#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:00:30 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180897 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/37/2103752.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103752_Fobs loop_ _publ_author_name 'Yasui, Masanori' 'Ishikawa, Yoshimitsu' 'Ishida, Takayuki' 'Nogami, Takashi' 'Iwasaki, Fujiko' _publ_section_title ; Bis(hfac)-copper(II) complexes bridged by pyrimidines showing magnetic interactions ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 772 _journal_page_last 779 _journal_volume 57 _journal_year 2001 _space_group_IT_number 88 _symmetry_space_group_name_Hall '-I 4ad' _symmetry_space_group_name_H-M 'I 41/a :2' _exptl_crystal_F_000 4496.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file oa00362asup4.hkl _cod_data_source_block 2a #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 609.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 85143.27 74667.05 677.52 o 2 2 0 1468.73 2114.26 136.60 o -2 4 0 119876.20 108401.68 1148.43 o 0 4 0 11857.84 13723.44 277.16 o 2 4 0 360167.09 310819.88 1968.04 o 4 4 0 37207.30 38071.73 769.51 o -4 6 0 2036.03 3282.59 273.21 o -2 6 0 845.48 848.45 76.20 o 0 6 0 58569.67 57087.39 1449.09 o 2 6 0 1170.90 1198.54 99.53 o 4 6 0 56071.20 47861.16 976.81 o 6 6 0 1273.38 1887.04 165.43 o -6 8 0 15784.22 17691.80 715.96 o -4 8 0 4575.40 4980.17 365.88 o -2 8 0 66033.27 68576.08 1253.45 o 0 8 0 2962.12 2447.53 225.84 o 2 8 0 16103.26 20027.79 682.33 o 4 8 0 29215.44 30768.63 881.40 o 6 8 0 2939.49 5617.20 425.60 o 8 8 0 10572.05 10213.65 584.17 o -8 10 0 47.17 96.10 125.62 o -6 10 0 339.51 345.97 70.70 o -4 10 0 1754.61 2165.74 205.25 o -2 10 0 143693.14 150084.81 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