#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:30 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180897 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/37/2103745.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103745_Fobs loop_ _publ_author_name 'Saraswathi, N. T.' 'Vijayan, M.' _publ_section_title ; X-ray studies on crystalline complexes involving amino acids and peptides. XXXVIII. Crystal structures of the complexes of L-arginine and L-histidine with glutaric acid and a comparative study of amino acid--glutaric acid complexes ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 842 _journal_page_last 849 _journal_volume 57 _journal_year 2001 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.109 _cell_angle_gamma 90.000 _cell_length_a 19.0078 _cell_length_b 5.0725 _cell_length_c 13.6723 _exptl_crystal_F_000 556.00 _reflns_d_resolution_high .7987 _cod_data_source_file de0013Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 6RPG3(Larginine complexed with glutaric acid)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7.76 11.39 1.54 o 4 0 0 .99 5.53 3.85 o 6 0 0 5330.87 6491.71 50.02 o 8 0 0 278.57 231.28 6.97 o 10 0 0 319.18 287.10 8.67 o 12 0 0 1813.87 2153.14 45.36 o 14 0 0 144.75 198.35 9.48 o 16 0 0 484.57 583.56 18.22 o 18 0 0 .90 9.07 6.14 o 20 0 0 24.79 28.92 10.12 o 22 0 0 178.61 265.13 10.52 o 1 1 0 3376.75 3127.90 26.80 o 3 1 0 4850.97 4338.30 35.53 o 5 1 0 238.06 206.65 6.19 o 7 1 0 2109.91 1973.77 29.12 o 9 1 0 315.23 299.56 8.85 o 11 1 0 505.57 523.93 16.05 o 13 1 0 19.24 4.81 6.72 o 15 1 0 29.57 32.19 9.14 o 17 1 0 8.73 .00 .18 o 19 1 0 82.58 76.16 6.09 o 21 1 0 91.51 100.11 6.19 o 23 1 0 3.87 -4.16 4.16 o 0 2 0 673.71 640.21 17.78 o 2 2 0 303.00 263.62 7.88 o 4 2 0 3.33 2.11 3.90 o 6 2 0 1016.00 1005.19 26.61 o 8 2 0 938.32 1045.34 29.72 o 10 2 0 27.81 36.27 5.19 o 12 2 0 93.86 103.35 8.21 o 14 2 0 564.72 632.56 19.66 o 16 2 0 13.30 23.67 8.11 o 18 2 0 23.87 23.17 4.92 o 20 2 0 31.42 33.73 4.99 o 22 2 0 3.27 1.63 2.48 o 1 3 0 1004.36 1030.29 27.77 o 3 3 0 165.42 147.93 8.18 o 5 3 0 1161.22 1279.24 33.87 o 7 3 0 147.11 171.31 9.86 o 9 3 0 282.21 266.60 12.30 o 11 3 0 1260.71 1421.57 42.83 o 13 3 0 282.59 319.51 13.95 o 15 3 0 158.22 161.59 10.26 o 17 3 0 88.33 93.22 7.02 o 19 3 0 6.01 4.99 5.17 o 0 4 0 201.95 207.27 13.18 o 2 4 0 6.87 1.66 7.35 o 4 4 0 187.46 202.22 13.01 o 6 4 0 683.97 663.49 22.22 o 8 4 0 33.03 30.98 13.77 o 10 4 0 23.15 20.17 12.79 o 12 4 0 111.25 136.90 10.71 o 14 4 0 .44 1.12 4.57 o 16 4 0 52.39 47.58 6.31 o 18 4 0 45.37 38.43 4.34 o 1 5 0 115.75 72.48 14.20 o 3 5 0 13.97 34.19 15.56 o 5 5 0 84.37 51.95 18.41 o 7 5 0 12.05 -4.45 7.48 o 9 5 0 35.68 39.58 8.62 o 11 5 0 11.02 1.25 6.13 o 13 5 0 70.55 87.86 7.81 o 0 6 0 37.78 57.09 13.81 o 2 6 0 41.78 38.92 18.11 o 4 6 0 7.47 24.74 16.05 o 6 6 0 23.23 50.57 14.91 o -22 0 1 .07 1.55 4.17 o -20 0 1 25.40 29.35 5.53 o -18 0 1 59.33 67.48 7.95 o -16 0 1 84.65 110.01 7.61 o -14 0 1 340.65 454.34 13.78 o -12 0 1 58.18 58.94 5.17 o -10 0 1 846.89 952.83 25.86 o -8 0 1 357.24 400.65 12.41 o -6 0 1 961.56 1179.87 21.44 o -4 0 1 327.38 390.99 10.69 o -2 0 1 1433.61 1534.54 15.28 o 0 0 1 655.47 704.36 14.28 o 2 0 1 1230.51 1006.49 11.38 o 4 0 1 796.38 748.13 13.37 o 6 0 1 2769.50 3078.95 33.64 o 8 0 1 81.61 87.63 4.03 o 10 0 1 712.75 796.18 20.58 o 12 0 1 660.61 840.42 25.02 o 14 0 1 173.98 233.99 10.28 o 16 0 1 4.09 11.20 6.22 o 18 0 1 .31 -8.58 8.58 o 20 0 1 259.12 374.11 13.53 o 22 0 1 18.75 15.61 6.27 o -23 1 1 9.52 13.77 2.69 o -21 1 1 21.25 20.28 5.82 o -19 1 1 221.09 198.49 8.73 o -17 1 1 408.13 374.56 12.52 o -15 1 1 56.59 59.76 6.65 o -13 1 1 248.24 242.06 9.22 o -11 1 1 242.24 262.64 8.30 o -9 1 1 297.27 317.97 8.65 o -7 1 1 325.73 298.94 9.32 o -5 1 1 7762.65 7484.85 52.20 o -3 1 1 11617.07 11815.82 62.22 o -1 1 1 3300.75 3494.49 29.91 o 1 1 1 9424.17 10180.63 54.40 o 3 1 1 6936.04 7341.89 49.41 o 5 1 1 5761.83 5472.59 45.91 o 7 1 1 42.46 38.92 2.86 o 9 1 1 1308.23 1282.93 27.18 o 11 1 1 711.38 637.50 19.76 o 13 1 1 183.58 183.55 8.02 o 15 1 1 61.53 60.82 6.07 o 17 1 1 11.27 2.91 5.10 o 19 1 1 69.00 59.57 5.39 o 21 1 1 1.60 -6.02 6.02 o -22 2 1 27.21 19.56 2.86 o -20 2 1 13.03 9.90 6.51 o -18 2 1 34.43 32.03 9.29 o -16 2 1 399.97 371.92 13.51 o -14 2 1 626.17 728.56 21.10 o -12 2 1 138.89 151.82 8.29 o -10 2 1 854.88 940.55 28.16 o -8 2 1 1840.45 1866.08 39.92 o -6 2 1 2685.62 2526.53 41.25 o -4 2 1 821.19 763.24 20.92 o -2 2 1 2595.05 2611.76 36.44 o 0 2 1 3893.40 3876.99 31.71 o 2 2 1 714.80 679.12 18.32 o 4 2 1 72.90 46.30 4.21 o 6 2 1 442.69 481.02 14.79 o 8 2 1 322.00 322.75 9.68 o 10 2 1 428.34 434.95 12.92 o 12 2 1 128.31 139.77 8.59 o 14 2 1 202.43 196.18 10.93 o 16 2 1 446.44 457.57 13.83 o 18 2 1 26.96 26.93 4.61 o 20 2 1 31.76 29.64 4.68 o -19 3 1 8.76 6.05 5.02 o -17 3 1 1.30 .00 .18 o -15 3 1 51.23 60.59 6.91 o -13 3 1 323.41 362.37 14.86 o -11 3 1 108.69 108.07 10.35 o -9 3 1 244.17 288.46 13.26 o -7 3 1 386.79 454.61 14.35 o -5 3 1 629.86 704.64 20.76 o -3 3 1 498.70 498.91 15.66 o -1 3 1 337.99 343.45 10.97 o 1 3 1 130.36 161.93 8.22 o 3 3 1 301.09 298.43 10.70 o 5 3 1 14.66 23.67 5.76 o 7 3 1 85.21 107.49 8.37 o 9 3 1 40.36 43.92 7.30 o 11 3 1 291.51 300.12 13.52 o 13 3 1 68.15 75.45 8.41 o 15 3 1 52.21 53.89 6.91 o 17 3 1 118.47 117.81 7.60 o 19 3 1 .81 .54 2.66 o -18 4 1 61.14 50.23 4.96 o -16 4 1 6.98 9.23 6.54 o -14 4 1 12.17 6.94 7.72 o -12 4 1 42.33 54.68 7.56 o -10 4 1 63.55 71.99 9.13 o -8 4 1 93.44 101.45 10.02 o -6 4 1 114.56 116.63 10.74 o -4 4 1 276.37 283.07 14.49 o -2 4 1 14.37 8.44 11.47 o 0 4 1 22.32 25.75 9.61 o 2 4 1 85.45 113.71 11.46 o 4 4 1 226.58 228.77 14.25 o 6 4 1 105.17 118.66 11.14 o 8 4 1 414.39 448.83 18.27 o 10 4 1 36.76 48.13 8.21 o 12 4 1 5.79 -1.19 5.15 o 14 4 1 21.43 23.17 9.33 o 16 4 1 29.18 23.55 8.22 o -13 5 1 17.39 2.48 6.34 o -11 5 1 126.54 122.86 10.44 o -9 5 1 47.31 69.27 9.62 o -7 5 1 29.35 -6.72 8.78 o -5 5 1 29.08 35.95 15.47 o -3 5 1 28.51 11.21 13.23 o -1 5 1 208.95 193.19 15.33 o 1 5 1 238.70 235.77 16.12 o 3 5 1 245.46 205.81 16.61 o 5 5 1 131.24 139.46 13.66 o 7 5 1 104.68 114.31 12.93 o 9 5 1 4.55 13.86 11.82 o 11 5 1 89.70 107.80 10.33 o 13 5 1 14.36 22.64 8.19 o -6 6 1 4.71 .00 .18 o -4 6 1 .40 9.47 12.32 o -2 6 1 3.45 31.42 14.76 o 0 6 1 1.83 28.09 10.98 o 2 6 1 1.80 6.72 9.52 o 4 6 1 1.33 9.40 9.47 o 6 6 1 4.64 26.24 12.94 o -22 0 2 16.69 25.68 4.36 o -20 0 2 45.32 42.51 5.97 o -18 0 2 149.54 168.14 9.43 o -16 0 2 68.76 83.85 7.39 o -14 0 2 .73 -4.28 5.40 o -12 0 2 162.74 183.92 8.04 o -10 0 2 85.84 106.97 5.28 o -8 0 2 381.90 342.11 10.47 o -6 0 2 1776.00 1941.37 27.72 o -4 0 2 6010.43 7533.36 47.55 o -2 0 2 284.92 319.64 8.22 o 0 0 2 .13 7.16 4.33 o 2 0 2 18751.77 19874.62 354.85 o 4 0 2 3787.98 3148.33 28.25 o 6 0 2 719.35 612.50 14.72 o 8 0 2 1087.86 966.84 21.05 o 10 0 2 88.15 88.12 4.54 o 12 0 2 24.57 26.24 7.84 o 14 0 2 568.11 729.68 20.39 o 16 0 2 67.66 65.95 7.86 o 18 0 2 30.94 37.41 6.09 o 20 0 2 28.24 20.28 8.96 o 22 0 2 .01 -1.01 2.82 o -23 1 2 .14 .36 1.75 o -21 1 2 10.48 8.98 5.31 o -19 1 2 235.59 203.86 9.22 o -17 1 2 16.12 13.08 7.68 o -15 1 2 51.58 45.01 12.82 o -13 1 2 107.60 124.61 7.20 o -11 1 2 549.37 586.48 16.98 o -9 1 2 547.14 536.48 15.63 o -7 1 2 3161.88 2985.90 37.59 o -5 1 2 11534.78 11303.32 68.82 o -3 1 2 11538.07 11533.87 64.21 o -1 1 2 2444.22 2425.67 25.92 o 1 1 2 1953.52 1822.53 22.32 o 3 1 2 222.13 214.07 6.32 o 5 1 2 418.26 345.00 10.52 o 7 1 2 1596.60 1468.98 26.05 o 9 1 2 427.30 410.28 12.55 o 11 1 2 597.49 583.98 16.95 o 13 1 2 207.73 190.22 8.17 o 15 1 2 63.24 71.99 6.16 o 17 1 2 73.31 70.17 5.86 o 19 1 2 5.79 1.50 3.78 o 21 1 2 36.89 39.77 4.41 o -22 2 2 22.69 15.09 4.50 o -20 2 2 3.17 -5.22 6.32 o -18 2 2 38.37 21.76 8.78 o -16 2 2 122.40 119.86 8.25 o -14 2 2 409.75 471.36 15.78 o -12 2 2 233.06 274.88 11.61 o -10 2 2 157.36 209.55 8.96 o -8 2 2 1266.29 1280.21 33.91 o -6 2 2 2850.12 2622.40 42.07 o -4 2 2 1176.11 1175.14 26.02 o -2 2 2 707.46 663.50 18.79 o 0 2 2 1221.76 1060.29 64.11 o 2 2 2 421.84 400.94 11.87 o 4 2 2 3354.56 3534.93 47.39 o 6 2 2 738.29 721.38 20.31 o 8 2 2 451.71 493.83 14.96 o 10 2 2 272.05 271.46 10.20 o 12 2 2 .57 3.49 5.58 o 14 2 2 1.75 .00 .18 o 16 2 2 68.31 65.95 6.33 o 18 2 2 15.56 24.07 3.96 o 20 2 2 8.67 2.73 3.83 o -19 3 2 34.44 35.95 5.01 o -17 3 2 21.33 19.21 7.77 o -15 3 2 9.75 19.80 8.02 o -13 3 2 121.44 127.94 10.04 o -11 3 2 8.17 4.91 8.58 o -9 3 2 223.98 230.00 12.24 o -7 3 2 167.28 182.81 10.19 o -5 3 2 572.06 589.08 17.67 o -3 3 2 491.42 498.84 15.66 o -1 3 2 120.32 112.92 7.15 o 1 3 2 62.02 51.95 6.20 o 3 3 2 357.71 375.63 11.48 o 5 3 2 112.56 108.65 8.41 o 7 3 2 303.84 336.71 12.85 o 9 3 2 95.69 113.16 8.30 o 11 3 2 329.75 323.03 14.03 o 13 3 2 117.76 114.03 9.19 o 15 3 2 .96 -2.35 5.60 o 17 3 2 53.85 47.02 5.89 o 19 3 2 16.59 16.16 5.40 o -18 4 2 26.44 26.37 4.14 o -16 4 2 16.34 22.64 8.19 o -14 4 2 101.65 94.01 9.13 o -12 4 2 .61 -3.65 6.11 o -10 4 2 163.37 174.50 12.09 o -8 4 2 44.06 29.79 14.68 o -6 4 2 8.23 27.63 10.61 o -4 4 2 12.45 -2.48 7.01 o -2 4 2 71.39 55.69 17.07 o 0 4 2 70.39 59.86 9.35 o 2 4 2 503.82 490.13 19.68 o 4 4 2 16.11 34.19 14.93 o 6 4 2 79.55 56.31 19.78 o 8 4 2 668.13 693.55 21.31 o 10 4 2 23.98 22.64 11.64 o 12 4 2 21.50 2.48 6.81 o 14 4 2 89.60 88.87 8.63 o 16 4 2 16.81 12.31 6.04 o -13 5 2 15.38 11.84 8.15 o -11 5 2 94.10 88.63 10.89 o -9 5 2 16.26 7.52 9.96 o -7 5 2 54.79 29.65 14.79 o -5 5 2 86.05 97.96 11.72 o -3 5 2 6.29 7.37 11.17 o -1 5 2 .86 -9.50 9.50 o 1 5 2 75.95 63.37 12.64 o 3 5 2 51.28 52.91 20.93 o 5 5 2 36.15 44.64 10.95 o 7 5 2 107.36 110.90 13.87 o 9 5 2 22.91 38.91 13.59 o 11 5 2 72.19 74.07 9.49 o 13 5 2 3.77 1.12 4.12 o -6 6 2 50.34 33.74 14.99 o -4 6 2 12.45 11.66 13.12 o -2 6 2 8.93 14.47 14.31 o 0 6 2 57.57 76.06 10.81 o 2 6 2 4.44 -.58 3.04 o 4 6 2 11.64 -6.29 6.29 o 6 6 2 4.53 -2.39 4.19 o -22 0 3 196.74 223.53 9.65 o -20 0 3 311.02 362.89 12.81 o -18 0 3 48.13 52.51 6.04 o -16 0 3 473.13 558.41 17.19 o -14 0 3 10.42 11.65 7.25 o -12 0 3 .79 .00 .18 o -10 0 3 5986.01 6387.85 69.01 o -8 0 3 2051.65 2192.49 34.49 o -6 0 3 12155.48 13878.73 79.86 o -4 0 3 1374.94 1252.55 19.32 o -2 0 3 1489.84 1322.19 17.95 o 0 0 3 1288.87 1538.00 27.36 o 2 0 3 11333.49 10961.58 56.48 o 4 0 3 3.49 4.99 2.51 o 6 0 3 7277.95 6436.00 49.93 o 8 0 3 207.35 173.29 5.31 o 10 0 3 .27 2.60 3.51 o 12 0 3 220.86 217.13 8.33 o 14 0 3 1.50 2.06 4.44 o 16 0 3 3.97 6.45 6.36 o 18 0 3 17.51 18.97 7.37 o 20 0 3 15.16 16.05 7.21 o 22 0 3 77.46 111.77 6.26 o -23 1 3 12.51 9.47 4.81 o -21 1 3 3.36 14.89 5.08 o -19 1 3 94.82 90.39 6.66 o -17 1 3 247.43 217.15 9.91 o -15 1 3 111.63 105.02 8.27 o -13 1 3 52.91 67.70 5.97 o -11 1 3 244.58 244.21 8.41 o -9 1 3 1105.87 1064.27 26.50 o -7 1 3 2604.47 2259.95 32.55 o -5 1 3 1048.77 963.93 19.37 o -3 1 3 423.75 441.18 12.48 o -1 1 3 57.17 78.56 3.09 o 1 1 3 4417.97 4236.36 38.32 o 3 1 3 459.79 359.10 10.24 o 5 1 3 1459.17 1298.02 23.49 o 7 1 3 800.09 741.33 19.87 o 9 1 3 29.05 28.20 3.43 o 11 1 3 255.00 239.59 8.33 o 13 1 3 621.65 616.13 18.07 o 15 1 3 215.34 236.52 9.52 o 17 1 3 22.01 27.78 4.10 o 19 1 3 47.65 51.36 4.81 o 21 1 3 19.64 29.06 3.18 o -22 2 3 7.39 10.06 3.83 o -20 2 3 33.60 20.17 6.99 o -18 2 3 9.41 12.88 6.18 o -16 2 3 15.05 16.59 8.76 o -14 2 3 44.09 45.19 7.05 o -12 2 3 184.22 214.67 10.64 o -10 2 3 253.14 279.48 10.35 o -8 2 3 289.07 240.59 8.77 o -6 2 3 2674.46 2480.53 40.84 o -4 2 3 82.56 84.87 4.47 o -2 2 3 350.73 362.58 10.77 o 0 2 3 817.01 707.97 13.42 o 2 2 3 268.71 308.38 9.00 o 4 2 3 203.13 181.88 6.90 o 6 2 3 13.27 20.89 6.14 o 8 2 3 1612.74 1670.33 38.80 o 10 2 3 113.07 113.74 7.16 o 12 2 3 130.73 125.22 8.43 o 14 2 3 76.44 72.69 6.65 o 16 2 3 20.05 19.68 7.16 o 18 2 3 2.97 3.00 4.05 o 20 2 3 15.98 14.48 3.27 o -19 3 3 27.03 25.83 5.19 o -17 3 3 28.41 27.90 4.97 o -15 3 3 8.96 3.96 7.23 o -13 3 3 237.41 261.20 13.49 o -11 3 3 821.82 908.11 26.84 o -9 3 3 441.03 433.75 15.15 o -7 3 3 33.07 50.97 6.15 o -5 3 3 1589.03 1807.33 47.27 o -3 3 3 168.21 190.92 8.92 o -1 3 3 229.21 258.24 9.94 o 1 3 3 990.67 977.32 28.73 o 3 3 3 229.87 217.18 10.31 o 5 3 3 256.59 243.36 10.51 o 7 3 3 670.67 690.27 20.55 o 9 3 3 287.73 322.44 13.53 o 11 3 3 143.14 143.96 9.68 o 13 3 3 88.80 75.93 7.50 o 15 3 3 8.50 19.80 7.17 o 17 3 3 10.72 21.50 6.36 o 19 3 3 60.45 52.34 4.09 o -18 4 3 .77 8.20 4.16 o -16 4 3 64.54 57.52 7.14 o -14 4 3 51.28 46.66 7.16 o -12 4 3 7.09 10.15 8.40 o -10 4 3 26.69 11.48 10.48 o -8 4 3 9.18 13.66 11.13 o -6 4 3 53.19 37.58 9.07 o -4 4 3 62.19 67.27 10.14 o -2 4 3 95.45 97.44 10.89 o 0 4 3 125.88 130.98 12.26 o 2 4 3 529.66 590.38 20.30 o 4 4 3 116.73 132.22 11.45 o 6 4 3 26.14 -7.90 10.26 o 8 4 3 64.43 72.44 9.15 o 10 4 3 199.65 175.29 12.11 o 12 4 3 .26 11.29 7.05 o 14 4 3 8.77 -6.50 6.50 o 16 4 3 31.97 17.59 6.44 o -13 5 3 1.17 15.94 6.76 o -11 5 3 1.26 -6.78 6.78 o -9 5 3 22.74 17.82 12.04 o -7 5 3 20.72 33.88 11.73 o -5 5 3 282.93 267.47 15.40 o -3 5 3 7.64 -10.73 10.73 o -1 5 3 56.83 28.64 16.54 o 1 5 3 6.43 -4.86 8.19 o 3 5 3 63.96 65.52 12.40 o 5 5 3 1.12 17.81 13.28 o 7 5 3 70.23 74.98 10.25 o 9 5 3 50.40 43.41 14.17 o 11 5 3 34.77 28.92 12.15 o 13 5 3 4.26 3.85 4.70 o -6 6 3 29.32 18.75 11.17 o -4 6 3 7.52 10.32 12.43 o -2 6 3 16.30 40.26 15.36 o 0 6 3 18.93 40.70 11.37 o 2 6 3 20.61 21.15 12.98 o 4 6 3 14.77 7.16 7.05 o -22 0 4 26.41 37.25 4.59 o -20 0 4 .00 -7.77 7.77 o -18 0 4 122.64 122.52 8.34 o -16 0 4 96.56 100.10 8.07 o -14 0 4 206.00 228.33 9.76 o -12 0 4 354.32 375.59 10.96 o -10 0 4 297.53 313.10 9.54 o -8 0 4 1192.47 1187.07 26.16 o -6 0 4 523.41 530.39 15.55 o -4 0 4 2026.10 1781.39 24.28 o -2 0 4 5803.87 5321.99 41.48 o 0 0 4 7035.63 7459.13 128.99 o 2 0 4 187.57 162.27 4.81 o 4 0 4 2695.31 2425.44 29.75 o 6 0 4 960.76 849.50 19.72 o 8 0 4 719.39 679.61 19.70 o 10 0 4 1127.33 1110.42 28.84 o 12 0 4 103.95 117.49 6.13 o 14 0 4 1.04 -7.73 7.73 o 16 0 4 2.99 -7.62 7.62 o 18 0 4 .98 .00 .18 o 20 0 4 .74 4.73 4.68 o -23 1 4 38.74 38.09 4.32 o 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