#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103701.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103701_Fobs loop_ _publ_author_name 'Ohhara, Takashi' 'Uekusa, Hidehiro' 'Ohashi, Yuji' 'Tanaka, Ichiro' 'Kumazawa, Shintaro' 'Niimura, Nobuo' _publ_section_title ; Direct observation of deuterium migration in crystalline-state reaction by single-crystal neutron diffraction. III. Photoracemization of 1-cyanoethyl cobaloxime complexes ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 551 _journal_page_last 559 _journal_volume 57 _journal_year 2001 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.626 _cell_angle_gamma 90.000 _cell_length_a 16.0665 _cell_length_b 12.5929 _cell_length_c 9.6440 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.7690 _[local]_cod_data_source_file bs00162-initialsup2.hkl _[local]_cod_data_source_block 2-initial #BEGIN Tags that were not found in dictionaries: _shelx_title ' master afc7r(right).xtl Nov.15 96 (Mo)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 223.57 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -16 0 496.31 464.68 23.20 o 1 -16 0 185.82 172.54 19.59 o 2 -16 0 150.49 152.54 18.85 o 3 -16 0 135.36 116.08 19.49 o 4 -16 0 43.76 27.02 31.61 o 1 -15 0 3.45 6.80 28.23 o 2 -15 0 31.06 45.83 16.62 o 3 -15 0 3.92 -12.99 29.61 o 4 -15 0 5.03 -15.56 30.27 o 5 -15 0 1.36 -31.05 31.05 o 6 -15 0 66.49 65.36 17.64 o 7 -15 0 20.70 12.74 28.67 o 8 -15 0 87.19 68.99 18.96 o 0 -14 0 84.32 72.58 16.42 o 1 -14 0 817.31 764.04 43.30 o 2 -14 0 93.69 97.42 16.61 o 3 -14 0 471.46 447.99 24.94 o 4 -14 0 100.96 128.72 17.05 o 5 -14 0 127.99 148.45 16.88 o 6 -14 0 6.53 -4.02 27.71 o 7 -14 0 189.61 194.10 18.60 o 8 -14 0 3.40 21.78 20.55 o 9 -14 0 137.17 148.30 18.91 o 10 -14 0 33.02 20.82 17.83 o 1 -13 0 39.39 33.84 26.02 o 2 -13 0 88.11 86.60 15.90 o 3 -13 0 27.78 15.62 27.48 o 4 -13 0 264.59 280.62 18.57 o 5 -13 0 140.17 116.50 16.82 o 6 -13 0 81.71 102.09 15.66 o 7 -13 0 57.53 33.25 28.73 o 8 -13 0 26.50 44.56 15.78 o 9 -13 0 229.38 244.86 19.43 o 10 -13 0 48.86 -6.50 29.08 o 11 -13 0 143.01 147.75 18.90 o 12 -13 0 109.08 103.50 19.15 o 0 -12 0 121.97 101.83 14.82 o 1 -12 0 8.36 -7.35 24.09 o 2 -12 0 776.33 762.48 36.61 o 3 -12 0 343.53 301.45 17.30 o 4 -12 0 1382.52 1372.82 45.06 o 5 -12 0 31.49 22.96 24.21 o 6 -12 0 418.15 424.72 22.80 o 7 -12 0 6.80 -8.25 26.10 o 8 -12 0 325.12 324.75 18.50 o 9 -12 0 95.24 78.74 17.94 o 10 -12 0 323.13 313.69 19.97 o 11 -12 0 110.11 126.58 17.94 o 12 -12 0 102.12 111.32 17.64 o 13 -12 0 71.31 27.81 33.02 o 14 -12 0 1.51 8.67 31.11 o 1 -11 0 46.40 29.10 23.27 o 2 -11 0 354.55 426.37 20.23 o 3 -11 0 68.73 104.99 13.24 o 4 -11 0 155.04 138.06 14.49 o 5 -11 0 148.15 139.68 14.66 o 6 -11 0 160.82 150.15 15.52 o 7 -11 0 124.70 125.07 15.35 o 8 -11 0 17.36 -0.96 24.95 o 9 -11 0 455.06 502.62 23.83 o 10 -11 0 78.52 30.44 28.91 o 11 -11 0 625.12 617.98 27.27 o 12 -11 0 98.38 99.78 17.34 o 13 -11 0 129.56 151.50 17.70 o 14 -11 0 101.73 119.38 17.35 o 15 -11 0 22.77 33.34 31.82 o 0 -10 0 1962.74 1942.26 43.66 o 1 -10 0 1434.83 1426.85 40.04 o 2 -10 0 301.52 299.91 14.78 o 3 -10 0 292.62 311.28 17.98 o 4 -10 0 496.04 451.66 20.16 o 5 -10 0 594.63 568.76 30.63 o 6 -10 0 766.07 766.56 34.70 o 7 -10 0 445.47 469.50 22.20 o 8 -10 0 51.79 84.98 13.66 o 9 -10 0 950.61 991.90 39.76 o 10 -10 0 72.65 97.66 15.54 o 11 -10 0 346.35 342.54 18.78 o 12 -10 0 122.26 114.76 17.41 o 13 -10 0 2.88 -26.93 28.39 o 14 -10 0 102.08 123.86 17.01 o 15 -10 0 56.07 42.25 31.97 o 16 -10 0 56.62 84.59 17.35 o 1 -9 0 54.21 62.99 11.60 o 2 -9 0 255.21 251.05 13.11 o 3 -9 0 165.64 175.94 12.58 o 4 -9 0 21.64 -19.79 19.79 o 5 -9 0 193.62 206.37 13.07 o 6 -9 0 437.08 473.90 19.53 o 7 -9 0 392.08 456.50 20.14 o 8 -9 0 496.70 546.22 31.06 o 9 -9 0 532.85 602.15 31.85 o 10 -9 0 483.52 567.09 23.54 o 11 -9 0 62.19 33.64 27.09 o 12 -9 0 293.65 327.13 18.13 o 13 -9 0 29.33 45.63 14.92 o 14 -9 0 337.41 375.72 20.66 o 15 -9 0 3.27 -27.67 27.67 o 16 -9 0 235.25 249.16 20.23 o 17 -9 0 6.02 7.82 30.09 o 0 -8 0 709.46 735.18 26.73 o 1 -8 0 4201.88 4023.43 52.65 o 2 -8 0 648.77 665.55 26.15 o 3 -8 0 1282.73 1243.24 33.24 o 4 -8 0 267.87 269.96 15.84 o 5 -8 0 679.71 771.29 28.88 o 6 -8 0 725.76 762.97 31.40 o 7 -8 0 2702.01 2918.58 50.90 o 8 -8 0 774.82 769.76 33.12 o 9 -8 0 582.00 606.45 31.73 o 10 -8 0 120.21 137.59 13.87 o 11 -8 0 18.70 23.32 22.37 o 12 -8 0 47.24 7.26 26.97 o 13 -8 0 138.71 167.39 16.35 o 14 -8 0 318.27 354.38 19.16 o 15 -8 0 142.27 154.43 17.55 o 16 -8 0 232.77 281.00 19.20 o 17 -8 0 37.58 36.18 29.76 o 18 -8 0 52.28 28.39 32.58 o 1 -7 0 99.60 86.07 9.77 o 2 -7 0 13.63 22.73 16.27 o 3 -7 0 608.63 584.83 24.58 o 4 -7 0 105.16 111.06 10.31 o 5 -7 0 10.64 16.18 16.49 o 6 -7 0 4518.67 4622.32 57.86 o 7 -7 0 323.20 326.10 16.76 o 8 -7 0 1512.26 1695.25 40.13 o 9 -7 0 989.82 1010.36 35.14 o 10 -7 0 112.52 96.55 13.07 o 11 -7 0 118.74 151.89 13.66 o 12 -7 0 21.27 28.91 22.56 o 13 -7 0 267.59 370.39 21.35 o 14 -7 0 257.32 276.36 17.87 o 15 -7 0 237.95 276.42 18.81 o 16 -7 0 257.58 274.72 19.02 o 17 -7 0 186.88 204.47 19.15 o 18 -7 0 26.32 71.45 16.87 o 0 -6 0 1489.57 1096.36 26.58 o 1 -6 0 139.30 157.68 9.59 o 2 -6 0 4252.81 4223.95 46.07 o 3 -6 0 30.82 13.60 11.58 o 4 -6 0 9035.11 9646.41 71.49 o 5 -6 0 413.05 429.83 22.45 o 6 -6 0 7086.70 7647.92 68.38 o 7 -6 0 528.26 559.52 25.34 o 8 -6 0 1533.09 1654.42 38.29 o 9 -6 0 143.23 142.45 12.77 o 10 -6 0 291.70 310.92 17.53 o 11 -6 0 156.29 178.79 13.79 o 12 -6 0 98.23 134.54 14.09 o 13 -6 0 182.63 207.37 15.95 o 14 -6 0 107.34 97.62 15.65 o 15 -6 0 356.42 436.86 24.37 o 16 -6 0 60.94 72.78 16.90 o 17 -6 0 206.14 225.37 19.09 o 18 -6 0 11.73 -29.41 29.41 o 19 -6 0 109.46 133.24 18.87 o 1 -5 0 34.02 55.06 8.30 o 2 -5 0 485.86 576.04 20.69 o 3 -5 0 5057.80 5471.27 49.29 o 4 -5 0 1349.12 1393.16 28.82 o 5 -5 0 5681.47 6336.33 56.81 o 6 -5 0 852.38 878.90 26.36 o 7 -5 0 816.00 876.80 27.23 o 8 -5 0 323.05 433.67 22.95 o 9 -5 0 316.71 295.71 16.01 o 10 -5 0 672.46 742.95 29.79 o 11 -5 0 640.18 728.18 31.06 o 12 -5 0 132.43 156.17 13.75 o 13 -5 0 730.65 772.35 36.98 o 14 -5 0 1.54 -3.45 23.61 o 15 -5 0 440.80 505.06 23.38 o 16 -5 0 43.30 37.88 27.19 o 17 -5 0 136.23 151.74 18.05 o 18 -5 0 42.68 -17.74 30.59 o 19 -5 0 93.30 90.50 18.50 o 0 -4 0 443.68 434.02 17.39 o 1 -4 0 1214.21 1162.36 22.51 o 2 -4 0 4643.65 4826.22 40.98 o 3 -4 0 30395.42 30599.40 102.72 o 4 -4 0 5323.96 5734.17 48.47 o 5 -4 0 22937.72 25192.21 103.04 o 6 -4 0 3170.58 3537.28 43.03 o 7 -4 0 1157.72 1198.47 28.49 o 8 -4 0 166.80 188.74 10.56 o 9 -4 0 160.00 147.57 11.02 o 10 -4 0 466.58 601.99 26.36 o 11 -4 0 947.52 1074.83 33.50 o 12 -4 0 278.61 322.60 15.03 o 13 -4 0 433.03 465.93 21.19 o 14 -4 0 189.81 237.98 15.36 o 15 -4 0 66.84 64.70 14.62 o 16 -4 0 75.35 30.83 26.60 o 17 -4 0 23.14 31.16 26.68 o 18 -4 0 104.41 93.43 17.07 o 19 -4 0 85.93 73.29 16.86 o 20 -4 0 87.08 84.12 18.04 o 1 -3 0 8031.30 8367.77 44.75 o 2 -3 0 43.67 17.21 12.68 o 3 -3 0 32461.78 33707.79 97.21 o 4 -3 0 3929.94 4116.22 38.63 o 5 -3 0 1197.55 1227.20 25.52 o 6 -3 0 4259.15 4594.96 45.80 o 7 -3 0 1206.49 1448.09 29.75 o 8 -3 0 1851.25 1872.91 35.15 o 9 -3 0 81.69 97.86 10.19 o 10 -3 0 1012.49 1066.86 31.44 o 11 -3 0 362.71 352.05 18.02 o 12 -3 0 1641.92 1735.77 42.35 o 13 -3 0 417.12 502.48 21.03 o 14 -3 0 162.64 198.71 14.23 o 15 -3 0 60.09 51.13 13.92 o 16 -3 0 58.87 30.85 26.48 o 17 -3 0 9.90 -27.04 27.04 o 18 -3 0 203.80 135.14 16.88 o 19 -3 0 1.55 16.90 27.82 o 20 -3 0 49.38 -15.08 31.02 o 0 -2 0 9611.23 9868.64 38.34 o 1 -2 0 22485.17 22393.18 59.22 o 2 -2 0 9355.77 9716.03 43.07 o 3 -2 0 32448.78 32628.60 85.88 o 4 -2 0 5350.51 5658.48 41.03 o 5 -2 0 1837.26 1649.30 26.60 o 6 -2 0 521.13 496.85 19.49 o 7 -2 0 6373.21 6988.51 56.82 o 8 -2 0 817.94 937.51 26.15 o 9 -2 0 2274.70 2624.74 41.37 o 10 -2 0 2213.39 2372.26 42.20 o 11 -2 0 50.72 57.51 10.87 o 12 -2 0 1232.79 1333.18 37.14 o 13 -2 0 198.14 250.53 14.73 o 14 -2 0 185.45 215.56 15.03 o 15 -2 0 56.97 79.73 14.40 o 16 -2 0 97.79 134.69 14.43 o 17 -2 0 16.41 -1.44 27.53 o 18 -2 0 77.33 9.12 26.91 o 19 -2 0 30.53 6.18 28.83 o 20 -2 0 49.23 18.10 29.84 o 2 -1 0 1931.79 2155.01 18.37 o 3 -1 0 68.29 55.26 5.90 o 4 -1 0 229.53 269.76 14.09 o 5 -1 0 527.56 521.36 17.98 o 6 -1 0 297.42 292.07 16.85 o 7 -1 0 3808.73 4005.33 43.12 o 8 -1 0 985.72 1001.69 26.33 o 9 -1 0 2405.37 2681.40 41.09 o 10 -1 0 3673.60 3875.91 50.99 o 11 -1 0 498.22 481.70 26.57 o 12 -1 0 823.25 940.64 31.36 o 13 -1 0 489.04 609.83 29.47 o 14 -1 0 96.34 126.00 13.55 o 15 -1 0 457.62 551.08 31.70 o 16 -1 0 164.95 148.12 15.91 o 17 -1 0 11.66 -18.29 25.60 o 18 -1 0 3.50 34.94 26.62 o 19 -1 0 39.29 35.21 16.22 o 20 -1 0 0.48 -31.00 31.00 o 2 0 0 49985.77 43335.61 206.06 o 3 0 0 0.33 -7.28 9.17 o 4 0 0 2558.84 2684.18 27.03 o 5 0 0 6.49 0.26 13.12 o 6 0 0 692.83 650.51 20.19 o 7 0 0 87.45 95.45 8.86 o 8 0 0 2849.01 2996.39 40.36 o 9 0 0 865.66 908.44 27.43 o 10 0 0 3502.04 3906.13 51.44 o 11 0 0 433.78 450.10 25.42 o 12 0 0 142.40 148.54 12.84 o 13 0 0 193.80 120.43 13.07 o 14 0 0 72.34 6.18 22.41 o 15 0 0 330.45 248.98 15.96 o 16 0 0 50.44 15.23 24.90 o 17 0 0 30.48 13.99 24.54 o 18 0 0 30.85 28.61 19.55 o 19 0 0 4.33 -3.54 25.29 o 20 0 0 3.96 26.59 28.66 o -4 -16 1 3.26 -5.84 31.45 o -3 -16 1 22.73 26.78 31.35 o -2 -16 1 8.18 -13.98 30.10 o -1 -16 1 22.77 12.62 30.88 o 0 -16 1 5.73 -21.77 21.77 o 1 -16 1 0.62 16.83 27.95 o 2 -16 1 28.21 14.20 31.12 o 3 -16 1 5.65 -19.07 30.58 o -8 -15 1 25.67 30.77 31.09 o -7 -15 1 34.66 3.11 29.02 o -6 -15 1 1.86 3.41 29.18 o -5 -15 1 87.16 81.70 16.93 o -4 -15 1 23.89 19.36 29.27 o -3 -15 1 383.19 354.15 21.39 o -2 -15 1 10.12 22.68 29.36 o -1 -15 1 310.72 312.13 20.28 o 0 -15 1 42.81 51.94 11.62 o 1 -15 1 449.79 419.52 21.30 o 2 -15 1 10.19 38.41 28.38 o 3 -15 1 346.96 317.93 20.69 o 4 -15 1 70.34 90.71 17.39 o 5 -15 1 320.09 299.28 21.28 o 6 -15 1 94.82 70.76 18.78 o 7 -15 1 237.47 218.91 20.16 o -10 -14 1 76.03 96.62 18.81 o -9 -14 1 62.43 83.35 17.30 o -8 -14 1 25.27 34.72 27.64 o -7 -14 1 24.64 37.32 26.65 o -6 -14 1 84.34 66.85 17.36 o -5 -14 1 67.83 70.25 16.32 o -4 -14 1 75.77 90.51 16.23 o -3 -14 1 113.81 80.00 16.58 o -2 -14 1 0.27 -20.22 26.58 o -1 -14 1 8.83 -21.25 25.33 o 0 -14 1 82.24 92.38 11.13 o 1 -14 1 8.52 -29.41 29.41 o 2 -14 1 3.18 -28.74 28.74 o 3 -14 1 1.95 18.37 25.77 o 4 -14 1 129.95 138.79 16.76 o 5 -14 1 9.38 28.24 19.78 o 6 -14 1 70.48 82.92 17.30 o 7 -14 1 152.17 144.60 18.13 o 8 -14 1 78.23 57.59 18.14 o 9 -14 1 116.73 115.41 17.59 o 10 -14 1 35.57 40.26 17.80 o -12 -13 1 46.46 77.01 17.01 o -11 -13 1 136.83 140.90 19.02 o -10 -13 1 9.05 -29.90 29.90 o -9 -13 1 51.23 -25.52 28.43 o -8 -13 1 14.60 15.12 27.90 o -7 -13 1 27.75 21.58 26.09 o -6 -13 1 202.43 215.07 17.29 o -5 -13 1 63.74 16.56 28.01 o -4 -13 1 200.80 214.92 16.87 o -3 -13 1 359.43 327.75 18.72 o -2 -13 1 530.80 590.73 34.08 o -1 -13 1 28.26 30.47 24.54 o 0 -13 1 659.66 655.26 21.80 o 1 -13 1 158.39 141.14 16.73 o 2 -13 1 436.02 452.04 24.75 o 3 -13 1 812.71 771.54 39.28 o 4 -13 1 594.24 666.36 38.24 o 5 -13 1 346.79 336.88 19.07 o 6 -13 1 239.64 220.22 17.32 o 7 -13 1 266.37 248.19 18.76 o 8 -13 1 28.93 -14.10 28.62 o 9 -13 1 279.01 270.83 19.19 o 10 -13 1 69.13 58.57 17.97 o 11 -13 1 96.86 114.17 17.92 o 12 -13 1 173.19 150.86 19.94 o -14 -12 1 4.25 30.83 27.59 o -13 -12 1 85.20 108.47 17.73 o -12 -12 1 3.08 23.66 15.46 o -11 -12 1 100.81 108.28 17.22 o -10 -12 1 13.97 0.25 26.84 o -9 -12 1 75.39 74.62 16.17 o -8 -12 1 20.04 17.26 26.44 o -7 -12 1 91.91 87.38 15.46 o -6 -12 1 122.03 147.04 15.55 o -5 -12 1 75.01 80.99 14.78 o -4 -12 1 263.32 249.04 17.11 o -3 -12 1 235.15 244.62 16.41 o -2 -12 1 180.58 175.47 15.69 o -1 -12 1 12.39 5.38 23.18 o 0 -12 1 42.61 36.54 11.66 o 1 -12 1 14.70 21.03 22.32 o 2 -12 1 197.82 191.93 15.40 o 3 -12 1 31.59 11.60 24.43 o 4 -12 1 25.02 -1.15 26.45 o 5 -12 1 471.74 487.77 23.68 o 6 -12 1 68.38 75.59 15.06 o 7 -12 1 361.45 389.77 19.24 o 8 -12 1 101.07 106.40 15.96 o 9 -12 1 503.97 518.05 26.43 o 10 -12 1 30.79 -14.92 28.50 o 11 -12 1 334.16 352.67 20.66 o 12 -12 1 138.97 136.39 18.70 o 13 -12 1 107.44 106.54 19.36 o -15 -11 1 20.76 30.68 21.47 o -14 -11 1 47.62 77.46 16.49 o -13 -11 1 50.30 48.13 16.92 o -12 -11 1 15.21 -14.37 28.14 o -11 -11 1 45.53 21.16 26.74 o -10 -11 1 87.54 96.08 15.91 o -9 -11 1 213.38 193.13 16.83 o -8 -11 1 49.33 55.76 14.32 o -7 -11 1 145.87 134.75 15.32 o -6 -11 1 482.21 504.67 22.46 o -5 -11 1 181.53 185.40 15.33 o -4 -11 1 1230.30 1155.82 41.22 o -3 -11 1 102.11 94.34 13.50 o -2 -11 1 197.77 193.32 14.50 o -1 -11 1 26.92 10.48 22.22 o 0 -11 1 1015.91 998.65 26.27 o 1 -11 1 23.15 24.85 21.91 o 2 -11 1 2285.09 2285.94 51.24 o 3 -11 1 359.32 354.48 16.91 o 4 -11 1 1639.73 1659.40 46.03 o 5 -11 1 66.94 45.89 13.79 o 6 -11 1 722.81 705.89 35.97 o 7 -11 1 96.41 94.19 14.57 o 8 -11 1 631.52 603.74 25.71 o 9 -11 1 295.92 273.17 18.52 o 10 -11 1 855.20 794.45 43.29 o 11 -11 1 238.03 265.83 19.09 o 12 -11 1 191.17 163.37 18.90 o 13 -11 1 87.91 61.93 17.20 o 14 -11 1 15.23 -21.88 28.93 o 15 -11 1 64.05 73.19 17.94 o -16 -10 1 44.11 32.73 30.77 o -15 -10 1 48.76 81.11 16.92 o -14 -10 1 105.59 120.00 17.66 o -13 -10 1 38.30 21.34 26.53 o -12 -10 1 64.12 -12.06 28.66 o -11 -10 1 209.54 237.59 16.57 o -10 -10 1 41.09 25.39 25.33 o -9 -10 1 164.23 163.99 15.16 o -8 -10 1 4.05 12.10 22.69 o -7 -10 1 68.92 75.54 13.55 o -6 -10 1 278.47 275.41 14.68 o -5 -10 1 35.34 39.00 12.77 o -4 -10 1 42.03 30.48 11.91 o -3 -10 1 37.33 35.97 11.72 o -2 -10 1 85.70 94.19 12.49 o -1 -10 1 34.09 19.83 22.10 o 0 -10 1 62.02 53.53 8.74 o 1 -10 1 16.11 9.30 14.59 o 2 -10 1 23.27 29.10 21.21 o 3 -10 1 68.38 55.26 12.87 o 4 -10 1 307.08 316.39 15.33 o 5 -10 1 99.20 102.14 13.52 o 6 -10 1 1106.26 1143.71 39.66 o 7 -10 1 18.29 8.35 13.41 o 8 -10 1 437.65 454.90 23.43 o 9 -10 1 1246.30 1300.60 45.00 o 10 -10 1 311.67 329.44 18.26 o 11 -10 1 867.58 853.52 41.20 o 12 -10 1 369.10 370.54 20.06 o 13 -10 1 86.64 87.19 16.58 o 14 -10 1 190.54 209.75 18.04 o 15 -10 1 35.24 14.52 32.43 o 16 -10 1 73.85 94.16 18.31 o -17 -9 1 1.59 -29.27 29.89 o 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21.32 o 11 -9 2 97.89 86.09 15.27 o 12 -9 2 819.81 834.43 42.30 o 13 -9 2 28.83 18.23 29.83 o 14 -9 2 291.02 318.81 19.45 o 15 -9 2 4.56 10.10 29.59 o 16 -9 2 27.01 14.45 30.28 o -18 -8 2 11.23 12.50 30.66 o -17 -8 2 37.42 30.61 21.73 o -16 -8 2 231.85 209.60 19.35 o -15 -8 2 120.23 134.09 16.46 o -14 -8 2 159.60 153.06 16.98 o -13 -8 2 127.85 112.56 15.59 o -12 -8 2 52.71 55.26 14.93 o -11 -8 2 199.63 221.94 15.46 o -10 -8 2 133.48 151.37 13.99 o -9 -8 2 60.56 67.81 12.84 o -8 -8 2 61.91 49.67 12.83 o -7 -8 2 347.41 381.61 17.58 o -6 -8 2 6.39 -10.97 18.63 o -5 -8 2 310.87 345.70 17.05 o -4 -8 2 701.77 721.43 28.55 o -3 -8 2 2574.32 2665.96 46.11 o -2 -8 2 742.06 751.55 28.84 o -1 -8 2 7305.07 7481.91 72.05 o 0 -8 2 514.31 503.22 18.38 o 1 -8 2 1733.22 1825.01 38.65 o 2 -8 2 259.79 272.21 15.69 o 3 -8 2 2198.12 2044.04 41.93 o 4 -8 2 144.08 139.87 12.00 o 5 -8 2 700.30 691.44 28.81 o 6 -8 2 180.72 165.95 12.85 o 7 -8 2 328.84 316.93 14.99 o 8 -8 2 292.59 293.21 14.48 o 9 -8 2 418.91 365.27 19.93 o 10 -8 2 37.72 22.96 23.29 o 11 -8 2 492.30 408.43 18.66 o 12 -8 2 239.85 247.90 17.42 o 13 -8 2 635.48 636.34 27.43 o 14 -8 2 141.51 167.65 17.80 o 15 -8 2 84.38 91.39 16.57 o 16 -8 2 25.04 24.46 15.89 o 17 -8 2 5.02 -23.92 30.72 o -18 -7 2 28.94 27.91 29.18 o -17 -7 2 98.29 91.54 17.39 o -16 -7 2 130.34 123.62 17.64 o -15 -7 2 183.88 183.21 16.75 o -14 -7 2 16.43 15.06 24.11 o -13 -7 2 337.67 352.46 17.71 o -12 -7 2 38.71 68.38 13.71 o -11 -7 2 290.05 343.08 20.03 o -10 -7 2 172.95 195.17 14.37 o -9 -7 2 349.33 377.17 19.00 o -8 -7 2 92.89 83.25 11.65 o -7 -7 2 254.73 239.33 12.69 o -6 -7 2 101.59 94.54 11.10 o -5 -7 2 58.42 72.65 10.37 o -4 -7 2 261.54 260.73 14.76 o -3 -7 2 574.80 584.40 25.08 o -2 -7 2 174.63 206.58 11.00 o -1 -7 2 394.11 403.52 21.45 o 0 -7 2 188.91 172.40 7.61 o 1 -7 2 21.50 2.08 16.56 o 2 -7 2 963.87 1048.00 29.32 o 3 -7 2 527.08 488.87 24.06 o 4 -7 2 107.11 132.22 10.78 o 5 -7 2 1884.67 1887.32 39.58 o 6 -7 2 24.87 32.66 10.75 o 7 -7 2 160.18 141.65 12.69 o 8 -7 2 160.46 172.99 13.62 o 9 -7 2 273.81 273.32 14.72 o 10 -7 2 52.81 61.24 13.48 o 11 -7 2 1011.21 1135.23 40.23 o 12 -7 2 188.99 190.75 16.00 o 13 -7 2 603.24 702.49 36.23 o 14 -7 2 231.21 244.09 18.00 o 15 -7 2 417.73 501.13 26.16 o 16 -7 2 63.29 77.64 17.15 o 17 -7 2 29.41 38.39 28.84 o 18 -7 2 26.37 -19.85 34.07 o -19 -6 2 124.15 77.51 18.29 o -18 -6 2 0.49 -10.79 29.15 o -17 -6 2 266.84 215.13 19.25 o -16 -6 2 4.64 -15.55 26.72 o -15 -6 2 267.49 282.40 17.70 o -14 -6 2 32.12 26.59 23.96 o -13 -6 2 391.08 385.30 21.76 o -12 -6 2 35.31 59.60 12.74 o -11 -6 2 83.34 82.69 13.02 o -10 -6 2 374.78 417.49 18.65 o -9 -6 2 187.49 197.83 12.98 o -8 -6 2 735.67 777.33 29.39 o -7 -6 2 179.89 187.03 11.80 o -6 -6 2 590.65 502.69 24.09 o -5 -6 2 23.99 31.44 9.58 o -4 -6 2 3890.77 3709.05 47.30 o -3 -6 2 202.21 206.83 10.80 o -2 -6 2 896.84 803.71 24.60 o -1 -6 2 25.85 45.04 8.67 o 0 -6 2 3265.17 3227.12 30.09 o 1 -6 2 93.38 93.42 9.38 o 2 -6 2 2741.34 2707.71 39.90 o 3 -6 2 777.54 821.06 25.99 o 4 -6 2 2259.19 2103.74 37.73 o 5 -6 2 291.15 338.70 15.70 o 6 -6 2 4388.63 4432.21 55.07 o 7 -6 2 171.54 195.33 12.30 o 8 -6 2 651.27 635.87 28.20 o 9 -6 2 174.42 211.09 12.98 o 10 -6 2 514.34 544.47 29.41 o 11 -6 2 276.52 308.47 15.23 o 12 -6 2 536.23 561.29 31.78 o 13 -6 2 258.67 266.50 16.61 o 14 -6 2 228.81 229.68 17.08 o 15 -6 2 305.36 325.17 19.01 o 16 -6 2 3.36 22.94 25.67 o 17 -6 2 132.16 133.73 18.05 o 18 -6 2 3.00 23.22 16.63 o -19 -5 2 120.41 100.22 18.32 o -18 -5 2 23.15 -31.71 31.71 o -17 -5 2 60.98 35.79 27.59 o -16 -5 2 32.10 61.55 13.67 o -15 -5 2 153.45 174.94 15.40 o -14 -5 2 159.62 148.34 15.44 o -13 -5 2 298.12 323.49 16.88 o -12 -5 2 83.18 89.97 13.64 o -11 -5 2 138.68 162.33 12.65 o -10 -5 2 314.97 326.48 16.80 o -9 -5 2 268.36 307.44 16.28 o -8 -5 2 515.75 610.61 26.20 o -7 -5 2 398.43 413.12 20.87 o -6 -5 2 944.38 915.02 26.84 o -5 -5 2 757.64 750.15 24.34 o -4 -5 2 510.78 547.65 21.89 o -3 -5 2 183.08 181.10 9.67 o -2 -5 2 20.91 24.65 8.23 o -1 -5 2 752.97 760.25 22.66 o 0 -5 2 38.07 50.46 5.96 o 1 -5 2 219.20 250.41 12.23 o 2 -5 2 2112.82 2277.56 35.24 o 3 -5 2 237.30 277.33 12.88 o 4 -5 2 1080.46 1140.37 27.96 o 5 -5 2 49.34 49.58 9.23 o 6 -5 2 1807.92 2100.23 37.64 o 7 -5 2 444.93 459.95 24.02 o 8 -5 2 948.84 1023.68 31.41 o 9 -5 2 31.76 17.92 10.97 o 10 -5 2 328.62 355.84 17.75 o 11 -5 2 391.73 398.37 19.79 o 12 -5 2 241.46 267.51 15.20 o 13 -5 2 545.18 606.36 32.82 o 14 -5 2 147.90 158.05 15.81 o 15 -5 2 859.91 1039.22 43.88 o 16 -5 2 204.79 214.80 18.43 o 17 -5 2 378.13 413.31 22.13 o 18 -5 2 28.11 4.78 32.42 o 19 -5 2 86.17 120.24 18.51 o -20 -4 2 115.70 86.47 17.56 o -19 -4 2 98.36 16.07 30.02 o -18 -4 2 193.43 128.11 17.71 o -17 -4 2 67.19 22.32 27.77 o -16 -4 2 167.87 151.25 16.00 o -15 -4 2 8.12 -24.73 24.73 o -14 -4 2 95.10 92.01 14.78 o -13 -4 2 192.09 210.04 15.15 o -12 -4 2 283.08 273.42 14.84 o -11 -4 2 31.31 34.54 11.09 o -10 -4 2 493.79 546.24 26.11 o -9 -4 2 37.31 48.37 10.15 o -8 -4 2 963.56 994.16 28.53 o -7 -4 2 783.95 904.84 26.83 o -6 -4 2 2996.82 2948.55 41.01 o -5 -4 2 1236.05 1265.86 27.77 o -4 -4 2 715.79 788.55 23.07 o -3 -4 2 159.79 128.67 8.75 o -2 -4 2 2393.12 2800.24 34.99 o -1 -4 2 584.93 662.05 20.37 o 0 -4 2 1039.98 988.72 35.04 o 1 -4 2 1827.74 1696.65 27.81 o 2 -4 2 2516.84 2486.32 33.36 o 3 -4 2 6828.72 6762.19 53.79 o 4 -4 2 1860.12 1856.60 31.79 o 5 -4 2 3375.35 3288.86 41.67 o 6 -4 2 1928.09 1911.52 34.65 o 7 -4 2 962.08 919.23 28.30 o 8 -4 2 1811.55 1766.78 36.96 o 9 -4 2 1357.04 1410.47 34.64 o 10 -4 2 1050.02 928.25 32.43 o 11 -4 2 336.91 337.57 19.49 o 12 -4 2 150.78 140.19 13.36 o 13 -4 2 29.42 20.61 22.78 o 14 -4 2 280.52 274.03 16.48 o 15 -4 2 141.79 171.23 16.48 o 16 -4 2 269.84 314.53 18.63 o 17 -4 2 92.66 124.90 16.25 o 18 -4 2 216.81 248.57 19.85 o 19 -4 2 36.21 27.99 18.58 o -20 -3 2 67.05 -17.68 32.76 o -19 -3 2 28.54 -29.13 29.13 o -18 -3 2 196.08 127.31 17.37 o -17 -3 2 4.75 27.27 25.19 o -16 -3 2 332.22 300.82 18.04 o -15 -3 2 5.70 0.30 25.50 o -14 -3 2 225.95 261.05 15.61 o -13 -3 2 53.66 71.46 12.58 o -12 -3 2 319.72 359.25 18.31 o -11 -3 2 141.86 171.88 12.11 o -10 -3 2 151.03 171.06 11.52 o -9 -3 2 99.55 109.65 10.26 o -8 -3 2 117.98 88.51 9.77 o -7 -3 2 1119.61 1125.61 27.66 o -6 -3 2 3398.63 3789.70 43.78 o -5 -3 2 520.54 583.58 21.21 o -4 -3 2 1027.10 970.39 23.33 o -3 -3 2 975.12 993.06 22.12 o -2 -3 2 578.47 610.26 18.95 o -1 -3 2 988.81 1085.00 21.62 o 0 -3 2 115.91 115.99 12.28 o 1 -3 2 38.83 43.31 7.60 o 2 -3 2 36.91 32.45 7.64 o 3 -3 2 1919.39 1746.38 27.86 o 4 -3 2 595.85 457.54 18.94 o 5 -3 2 994.81 784.78 23.33 o 6 -3 2 895.99 813.66 23.85 o 7 -3 2 687.31 597.81 23.51 o 8 -3 2 2908.86 2264.56 39.24 o 9 -3 2 185.91 150.63 11.46 o 10 -3 2 2282.95 1791.81 40.64 o 11 -3 2 345.43 303.25 17.40 o 12 -3 2 413.89 327.06 18.57 o 13 -3 2 167.36 115.74 14.00 o 14 -3 2 635.80 454.97 21.93 o 15 -3 2 40.84 45.25 14.26 o 16 -3 2 830.08 1073.42 44.24 o 17 -3 2 10.87 10.17 19.74 o 18 -3 2 423.97 597.50 27.31 o 19 -3 2 10.85 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209.13 206.95 10.22 o -7 0 2 0.72 9.10 14.44 o -6 0 2 3167.28 3633.06 39.53 o -5 0 2 31.25 25.65 7.92 o -4 0 2 2396.17 2615.36 30.10 o -3 0 2 591.40 572.24 16.63 o -2 0 2 16590.69 17537.92 61.84 o -1 0 2 1.41 -1.08 10.11 o 0 0 2 10792.71 10717.39 45.97 o 15 0 2 285.99 303.34 17.53 o 16 0 2 288.89 375.15 18.75 o 17 0 2 193.01 200.13 17.48 o 18 0 2 4.76 23.86 28.57 o 19 0 2 270.51 324.27 20.13 o 20 0 2 16.02 28.15 31.22 o -7 -15 3 6.70 -29.20 30.07 o -6 -15 3 5.24 51.81 16.33 o -5 -15 3 248.14 257.65 20.45 o -4 -15 3 20.81 -6.75 30.02 o -3 -15 3 384.77 356.88 21.62 o -2 -15 3 18.44 -31.48 31.48 o -1 -15 3 86.51 -13.62 33.14 o 0 -15 3 4.19 18.82 19.87 o 1 -15 3 34.99 34.55 26.46 o 2 -15 3 0.74 10.49 29.23 o 3 -15 3 80.71 74.12 18.52 o 4 -15 3 25.46 2.73 30.07 o 5 -15 3 209.23 182.47 20.66 o 6 -15 3 16.56 45.27 33.09 o -9 -14 3 90.03 97.51 18.73 o -8 -14 3 35.58 31.29 30.56 o -7 -14 3 127.25 1.02 35.54 o -6 -14 3 74.84 91.52 16.95 o -5 -14 3 33.71 70.32 15.99 o -4 -14 3 17.70 40.70 27.26 o 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253.08 20.14 o 10 -13 3 13.76 0.53 30.44 o 11 -13 3 19.35 22.44 29.16 o -13 -12 3 74.28 77.14 18.13 o -12 -12 3 10.93 -12.74 29.81 o -11 -12 3 148.52 148.40 18.03 o -10 -12 3 76.70 32.82 30.32 o -9 -12 3 277.89 292.53 18.50 o -8 -12 3 92.94 93.53 16.98 o -7 -12 3 316.98 309.20 19.24 o -6 -12 3 64.42 53.67 15.36 o -5 -12 3 47.64 48.89 15.05 o -4 -12 3 17.76 -25.89 25.89 o -3 -12 3 104.93 112.76 15.55 o -2 -12 3 44.16 28.32 25.44 o -1 -12 3 4.24 -15.22 26.43 o 0 -12 3 49.91 49.67 10.26 o 1 -12 3 18.53 33.49 13.50 o 2 -12 3 104.67 76.20 15.59 o 3 -12 3 4.90 30.18 23.30 o 4 -12 3 170.44 188.88 16.69 o 5 -12 3 12.29 45.16 14.08 o 6 -12 3 7.18 -10.85 26.63 o 7 -12 3 103.16 111.95 16.14 o 8 -12 3 41.93 7.81 28.61 o 9 -12 3 169.42 208.39 18.33 o 10 -12 3 24.94 -14.50 29.41 o 11 -12 3 87.47 101.10 18.09 o 12 -12 3 3.52 -31.19 31.19 o -14 -11 3 16.40 31.24 29.05 o -13 -11 3 157.88 119.07 18.58 o -12 -11 3 49.18 42.58 28.91 o -11 -11 3 123.72 98.64 16.97 o -10 -11 3 202.75 193.90 17.51 o -9 -11 3 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