091.33 4012.33 13.78 o 3 2 0 1886.64 1950.88 21.97 o 4 2 0 286.62 221.59 2.40 o 5 2 0 456.37 467.66 5.65 o 6 2 0 26.98 27.40 1.34 o 7 2 0 26.56 30.71 0.76 o 8 2 0 560.44 545.85 3.46 o 9 2 0 1133.45 1184.19 25.28 o 10 2 0 45.16 40.13 1.04 o 11 2 0 263.66 218.97 5.62 o 12 2 0 0.26 0.12 0.42 o 13 2 0 100.09 100.70 3.87 o 14 2 0 58.58 58.02 2.76 o 15 2 0 147.40 145.87 3.16 o 16 2 0 676.06 650.09 7.76 o 17 2 0 63.24 61.54 2.19 o 18 2 0 49.47 49.26 2.97 o 1 3 0 138.73 185.02 1.34 o 2 3 0 2.46 3.19 0.58 o 3 3 0 30.09 48.10 0.64 o 4 3 0 198.81 200.52 3.02 o 5 3 0 866.92 925.70 14.38 o 6 3 0 95.58 89.25 1.09 o 7 3 0 10.14 11.39 0.59 o 8 3 0 35.07 34.47 0.89 o 9 3 0 166.32 178.92 2.03 o 10 3 0 19.79 22.11 0.84 o 11 3 0 46.20 53.87 1.64 o 12 3 0 51.64 44.16 1.55 o 13 3 0 476.67 473.05 13.39 o 14 3 0 78.88 83.70 2.24 o 15 3 0 19.71 21.23 1.32 o 16 3 0 16.01 15.89 1.87 o 17 3 0 16.22 16.05 1.41 o 0 4 0 5911.94 5637.48 23.83 o 1 4 0 31.37 24.93 1.81 o 2 4 0 59.30 56.42 0.87 o 3 4 0 369.48 363.13 2.30 o 4 4 0 1829.73 1840.16 11.32 o 5 4 0 885.25 890.29 13.58 o 6 4 0 205.20 186.95 1.74 o 7 4 0 988.64 997.58 10.63 o 8 4 0 1091.93 1080.94 6.15 o 9 4 0 79.40 83.57 1.86 o 10 4 0 191.19 174.86 2.79 o 11 4 0 5.66 5.57 0.75 o 12 4 0 117.69 114.32 6.58 o 13 4 0 15.66 13.42 1.05 o 14 4 0 136.70 130.85 4.33 o 15 4 0 60.66 58.56 2.04 o 16 4 0 242.32 229.96 5.00 o 1 5 0 375.76 353.25 2.45 o 2 5 0 203.34 198.05 2.03 o 3 5 0 2504.79 2461.60 9.24 o 4 5 0 345.26 354.93 3.78 o 5 5 0 1364.52 1334.43 5.85 o 6 5 0 222.07 220.43 3.29 o 7 5 0 41.76 41.91 0.96 o 8 5 0 8.71 9.59 0.84 o 9 5 0 295.80 289.99 3.68 o 10 5 0 6.64 7.15 0.80 o 11 5 0 867.99 827.86 7.11 o 12 5 0 29.39 27.64 1.51 o 13 5 0 64.00 61.20 5.88 o 14 5 0 22.80 25.68 1.50 o 15 5 0 142.06 142.77 3.27 o 0 6 0 1.36 1.80 0.56 o 1 6 0 164.16 164.05 3.20 o 2 6 0 77.47 67.30 1.56 o 3 6 0 22.10 20.12 0.76 o 4 6 0 135.67 143.21 1.75 o 5 6 0 110.64 111.65 1.57 o 6 6 0 37.35 37.86 1.07 o 7 6 0 5.71 6.04 0.61 o 8 6 0 49.25 45.21 1.31 o 9 6 0 113.54 106.24 3.29 o 10 6 0 36.36 36.74 1.53 o 11 6 0 5.47 2.62 0.74 o 12 6 0 215.65 215.25 7.59 o 13 6 0 33.09 31.48 2.33 o 14 6 0 30.30 30.59 2.20 o 1 7 0 352.30 350.57 2.96 o 2 7 0 2.40 1.52 0.40 o 3 7 0 170.19 180.79 2.48 o 4 7 0 62.78 64.54 1.31 o 5 7 0 449.52 454.99 7.94 o 6 7 0 175.58 177.65 3.17 o 7 7 0 13.38 13.35 1.08 o 8 7 0 1.79 1.73 0.67 o 9 7 0 21.30 19.03 1.72 o 10 7 0 0.09 0.43 0.91 o 11 7 0 54.06 53.65 2.74 o 12 7 0 0.21 -0.84 0.94 o 0 8 0 35.29 45.24 2.59 o 1 8 0 131.28 129.43 5.54 o 2 8 0 2.27 2.14 0.75 o 3 8 0 70.72 72.61 2.20 o 4 8 0 36.94 41.17 1.75 o 5 8 0 67.59 71.62 2.22 o 6 8 0 2.15 3.23 0.84 o 7 8 0 52.32 60.46 2.11 o 8 8 0 0.75 1.64 0.77 o 9 8 0 12.62 11.22 1.62 o 1 9 0 260.47 284.92 4.66 o 2 9 0 0.19 1.46 0.92 o 3 9 0 208.11 236.52 6.18 o 4 9 0 10.37 12.03 1.85 o -18 1 1 368.11 371.97 5.58 o -17 1 1 21.52 20.95 1.44 o -16 1 1 262.72 277.47 7.13 o -15 1 1 85.30 96.55 2.54 o -14 1 1 264.15 267.65 15.05 o -13 1 1 33.32 41.28 1.95 o -12 1 1 0.69 1.31 0.52 o -11 1 1 72.11 82.76 2.93 o -10 1 1 2014.00 2020.32 32.54 o -9 1 1 38.50 38.58 0.91 o -8 1 1 277.65 308.83 2.37 o -7 1 1 1873.32 1915.85 33.47 o -6 1 1 463.43 430.46 9.37 o -5 1 1 4794.18 5078.82 80.02 o -4 1 1 1682.07 1668.77 16.72 o -3 1 1 2690.49 2717.24 26.59 o -2 1 1 8677.56 7905.24 279.94 o 2 1 1 5507.18 5756.73 23.74 o 3 1 1 89.23 64.09 1.66 o 4 1 1 1659.48 1781.38 25.84 o 5 1 1 101.38 161.17 2.78 o 6 1 1 4094.77 4299.43 34.52 o 7 1 1 131.22 141.95 4.80 o 8 1 1 1.86 2.43 0.30 o 9 1 1 120.07 112.97 1.57 o 10 1 1 355.27 352.61 6.14 o 11 1 1 321.32 269.77 2.71 o 12 1 1 21.04 16.82 0.81 o 13 1 1 294.85 299.65 4.55 o 14 1 1 718.30 728.36 6.78 o 15 1 1 12.61 13.34 1.18 o 16 1 1 71.80 75.79 6.62 o 17 1 1 336.90 334.43 19.85 o 18 1 1 124.59 128.89 3.23 o -17 2 1 16.13 17.44 1.36 o -16 2 1 6.70 6.96 0.99 o -15 2 1 19.40 19.21 1.24 o -14 2 1 8.91 8.35 1.22 o -13 2 1 4.45 4.77 0.89 o -12 2 1 258.50 248.06 8.05 o -11 2 1 125.34 144.76 4.92 o -10 2 1 240.65 277.37 9.52 o -9 2 1 265.12 273.62 3.80 o -8 2 1 297.32 303.54 7.73 o -7 2 1 52.34 45.47 1.66 o -6 2 1 50.24 71.77 0.86 o -5 2 1 3897.32 4206.94 29.45 o -4 2 1 450.16 496.81 5.57 o -3 2 1 618.50 611.29 7.35 o -2 2 1 1030.39 1070.29 4.31 o -1 2 1 63.20 64.57 0.65 o 0 2 1 817.45 703.76 4.39 o 1 2 1 628.56 573.15 3.14 o 2 2 1 279.35 327.18 3.33 o 3 2 1 506.69 492.67 4.45 o 4 2 1 247.72 251.26 3.12 o 5 2 1 595.52 603.78 12.21 o 6 2 1 1272.67 1390.19 10.21 o 7 2 1 5.85 3.99 0.35 o 8 2 1 588.19 622.81 18.12 o 9 2 1 214.57 224.35 3.33 o 10 2 1 11.65 15.39 0.74 o 11 2 1 169.36 201.95 3.08 o 12 2 1 206.57 229.10 2.63 o 13 2 1 27.90 24.07 2.28 o 14 2 1 102.93 92.79 2.31 o 15 2 1 144.26 142.31 2.99 o 16 2 1 0.01 -0.12 0.64 o 17 2 1 8.22 7.90 1.06 o 18 2 1 0.45 1.67 1.17 o -17 3 1 25.30 23.58 1.58 o -16 3 1 3.65 2.73 0.83 o -15 3 1 99.29 98.93 5.04 o -14 3 1 158.54 147.95 6.95 o -13 3 1 29.12 26.07 1.31 o -12 3 1 6.45 8.26 0.87 o -11 3 1 98.18 116.31 6.46 o -10 3 1 267.07 221.28 7.15 o -9 3 1 64.34 61.07 3.78 o -8 3 1 44.64 38.07 0.91 o -7 3 1 1170.23 1178.91 7.75 o -6 3 1 720.81 683.23 8.60 o -5 3 1 2.88 1.45 0.18 o -4 3 1 138.82 137.96 1.01 o -3 3 1 2841.30 2791.94 21.80 o -2 3 1 4761.61 4449.50 25.76 o -1 3 1 1087.42 1126.26 6.93 o 0 3 1 970.81 1031.37 12.42 o 1 3 1 457.12 447.62 2.37 o 2 3 1 204.07 155.83 1.45 o 3 3 1 108.08 103.59 1.05 o 4 3 1 389.26 431.77 2.38 o 5 3 1 699.88 699.35 9.50 o 6 3 1 1156.39 1101.18 10.29 o 7 3 1 1210.42 1290.28 12.11 o 8 3 1 142.84 136.56 3.31 o 9 3 1 835.20 792.94 4.72 o 10 3 1 329.97 322.67 2.90 o 11 3 1 166.25 150.93 2.38 o 12 3 1 68.44 67.28 1.82 o 13 3 1 97.52 86.14 2.41 o 14 3 1 249.47 236.47 3.82 o 15 3 1 0.01 -0.13 0.57 o 16 3 1 107.13 102.21 2.69 o 17 3 1 254.83 248.62 4.33 o -16 4 1 6.04 7.59 1.13 o -15 4 1 136.74 138.60 6.61 o -14 4 1 72.68 71.62 5.11 o -13 4 1 111.03 109.70 3.81 o -12 4 1 2.34 3.37 1.11 o -11 4 1 9.65 8.29 0.82 o -10 4 1 462.20 433.91 4.54 o -9 4 1 61.17 67.85 1.73 o -8 4 1 234.93 236.53 4.15 o -7 4 1 855.10 886.27 4.64 o -6 4 1 31.03 35.93 0.82 o -5 4 1 903.59 881.77 9.65 o -4 4 1 46.34 50.69 0.87 o -3 4 1 120.17 120.14 1.25 o -2 4 1 756.57 745.44 7.63 o -1 4 1 552.54 499.57 2.69 o 0 4 1 122.52 138.08 1.53 o 1 4 1 414.30 402.03 4.22 o 2 4 1 100.01 118.24 1.36 o 3 4 1 60.42 56.37 0.89 o 4 4 1 0.83 2.03 0.24 o 5 4 1 304.51 296.76 3.64 o 6 4 1 613.47 598.29 7.61 o 7 4 1 56.12 50.71 1.14 o 8 4 1 35.51 36.78 1.01 o 9 4 1 383.67 381.05 9.72 o 10 4 1 63.53 64.03 1.38 o 11 4 1 225.44 220.97 3.31 o 12 4 1 44.82 39.11 1.52 o 13 4 1 106.12 100.79 2.42 o 14 4 1 60.31 58.12 1.98 o 15 4 1 71.05 64.14 3.04 o 16 4 1 107.80 103.31 2.76 o -15 5 1 47.21 45.27 1.89 o -14 5 1 59.56 55.87 2.00 o -13 5 1 0.96 1.00 0.67 o -12 5 1 4.93 4.45 0.78 o -11 5 1 258.74 250.11 6.12 o -10 5 1 372.50 332.33 9.98 o -9 5 1 66.72 63.02 1.46 o -8 5 1 5.28 5.08 0.54 o -7 5 1 164.73 156.83 2.15 o -6 5 1 948.63 931.20 12.11 o -5 5 1 85.99 80.54 1.24 o -4 5 1 273.10 267.33 3.95 o -3 5 1 266.98 279.44 2.26 o -2 5 1 841.93 859.25 4.78 o -1 5 1 159.04 150.33 1.56 o 0 5 1 84.33 91.31 1.21 o 1 5 1 10.24 11.17 0.54 o 2 5 1 146.46 160.90 1.63 o 3 5 1 0.33 4.35 1.36 o 4 5 1 2.62 2.49 0.34 o 5 5 1 37.22 38.24 0.92 o 6 5 1 314.81 328.44 4.72 o 7 5 1 130.46 128.26 4.16 o 8 5 1 129.77 133.30 2.33 o 9 5 1 108.73 107.31 1.81 o 10 5 1 134.32 128.50 2.54 o 11 5 1 56.91 47.60 1.68 o 12 5 1 59.45 59.50 1.93 o 13 5 1 173.88 178.87 4.90 o 14 5 1 157.34 145.30 4.45 o 15 5 1 1.79 1.60 1.04 o -14 6 1 10.42 11.83 1.22 o -13 6 1 113.87 104.14 6.97 o -12 6 1 1.55 1.95 0.81 o -11 6 1 148.92 151.17 2.97 o -10 6 1 155.17 156.05 2.98 o -9 6 1 49.37 47.53 2.26 o -8 6 1 518.21 503.13 4.27 o -7 6 1 315.00 308.38 3.53 o -6 6 1 81.11 78.88 1.60 o -5 6 1 755.85 760.73 8.93 o -4 6 1 670.99 673.71 4.83 o -3 6 1 88.13 86.74 1.36 o -2 6 1 320.13 305.06 2.51 o -1 6 1 553.90 562.81 6.84 o 0 6 1 230.82 228.89 4.05 o 1 6 1 1070.76 1004.77 5.01 o 2 6 1 30.01 24.02 0.80 o 3 6 1 263.42 258.40 3.87 o 4 6 1 31.12 30.36 0.96 o 5 6 1 360.31 370.67 5.05 o 6 6 1 240.86 237.30 4.23 o 7 6 1 141.05 142.73 3.26 o 8 6 1 65.85 62.31 1.80 o 9 6 1 75.66 73.03 2.87 o 10 6 1 20.57 17.89 1.67 o 11 6 1 344.48 326.61 6.40 o 12 6 1 91.39 83.07 3.27 o 13 6 1 0.13 0.05 0.99 o 14 6 1 87.11 85.49 3.68 o -12 7 1 5.12 5.22 1.27 o -11 7 1 138.32 134.93 3.34 o -10 7 1 0.31 0.09 0.62 o -9 7 1 22.16 23.59 1.11 o -8 7 1 43.49 43.23 1.38 o -7 7 1 46.86 48.80 1.43 o -6 7 1 23.71 22.88 1.05 o -5 7 1 18.27 19.33 0.98 o -4 7 1 11.99 10.96 0.80 o -3 7 1 23.74 26.55 1.10 o -2 7 1 100.04 105.57 3.60 o -1 7 1 58.44 62.07 1.50 o 0 7 1 354.26 342.13 3.44 o 1 7 1 0.15 0.70 0.44 o 2 7 1 313.60 310.09 4.73 o 3 7 1 322.34 319.41 3.36 o 4 7 1 60.64 60.21 1.64 o 5 7 1 125.36 132.99 2.33 o 6 7 1 11.49 9.79 0.81 o 7 7 1 46.80 44.87 2.36 o 8 7 1 24.82 23.77 1.90 o 9 7 1 5.40 4.89 1.11 o 10 7 1 53.38 51.27 2.69 o 11 7 1 17.29 15.76 1.75 o 12 7 1 18.59 18.29 1.95 o -9 8 1 110.10 117.37 4.36 o -8 8 1 27.07 23.97 2.20 o -7 8 1 4.19 4.36 1.27 o -6 8 1 108.46 107.51 3.96 o -5 8 1 125.35 128.67 4.29 o -4 8 1 22.91 24.23 2.10 o -3 8 1 18.77 20.74 1.32 o -2 8 1 55.78 65.44 1.70 o -1 8 1 210.96 220.50 2.99 o 0 8 1 223.87 223.47 4.34 o 1 8 1 262.30 274.12 6.64 o 2 8 1 9.10 8.08 0.80 o 3 8 1 266.49 288.05 6.88 o 4 8 1 22.67 22.48 1.13 o 5 8 1 67.67 72.52 1.82 o 6 8 1 44.35 50.69 1.98 o 7 8 1 53.23 54.48 2.84 o 8 8 1 7.00 5.98 1.34 o 9 8 1 215.63 227.24 5.70 o -4 9 1 25.32 26.05 2.38 o -3 9 1 51.31 52.83 3.17 o -2 9 1 1.10 1.55 1.27 o -1 9 1 0.07 -0.35 1.09 o 0 9 1 0.01 0.82 0.84 o 1 9 1 0.03 -0.02 1.00 o 2 9 1 0.14 -0.78 0.78 o 3 9 1 11.66 10.67 1.25 o 4 9 1 1.18 1.37 1.22 o -18 0 2 0.01 -0.41 1.04 o -17 0 2 169.07 177.42 5.28 o -16 0 2 349.96 390.73 7.62 o -15 0 2 824.92 891.40 11.53 o -14 0 2 351.00 355.70 6.63 o -13 0 2 538.58 531.04 7.87 o -12 0 2 0.44 0.84 0.68 o -11 0 2 12.19 12.24 1.37 o -10 0 2 641.45 657.08 7.76 o -9 0 2 4457.95 4362.97 28.25 o -8 0 2 764.15 748.01 7.51 o -7 0 2 1749.37 1789.36 41.69 o -6 0 2 420.53 395.30 5.88 o -5 0 2 1707.33 1799.32 32.47 o -4 0 2 179.15 172.74 7.82 o -3 0 2 2923.40 2785.90 15.46 o -2 0 2 192.08 183.43 2.08 o -1 0 2 7342.29 6329.43 36.95 o 1 0 2 10445.93 10166.99 59.14 o 2 0 2 1950.76 2262.33 14.26 o 3 0 2 9801.17 9656.98 54.97 o 4 0 2 4507.17 4548.39 26.84 o 5 0 2 1420.15 1791.85 12.37 o 6 0 2 84.80 88.51 1.98 o 7 0 2 7325.98 7565.76 43.99 o 8 0 2 46.07 40.46 1.62 o 9 0 2 698.16 647.41 7.03 o 10 0 2 0.49 -0.08 0.46 o 11 0 2 801.92 803.18 8.86 o 12 0 2 320.76 359.03 4.09 o 13 0 2 42.33 39.52 1.47 o 14 0 2 171.26 157.06 5.02 o 15 0 2 874.38 870.79 7.50 o 16 0 2 205.75 201.62 3.56 o 17 0 2 166.35 163.28 4.78 o 18 0 2 15.78 14.54 1.93 o -18 1 2 20.36 24.74 1.66 o -17 1 2 0.09 0.08 0.69 o -16 1 2 1.12 1.11 0.71 o -15 1 2 27.50 29.48 2.74 o -14 1 2 72.77 73.99 2.11 o -13 1 2 1.86 1.95 0.62 o -12 1 2 0.46 -0.10 0.39 o -11 1 2 66.39 70.75 4.10 o -10 1 2 1137.51 1136.63 7.71 o -9 1 2 22.11 18.22 1.03 o -8 1 2 343.31 390.12 8.74 o -7 1 2 522.75 585.63 6.61 o -6 1 2 7.80 11.24 1.09 o -5 1 2 1.33 0.23 0.12 o -4 1 2 9385.52 8861.22 96.65 o -3 1 2 2744.81 2850.26 98.93 o -2 1 2 475.50 522.69 6.55 o -1 1 2 831.98 823.52 10.17 o 0 1 2 1471.53 1497.98 20.38 o 1 1 2 3987.22 4149.37 17.38 o 2 1 2 2172.95 2406.90 14.35 o 3 1 2 1691.25 1811.66 8.69 o 4 1 2 1284.15 1362.70 8.95 o 5 1 2 102.56 111.87 1.21 o 6 1 2 4.12 5.28 0.36 o 7 1 2 614.06 671.63 7.69 o 8 1 2 76.41 77.35 1.37 o 9 1 2 67.55 66.45 1.21 o 10 1 2 618.50 597.52 8.16 o 11 1 2 0.07 -0.21 0.32 o 12 1 2 4.02 11.32 1.44 o 13 1 2 38.09 41.47 1.21 o 14 1 2 253.32 242.08 3.94 o 15 1 2 0.10 -0.30 0.46 o 16 1 2 0.85 2.58 0.67 o 17 1 2 6.90 7.23 0.85 o 18 1 2 30.99 34.67 1.87 o -17 2 2 274.21 286.75 4.71 o -16 2 2 42.57 42.68 1.85 o -15 2 2 9.03 6.96 0.91 o -14 2 2 30.44 31.24 1.46 o -13 2 2 372.60 386.14 4.67 o -12 2 2 365.70 367.80 4.38 o -11 2 2 19.80 16.92 1.01 o -10 2 2 341.71 373.59 4.02 o -9 2 2 1455.58 1449.92 29.00 o -8 2 2 409.17 410.39 17.75 o -7 2 2 95.33 91.83 0.91 o -6 2 2 22.05 24.76 0.59 o -5 2 2 1474.56 1405.17 48.22 o -4 2 2 2210.45 2196.33 46.08 o -3 2 2 713.37 781.67 10.49 o -2 2 2 346.39 358.33 5.39 o -1 2 2 1088.99 953.34 5.29 o 0 2 2 3016.36 2949.52 41.63 o 1 2 2 889.25 821.88 6.49 o 2 2 2 1698.91 1706.62 15.19 o 3 2 2 252.84 344.68 3.13 o 4 2 2 325.60 278.36 2.31 o 5 2 2 3.68 5.38 1.08 o 6 2 2 6.53 6.88 0.44 o 7 2 2 233.53 208.47 3.77 o 8 2 2 448.54 459.83 3.25 o 9 2 2 301.25 304.56 2.70 o 10 2 2 363.68 366.49 7.23 o 11 2 2 770.72 752.00 13.68 o 12 2 2 1.51 3.99 1.26 o 13 2 2 8.70 6.23 0.65 o 14 2 2 147.69 140.42 3.98 o 15 2 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