#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103711.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103711_Fobs loop_ _publ_author_name 'K\'alm\'an, Alajos' 'Argay, Gyula' 'F\'abi\'an, L\'aszl\'o' 'Bern\'ath, G\'abor' 'F\"ul\"op, Ferenc' _publ_section_title ; Basic forms of supramolecular self-assembly organized by parallel and antiparallel hydrogen bonds in the racemic crystal structures of six disubstituted and trisubstituted cyclopentane derivatives ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 539 _journal_page_last 550 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.030 _cell_angle_gamma 90.000 _cell_length_a 16.8620 _cell_length_b 6.1040 _cell_length_c 10.5190 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.7981 _[local]_cod_data_source_file de00115sup6.hkl _[local]_cod_data_source_block 5 #BEGIN Tags that were not found in dictionaries: _shelx_title ' BG29 C10-H18-O3 P21/C Z=4' _shelx_refln_list_code 4 _shelx_F_calc_maximum 112.59 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y+1/2, z+1/2' '-x, -y, -z' '-x, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4630.77 5887.77 106.20 o 2 0 0 261.02 243.38 4.15 o 3 0 0 356.24 293.22 7.67 o 4 0 0 6371.69 6060.47 40.52 o 5 0 0 141.61 140.75 4.79 o 6 0 0 975.97 919.49 19.15 o 7 0 0 80.02 67.92 2.94 o 8 0 0 1748.09 1715.27 31.45 o 9 0 0 1806.16 1762.83 34.67 o 10 0 0 495.31 481.33 20.16 o 11 0 0 618.93 658.00 25.18 o 12 0 0 155.13 157.74 7.82 o 13 0 0 142.51 135.66 7.70 o 14 0 0 27.41 26.79 1.33 o 15 0 0 0.48 0.00 0.00 o 16 0 0 33.67 37.24 1.55 o 17 0 0 1.00 1.82 0.56 o 18 0 0 6.05 7.23 0.80 o 19 0 0 5.89 8.65 0.74 o 20 0 0 2.55 5.65 0.65 o 1 1 0 39.31 34.38 1.61 o 2 1 0 247.97 211.91 6.66 o 3 1 0 2.58 3.37 0.31 o 4 1 0 150.90 123.38 6.06 o 5 1 0 475.79 388.23 11.72 o 6 1 0 65.16 59.94 2.97 o 7 1 0 705.88 614.33 17.46 o 8 1 0 20.89 20.15 0.83 o 9 1 0 335.38 340.71 15.53 o 10 1 0 144.55 130.94 7.45 o 11 1 0 67.71 66.85 3.18 o 12 1 0 9.38 7.01 0.80 o 13 1 0 1.92 2.38 3.37 o 14 1 0 8.73 7.05 0.77 o 15 1 0 66.81 65.46 3.83 o 16 1 0 9.53 10.35 0.83 o 17 1 0 2.86 2.63 0.65 o 18 1 0 24.79 26.05 1.45 o 19 1 0 0.04 0.00 0.00 o 20 1 0 0.54 0.90 0.49 o 0 2 0 4837.16 5131.31 44.31 o 1 2 0 162.63 141.00 5.38 o 2 2 0 770.08 756.55 17.27 o 3 2 0 717.24 730.29 17.41 o 4 2 0 328.78 307.49 11.73 o 5 2 0 97.84 83.85 3.86 o 6 2 0 524.43 499.93 16.61 o 7 2 0 15.36 11.87 0.77 o 8 2 0 103.49 110.89 5.38 o 9 2 0 17.89 13.84 0.87 o 10 2 0 0.39 0.80 0.49 o 11 2 0 16.22 16.16 1.05 o 12 2 0 35.26 33.53 1.73 o 13 2 0 89.98 74.12 4.02 o 14 2 0 2.52 1.58 0.68 o 15 2 0 0.02 1.61 0.49 o 16 2 0 9.72 13.10 1.02 o 17 2 0 21.63 23.27 1.14 o 18 2 0 1.39 1.88 0.49 o 19 2 0 2.82 3.49 0.49 o 1 3 0 40.50 46.21 2.04 o 2 3 0 1674.47 1687.50 33.64 o 3 3 0 1232.39 1194.18 29.12 o 4 3 0 311.28 319.93 15.41 o 5 3 0 2.00 2.01 0.53 o 6 3 0 253.08 247.71 10.46 o 7 3 0 162.61 164.37 7.30 o 8 3 0 354.98 322.42 13.03 o 9 3 0 79.29 86.82 3.80 o 10 3 0 0.34 0.00 0.00 o 11 3 0 17.08 13.54 1.02 o 12 3 0 6.81 5.96 0.80 o 13 3 0 50.57 50.78 2.53 o 14 3 0 153.72 152.14 6.86 o 15 3 0 55.62 53.16 3.21 o 16 3 0 4.51 2.44 3.15 o 17 3 0 10.36 11.68 0.87 o 18 3 0 0.34 0.00 0.00 o 0 4 0 347.27 428.38 21.32 o 1 4 0 48.45 48.31 2.47 o 2 4 0 43.88 51.37 2.53 o 3 4 0 12.57 9.36 0.96 o 4 4 0 285.38 338.02 14.60 o 5 4 0 51.67 52.02 2.10 o 6 4 0 141.61 159.87 8.50 o 7 4 0 184.82 192.14 9.46 o 8 4 0 0.00 1.36 3.62 o 9 4 0 82.04 82.22 3.80 o 11 4 0 0.23 0.00 0.00 o 12 4 0 2.57 2.29 3.24 o 13 4 0 92.34 82.66 4.48 o 14 4 0 20.35 17.40 1.11 o 15 4 0 38.27 40.61 2.07 o 16 4 0 4.01 4.20 0.59 o 17 4 0 24.69 30.26 1.73 o 1 5 0 36.05 46.79 2.01 o 2 5 0 16.52 14.62 1.30 o 3 5 0 0.65 0.00 0.00 o 5 5 0 35.31 37.64 1.85 o 6 5 0 1.39 1.55 4.08 o 7 5 0 8.94 8.37 0.96 o 8 5 0 43.29 46.23 2.16 o 9 5 0 11.77 9.33 0.99 o 10 5 0 4.64 3.03 0.90 o 11 5 0 57.17 45.90 2.60 o 12 5 0 18.29 13.26 1.08 o 13 5 0 2.74 2.47 0.56 o 14 5 0 2.61 1.85 2.41 o 15 5 0 4.06 4.14 0.59 o 0 6 0 82.54 70.16 2.81 o 1 6 0 27.80 30.32 1.92 o 2 6 0 7.46 6.74 1.11 o 3 6 0 27.73 29.48 1.70 o 4 6 0 71.03 70.01 3.46 o 5 6 0 111.99 96.05 5.97 o 6 6 0 45.20 39.71 1.79 o 8 6 0 0.65 0.96 0.56 o 9 6 0 11.65 11.37 0.96 o 10 6 0 0.01 0.00 0.00 o 11 6 0 21.12 16.10 1.14 o 12 6 0 0.45 0.00 0.00 o 2 7 0 13.34 15.27 1.14 o 3 7 0 0.18 0.00 0.00 o 4 7 0 17.89 17.83 1.17 o 5 7 0 3.07 1.33 0.71 o 6 7 0 2.27 1.33 1.88 o 7 7 0 0.08 0.00 0.00 o 8 7 0 9.44 7.97 0.83 o -20 1 1 0.16 0.00 0.00 o -19 1 1 2.72 1.48 2.78 o -18 1 1 14.71 16.32 1.11 o -17 1 1 51.26 56.81 2.84 o -16 1 1 2.58 1.17 3.12 o -15 1 1 9.98 11.77 1.17 o -14 1 1 33.70 42.52 2.35 o -13 1 1 370.89 417.15 16.96 o -12 1 1 72.16 63.89 3.28 o -10 1 1 301.16 337.20 12.34 o -9 1 1 27.68 29.54 1.51 o -8 1 1 369.91 381.63 15.54 o -7 1 1 849.54 818.38 20.95 o -6 1 1 199.98 215.30 9.87 o -5 1 1 1.58 3.09 0.37 o -4 1 1 612.90 593.74 13.66 o -3 1 1 1756.70 1748.67 21.36 o -2 1 1 12677.45 13034.59 264.00 o -1 1 1 435.85 399.22 9.07 o 0 1 1 9946.67 10828.51 226.11 o 1 1 1 56.12 46.32 2.35 o 2 1 1 1413.16 1348.76 17.53 o 3 1 1 81.76 82.47 3.34 o 4 1 1 1359.96 1270.98 20.03 o 5 1 1 735.55 681.33 16.02 o 6 1 1 1733.61 1563.01 26.11 o 7 1 1 20.70 23.58 0.93 o 8 1 1 1.84 0.62 1.61 o 9 1 1 0.84 0.12 0.40 o 10 1 1 19.05 18.79 0.93 o 11 1 1 12.42 13.94 0.90 o 12 1 1 5.64 4.48 0.65 o 13 1 1 10.02 13.26 1.05 o 14 1 1 309.04 296.25 13.39 o 15 1 1 45.46 47.44 2.38 o 16 1 1 0.01 0.00 0.00 o 17 1 1 0.02 0.00 0.00 o 18 1 1 2.30 0.62 3.12 o 19 1 1 0.53 0.00 0.00 o -19 2 1 0.63 0.00 0.00 o -18 2 1 0.02 0.00 0.00 o -17 2 1 10.50 7.45 0.90 o -16 2 1 0.45 1.42 0.62 o -15 2 1 46.86 43.92 2.41 o -14 2 1 104.39 96.04 3.71 o -13 2 1 4.30 4.42 0.71 o -12 2 1 7.59 6.95 0.77 o -11 2 1 59.86 66.88 3.09 o -10 2 1 246.04 259.19 12.00 o -9 2 1 300.33 296.70 11.51 o -8 2 1 279.64 246.89 9.78 o -7 2 1 194.17 197.14 8.10 o -6 2 1 17.41 13.41 0.68 o -5 2 1 48.06 57.15 2.53 o -4 2 1 102.30 107.85 5.04 o -3 2 1 641.96 578.30 15.92 o -2 2 1 535.84 502.61 14.36 o -1 2 1 857.04 813.67 18.09 o 0 2 1 6501.25 6266.60 48.89 o 1 2 1 1936.53 1826.91 26.60 o 2 2 1 72.82 58.68 2.97 o 3 2 1 17.23 9.77 0.49 o 4 2 1 10.03 7.26 0.49 o 5 2 1 153.61 137.55 6.03 o 6 2 1 21.23 23.86 1.27 o 7 2 1 14.46 12.61 0.71 o 8 2 1 124.58 113.77 6.65 o 9 2 1 0.27 0.00 0.00 o 10 2 1 170.49 151.20 7.17 o 11 2 1 212.59 221.32 11.10 o 12 2 1 153.12 160.89 8.16 o 13 2 1 29.04 28.65 1.36 o 14 2 1 32.86 34.43 1.82 o 15 2 1 2.33 2.22 0.62 o 16 2 1 0.35 0.00 0.00 o 17 2 1 18.60 22.44 1.39 o 18 2 1 0.88 0.00 0.00 o -18 3 1 6.96 6.86 0.68 o -17 3 1 93.73 102.29 4.82 o -16 3 1 16.65 18.88 1.11 o -15 3 1 37.77 33.56 1.61 o -14 3 1 6.42 8.90 0.93 o -13 3 1 48.81 47.66 2.41 o -12 3 1 58.76 55.97 3.74 o -11 3 1 34.43 32.51 1.55 o -10 3 1 0.00 0.00 0.00 o -9 3 1 186.18 202.97 8.91 o -8 3 1 38.75 54.58 2.75 o -7 3 1 66.11 78.57 4.42 o -6 3 1 54.06 56.50 3.34 o -5 3 1 22.13 26.24 1.14 o -4 3 1 0.28 0.00 0.00 o -3 3 1 25.56 25.34 1.24 o -2 3 1 1076.36 1264.50 29.45 o -1 3 1 102.19 118.53 5.29 o 0 3 1 703.63 762.54 21.80 o 1 3 1 414.98 439.79 17.34 o 2 3 1 92.01 86.65 4.85 o 3 3 1 64.64 58.45 3.12 o 4 3 1 63.64 64.07 3.00 o 5 3 1 62.44 67.35 3.15 o 6 3 1 320.69 391.18 18.94 o 7 3 1 262.63 267.65 11.51 o 8 3 1 5.92 6.09 0.83 o 9 3 1 10.41 8.22 0.80 o 10 3 1 0.94 1.17 3.09 o 11 3 1 4.15 6.03 0.77 o 12 3 1 31.78 28.71 1.42 o 13 3 1 56.96 47.07 2.47 o 14 3 1 0.97 0.34 0.53 o 15 3 1 32.51 33.93 1.79 o 16 3 1 16.59 14.65 0.93 o 17 3 1 0.49 1.45 0.46 o 18 3 1 2.03 2.44 0.53 o -17 4 1 16.76 16.72 1.05 o -16 4 1 2.46 1.45 2.04 o -15 4 1 16.05 15.14 1.02 o -14 4 1 14.02 9.49 0.93 o -13 4 1 1.69 1.48 0.65 o -12 4 1 156.41 137.40 6.18 o -11 4 1 51.87 43.61 1.92 o -10 4 1 41.49 43.76 2.13 o -9 4 1 0.14 0.00 0.00 o -8 4 1 3.87 7.32 0.99 o -7 4 1 52.68 46.85 2.04 o -6 4 1 88.18 106.24 4.67 o -5 4 1 311.22 376.38 15.62 o -4 4 1 124.44 149.63 6.92 o -3 4 1 327.05 402.25 15.81 o -2 4 1 314.92 329.37 14.29 o -1 4 1 7.91 11.96 0.96 o 0 4 1 94.13 126.77 7.14 o 1 4 1 152.79 180.94 8.84 o 2 4 1 46.78 43.89 1.95 o 3 4 1 324.96 390.60 15.78 o 4 4 1 124.96 136.06 7.82 o 5 4 1 3.17 3.68 0.87 o 6 4 1 687.62 710.63 31.81 o 7 4 1 126.83 152.35 7.17 o 8 4 1 8.63 8.93 0.93 o 9 4 1 70.24 63.14 3.68 o 10 4 1 58.98 58.72 3.18 o 11 4 1 138.31 121.31 5.69 o 13 4 1 8.49 8.19 0.83 o 14 4 1 59.17 62.87 3.00 o 15 4 1 27.82 30.90 1.82 o 16 4 1 1.66 1.82 0.49 o -15 5 1 0.97 1.48 0.49 o -14 5 1 0.07 0.00 0.00 o -13 5 1 0.22 0.00 0.00 o -12 5 1 1.80 0.00 0.00 o -11 5 1 11.27 7.23 0.90 o -10 5 1 0.60 1.05 0.65 o -9 5 1 8.85 7.94 1.02 o -8 5 1 16.69 15.51 1.30 o -7 5 1 48.48 47.16 2.94 o -6 5 1 47.76 53.53 2.38 o -5 5 1 18.71 19.47 1.64 o -4 5 1 10.02 15.39 1.36 o -3 5 1 74.78 89.82 4.54 o -2 5 1 88.11 94.74 3.77 o -1 5 1 2.54 4.70 0.96 o 0 5 1 18.26 6.18 7.26 o 1 5 1 17.50 22.96 1.55 o 3 5 1 38.85 45.34 2.19 o 4 5 1 24.72 28.25 1.61 o 5 5 1 42.63 46.85 1.98 o 6 5 1 0.10 0.00 0.00 o 7 5 1 0.36 0.00 0.00 o 8 5 1 0.54 0.00 0.00 o 9 5 1 42.42 38.85 2.07 o 10 5 1 31.83 28.49 1.45 o 11 5 1 0.29 0.00 0.00 o 12 5 1 1.66 0.00 0.00 o 13 5 1 0.55 0.65 1.76 o 14 5 1 4.46 5.56 0.65 o -12 6 1 22.75 16.19 1.14 o -11 6 1 2.86 2.75 0.62 o -9 6 1 5.03 4.98 0.77 o -8 6 1 1.06 1.67 0.59 o -7 6 1 0.01 0.00 0.00 o -6 6 1 3.97 4.17 0.87 o -5 6 1 0.22 0.68 0.65 o -4 6 1 5.78 5.22 0.96 o -3 6 1 17.19 15.20 1.42 o -2 6 1 77.32 75.48 4.23 o -1 6 1 34.70 39.74 2.04 o 0 6 1 28.91 27.75 1.70 o 1 6 1 26.16 26.18 1.61 o 2 6 1 3.13 3.15 0.90 o 3 6 1 0.19 0.56 0.74 o 4 6 1 5.72 5.93 0.90 o 5 6 1 2.34 3.77 0.80 o 6 6 1 39.21 37.12 1.70 o 7 6 1 8.81 5.22 5.62 o 8 6 1 1.79 0.93 2.47 o 9 6 1 0.12 1.08 0.40 o 10 6 1 5.35 5.10 0.71 o 11 6 1 1.28 0.43 0.49 o -8 7 1 6.39 5.87 0.77 o -7 7 1 3.94 1.79 2.32 o -6 7 1 0.16 0.22 0.49 o -5 7 1 1.26 1.88 0.68 o -4 7 1 0.02 0.00 0.00 o -3 7 1 22.00 20.95 1.27 o -2 7 1 13.48 11.59 1.21 o -1 7 1 0.02 0.00 0.00 o 0 7 1 1.32 1.42 0.65 o 1 7 1 1.05 0.00 0.00 o 2 7 1 0.40 0.00 0.00 o 3 7 1 8.22 8.13 0.83 o 4 7 1 13.69 12.98 1.05 o 5 7 1 7.60 6.33 0.77 o 6 7 1 2.20 1.33 0.62 o 7 7 1 5.25 5.32 0.68 o -20 0 2 4.60 6.77 0.83 o -19 0 2 1.19 2.07 0.65 o -18 0 2 6.31 1.14 4.08 o -17 0 2 0.17 0.00 0.00 o -16 0 2 36.66 41.57 1.89 o -15 0 2 0.01 1.58 0.71 o -14 0 2 970.02 1026.71 39.16 o -13 0 2 52.97 46.42 2.29 o -12 0 2 681.11 669.92 27.79 o -11 0 2 405.04 439.25 20.37 o -10 0 2 136.95 167.76 8.10 o -9 0 2 639.94 575.09 19.15 o -8 0 2 301.46 247.30 11.33 o -7 0 2 940.94 844.72 19.26 o -6 0 2 2387.63 2003.57 27.26 o -5 0 2 2881.65 2331.56 27.10 o -4 0 2 1.75 1.21 0.31 o -3 0 2 3661.07 3379.51 28.72 o -1 0 2 2018.81 1589.93 16.61 o 0 0 2 108.01 125.77 6.00 o 1 0 2 1602.36 1758.91 21.10 o 2 0 2 0.21 0.00 0.00 o 3 0 2 3873.30 3523.05 32.17 o 4 0 2 67.08 59.42 2.72 o 5 0 2 586.70 542.36 14.45 o 6 0 2 1090.78 1059.83 21.91 o 7 0 2 53.28 56.65 2.84 o 8 0 2 51.06 54.43 2.69 o 9 0 2 86.71 79.91 3.49 o 11 0 2 243.15 248.41 11.41 o 12 0 2 533.58 521.90 24.52 o 13 0 2 48.57 45.96 2.13 o 14 0 2 297.89 276.69 12.13 o 15 0 2 0.84 0.90 3.18 o 16 0 2 0.83 1.64 0.49 o 17 0 2 8.59 9.09 0.74 o 18 0 2 0.36 0.49 1.82 o 19 0 2 8.62 11.62 0.74 o -20 1 2 4.89 8.31 0.87 o -19 1 2 0.15 0.00 0.00 o -18 1 2 10.17 10.44 0.96 o -17 1 2 4.57 2.94 0.74 o -16 1 2 1.55 0.00 0.00 o -15 1 2 0.69 0.00 0.00 o -14 1 2 0.00 0.00 0.00 o -13 1 2 79.97 92.85 4.51 o -12 1 2 338.00 356.42 15.07 o -11 1 2 121.25 146.97 5.66 o -10 1 2 6.20 6.21 0.62 o -9 1 2 13.02 14.62 0.80 o -8 1 2 297.07 298.34 14.17 o -7 1 2 1745.39 1698.35 30.84 o -6 1 2 91.06 67.49 4.30 o -5 1 2 5.19 5.01 0.46 o -4 1 2 98.89 94.93 4.11 o -3 1 2 3602.49 3097.81 29.77 o -2 1 2 1082.80 878.72 14.57 o -1 1 2 132.70 117.13 5.57 o 0 1 2 29.19 26.89 1.24 o 1 1 2 1664.26 1611.19 20.33 o 2 1 2 525.70 480.07 11.66 o 3 1 2 145.12 148.37 4.92 o 4 1 2 3282.32 3010.45 33.49 o 5 1 2 671.71 565.54 15.51 o 6 1 2 106.26 86.60 4.79 o 7 1 2 66.63 82.16 4.02 o 8 1 2 180.69 158.92 7.39 o 9 1 2 257.64 241.11 9.90 o 10 1 2 4.69 4.67 0.65 o 11 1 2 6.43 4.88 0.62 o 12 1 2 144.84 161.48 7.76 o 13 1 2 157.11 158.54 9.80 o 14 1 2 41.90 35.57 1.73 o 15 1 2 69.39 69.73 3.43 o 16 1 2 9.13 8.16 0.71 o 17 1 2 8.36 11.25 0.77 o 18 1 2 0.52 1.42 1.82 o -20 2 2 0.03 0.49 1.76 o -19 2 2 17.07 20.92 1.17 o -18 2 2 0.08 0.00 0.00 o -17 2 2 39.81 47.50 2.19 o -16 2 2 3.39 2.47 3.49 o -15 2 2 53.14 53.87 3.43 o -14 2 2 48.03 42.34 1.79 o -13 2 2 5.33 2.97 5.56 o -12 2 2 341.67 375.32 17.05 o -11 2 2 45.28 57.82 3.00 o -10 2 2 144.42 193.45 10.85 o -9 2 2 236.31 262.14 11.72 o -8 2 2 8.59 7.51 0.68 o -7 2 2 161.97 186.47 8.44 o -6 2 2 0.76 1.27 2.41 o -5 2 2 877.29 959.10 23.56 o -4 2 2 979.53 1061.91 23.68 o -3 2 2 986.28 1006.25 21.82 o -2 2 2 165.69 136.66 5.72 o -1 2 2 44.86 50.41 2.26 o 0 2 2 7.48 12.52 0.74 o 1 2 2 658.49 716.17 17.62 o 2 2 2 909.42 923.38 20.47 o 3 2 2 280.17 327.72 12.35 o 4 2 2 712.62 664.37 18.42 o 5 2 2 302.39 284.16 12.63 o 6 2 2 327.17 278.35 13.37 o 7 2 2 589.44 594.70 20.94 o 8 2 2 49.95 48.40 2.44 o 9 2 2 125.81 121.03 6.15 o 10 2 2 59.48 59.77 3.37 o 11 2 2 358.92 399.00 14.97 o 12 2 2 261.06 225.19 11.51 o 13 2 2 41.62 38.26 2.72 o 14 2 2 101.08 84.76 4.17 o 15 2 2 8.20 9.73 0.80 o 16 2 2 8.92 9.55 0.74 o 17 2 2 12.83 15.14 1.05 o 18 2 2 6.76 11.56 0.68 o -19 3 2 1.92 0.96 2.75 o -18 3 2 18.86 21.88 1.17 o -17 3 2 21.04 20.21 1.17 o -16 3 2 2.78 2.10 2.97 o -15 3 2 51.12 52.60 2.35 o -14 3 2 88.12 85.09 4.11 o -13 3 2 6.63 8.31 1.14 o -12 3 2 1.17 0.00 0.00 o -11 3 2 0.12 0.00 0.00 o -10 3 2 0.30 0.00 0.00 o -9 3 2 0.10 0.00 0.00 o -8 3 2 1.15 0.00 0.00 o -7 3 2 141.95 163.19 7.67 o -6 3 2 47.69 59.40 2.75 o -5 3 2 43.01 41.75 2.04 o -4 3 2 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