#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/38/2103838.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103838_Fobs loop_ _publ_author_name 'Bowes, Katharine F.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; Salts of maleic and fumaric acids with organic polyamines: comparison of isomeric acids as building blocks in supramolecular chemistry ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 100 _journal_page_last 117 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 118.394 _cell_angle_gamma 90.000 _cell_length_a 21.0296 _cell_length_b 4.7456 _cell_length_c 16.6875 _exptl_crystal_F_000 632.00 _reflns_d_resolution_high 0.7710 _[local]_cod_data_source_file na0143VIIsup8.hkl _[local]_cod_data_source_block VII #BEGIN Tags that were not found in dictionaries: _shelx_title ' 214 - SHELXL' _shelx_refln_list_code 4 _shelx_F_calc_maximum 133.58 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5414.89 5516.76 502.50 o 6 0 0 792.86 665.05 32.45 o 8 0 0 680.98 637.49 35.30 o 10 0 0 132.10 161.27 7.27 o 12 0 0 1657.59 1657.04 82.83 o 14 0 0 1018.32 1066.47 60.83 o 16 0 0 112.37 110.51 11.93 o 18 0 0 2.33 -2.73 5.94 o 20 0 0 804.36 854.59 62.14 o 22 0 0 81.41 49.45 9.71 o 3 1 0 908.05 842.70 34.47 o 5 1 0 2852.14 2562.11 112.38 o 7 1 0 2736.36 2857.29 131.28 o 9 1 0 1957.82 1972.93 110.11 o 11 1 0 368.89 345.32 16.04 o 13 1 0 1689.86 1878.18 105.13 o 15 1 0 63.92 80.93 12.17 o 17 1 0 274.39 301.41 24.50 o 19 1 0 36.88 28.33 9.07 o 21 1 0 430.51 423.60 51.47 o 23 1 0 7.23 8.58 7.29 o 2 2 0 343.16 292.21 30.39 o 4 2 0 765.47 758.86 51.63 o 6 2 0 1629.63 1630.76 83.60 o 8 2 0 318.40 311.02 16.38 o 10 2 0 9.12 11.27 5.35 o 12 2 0 1097.85 1097.72 47.93 o 14 2 0 250.92 252.30 14.77 o 16 2 0 64.53 62.57 8.03 o 18 2 0 32.09 18.15 6.12 o 20 2 0 31.44 44.87 9.84 o 22 2 0 55.61 50.34 10.15 o 1 3 0 1936.49 1879.62 92.70 o 3 3 0 478.59 443.88 39.59 o 5 3 0 1.37 4.89 5.94 o 7 3 0 71.93 94.42 15.19 o 9 3 0 16.31 20.08 11.93 o 11 3 0 1220.32 1328.72 61.37 o 13 3 0 317.53 346.67 16.57 o 15 3 0 82.18 82.54 4.90 o 17 3 0 6.03 6.04 6.67 o 19 3 0 132.04 178.67 22.71 o 0 4 0 30.75 28.00 10.86 o 2 4 0 205.56 199.16 14.18 o 4 4 0 78.09 76.37 8.53 o 6 4 0 1302.49 1400.48 72.47 o 8 4 0 1.53 -6.16 7.28 o 10 4 0 387.39 437.34 31.13 o 12 4 0 7.35 9.75 6.41 o 14 4 0 62.88 52.30 7.68 o 16 4 0 3.09 -4.89 14.14 o 1 5 0 31.51 28.64 3.49 o 3 5 0 20.65 28.53 5.80 o 5 5 0 8.89 13.95 5.12 o 7 5 0 172.47 186.57 16.65 o 9 5 0 48.85 50.07 8.55 o 11 5 0 102.21 98.11 13.92 o 13 5 0 0.00 -0.04 5.23 o 0 6 0 102.24 103.57 24.29 o 2 6 0 42.13 81.86 21.56 o 4 6 0 0.10 11.30 17.19 o -23 1 1 88.82 73.74 13.67 o -21 1 1 138.05 112.49 15.22 o -19 1 1 80.57 85.91 13.62 o -17 1 1 159.20 152.66 11.54 o -15 1 1 267.03 241.94 10.90 o -13 1 1 927.83 939.10 42.75 o -11 1 1 41.38 55.46 5.53 o -9 1 1 2583.55 2598.09 115.26 o -7 1 1 89.43 86.44 4.83 o -5 1 1 2.50 15.68 3.63 o -3 1 1 1478.27 1425.84 69.54 o -1 1 1 245.62 193.84 11.41 o 3 1 1 7371.91 7283.46 663.54 o 5 1 1 5438.61 4809.90 261.42 o 7 1 1 688.32 781.05 37.55 o 9 1 1 738.20 655.47 28.34 o 11 1 1 10.03 15.97 4.76 o 13 1 1 89.25 80.86 6.57 o 15 1 1 125.36 123.07 9.08 o 17 1 1 180.23 193.61 16.32 o 19 1 1 1.27 1.85 9.17 o 21 1 1 20.60 23.01 7.00 o 23 1 1 15.34 8.98 11.48 o -22 2 1 7.23 7.47 8.05 o -20 2 1 10.83 14.04 9.12 o -18 2 1 169.49 159.29 11.76 o -16 2 1 73.95 75.65 6.67 o -14 2 1 784.37 757.69 33.95 o -12 2 1 217.16 200.43 12.68 o -10 2 1 968.35 958.32 34.43 o -8 2 1 526.12 453.25 18.80 o -6 2 1 384.10 466.33 28.11 o -4 2 1 370.66 254.83 18.45 o -2 2 1 226.06 216.71 13.56 o 2 2 1 5886.16 5603.83 395.73 o 4 2 1 51.38 67.29 8.67 o 6 2 1 117.10 112.53 8.00 o 8 2 1 1153.63 1194.22 51.50 o 10 2 1 725.44 737.78 29.60 o 12 2 1 21.90 12.82 4.01 o 14 2 1 169.21 147.70 14.77 o 16 2 1 144.96 134.91 13.07 o 18 2 1 59.07 54.91 10.13 o 20 2 1 325.09 346.08 33.53 o 22 2 1 21.26 6.17 8.42 o -21 3 1 43.37 32.40 10.75 o -19 3 1 531.45 549.53 63.66 o -17 3 1 71.87 60.58 5.99 o -15 3 1 146.69 146.59 10.36 o -13 3 1 846.40 899.33 44.18 o -11 3 1 1411.61 1492.52 58.24 o -9 3 1 138.00 124.34 13.04 o -7 3 1 3.34 17.35 10.30 o -5 3 1 95.22 149.15 14.14 o -3 3 1 1400.27 1438.64 82.59 o -1 3 1 2020.91 2032.98 112.43 o 1 3 1 537.18 563.77 27.69 o 3 3 1 1.11 5.11 5.10 o 5 3 1 286.17 291.79 13.58 o 7 3 1 869.73 827.23 42.18 o 9 3 1 2056.03 2084.28 98.23 o 11 3 1 1648.15 1745.47 60.65 o 13 3 1 67.86 67.11 7.62 o 15 3 1 53.91 62.06 16.22 o 17 3 1 1.66 -0.30 5.82 o 19 3 1 139.08 123.51 13.51 o -16 4 1 1.18 2.43 3.55 o -14 4 1 191.21 238.11 21.09 o -12 4 1 6.15 1.18 4.93 o -10 4 1 45.28 42.90 12.51 o -8 4 1 1776.41 1908.76 190.27 o -6 4 1 14.67 3.79 11.93 o -4 4 1 255.14 290.52 25.50 o -2 4 1 71.76 86.59 14.62 o 0 4 1 695.89 769.73 25.85 o 2 4 1 0.44 2.61 3.71 o 4 4 1 607.28 617.89 26.18 o 6 4 1 16.84 15.09 6.44 o 8 4 1 9.14 15.26 9.91 o 10 4 1 1.54 9.17 8.33 o 12 4 1 64.02 59.18 6.59 o 14 4 1 40.39 33.59 6.83 o 16 4 1 12.91 18.32 11.03 o -13 5 1 31.14 27.08 7.52 o -11 5 1 3.18 14.12 10.09 o -9 5 1 12.13 4.51 9.82 o -7 5 1 0.49 3.13 5.69 o -5 5 1 203.19 225.62 17.98 o -3 5 1 0.65 4.40 3.46 o -1 5 1 11.47 7.26 7.60 o 1 5 1 4.77 7.32 2.06 o 3 5 1 101.91 129.53 10.70 o 5 5 1 155.15 163.75 14.27 o 7 5 1 38.10 35.97 9.90 o 9 5 1 0.10 0.68 6.59 o 11 5 1 19.16 4.37 6.16 o 13 5 1 0.39 4.31 13.93 o -4 6 1 0.18 10.20 11.30 o -2 6 1 82.32 90.48 22.08 o 0 6 1 18.07 16.72 15.09 o 2 6 1 56.78 50.10 19.40 o 4 6 1 0.05 6.47 9.15 o -24 0 2 75.99 55.31 10.88 o -22 0 2 6.47 3.26 5.42 o -20 0 2 1487.64 1585.53 115.87 o -18 0 2 92.58 76.20 12.25 o -16 0 2 264.92 270.63 17.61 o -14 0 2 0.84 2.43 4.18 o -12 0 2 5161.24 5708.45 334.32 o -10 0 2 2.46 4.50 3.22 o -8 0 2 10946.26 10347.76 609.15 o -6 0 2 17.09 14.05 2.60 o 0 0 2 295.58 171.34 18.82 o 2 0 2 1841.97 1479.90 69.54 o 4 0 2 883.65 698.13 47.74 o 6 0 2 41.68 46.12 3.27 o 8 0 2 2371.38 2534.07 230.54 o 10 0 2 3996.05 4128.33 421.07 o 12 0 2 182.07 173.38 11.06 o 14 0 2 488.46 515.13 30.39 o 16 0 2 2.13 -1.05 5.89 o 18 0 2 29.71 24.95 5.52 o 20 0 2 80.44 66.02 8.77 o 22 0 2 122.69 88.75 19.82 o -23 1 2 58.01 68.61 16.88 o -21 1 2 2.58 1.71 4.01 o -19 1 2 811.34 838.45 54.64 o -17 1 2 3.16 4.34 2.60 o -15 1 2 0.15 1.76 3.79 o -13 1 2 344.03 357.91 14.51 o -11 1 2 1139.79 1203.19 44.22 o -9 1 2 2.37 8.19 2.06 o -7 1 2 466.61 495.63 21.54 o -5 1 2 6009.78 5205.87 270.41 o -3 1 2 779.08 847.95 39.72 o -1 1 2 364.00 454.32 24.11 o 3 1 2 15168.63 13933.16 689.25 o 5 1 2 2626.13 2337.66 220.39 o 7 1 2 180.11 177.29 9.12 o 9 1 2 693.33 649.23 41.63 o 11 1 2 587.29 639.76 39.18 o 13 1 2 81.86 77.02 7.24 o 15 1 2 357.29 386.66 21.99 o 17 1 2 385.73 417.13 25.09 o 19 1 2 5.74 2.00 4.96 o 21 1 2 107.11 98.23 13.52 o -22 2 2 0.34 -4.12 7.62 o -20 2 2 48.96 60.36 5.24 o -18 2 2 38.80 32.90 4.81 o -16 2 2 179.14 190.42 14.72 o -14 2 2 133.05 114.20 9.68 o -12 2 2 17.52 23.28 3.75 o -10 2 2 17.80 10.87 3.27 o -8 2 2 296.93 269.56 14.59 o -6 2 2 2.13 2.16 5.42 o -4 2 2 944.65 1119.93 93.84 o -2 2 2 6.83 3.26 4.31 o 0 2 2 2233.00 2192.45 126.52 o 2 2 2 6398.28 6492.62 280.49 o 4 2 2 467.21 433.05 29.70 o 6 2 2 75.17 90.71 20.49 o 8 2 2 27.52 51.15 10.05 o 10 2 2 142.33 142.52 11.93 o 12 2 2 195.78 194.53 15.24 o 14 2 2 2097.71 2230.77 134.70 o 16 2 2 195.82 202.70 23.89 o 18 2 2 2.97 7.65 7.02 o 20 2 2 78.43 84.75 11.82 o -21 3 2 96.83 77.04 13.77 o -19 3 2 4.90 8.78 4.42 o -17 3 2 3.70 2.67 4.99 o -15 3 2 33.74 40.39 4.30 o -13 3 2 193.45 226.15 11.88 o -11 3 2 700.07 764.70 31.82 o -9 3 2 255.50 239.00 20.66 o -7 3 2 30.35 27.71 14.09 o -5 3 2 1.52 8.15 7.57 o -3 3 2 784.91 743.08 44.53 o -1 3 2 125.54 121.24 8.31 o 1 3 2 288.33 347.75 17.61 o 3 3 2 0.20 -0.82 1.77 o 5 3 2 204.03 156.57 12.09 o 7 3 2 2125.79 2193.56 82.25 o 9 3 2 1817.09 1883.42 106.41 o 11 3 2 353.80 378.46 16.16 o 13 3 2 117.69 135.56 12.35 o 15 3 2 116.86 123.63 11.22 o 17 3 2 5.53 9.62 6.39 o 19 3 2 2.88 1.17 11.29 o -18 4 2 45.93 55.89 6.82 o -16 4 2 0.46 -3.64 3.64 o -14 4 2 182.07 183.96 33.91 o -12 4 2 12.48 9.50 5.15 o -10 4 2 2602.81 2930.75 245.00 o -8 4 2 186.46 215.66 25.03 o -6 4 2 587.71 594.77 48.37 o -4 4 2 29.13 45.53 10.83 o -2 4 2 114.05 117.98 17.88 o 0 4 2 98.80 116.67 10.91 o 2 4 2 283.20 283.87 13.80 o 4 4 2 467.85 464.84 20.63 o 6 4 2 8.10 11.05 5.04 o 8 4 2 41.74 43.53 5.92 o 10 4 2 229.44 251.94 15.09 o 12 4 2 185.75 157.44 13.89 o 14 4 2 53.56 39.52 12.00 o 16 4 2 2.71 1.35 13.98 o -15 5 2 2.53 14.09 9.73 o -13 5 2 7.64 2.48 7.04 o -11 5 2 33.81 25.06 20.08 o -9 5 2 38.46 34.73 11.55 o -7 5 2 10.62 -0.16 6.51 o -5 5 2 211.20 224.53 32.02 o -3 5 2 353.99 334.83 32.49 o -1 5 2 21.63 24.37 10.25 o 1 5 2 199.91 221.99 16.50 o 3 5 2 184.24 172.06 18.25 o 5 5 2 83.56 69.46 7.66 o 7 5 2 97.31 106.07 11.58 o 9 5 2 0.20 -2.48 5.46 o 11 5 2 177.25 181.77 22.03 o -6 6 2 8.63 10.73 12.88 o -4 6 2 0.97 -1.05 12.88 o -2 6 2 85.70 84.34 16.28 o 0 6 2 0.02 14.04 12.93 o 2 6 2 0.44 3.21 11.30 o -25 1 3 6.45 11.99 15.25 o -23 1 3 70.79 77.41 18.77 o -21 1 3 6.64 -0.33 3.57 o -19 1 3 6.04 7.72 3.54 o -17 1 3 195.98 202.70 9.48 o -15 1 3 492.41 481.58 19.17 o -13 1 3 215.18 245.48 9.99 o -11 1 3 88.21 62.04 3.42 o -9 1 3 494.26 480.41 21.77 o -7 1 3 2324.83 2296.79 119.31 o -5 1 3 798.90 836.03 48.67 o -3 1 3 392.52 318.85 17.16 o -1 1 3 5374.92 5135.97 183.50 o 1 1 3 17844.88 16340.62 613.43 o 3 1 3 268.43 249.04 8.35 o 5 1 3 2106.78 1868.75 106.21 o 7 1 3 34.33 38.41 3.33 o 9 1 3 668.77 620.89 23.01 o 11 1 3 213.98 202.69 10.80 o 13 1 3 1580.19 1679.82 74.00 o 15 1 3 23.53 32.55 7.85 o 17 1 3 30.05 42.02 8.21 o 19 1 3 66.84 53.70 8.92 o 21 1 3 144.04 122.11 23.90 o -24 2 3 0.03 -2.10 8.78 o -22 2 3 33.91 33.83 6.33 o -20 2 3 123.88 115.22 13.78 o -18 2 3 218.58 224.97 18.51 o -16 2 3 32.48 48.83 5.85 o -14 2 3 0.80 6.76 7.81 o -12 2 3 1815.27 1874.01 79.48 o -10 2 3 769.19 829.64 29.60 o -8 2 3 4755.35 5018.09 276.50 o -6 2 3 422.91 386.47 21.83 o -4 2 3 244.17 250.16 12.30 o -2 2 3 3803.58 3557.20 142.39 o 0 2 3 2137.21 2150.50 135.34 o 2 2 3 14.34 12.93 6.26 o 4 2 3 261.64 284.73 19.98 o 6 2 3 4995.30 5049.65 272.63 o 8 2 3 253.31 231.29 10.51 o 10 2 3 522.63 508.28 23.32 o 12 2 3 2784.02 2945.97 111.17 o 14 2 3 110.79 121.45 12.37 o 16 2 3 50.03 52.88 8.53 o 18 2 3 1.72 -5.81 5.81 o 20 2 3 14.38 12.04 8.35 o -21 3 3 194.76 184.70 13.17 o -19 3 3 274.43 298.38 24.43 o -17 3 3 0.50 -0.47 4.08 o -15 3 3 225.95 231.03 16.16 o -13 3 3 888.64 949.03 37.71 o -11 3 3 10.66 7.33 1.94 o -9 3 3 1057.42 1189.49 102.78 o -7 3 3 165.50 150.84 20.08 o -5 3 3 5.25 26.02 10.30 o -3 3 3 735.14 785.19 45.58 o -1 3 3 817.39 768.61 47.45 o 1 3 3 1622.39 1733.82 80.27 o 3 3 3 685.13 736.73 34.99 o 5 3 3 41.52 29.05 5.17 o 7 3 3 32.29 49.65 8.02 o 9 3 3 120.67 139.09 10.40 o 11 3 3 0.21 -0.47 4.30 o 13 3 3 1.20 0.83 2.86 o 15 3 3 0.23 2.46 5.64 o 17 3 3 3.67 9.91 6.37 o -18 4 3 14.87 15.99 5.95 o -16 4 3 220.02 210.38 21.13 o -14 4 3 0.38 2.17 6.32 o -12 4 3 495.77 506.66 47.95 o -10 4 3 93.26 104.94 20.66 o -8 4 3 18.14 54.89 9.25 o -6 4 3 407.46 397.67 52.10 o -4 4 3 4.13 -3.79 9.20 o -2 4 3 6.15 11.88 11.36 o 0 4 3 206.00 211.45 11.32 o 2 4 3 222.59 208.72 10.49 o 4 4 3 51.87 50.73 5.80 o 6 4 3 11.74 6.83 4.90 o 8 4 3 22.20 30.25 7.40 o 10 4 3 59.43 56.98 7.14 o 12 4 3 2.04 -1.31 6.46 o 14 4 3 2.64 0.52 9.17 o 16 4 3 53.07 71.71 27.29 o -15 5 3 40.49 36.35 9.32 o -13 5 3 28.32 20.14 9.25 o -11 5 3 202.31 154.62 21.77 o -9 5 3 473.32 466.60 61.51 o -7 5 3 450.70 434.47 51.10 o -5 5 3 245.90 264.08 30.39 o -3 5 3 51.58 48.16 14.62 o -1 5 3 15.30 11.80 3.02 o 1 5 3 100.24 108.00 10.06 o 3 5 3 113.19 109.58 10.99 o 5 5 3 0.35 0.76 4.47 o 7 5 3 25.51 11.52 6.88 o 9 5 3 7.83 14.92 6.76 o 11 5 3 340.73 374.22 72.60 o -6 6 3 33.19 5.89 18.77 o -4 6 3 65.63 35.43 16.67 o -2 6 3 97.47 108.67 27.02 o 0 6 3 55.01 64.77 23.19 o 2 6 3 6.18 14.56 11.30 o -24 0 4 760.11 778.42 66.60 o -22 0 4 405.71 408.33 21.47 o -20 0 4 116.87 106.84 8.76 o -18 0 4 776.92 814.30 39.32 o -16 0 4 23.29 45.76 5.82 o -14 0 4 288.19 315.06 20.71 o -12 0 4 1755.20 1822.37 95.07 o -10 0 4 54.77 85.87 6.08 o -8 0 4 125.75 133.32 8.29 o -6 0 4 296.49 317.89 18.20 o -4 0 4 7286.94 6121.03 349.00 o -2 0 4 5472.38 4833.56 307.45 o 0 0 4 1106.19 979.71 40.53 o 2 0 4 8999.65 8104.41 354.11 o 4 0 4 779.79 765.55 39.81 o 6 0 4 16.87 15.67 6.47 o 8 0 4 0.59 3.51 2.31 o 10 0 4 439.50 428.90 20.65 o 12 0 4 798.87 867.70 41.78 o 14 0 4 291.26 306.67 18.53 o 16 0 4 2910.16 3189.70 307.20 o 18 0 4 0.93 -1.32 4.55 o 20 0 4 249.51 229.96 44.95 o -25 1 4 0.75 -3.12 7.02 o -23 1 4 251.84 202.76 44.56 o -21 1 4 37.76 24.03 6.69 o -19 1 4 12.80 9.61 3.50 o -17 1 4 0.00 5.65 3.09 o -15 1 4 7.77 10.55 5.20 o -13 1 4 36.52 48.67 3.93 o -11 1 4 61.27 57.40 3.93 o -9 1 4 2.72 9.36 2.23 o -7 1 4 2399.59 2216.52 106.97 o -5 1 4 2201.28 2293.62 129.69 o -3 1 4 7834.61 7340.90 321.94 o -1 1 4 9791.52 9448.49 355.47 o 1 1 4 4193.15 3920.80 120.35 o 3 1 4 6132.02 5969.84 221.72 o 5 1 4 0.38 0.60 3.43 o 7 1 4 32.74 26.11 6.18 o 9 1 4 66.58 73.31 11.67 o 11 1 4 89.85 98.76 7.23 o 13 1 4 835.19 850.14 41.97 o 15 1 4 821.60 857.36 53.30 o 17 1 4 122.71 121.19 10.32 o 19 1 4 6.08 14.19 9.28 o -24 2 4 39.17 31.65 17.45 o -22 2 4 144.17 112.50 25.92 o -20 2 4 8.08 8.48 4.23 o -18 2 4 1716.91 1822.99 90.39 o -16 2 4 83.33 74.54 6.88 o -14 2 4 4.93 5.78 3.56 o -12 2 4 162.30 208.68 11.04 o -10 2 4 30.52 37.03 4.70 o -8 2 4 698.94 714.20 46.11 o -6 2 4 1317.69 1439.63 84.04 o -4 2 4 7.78 5.42 2.80 o -2 2 4 99.83 124.14 4.74 o 0 2 4 1066.40 1016.16 34.74 o 2 2 4 1852.87 1923.45 116.61 o 4 2 4 7432.72 7440.60 287.41 o 6 2 4 14.91 15.09 4.93 o 8 2 4 354.54 409.08 16.28 o 10 2 4 2914.16 2936.05 152.19 o 12 2 4 193.27 184.01 10.91 o 14 2 4 222.99 238.61 18.23 o 16 2 4 29.34 29.29 10.58 o 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