#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/36/2103693.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103693_Fobs loop_ _publ_author_name 'Cai, Jiwen' 'Chen, Cai-Hong' 'Liao, Cheng-Zhu' 'Feng, Xiao-Long' 'Chen, Xiao-Ming' _publ_section_title ; Solid-state structures of group 1 and group 2 metal 1,5-naphthalenedisulfonates: systematic investigation of lamellar three-dimensional networks constructed by metal arenedisulfonate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 520 _journal_page_last 530 _journal_volume 57 _journal_year 2001 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7662 _cell_length_b 22.0801 _cell_length_c 5.9870 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.7114 _[local]_cod_data_source_file bm00447sup8.hkl _[local]_cod_data_source_block 7 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 10211 in Pnma' _shelx_refln_list_code 4 _shelx_F_calc_maximum 308.87 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 239.97 267.80 14.02 o 4 0 0 170.33 280.85 21.35 o 6 0 0 12731.24 12688.21 172.35 o 8 0 0 378.24 482.96 41.85 o 10 0 0 40.91 13.16 22.33 o 12 0 0 1824.84 1805.45 99.12 o 2 1 0 26632.44 29338.85 152.14 o 4 1 0 8886.99 10073.95 89.25 o 6 1 0 20209.69 20745.76 164.45 o 8 1 0 4278.48 4274.94 80.22 o 10 1 0 5895.89 5427.48 115.19 o 12 1 0 3915.26 4178.10 105.03 o 2 2 0 33132.97 34967.74 142.56 o 4 2 0 7280.66 7292.99 82.08 o 6 2 0 8814.52 9202.42 103.39 o 8 2 0 445.35 547.11 30.37 o 10 2 0 717.57 701.16 40.46 o 12 2 0 1897.10 1772.47 110.55 o 2 3 0 117.28 164.08 7.29 o 4 3 0 22024.25 23378.68 152.59 o 6 3 0 12093.22 11999.62 119.71 o 8 3 0 11211.99 11355.52 193.49 o 10 3 0 5025.70 4921.04 135.14 o 12 3 0 848.48 868.59 50.98 o 0 4 0 25285.21 23698.99 182.70 o 2 4 0 47957.62 49519.97 412.48 o 4 4 0 12009.84 13003.89 186.52 o 6 4 0 121.25 116.54 15.45 o 8 4 0 2063.83 2162.89 134.71 o 10 4 0 2957.37 3043.55 95.61 o 12 4 0 745.99 704.18 47.05 o 2 5 0 1975.31 2124.64 22.96 o 4 5 0 32012.13 33103.49 136.74 o 6 5 0 7300.79 7404.41 94.30 o 8 5 0 11692.68 11891.15 141.12 o 10 5 0 6158.31 6033.00 112.53 o 12 5 0 847.23 792.18 49.60 o 0 6 0 63.42 164.76 21.35 o 2 6 0 47005.47 46940.63 419.66 o 4 6 0 22836.40 24932.35 330.02 o 6 6 0 1388.28 1575.64 85.95 o 8 6 0 84.79 94.02 22.31 o 10 6 0 2090.84 2160.17 68.02 o 12 6 0 1104.82 1163.86 64.71 o 2 7 0 9.12 33.49 13.48 o 4 7 0 11068.95 10984.46 70.52 o 6 7 0 16522.18 18057.77 108.37 o 8 7 0 11656.69 11768.21 143.53 o 10 7 0 3116.61 3334.04 85.29 o 12 7 0 906.10 876.45 52.97 o 0 8 0 5507.70 4861.47 55.55 o 2 8 0 32594.79 33239.51 153.90 o 4 8 0 19780.07 20580.07 105.39 o 6 8 0 463.09 473.80 18.21 o 8 8 0 8.31 18.63 12.32 o 10 8 0 514.82 572.61 38.39 o 12 8 0 1602.76 1709.03 102.24 o 2 9 0 1446.60 1278.76 28.85 o 4 9 0 4930.95 5186.02 50.50 o 6 9 0 18427.42 18671.68 175.33 o 8 9 0 6882.46 6886.41 227.19 o 10 9 0 3289.12 3396.22 87.52 o 0 10 0 95398.99 86265.77 1595.03 o 2 10 0 2784.75 2779.63 40.49 o 4 10 0 6572.53 6650.69 57.58 o 6 10 0 7767.96 8044.18 78.09 o 8 10 0 847.20 886.68 41.06 o 10 10 0 141.92 151.14 26.40 o 2 11 0 17052.08 17464.33 94.94 o 4 11 0 2405.92 2419.03 34.94 o 6 11 0 16981.88 17449.24 113.59 o 8 11 0 2636.19 2549.91 81.97 o 10 11 0 4345.56 4239.35 173.70 o 0 12 0 67878.84 64263.13 789.21 o 2 12 0 9603.99 9561.21 124.16 o 4 12 0 1460.44 1426.82 33.24 o 6 12 0 5467.21 5398.00 61.20 o 8 12 0 498.11 485.77 33.21 o 10 12 0 15.43 30.32 21.53 o 2 13 0 1060.65 1010.28 23.22 o 4 13 0 9746.26 10022.13 116.79 o 6 13 0 8131.64 8127.58 91.04 o 8 13 0 6557.16 6482.14 93.35 o 10 13 0 2926.70 2956.44 108.39 o 0 14 0 19782.78 19691.03 157.07 o 2 14 0 15354.21 14586.90 173.34 o 4 14 0 3859.97 3894.85 56.09 o 6 14 0 976.95 935.93 27.86 o 8 14 0 1103.96 1050.66 40.23 o 10 14 0 3585.31 3469.79 92.92 o 2 15 0 155.51 179.52 15.24 o 4 15 0 24398.69 24126.14 189.62 o 6 15 0 698.63 696.65 30.24 o 8 15 0 4902.68 4743.25 111.45 o 10 15 0 6793.16 6510.21 129.08 o 0 16 0 6547.77 6242.19 299.29 o 2 16 0 22609.04 22206.40 386.65 o 4 16 0 1447.31 1459.91 29.26 o 6 16 0 866.35 901.97 34.67 o 8 16 0 460.47 445.29 29.81 o 10 16 0 881.35 835.01 51.00 o 2 17 0 353.04 347.43 17.66 o 4 17 0 5078.27 4877.56 59.57 o 6 17 0 6239.62 6092.03 90.80 o 8 17 0 7093.88 7178.92 164.64 o 10 17 0 1658.79 1694.30 109.90 o 0 18 0 5335.01 5041.51 239.97 o 2 18 0 7870.91 8017.47 117.22 o 4 18 0 11552.58 11397.64 119.57 o 6 18 0 261.91 299.53 36.89 o 8 18 0 11.29 13.16 18.55 o 10 18 0 544.70 531.56 45.31 o 2 19 0 2154.32 2077.04 53.36 o 4 19 0 2129.42 2115.60 41.94 o 6 19 0 7275.30 7206.31 98.80 o 8 19 0 3418.45 3617.70 77.54 o 0 20 0 15632.24 15521.92 399.49 o 2 20 0 4579.83 4399.35 59.16 o 4 20 0 2850.02 2875.44 58.16 o 6 20 0 1892.78 1872.70 52.39 o 8 20 0 280.67 313.31 31.78 o 2 21 0 2627.87 2860.23 67.63 o 4 21 0 318.06 324.55 26.98 o 6 21 0 9099.65 8804.62 155.25 o 8 21 0 2291.89 2618.12 126.94 o 0 22 0 11985.26 12327.27 266.13 o 2 22 0 2455.17 2547.04 75.30 o 4 22 0 4760.01 4786.51 99.84 o 6 22 0 1125.12 1158.99 56.18 o 8 22 0 262.07 225.38 39.67 o 2 23 0 1355.56 1558.52 56.75 o 4 23 0 1460.75 1638.62 113.30 o 6 23 0 4769.59 4990.76 320.05 o 8 23 0 2458.12 2692.26 214.46 o 0 24 0 5311.67 5476.22 148.19 o 2 24 0 5627.93 5864.78 109.69 o 4 24 0 1326.87 1614.23 90.81 o 6 24 0 627.51 635.04 66.44 o 8 24 0 86.29 119.50 56.51 o 2 25 0 179.98 296.59 45.19 o 4 25 0 8143.35 8551.85 207.83 o 6 25 0 706.40 840.50 76.58 o 8 25 0 2032.36 2371.25 128.88 o 0 26 0 1547.57 1719.28 88.76 o 2 26 0 7759.22 8403.77 197.48 o 4 26 0 517.52 521.36 59.75 o 6 26 0 253.37 285.38 60.51 o 2 27 0 164.63 265.64 49.72 o 4 27 0 3839.92 4315.29 151.53 o 6 27 0 696.86 737.71 75.93 o 0 28 0 3452.84 3552.77 125.86 o 2 28 0 2269.23 2248.94 106.45 o 4 28 0 2195.14 2419.67 117.45 o 2 29 0 602.74 566.44 64.28 o 4 29 0 399.47 461.07 68.70 o 0 30 0 5916.68 6592.49 183.89 o 2 30 0 1160.82 1191.23 86.17 o 1 0 1 20483.91 22243.57 129.00 o 2 0 1 11248.14 12744.06 420.73 o 3 0 1 31031.00 33238.74 205.40 o 4 0 1 12300.37 13625.59 108.10 o 5 0 1 12022.20 12447.34 252.48 o 6 0 1 2841.70 2919.52 140.75 o 7 0 1 2570.98 2514.00 65.52 o 8 0 1 4165.87 4347.23 82.01 o 9 0 1 10833.09 10786.25 139.79 o 10 0 1 1605.38 1642.39 86.44 o 11 0 1 1660.13 1598.71 62.17 o 12 0 1 16.27 4.85 21.62 o 0 1 1 962.51 991.79 47.19 o 1 1 1 14800.40 16097.83 149.69 o 2 1 1 15149.77 16573.15 98.45 o 3 1 1 34158.56 35821.69 139.35 o 4 1 1 4490.28 4899.45 36.79 o 5 1 1 1098.38 1289.32 24.39 o 6 1 1 274.77 276.66 13.75 o 7 1 1 1780.00 1856.75 35.06 o 8 1 1 239.77 257.61 17.37 o 9 1 1 430.66 378.68 20.88 o 10 1 1 751.28 821.80 30.04 o 11 1 1 1807.13 1865.20 47.24 o 12 1 1 178.77 192.62 22.30 o 1 2 1 640.09 696.58 11.72 o 2 2 1 11525.97 12786.35 153.44 o 3 2 1 1031.78 1009.09 14.84 o 4 2 1 2257.96 2373.19 41.57 o 5 2 1 14473.05 15699.37 79.82 o 6 2 1 1837.80 1905.64 33.44 o 7 2 1 7422.28 7613.35 71.87 o 8 2 1 2911.46 2909.26 47.34 o 9 2 1 8036.81 7971.52 87.28 o 10 2 1 1499.54 1492.23 39.68 o 11 2 1 849.45 822.76 32.52 o 12 2 1 707.98 685.16 32.96 o 0 3 1 13950.00 13542.22 86.47 o 1 3 1 23600.78 24618.73 240.06 o 2 3 1 7096.74 7540.25 39.24 o 3 3 1 13257.16 13828.82 69.55 o 4 3 1 3736.95 3989.93 38.03 o 5 3 1 8700.02 9327.72 123.93 o 6 3 1 540.77 551.99 18.35 o 7 3 1 2.41 5.47 8.14 o 8 3 1 1.29 -7.97 8.39 o 9 3 1 208.03 205.68 17.44 o 10 3 1 5.40 0.97 11.56 o 11 3 1 368.41 400.17 26.01 o 12 3 1 914.42 941.57 37.50 o 1 4 1 21076.91 21527.75 245.32 o 2 4 1 6.81 9.60 2.62 o 3 4 1 10336.83 11597.64 84.46 o 4 4 1 1049.47 1064.99 16.68 o 5 4 1 2112.19 2212.95 28.62 o 6 4 1 9110.84 9727.05 67.51 o 7 4 1 15669.41 16223.56 141.21 o 8 4 1 2141.56 2142.18 40.99 o 9 4 1 1927.37 1857.91 41.14 o 10 4 1 881.62 845.97 30.79 o 11 4 1 4089.66 4053.23 60.73 o 12 4 1 633.36 642.41 32.39 o 0 5 1 22587.40 21471.12 120.40 o 1 5 1 29558.35 29632.81 127.26 o 2 5 1 1559.40 1631.86 27.59 o 3 5 1 7920.18 8628.07 94.14 o 4 5 1 4492.93 4841.56 31.61 o 5 5 1 8468.88 8531.85 47.43 o 6 5 1 2830.97 3015.82 33.60 o 7 5 1 297.26 292.72 15.02 o 8 5 1 593.04 624.06 20.85 o 9 5 1 10.16 14.79 10.13 o 10 5 1 144.11 126.31 14.79 o 11 5 1 488.24 457.98 23.43 o 12 5 1 124.39 116.20 21.00 o 1 6 1 23505.02 23516.66 130.09 o 2 6 1 640.35 633.69 15.61 o 3 6 1 3425.40 3684.11 52.71 o 4 6 1 4110.78 4418.80 43.05 o 5 6 1 3344.27 3537.26 29.91 o 6 6 1 4616.38 4602.82 42.75 o 7 6 1 13877.20 14277.38 105.73 o 8 6 1 999.22 1001.63 25.75 o 9 6 1 3334.08 3336.41 48.81 o 10 6 1 1537.31 1523.09 35.86 o 11 6 1 2004.41 2091.64 50.73 o 12 6 1 706.41 746.26 34.64 o 0 7 1 16922.09 16481.23 136.80 o 1 7 1 19293.31 19052.46 79.98 o 2 7 1 5620.49 5812.00 30.94 o 3 7 1 17614.06 18759.38 180.69 o 4 7 1 1213.84 1121.77 16.15 o 5 7 1 3341.19 3201.06 31.46 o 6 7 1 868.42 847.34 16.90 o 7 7 1 37.21 31.86 8.20 o 8 7 1 4.58 13.11 8.99 o 9 7 1 2.62 4.77 10.11 o 10 7 1 55.24 39.26 12.08 o 11 7 1 462.94 448.49 26.65 o 12 7 1 691.22 611.35 72.64 o 1 8 1 6319.90 6846.54 50.50 o 2 8 1 5160.31 5428.46 67.69 o 3 8 1 6950.48 7353.42 71.04 o 4 8 1 1433.53 1373.79 16.96 o 5 8 1 3984.39 4096.53 43.94 o 6 8 1 2395.55 2357.67 31.31 o 7 8 1 8830.46 8941.52 98.60 o 8 8 1 2662.19 2528.14 40.34 o 9 8 1 4577.48 4628.30 58.28 o 10 8 1 1118.59 1110.38 31.62 o 11 8 1 1433.00 1386.91 42.90 o 12 8 1 497.73 530.85 61.58 o 0 9 1 18259.04 18189.34 87.92 o 1 9 1 9205.68 8847.46 89.56 o 2 9 1 5798.99 5575.76 45.55 o 3 9 1 22427.71 22885.19 91.60 o 4 9 1 460.98 482.35 17.91 o 5 9 1 1305.24 1318.38 18.63 o 6 9 1 502.08 493.51 15.70 o 7 9 1 469.24 480.93 16.85 o 8 9 1 129.91 132.91 12.57 o 9 9 1 58.23 58.84 12.38 o 10 9 1 316.85 290.95 19.88 o 11 9 1 1430.06 1425.91 43.95 o 12 9 1 182.86 171.27 47.56 o 1 10 1 3351.57 3346.55 25.64 o 2 10 1 240.78 246.50 8.73 o 3 10 1 8166.51 8239.04 40.10 o 4 10 1 8215.56 8566.50 61.98 o 5 10 1 7855.08 7819.99 46.72 o 6 10 1 637.57 628.48 17.57 o 7 10 1 3652.73 3562.15 46.09 o 8 10 1 1817.43 1743.93 31.68 o 9 10 1 8198.03 7910.17 77.78 o 10 10 1 1693.49 1672.98 44.48 o 11 10 1 715.80 732.71 33.12 o 12 10 1 165.89 218.62 51.88 o 0 11 1 1179.78 1020.78 20.50 o 1 11 1 9486.92 8926.74 55.66 o 2 11 1 9284.68 9437.98 105.59 o 3 11 1 22229.67 22327.26 191.35 o 4 11 1 1655.97 1684.56 20.73 o 5 11 1 25.59 42.71 7.01 o 6 11 1 250.26 244.09 12.98 o 7 11 1 1918.29 1893.79 31.65 o 8 11 1 225.07 237.57 15.32 o 9 11 1 250.47 246.66 18.36 o 10 11 1 795.48 782.10 32.55 o 11 11 1 1480.13 1571.46 46.41 o 1 12 1 324.20 300.20 9.40 o 2 12 1 818.82 811.18 14.21 o 3 12 1 3903.75 3840.75 31.34 o 4 12 1 2207.67 2157.57 24.28 o 5 12 1 10778.13 10822.02 71.23 o 6 12 1 1017.81 1049.46 21.73 o 7 12 1 2123.73 2146.77 34.29 o 8 12 1 3239.90 3194.50 51.07 o 9 12 1 6805.01 6664.24 75.47 o 10 12 1 1041.15 1073.71 37.58 o 11 12 1 722.49 726.70 34.17 o 0 13 1 5131.98 5079.28 60.24 o 1 13 1 10188.73 9797.69 85.82 o 2 13 1 4538.82 4463.87 68.39 o 3 13 1 6468.98 6341.08 51.43 o 4 13 1 1589.64 1549.88 21.26 o 5 13 1 5327.53 5362.43 46.04 o 6 13 1 50.59 50.84 8.70 o 7 13 1 69.07 75.22 10.65 o 8 13 1 173.54 197.13 15.04 o 9 13 1 370.99 375.86 21.90 o 10 13 1 15.14 22.08 15.78 o 11 13 1 490.60 517.12 35.72 o 1 14 1 1291.18 1176.68 24.36 o 2 14 1 897.11 807.96 15.37 o 3 14 1 1774.83 1777.30 27.30 o 4 14 1 423.38 438.98 14.00 o 5 14 1 3619.87 3573.35 38.45 o 6 14 1 4038.58 3983.58 78.12 o 7 14 1 10361.73 10301.81 104.38 o 8 14 1 1055.55 1088.17 27.74 o 9 14 1 861.50 854.39 29.47 o 10 14 1 644.89 624.49 31.21 o 11 14 1 2828.89 2832.42 121.44 o 0 15 1 3415.01 3343.14 57.45 o 1 15 1 17178.19 16565.78 91.11 o 2 15 1 721.22 734.25 15.37 o 3 15 1 521.68 540.89 13.95 o 4 15 1 5158.48 5083.63 44.62 o 5 15 1 7395.12 7399.50 57.32 o 6 15 1 1834.63 1862.54 30.26 o 7 15 1 41.28 32.07 10.21 o 8 15 1 1092.88 1068.98 30.95 o 9 15 1 101.16 114.68 16.92 o 10 15 1 22.21 -7.75 19.56 o 1 16 1 8025.23 7853.17 61.15 o 2 16 1 76.51 75.02 7.98 o 3 16 1 1000.27 997.52 18.74 o 4 16 1 423.23 384.37 14.75 o 5 16 1 3416.56 3367.01 39.29 o 6 16 1 5516.63 5516.29 52.54 o 7 16 1 5095.05 5017.92 52.91 o 8 16 1 1150.87 1224.19 45.64 o 9 16 1 1916.68 1935.58 49.65 o 10 16 1 396.02 440.66 35.47 o 0 17 1 2280.62 2228.37 44.68 o 1 17 1 7858.90 7845.69 65.67 o 2 17 1 2827.51 2780.81 30.51 o 3 17 1 4766.70 4519.80 51.52 o 4 17 1 1794.54 1726.22 31.37 o 5 17 1 3036.43 3016.98 39.43 o 6 17 1 100.69 113.77 13.06 o 7 17 1 4.63 0.11 11.38 o 8 17 1 16.15 8.83 15.00 o 9 17 1 34.72 37.48 18.04 o 10 17 1 18.68 -11.51 22.87 o 1 18 1 459.57 607.65 25.72 o 2 18 1 599.24 611.63 17.63 o 3 18 1 3446.35 3331.46 41.68 o 4 18 1 1337.47 1322.37 27.86 o 5 18 1 1540.74 1623.17 31.75 o 6 18 1 1017.44 1042.30 27.00 o 7 18 1 5647.81 5807.87 84.79 o 8 18 1 1016.36 1045.30 37.26 o 9 18 1 2160.39 2337.45 56.35 o 10 18 1 747.20 752.72 52.98 o 0 19 1 2872.73 2989.49 79.43 o 1 19 1 5268.44 5353.58 68.35 o 2 19 1 2050.77 1969.82 41.61 o 3 19 1 8202.75 8016.05 112.87 o 4 19 1 866.10 818.64 25.81 o 5 19 1 211.71 221.24 15.93 o 6 19 1 484.66 476.06 20.46 o 7 19 1 170.25 160.84 18.33 o 8 19 1 1.99 -3.27 17.12 o 9 19 1 2.24 8.81 19.68 o 10 19 1 271.10 322.16 61.80 o 1 20 1 48.86 76.10 13.85 o 2 20 1 4.78 16.34 9.77 o 3 20 1 2882.92 2926.24 78.15 o 4 20 1 2435.97 2440.25 43.34 o 5 20 1 2883.62 2842.94 47.87 o 6 20 1 926.82 907.81 30.07 o 7 20 1 1301.13 1295.66 41.71 o 8 20 1 838.93 892.40 43.43 o 9 20 1 4232.44 4343.96 116.80 o 10 20 1 682.73 846.00 84.88 o 0 21 1 2699.33 2600.44 61.47 o 1 21 1 2562.64 2548.33 45.04 o 2 21 1 2849.27 2895.31 53.77 o 3 21 1 9839.63 9822.26 154.02 o 4 21 1 136.69 146.78 16.30 o 5 21 1 25.03 16.93 12.89 o 6 21 1 152.19 168.90 20.57 o 7 21 1 615.23 603.21 31.31 o 8 21 1 83.32 86.75 24.64 o 9 21 1 76.36 109.69 51.98 o 1 22 1 380.96 453.73 19.07 o 2 22 1 1059.15 996.25 29.25 o 3 22 1 2263.20 2241.60 42.70 o 4 22 1 1532.51 1531.73 36.90 o 5 22 1 2666.99 2686.38 49.15 o 6 22 1 62.33 63.19 18.20 o 7 22 1 1801.17 1843.60 51.20 o 8 22 1 1122.01 1132.71 43.85 o 9 22 1 2767.76 3138.73 142.47 o 0 23 1 1955.28 2023.38 52.06 o 1 23 1 3381.58 3442.52 67.58 o 2 23 1 1988.37 2048.48 56.01 o 3 23 1 4164.46 4169.39 85.62 o 4 23 1 290.41 307.67 21.88 o 5 23 1 550.04 568.32 26.38 o 6 23 1 17.57 5.25 17.71 o 7 23 1 98.09 79.85 22.53 o 8 23 1 239.08 259.96 33.46 o 9 23 1 19.13 48.43 52.09 o 1 24 1 415.95 511.95 23.55 o 2 24 1 700.89 717.15 26.87 o 3 24 1 566.34 559.26 25.30 o 4 24 1 344.67 381.69 24.58 o 5 24 1 2199.20 2256.13 54.14 o 6 24 1 723.27 738.41 35.25 o 7 24 1 2575.60 2753.49 64.02 o 8 24 1 567.14 646.03 53.89 o 0 25 1 3878.69 3997.77 135.14 o 1 25 1 4861.82 4977.33 83.76 o 2 25 1 288.86 307.82 22.55 o 3 25 1 225.69 257.82 21.31 o 4 25 1 492.59 518.35 26.34 o 5 25 1 3457.24 3631.58 136.12 o 6 25 1 556.71 550.54 33.03 o 7 25 1 7.88 7.38 32.68 o 1 26 1 1985.24 2235.58 45.90 o 2 26 1 279.80 280.41 24.93 o 3 26 1 131.83 118.92 21.19 o 4 26 1 17.77 21.68 21.86 o 5 26 1 1473.66 1638.94 57.56 o 6 26 1 1842.96 2018.27 104.68 o 7 26 1 2693.51 2703.58 93.54 o 0 27 1 560.35 476.49 54.90 o 1 27 1 3882.49 4185.35 81.82 o 2 27 1 553.08 571.94 34.94 o 3 27 1 367.14 375.73 29.20 o 4 27 1 1244.25 1317.74 51.69 o 5 27 1 1637.50 1738.98 99.41 o 6 27 1 85.99 152.43 39.68 o 1 28 1 59.83 97.57 23.56 o 2 28 1 75.99 118.66 25.51 o 3 28 1 1025.72 1087.06 59.36 o 4 28 1 279.84 358.15 42.39 o 5 28 1 784.84 874.95 70.91 o 0 29 1 293.91 364.76 60.94 o 1 29 1 1410.09 1380.01 63.09 o 2 29 1 1056.21 1158.58 78.30 o 3 29 1 2454.70 2853.85 99.60 o 4 29 1 303.94 314.04 43.05 o 1 30 1 1.51 49.29 55.76 o 2 30 1 144.54 191.83 31.79 o 3 30 1 829.38 847.32 55.63 o 0 0 2 12559.13 12347.84 83.48 o 1 0 2 10617.38 10120.07 136.09 o 2 0 2 9.34 31.21 11.65 o 3 0 2 12382.25 13306.89 102.96 o 4 0 2 10738.31 12305.55 107.76 o 5 0 2 26227.32 26924.01 139.25 o 6 0 2 930.51 945.10 34.20 o 7 0 2 1035.00 1099.75 40.08 o 8 0 2 809.10 825.95 37.59 o 9 0 2 514.70 496.87 39.80 o 10 0 2 130.30 158.53 25.32 o 11 0 2 106.39 129.13 27.45 o 12 0 2 171.20 250.02 45.03 o 1 1 2 7065.71 6866.21 39.37 o 2 1 2 415.60 504.17 9.06 o 3 1 2 872.80 903.59 15.04 o 4 1 2 1142.21 1255.40 22.76 o 5 1 2 7907.91 8019.49 65.26 o 6 1 2 8496.27 8562.04 72.07 o 7 1 2 17329.66 17103.56 136.94 o 8 1 2 655.27 712.03 24.67 o 9 1 2 1911.12 1861.56 41.31 o 10 1 2 424.94 404.81 22.87 o 11 1 2 3075.42 3103.21 60.80 o 12 1 2 754.33 749.72 34.33 o 0 2 2 15439.06 15626.44 123.34 o 1 2 2 24754.32 24468.06 186.19 o 2 2 2 2910.01 3221.77 30.21 o 3 2 2 17746.42 18622.71 183.67 o 4 2 2 38.93 33.03 5.51 o 5 2 2 2158.39 2110.37 27.53 o 6 2 2 3376.09 3491.82 46.78 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2 814.73 786.19 34.78 o 5 23 2 1440.16 1382.39 38.43 o 6 23 2 396.18 406.57 26.71 o 7 23 2 3904.71 4052.35 149.70 o 8 23 2 251.44 241.59 54.79 o 0 24 2 913.69 909.71 63.90 o 1 24 2 2386.02 2370.37 52.77 o 2 24 2 1166.70 1139.14 34.13 o 3 24 2 4294.99 4225.22 63.52 o 4 24 2 130.60 160.75 19.74 o 5 24 2 562.43 538.22 28.36 o 6 24 2 31.14 29.20 17.47 o 7 24 2 147.00 134.17 51.23 o 8 24 2 66.36 65.25 48.86 o 1 25 2 222.01 214.41 23.08 o 2 25 2 3.04 22.97 15.41 o 3 25 2 1868.91 1904.72 44.24 o 4 25 2 1172.43 1188.97 37.26 o 5 25 2 2272.71 2383.10 51.86 o 6 25 2 189.80 232.24 30.69 o 7 25 2 538.85 438.42 64.17 o 0 26 2 13.56 7.78 25.25 o 1 26 2 1560.12 1559.48 45.40 o 2 26 2 1620.73 1608.63 46.59 o 3 26 2 5641.16 5632.70 93.96 o 4 26 2 199.05 193.66 22.53 o 5 26 2 4.14 21.10 21.29 o 6 26 2 32.98 18.26 33.41 o 1 27 2 18.35 64.00 24.13 o 2 27 2 124.41 101.41 22.26 o 3 27 2 1255.43 1247.55 38.57 o 4 27 2 1266.02 1381.80 46.65 o 5 27 2 1160.93 1215.08 51.73 o 0 28 2 951.01 1042.94 57.95 o 1 28 2 2622.97 2663.95 61.14 o 2 28 2 255.18 235.52 29.59 o 3 28 2 1354.68 1420.71 63.87 o 4 28 2 273.82 296.26 33.65 o 1 29 2 815.48 845.16 53.86 o 2 29 2 157.81 104.47 33.43 o 3 29 2 558.71 608.13 49.67 o 0 30 2 230.66 259.60 57.59 o 1 30 2 2386.93 2596.56 192.41 o 1 0 3 389.86 444.43 11.67 o 2 0 3 4219.13 4688.86 51.78 o 3 0 3 16.37 27.12 7.12 o 4 0 3 18232.08 18839.33 325.66 o 5 0 3 412.73 457.70 24.09 o 6 0 3 1088.78 1086.45 38.17 o 7 0 3 178.21 189.29 21.56 o 8 0 3 11134.67 10615.38 136.35 o 9 0 3 161.58 157.99 23.70 o 10 0 3 4317.98 4260.67 96.88 o 11 0 3 105.82 128.54 27.84 o 0 1 3 12092.62 12431.67 62.56 o 1 1 3 131.53 133.90 5.45 o 2 1 3 33087.39 32640.58 184.09 o 3 1 3 19.21 29.34 4.86 o 4 1 3 3665.50 3724.87 42.29 o 5 1 3 295.48 298.47 14.36 o 6 1 3 59.90 73.77 13.55 o 7 1 3 45.74 32.94 10.10 o 8 1 3 1720.57 1594.69 37.28 o 9 1 3 4.88 17.62 11.69 o 10 1 3 1808.52 1701.50 43.60 o 11 1 3 0.54 13.18 16.00 o 12 1 3 924.13 882.79 66.65 o 1 2 3 682.90 735.85 11.52 o 2 2 3 3557.70 3637.85 53.40 o 3 2 3 274.16 272.63 9.16 o 4 2 3 11618.85 11652.65 62.67 o 5 2 3 13.41 11.84 6.53 o 6 2 3 6263.68 6363.15 81.97 o 7 2 3 2015.05 2087.38 39.45 o 8 2 3 6236.89 5956.01 71.86 o 9 2 3 102.14 98.78 15.36 o 10 2 3 4421.92 4337.14 77.85 o 11 2 3 11.86 6.19 14.69 o 12 2 3 925.51 873.88 52.33 o 0 3 3 37097.62 37125.05 350.97 o 1 3 3 117.65 115.22 5.30 o 2 3 3 10033.72 9760.87 52.57 o 3 3 3 30.01 35.31 5.24 o 4 3 3 6194.32 6212.02 47.70 o 5 3 3 330.58 332.18 12.43 o 6 3 3 4201.64 4049.41 46.31 o 7 3 3 0.36 0.65 8.03 o 8 3 3 484.70 485.04 20.22 o 9 3 3 0.48 -7.13 10.19 o 10 3 3 275.46 265.88 19.95 o 11 3 3 0.03 19.05 14.77 o 12 3 3 1080.43 1098.80 85.63 o 1 4 3 136.62 176.21 5.75 o 2 4 3 3260.53 3302.86 38.66 o 3 4 3 237.32 238.09 10.32 o 4 4 3 2163.54 2183.00 26.50 o 5 4 3 354.32 332.16 12.38 o 6 4 3 17549.34 17090.79 163.76 o 7 4 3 459.70 483.92 18.92 o 8 4 3 5082.44 4958.62 58.51 o 9 4 3 223.85 228.49 17.77 o 10 4 3 2342.07 2282.69 45.44 o 11 4 3 99.41 99.92 20.28 o 12 4 3 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37.33 o 9 7 3 26.70 15.97 13.07 o 10 7 3 342.93 419.64 27.12 o 11 7 3 16.98 10.81 19.01 o 12 7 3 824.68 763.81 69.78 o 1 8 3 51.71 58.58 7.62 o 2 8 3 122.83 146.02 9.35 o 3 8 3 13.07 7.91 6.02 o 4 8 3 8846.51 8880.35 60.50 o 5 8 3 117.62 106.86 10.87 o 6 8 3 11026.79 10482.12 92.79 o 7 8 3 92.76 85.97 12.43 o 8 8 3 4821.56 4904.03 68.16 o 9 8 3 20.86 27.45 13.84 o 10 8 3 2942.63 3004.78 68.67 o 11 8 3 78.58 87.53 22.06 o 12 8 3 957.03 849.66 72.69 o 0 9 3 10426.92 10049.94 111.01 o 1 9 3 282.84 293.39 15.03 o 2 9 3 15714.32 15193.86 170.90 o 3 9 3 30.90 53.14 9.13 o 4 9 3 6289.55 6087.62 58.11 o 5 9 3 614.45 608.46 19.34 o 6 9 3 537.64 562.11 19.98 o 7 9 3 2.76 -1.11 9.34 o 8 9 3 280.28 330.97 22.96 o 9 9 3 77.52 77.61 24.54 o 10 9 3 1350.81 1403.22 42.16 o 11 9 3 64.05 75.59 26.09 o 12 9 3 543.77 487.17 58.67 o 1 10 3 1.07 -5.49 7.35 o 2 10 3 699.80 788.23 26.04 o 3 10 3 148.60 145.12 12.16 o 4 10 3 14148.28 13732.68 192.50 o 5 10 3 318.30 307.14 20.31 o 6 10 3 1837.25 1794.93 39.20 o 7 10 3 63.08 83.69 14.62 o 8 10 3 7015.45 6963.08 129.13 o 9 10 3 19.76 15.99 14.39 o 10 10 3 3537.82 3474.15 123.65 o 11 10 3 56.37 71.40 39.15 o 12 10 3 446.92 545.19 69.24 o 0 11 3 3378.68 3416.73 66.24 o 1 11 3 194.64 178.31 14.03 o 2 11 3 24221.27 23028.44 263.34 o 3 11 3 12.23 8.42 8.46 o 4 11 3 2869.73 2769.92 40.98 o 5 11 3 40.23 32.20 11.28 o 6 11 3 110.99 152.09 16.26 o 7 11 3 12.42 3.64 11.75 o 8 11 3 1064.68 1009.19 34.27 o 9 11 3 34.71 20.25 18.40 o 10 11 3 1483.11 1465.78 52.70 o 11 11 3 1.65 -15.53 35.70 o 1 12 3 70.39 60.47 10.79 o 2 12 3 736.77 764.05 22.03 o 3 12 3 63.29 47.18 9.95 o 4 12 3 9897.29 9345.00 121.58 o 5 12 3 0.45 -8.05 10.71 o 6 12 3 2956.60 2981.62 54.02 o 7 12 3 293.17 272.60 21.61 o 8 12 3 5386.41 5195.81 78.21 o 9 12 3 12.13 -9.61 17.41 o 10 12 3 3328.63 3207.67 76.05 o 11 12 3 37.79 45.30 38.18 o 0 13 3 18008.97 17335.17 194.67 o 1 13 3 74.36 80.59 14.05 o 2 13 3 7965.47 7773.59 69.19 o 3 13 3 653.41 617.49 20.85 o 4 13 3 3648.85 3667.02 52.76 o 5 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5502.08 5510.81 75.65 o 6 3 4 1204.12 1195.02 32.33 o 7 3 4 3272.67 3217.55 56.76 o 8 3 4 1989.70 1999.97 43.92 o 9 3 4 3215.16 3112.76 58.01 o 10 3 4 1414.12 1433.07 42.86 o 11 3 4 539.53 555.11 36.30 o 12 3 4 246.55 228.65 53.82 o 0 4 4 2034.39 1956.54 31.36 o 1 4 4 6236.46 6242.97 46.21 o 2 4 4 6926.01 6919.02 57.56 o 3 4 4 11279.61 10945.95 142.71 o 4 4 4 1233.62 1179.92 27.35 o 5 4 4 23.26 18.71 9.26 o 6 4 4 366.32 362.42 19.13 o 7 4 4 422.78 419.38 21.77 o 8 4 4 62.74 66.01 14.67 o 9 4 4 13.48 32.22 15.40 o 10 4 4 48.78 55.16 17.10 o 11 4 4 955.41 934.93 43.90 o 1 5 4 725.32 688.06 16.10 o 2 5 4 838.31 840.86 19.59 o 3 5 4 6817.95 6741.38 115.33 o 4 5 4 968.53 1047.15 32.79 o 5 5 4 3733.90 3650.64 88.18 o 6 5 4 2434.40 2347.73 52.94 o 7 5 4 1504.26 1477.35 66.33 o 8 5 4 2672.34 2478.21 58.98 o 9 5 4 4805.30 4828.17 143.77 o 10 5 4 620.71 662.58 37.14 o 11 5 4 521.61 444.57 61.26 o 0 6 4 3007.57 2969.07 47.74 o 1 6 4 4678.35 4648.34 43.81 o 2 6 4 3337.95 3298.34 38.76 o 3 6 4 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1501.18 31.08 o 4 9 4 1290.36 1262.49 29.57 o 5 9 4 2007.17 2046.98 42.34 o 6 9 4 1610.11 1588.51 46.62 o 7 9 4 6170.60 5969.50 93.31 o 8 9 4 1537.93 1498.66 49.44 o 9 9 4 762.85 758.67 50.05 o 10 9 4 1130.59 1137.97 58.29 o 11 9 4 1484.09 1533.88 95.34 o 0 10 4 3545.32 3308.03 69.56 o 1 10 4 8725.13 8287.74 79.24 o 2 10 4 3006.68 2845.34 42.27 o 3 10 4 1148.50 1092.15 27.39 o 4 10 4 1910.59 1856.14 35.81 o 5 10 4 3865.81 3715.27 58.56 o 6 10 4 407.73 398.80 26.81 o 7 10 4 89.75 89.74 19.12 o 8 10 4 8.79 -5.57 16.89 o 9 10 4 1.15 -3.92 18.90 o 10 10 4 5.36 3.99 34.62 o 11 10 4 250.52 271.79 54.90 o 1 11 4 6680.43 6198.92 103.13 o 2 11 4 2562.47 2382.06 39.53 o 3 11 4 787.11 742.38 23.56 o 4 11 4 298.80 321.53 20.87 o 5 11 4 1270.34 1280.60 35.68 o 6 11 4 1994.80 1957.15 44.38 o 7 11 4 4964.93 4770.81 85.00 o 8 11 4 1193.73 1144.07 45.33 o 9 11 4 989.31 976.52 44.00 o 10 11 4 679.63 685.08 65.57 o 11 11 4 1273.63 1248.61 89.30 o 0 12 4 8521.95 8029.24 114.78 o 1 12 4 6229.22 5947.78 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34.21 o 5 15 4 1569.87 1526.13 41.93 o 6 15 4 834.75 815.97 32.81 o 7 15 4 891.00 930.82 36.11 o 8 15 4 1690.65 1791.44 59.45 o 9 15 4 3610.45 3773.01 142.37 o 10 15 4 537.57 543.25 65.79 o 0 16 4 1753.21 1676.81 57.16 o 1 16 4 2777.30 2667.67 51.26 o 2 16 4 1714.36 1691.93 37.64 o 3 16 4 6672.83 6537.38 77.96 o 4 16 4 1984.42 1924.13 40.67 o 5 16 4 32.98 18.93 15.13 o 6 16 4 92.23 85.79 17.86 o 7 16 4 542.00 509.31 29.59 o 8 16 4 41.74 28.69 37.64 o 9 16 4 15.38 30.63 40.12 o 1 17 4 313.26 315.76 22.59 o 2 17 4 4.66 -0.03 12.18 o 3 17 4 1163.23 1148.78 32.44 o 4 17 4 746.69 693.26 30.42 o 5 17 4 3178.21 3182.35 61.10 o 6 17 4 1860.00 1809.35 48.12 o 7 17 4 1251.74 1282.32 42.92 o 8 17 4 1015.42 1053.50 79.27 o 9 17 4 2003.81 1942.86 105.37 o 0 18 4 1260.34 1257.01 54.05 o 1 18 4 2752.32 2764.04 54.74 o 2 18 4 1769.81 1762.37 39.81 o 3 18 4 2300.33 2212.93 50.20 o 4 18 4 984.43 977.15 35.47 o 5 18 4 1408.64 1354.61 41.85 o 6 18 4 665.81 659.56 32.41 o 7 18 4 19.97 38.26 27.47 o 8 18 4 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8951.97 8522.52 108.88 o 4 1 5 872.57 807.22 29.84 o 5 1 5 604.71 570.77 27.94 o 6 1 5 2.15 -1.34 12.50 o 7 1 5 551.38 604.55 32.63 o 8 1 5 28.50 36.74 16.83 o 9 1 5 130.42 117.08 24.30 o 10 1 5 414.72 427.64 37.17 o 1 2 5 3.66 0.03 7.30 o 2 2 5 235.07 237.87 13.56 o 3 2 5 3335.94 3364.28 49.74 o 4 2 5 905.90 941.03 32.01 o 5 2 5 3821.15 3742.35 68.15 o 6 2 5 1104.77 1025.09 36.85 o 7 2 5 3163.42 3042.69 79.23 o 8 2 5 726.74 694.30 34.72 o 9 2 5 2101.62 2167.83 61.22 o 10 2 5 138.92 123.96 25.83 o 0 3 5 887.87 900.71 26.92 o 1 3 5 10379.18 10483.92 61.11 o 2 3 5 1190.04 1168.77 26.35 o 3 3 5 1949.78 1988.76 35.53 o 4 3 5 283.87 308.34 18.86 o 5 3 5 2600.97 2544.63 47.77 o 6 3 5 83.85 99.90 20.56 o 7 3 5 173.76 192.73 27.89 o 8 3 5 27.74 41.46 21.18 o 9 3 5 50.38 55.51 25.28 o 10 3 5 54.40 53.18 27.07 o 1 4 5 1863.67 1977.02 29.27 o 2 4 5 1315.71 1306.08 26.14 o 3 4 5 828.24 786.76 23.65 o 4 4 5 190.03 203.87 20.23 o 5 4 5 3687.17 3740.96 97.80 o 6 4 5 812.13 838.58 35.09 o 7 4 5 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