#------------------------------------------------------------------------------
#$Date: 2016-04-02 23:00:40 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180898 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/38/2103836.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2103836_Fobs
loop_
_publ_author_name
'Bowes, Katharine F.'
'Ferguson, George'
'Lough, Alan J.'
'Glidewell, Christopher'
_publ_section_title
;
 Salts of maleic and fumaric acids with organic polyamines: comparison
 of isomeric acids as building blocks in supramolecular chemistry
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              100
_journal_page_last               117
_journal_volume                  59
_journal_year                    2003
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                109.757
_cell_angle_beta                 97.246
_cell_angle_gamma                96.813
_cell_length_a                   3.8040
_cell_length_b                   8.8743
_cell_length_c                   9.8764
_exptl_crystal_F_000             142.00
_reflns_d_resolution_high        0.7697
_cod_data_source_file            na0143Vsup6.hkl
_cod_data_source_block           V
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' 220    - SHELXL                 P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            28.90
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 62.37 60.66 1.94 o
2 0 0 0.50 0.18 0.09 o
3 0 0 8.59 9.16 0.39 o
4 0 0 9.49 9.90 0.72 o
-4 1 0 2.97 2.79 0.25 o
-3 1 0 80.09 80.02 2.81 o
-2 1 0 10.58 10.92 0.43 o
-1 1 0 3.91 3.68 0.20 o
1 1 0 13.44 8.68 0.35 o
2 1 0 19.18 22.85 0.66 o
3 1 0 75.25 83.15 3.04 o
4 1 0 0.95 0.57 0.33 o
-4 2 0 0.12 0.09 0.15 o
-3 2 0 11.27 9.53 0.40 o
-2 2 0 166.99 149.09 5.49 o
-1 2 0 331.60 313.13 14.32 o
0 2 0 246.50 234.95 7.89 o
1 2 0 22.53 20.98 0.96 o
2 2 0 129.59 130.88 4.77 o
3 2 0 3.02 2.92 0.36 o
4 2 0 7.99 6.86 0.81 o
-4 3 0 11.88 13.80 0.74 o
-3 3 0 74.47 79.32 2.36 o
-2 3 0 184.18 187.17 6.34 o
-1 3 0 128.57 130.24 5.40 o
0 3 0 104.45 105.87 3.93 o
1 3 0 13.03 11.45 0.47 o
2 3 0 18.33 19.11 0.75 o
3 3 0 32.46 36.71 2.44 o
4 3 0 0.97 1.26 0.54 o
-4 4 0 0.00 -0.06 0.18 o
-3 4 0 1.14 0.96 0.24 o
-2 4 0 0.00 -0.02 0.33 o
-1 4 0 123.48 136.69 5.24 o
0 4 0 757.13 795.17 34.93 o
1 4 0 67.53 67.16 1.86 o
2 4 0 0.17 0.44 0.15 o
3 4 0 25.26 27.11 1.31 o
4 4 0 3.44 4.62 0.91 o
-4 5 0 20.88 23.08 2.49 o
-3 5 0 24.85 27.57 0.99 o
-2 5 0 0.12 0.53 0.22 o
-1 5 0 44.67 40.92 1.32 o
0 5 0 23.15 20.93 0.70 o
1 5 0 0.09 0.27 0.24 o
2 5 0 123.42 139.88 4.98 o
3 5 0 16.38 17.67 1.99 o
-4 6 0 26.72 27.11 2.53 o
-3 6 0 0.24 -0.02 0.32 o
-2 6 0 54.33 53.59 1.81 o
-1 6 0 138.48 144.45 4.01 o
0 6 0 28.25 35.21 1.31 o
1 6 0 0.15 0.22 0.33 o
2 6 0 216.95 232.58 9.67 o
3 6 0 21.09 25.43 2.40 o
-4 7 0 0.37 0.69 1.45 o
-3 7 0 181.87 195.28 7.27 o
-2 7 0 31.50 30.98 1.37 o
-1 7 0 9.36 6.54 0.46 o
0 7 0 17.69 13.92 0.74 o
1 7 0 8.01 7.95 1.33 o
2 7 0 1.50 1.80 0.75 o
3 7 0 32.61 30.93 2.79 o
-3 8 0 4.43 3.63 0.56 o
-2 8 0 39.07 41.31 2.04 o
-1 8 0 10.70 8.52 0.54 o
0 8 0 3.35 2.06 0.41 o
1 8 0 27.41 26.96 2.57 o
2 8 0 0.64 0.00 1.17 o
-3 9 0 0.01 -0.18 0.42 o
-2 9 0 2.79 3.64 0.63 o
-1 9 0 30.87 28.03 1.72 o
0 9 0 7.55 6.48 1.05 o
1 9 0 45.72 50.52 3.92 o
-2 10 0 0.89 -0.12 0.60 o
-1 10 0 1.20 0.27 0.63 o
0 10 0 3.59 2.58 0.58 o
1 10 0 0.61 1.11 1.11 o
1 -11 1 18.54 19.55 2.02 o
-1 -10 1 0.66 0.00 0.66 o
0 -10 1 8.59 5.43 0.69 o
1 -10 1 8.51 7.69 0.93 o
2 -10 1 0.17 0.15 0.44 o
-2 -9 1 0.61 1.11 1.05 o
-1 -9 1 3.84 5.68 1.14 o
0 -9 1 3.10 2.30 0.64 o
1 -9 1 4.72 3.77 0.63 o
2 -9 1 19.11 20.74 1.27 o
3 -9 1 4.53 5.00 0.62 o
-2 -8 1 2.56 1.65 0.96 o
-1 -8 1 46.54 41.48 3.14 o
0 -8 1 55.54 47.03 2.05 o
1 -8 1 20.25 18.52 0.92 o
2 -8 1 99.39 106.94 3.95 o
3 -8 1 2.04 2.81 0.60 o
-3 -7 1 38.55 38.62 3.81 o
-2 -7 1 0.28 -0.08 0.40 o
-1 -7 1 17.11 17.73 1.12 o
0 -7 1 29.95 29.10 1.03 o
1 -7 1 0.80 0.32 0.23 o
2 -7 1 43.15 44.35 1.99 o
3 -7 1 99.61 110.06 5.94 o
4 -7 1 4.57 5.30 1.37 o
-3 -6 1 105.67 112.59 7.13 o
-2 -6 1 0.17 -0.07 0.29 o
-1 -6 1 15.29 17.14 0.99 o
0 -6 1 5.69 5.35 0.64 o
1 -6 1 17.25 17.03 0.83 o
2 -6 1 111.89 114.93 4.25 o
3 -6 1 163.41 182.56 6.17 o
4 -6 1 0.27 0.51 1.15 o
-4 -5 1 18.51 17.76 2.01 o
-3 -5 1 0.21 -0.36 0.36 o
-2 -5 1 22.86 22.65 1.13 o
-1 -5 1 108.76 118.47 5.20 o
0 -5 1 284.78 315.69 12.05 o
1 -5 1 149.28 158.48 6.26 o
2 -5 1 107.66 106.00 3.93 o
3 -5 1 25.17 25.21 1.04 o
4 -5 1 1.68 0.78 0.41 o
-4 -4 1 2.04 1.83 1.07 o
-3 -4 1 2.34 2.21 0.23 o
-2 -4 1 26.46 23.45 1.03 o
-1 -4 1 13.86 16.60 1.06 o
0 -4 1 27.41 35.28 1.33 o
1 -4 1 3.56 4.83 0.42 o
2 -4 1 78.51 84.78 2.57 o
3 -4 1 19.21 19.94 0.80 o
4 -4 1 0.66 0.81 0.28 o
-4 -3 1 0.19 0.25 0.37 o
-3 -3 1 15.02 15.92 0.82 o
-2 -3 1 31.54 31.99 1.15 o
-1 -3 1 21.51 16.69 1.02 o
0 -3 1 222.12 225.21 10.76 o
1 -3 1 97.57 95.97 3.29 o
2 -3 1 1.85 2.07 0.20 o
3 -3 1 12.44 12.41 0.46 o
4 -3 1 0.17 0.62 0.24 o
-4 -2 1 13.66 12.79 0.78 o
-3 -2 1 29.38 32.71 1.13 o
-2 -2 1 38.39 40.06 1.55 o
-1 -2 1 69.69 57.60 1.88 o
0 -2 1 48.89 49.98 1.86 o
1 -2 1 114.03 107.64 3.77 o
2 -2 1 699.23 678.53 36.67 o
3 -2 1 17.58 18.23 0.84 o
4 -2 1 0.00 -0.14 0.27 o
-4 -1 1 9.39 9.39 0.53 o
-3 -1 1 18.44 20.20 0.63 o
-2 -1 1 3.23 3.23 0.16 o
0 -1 1 65.79 41.09 4.92 o
1 -1 1 537.36 477.30 11.34 o
2 -1 1 28.32 24.04 0.77 o
3 -1 1 0.26 0.05 0.18 o
4 -1 1 1.74 1.83 0.42 o
-4 0 1 5.81 5.44 1.00 o
-3 0 1 14.68 18.18 0.69 o
-2 0 1 1.62 1.37 0.10 o
-1 0 1 130.79 112.54 4.35 o
1 0 1 15.14 11.66 0.42 o
2 0 1 90.99 96.61 2.44 o
3 0 1 0.24 0.40 0.19 o
4 0 1 0.51 0.68 0.33 o
-4 1 1 1.55 1.21 0.91 o
-3 1 1 43.45 43.65 2.39 o
-2 1 1 331.38 322.40 10.57 o
-1 1 1 401.52 376.34 12.33 o
1 1 1 42.03 40.24 1.87 o
2 1 1 39.63 44.28 1.63 o
3 1 1 53.92 55.79 1.95 o
4 1 1 5.14 5.34 0.53 o
-4 2 1 24.22 25.04 2.42 o
-3 2 1 159.98 162.04 6.73 o
-2 2 1 40.93 42.04 1.40 o
-1 2 1 59.35 61.70 1.89 o
0 2 1 22.42 15.56 0.51 o
1 2 1 84.61 84.31 3.76 o
2 2 1 95.31 117.10 3.69 o
3 2 1 11.39 12.32 0.60 o
4 2 1 1.09 0.77 0.56 o
-4 3 1 3.97 3.57 0.70 o
-3 3 1 2.26 2.11 0.25 o
-2 3 1 29.20 31.86 1.26 o
-1 3 1 478.88 477.07 14.64 o
0 3 1 213.86 208.85 6.37 o
1 3 1 42.21 41.76 1.61 o
2 3 1 7.96 8.05 0.44 o
3 3 1 0.62 1.29 0.48 o
4 3 1 8.87 9.38 0.93 o
-4 4 1 0.39 -0.17 0.92 o
-3 4 1 19.74 21.08 0.75 o
-2 4 1 16.05 14.96 0.95 o
-1 4 1 0.01 0.34 0.20 o
0 4 1 11.15 15.34 0.60 o
1 4 1 89.31 91.87 2.82 o
2 4 1 16.49 17.81 0.64 o
3 4 1 0.54 0.59 0.42 o
4 4 1 8.50 6.62 0.84 o
-4 5 1 5.60 4.29 0.76 o
-3 5 1 60.02 63.81 1.89 o
-2 5 1 114.69 123.93 4.24 o
-1 5 1 224.94 249.97 7.15 o
0 5 1 20.96 23.62 0.89 o
1 5 1 197.83 195.17 5.63 o
2 5 1 17.94 19.02 0.91 o
3 5 1 30.37 33.53 3.43 o
-4 6 1 97.84 107.70 6.35 o
-3 6 1 33.43 35.47 1.28 o
-2 6 1 0.95 1.14 0.29 o
-1 6 1 8.99 8.30 0.53 o
0 6 1 10.95 13.94 0.49 o
1 6 1 1.27 1.94 0.53 o
2 6 1 150.02 160.88 5.16 o
3 6 1 7.17 10.15 1.35 o
-4 7 1 39.47 41.87 2.64 o
-3 7 1 38.45 38.83 1.74 o
-2 7 1 3.40 4.08 0.46 o
-1 7 1 5.46 4.34 0.52 o
0 7 1 80.03 81.07 2.96 o
1 7 1 8.57 9.12 0.74 o
2 7 1 20.73 19.73 1.62 o
-3 8 1 11.84 9.07 0.93 o
-2 8 1 20.40 18.26 0.97 o
-1 8 1 37.91 36.94 1.55 o
0 8 1 71.17 68.87 3.65 o
1 8 1 1.23 -0.09 0.63 o
2 8 1 1.06 0.87 0.84 o
-3 9 1 11.31 10.73 1.06 o
-2 9 1 0.58 0.51 0.47 o
-1 9 1 2.48 0.33 0.97 o
0 9 1 1.22 -0.18 0.45 o
1 9 1 6.51 9.39 1.32 o
-2 10 1 1.68 1.01 0.75 o
-1 10 1 0.26 -0.39 0.72 o
0 10 1 4.48 5.32 1.22 o
0 -11 2 0.12 1.79 1.32 o
1 -11 2 4.86 5.00 0.99 o
-1 -10 2 1.00 0.60 0.78 o
0 -10 2 0.02 0.32 0.46 o
1 -10 2 14.49 14.92 1.25 o
2 -10 2 0.04 -0.13 0.57 o
-2 -9 2 33.72 36.16 3.09 o
-1 -9 2 25.45 25.53 2.22 o
0 -9 2 24.21 24.83 1.29 o
1 -9 2 1.76 1.70 0.55 o
2 -9 2 1.48 1.24 0.41 o
3 -9 2 0.46 0.52 0.51 o
-2 -8 2 14.44 14.51 1.41 o
-1 -8 2 7.03 6.21 0.89 o
0 -8 2 7.32 4.92 0.45 o
1 -8 2 93.39 96.71 3.16 o
2 -8 2 42.28 46.47 2.64 o
3 -8 2 1.02 1.03 0.58 o
-3 -7 2 0.00 -0.27 0.90 o
-2 -7 2 7.73 6.40 0.62 o
-1 -7 2 2.28 1.56 0.48 o
0 -7 2 0.48 0.80 0.27 o
1 -7 2 99.78 95.29 3.47 o
2 -7 2 396.39 434.70 14.79 o
3 -7 2 9.57 10.13 0.70 o
4 -7 2 1.39 2.22 1.25 o
-3 -6 2 71.56 78.95 4.89 o
-2 -6 2 0.67 0.37 0.27 o
-1 -6 2 85.37 92.16 4.73 o
0 -6 2 234.54 252.78 10.28 o
1 -6 2 166.61 155.00 6.09 o
2 -6 2 48.43 49.53 1.73 o
3 -6 2 6.39 6.75 0.51 o
4 -6 2 4.51 2.83 0.65 o
-4 -5 2 7.38 7.82 1.07 o
-3 -5 2 42.52 49.26 2.15 o
-2 -5 2 0.83 1.17 0.43 o
-1 -5 2 3.25 1.92 0.38 o
0 -5 2 19.26 14.38 0.79 o
1 -5 2 2.94 2.61 0.73 o
2 -5 2 5.34 5.58 0.35 o
3 -5 2 12.44 11.85 0.87 o
4 -5 2 2.56 2.34 0.49 o
-4 -4 2 1.99 1.40 0.68 o
-3 -4 2 0.00 0.09 0.19 o
-2 -4 2 32.23 28.13 1.21 o
-1 -4 2 568.10 575.95 16.05 o
0 -4 2 43.49 47.17 2.45 o
1 -4 2 50.44 57.73 1.87 o
2 -4 2 11.18 12.83 0.50 o
3 -4 2 2.92 3.57 0.34 o
4 -4 2 0.63 0.29 0.31 o
-4 -3 2 15.67 14.28 0.73 o
-3 -3 2 11.08 12.59 0.49 o
-2 -3 2 4.14 5.08 0.23 o
-1 -3 2 31.44 32.13 1.09 o
0 -3 2 238.10 232.21 9.63 o
2 -3 2 89.78 98.13 2.90 o
3 -3 2 34.63 39.10 1.32 o
4 -3 2 7.00 5.69 0.47 o
-4 -2 2 6.21 5.13 0.35 o
-3 -2 2 11.17 11.06 0.42 o
-2 -2 2 83.81 91.54 3.04 o
-1 -2 2 163.44 155.68 4.58 o
0 -2 2 835.25 785.95 38.98 o
1 -2 2 300.37 253.70 6.60 o
2 -2 2 40.58 39.54 1.09 o
3 -2 2 0.95 0.45 0.21 o
4 -2 2 122.81 137.47 5.59 o
-4 -1 2 19.95 21.62 1.70 o
-3 -1 2 2.34 2.75 0.20 o
-2 -1 2 5.20 6.61 0.29 o
-1 -1 2 9.07 8.30 0.23 o
0 -1 2 0.13 0.09 0.09 o
1 -1 2 34.26 28.95 1.02 o
2 -1 2 42.54 37.77 1.27 o
3 -1 2 8.84 9.55 0.49 o
4 -1 2 21.75 21.00 2.41 o
-4 0 2 1.51 0.52 0.47 o
-3 0 2 19.73 20.46 0.95 o
-2 0 2 14.51 15.22 0.69 o
0 0 2 176.91 170.69 6.55 o
1 0 2 45.21 53.32 2.10 o
2 0 2 150.64 154.01 4.26 o
3 0 2 50.96 56.38 2.10 o
4 0 2 45.80 45.70 2.34 o
-4 1 2 37.14 38.88 3.60 o
-3 1 2 2.32 2.42 0.76 o
-2 1 2 1.02 1.19 0.22 o
-1 1 2 5.95 7.43 0.27 o
0 1 2 51.43 42.15 1.26 o
1 1 2 95.60 101.91 3.93 o
2 1 2 171.51 170.07 5.43 o
3 1 2 0.87 0.70 0.28 o
4 1 2 3.77 3.97 0.85 o
-4 2 2 0.96 0.36 0.50 o
-3 2 2 29.60 28.76 1.22 o
-2 2 2 3.24 3.29 1.70 o
-1 2 2 5.68 7.28 0.31 o
0 2 2 213.53 204.96 6.95 o
1 2 2 352.95 368.27 11.64 o
2 2 2 0.21 0.02 0.27 o
3 2 2 11.99 12.77 0.60 o
4 2 2 12.52 12.67 1.01 o
-4 3 2 31.96 32.44 2.05 o
-3 3 2 6.43 5.64 0.52 o
-2 3 2 19.82 21.65 0.72 o
-1 3 2 75.16 79.48 7.35 o
0 3 2 64.87 64.65 2.12 o
1 3 2 3.31 4.56 0.39 o
2 3 2 40.80 44.68 1.52 o
3 3 2 20.82 22.26 1.24 o
4 3 2 0.05 -0.37 0.67 o
-4 4 2 7.02 6.29 0.84 o
-3 4 2 8.26 7.32 0.54 o
-2 4 2 117.37 126.42 3.77 o
-1 4 2 233.23 245.50 8.76 o
0 4 2 1.35 1.03 0.18 o
1 4 2 2.84 3.43 0.29 o
2 4 2 92.73 99.64 3.46 o
3 4 2 17.12 18.56 1.39 o
-4 5 2 14.23 14.69 1.20 o
-3 5 2 0.00 0.53 0.23 o
-2 5 2 26.85 27.39 1.04 o
-1 5 2 15.28 16.03 0.60 o
0 5 2 0.99 0.53 0.23 o
1 5 2 196.27 209.01 5.68 o
2 5 2 26.85 31.28 1.87 o
3 5 2 0.00 -1.02 1.02 o
-4 6 2 4.76 4.68 1.10 o
-3 6 2 5.62 4.69 0.49 o
-2 6 2 27.33 26.56 1.16 o
-1 6 2 4.72 3.52 0.45 o
0 6 2 2.14 3.48 0.37 o
1 6 2 282.58 298.35 11.69 o
2 6 2 64.30 74.61 6.97 o
3 6 2 0.74 1.56 1.35 o
-4 7 2 42.46 43.13 3.23 o
-3 7 2 11.13 9.35 0.66 o
-2 7 2 17.82 16.83 0.91 o
-1 7 2 33.60 30.01 1.46 o
0 7 2 4.91 4.74 0.53 o
1 7 2 7.07 7.70 1.26 o
2 7 2 15.90 17.10 2.07 o
-3 8 2 4.46 4.08 0.92 o
-2 8 2 7.64 6.76 0.80 o
-1 8 2 2.05 1.90 0.50 o
0 8 2 12.08 10.81 0.94 o
1 8 2 0.92 0.27 0.75 o
2 8 2 15.57 15.65 2.58 o
-2 9 2 16.00 14.84 1.67 o
-1 9 2 0.24 0.24 1.29 o
0 9 2 28.93 35.30 5.68 o
1 9 2 3.41 4.16 1.14 o
-1 10 2 9.61 8.33 1.15 o
0 -11 3 3.99 4.85 1.41 o
1 -11 3 7.52 5.26 1.01 o
2 -11 3 14.83 20.98 3.14 o
-1 -10 3 12.69 11.25 1.74 o
0 -10 3 7.30 6.12 0.68 o
1 -10 3 0.03 0.28 0.43 o
2 -10 3 7.03 7.32 0.72 o
-2 -9 3 4.50 4.22 0.90 o
-1 -9 3 4.37 3.00 0.62 o
0 -9 3 33.91 35.97 2.00 o
1 -9 3 7.65 7.04 1.35 o
2 -9 3 8.66 7.92 0.68 o
3 -9 3 8.82 7.24 0.99 o
-3 -8 3 2.39 2.07 0.90 o
-2 -8 3 11.73 12.11 1.17 o
-1 -8 3 24.61 22.41 1.50 o
0 -8 3 27.42 26.43 1.18 o
1 -8 3 287.84 291.04 10.31 o
2 -8 3 31.34 35.15 1.26 o
3 -8 3 6.11 5.49 0.78 o
-3 -7 3 0.22 0.54 0.87 o
-2 -7 3 0.50 0.30 0.38 o
-1 -7 3 59.39 61.67 2.55 o
0 -7 3 25.93 24.78 1.22 o
1 -7 3 1.18 1.31 0.43 o
2 -7 3 102.38 108.11 3.03 o
3 -7 3 6.10 7.45 0.63 o
4 -7 3 8.72 7.49 0.91 o
-3 -6 3 1.06 0.98 0.45 o
-2 -6 3 5.47 5.06 0.48 o
-1 -6 3 1.44 1.54 0.25 o
0 -6 3 20.89 20.31 1.38 o
1 -6 3 171.15 171.42 5.59 o
2 -6 3 146.91 155.16 5.42 o
3 -6 3 1.13 0.71 0.36 o
4 -6 3 0.29 -0.70 0.70 o
-4 -5 3 2.65 1.49 0.69 o
-3 -5 3 0.29 0.57 0.37 o
-2 -5 3 132.23 148.57 4.86 o
-1 -5 3 84.37 89.71 3.46 o
0 -5 3 13.60 14.54 1.10 o
1 -5 3 52.50 44.12 1.28 o
2 -5 3 33.72 32.47 1.27 o
3 -5 3 10.83 11.07 0.59 o
4 -5 3 39.94 41.19 3.02 o
-4 -4 3 0.19 -0.52 0.77 o
-3 -4 3 0.17 0.00 0.19 o
-2 -4 3 3.75 3.18 0.33 o
-1 -4 3 56.37 58.95 1.66 o
0 -4 3 172.32 169.55 6.72 o
1 -4 3 150.61 162.65 5.15 o
2 -4 3 136.18 145.48 4.14 o
3 -4 3 4.45 4.79 0.36 o
4 -4 3 1.29 0.94 0.67 o
-4 -3 3 4.48 4.08 0.43 o
-3 -3 3 2.47 2.01 0.22 o
-2 -3 3 10.61 12.92 0.42 o
-1 -3 3 1.06 0.89 0.09 o
0 -3 3 157.59 144.18 6.16 o
1 -3 3 13.93 13.42 0.40 o
2 -3 3 4.91 5.35 0.26 o
3 -3 3 21.55 22.11 0.87 o
4 -3 3 9.74 8.87 2.02 o
-4 -2 3 7.30 6.31 0.76 o
-3 -2 3 5.36 4.72 0.28 o
-2 -2 3 34.81 30.03 0.75 o
-1 -2 3 3.43 3.85 0.24 o
0 -2 3 88.44 81.34 3.22 o
2 -2 3 10.91 12.60 0.53 o
3 -2 3 11.76 11.83 0.60 o
4 -2 3 12.78 12.13 1.08 o
-4 -1 3 1.88 1.09 0.48 o
-3 -1 3 0.10 0.02 0.31 o
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