#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/38/2103863.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103863_Fobs loop_ _publ_author_name 'Bowes, Katharine F.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; Phosphonopropionic acid as a building block in supramolecular chemistry: salts with organic diamines ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 248 _journal_page_last 262 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.634 _cell_angle_beta 73.176 _cell_angle_gamma 87.386 _cell_length_a 7.5651 _cell_length_b 8.6472 _cell_length_c 9.0077 _exptl_crystal_F_000 258.00 _reflns_d_resolution_high 0.7664 _[local]_cod_data_source_file bm0061VIsup7.hkl _[local]_cod_data_source_block VI #BEGIN Tags that were not found in dictionaries: _shelx_title ' 204 KFB05' _shelx_refln_list_code 4 _shelx_F_calc_maximum 70.13 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 122.61 96.50 7.43 o 2 0 0 394.08 354.80 15.62 o 3 0 0 20.67 21.73 0.99 o 4 0 0 0.67 0.35 0.17 o 5 0 0 110.49 102.06 3.89 o 6 0 0 183.27 181.10 6.98 o 7 0 0 143.25 146.72 7.13 o 8 0 0 119.39 127.31 9.91 o 9 0 0 0.13 -0.15 2.01 o -9 1 0 9.89 6.47 3.20 o -8 1 0 19.62 18.53 2.45 o -7 1 0 1.77 3.01 1.30 o -6 1 0 426.96 446.24 21.82 o -5 1 0 0.70 0.61 0.93 o -4 1 0 86.24 100.23 4.28 o -3 1 0 52.43 43.49 1.94 o -2 1 0 232.09 234.86 8.10 o -1 1 0 40.08 51.24 2.02 o 1 1 0 7.31 6.37 0.33 o 2 1 0 422.46 375.67 10.69 o 3 1 0 660.58 674.13 26.98 o 4 1 0 5.82 7.58 0.51 o 5 1 0 115.71 126.34 3.98 o 6 1 0 46.47 47.58 2.47 o 7 1 0 14.99 14.25 2.57 o 8 1 0 107.92 99.86 6.44 o 9 1 0 136.39 131.23 18.59 o -9 2 0 4.42 4.01 3.19 o -8 2 0 28.23 31.89 3.37 o -7 2 0 67.66 61.56 4.36 o -6 2 0 1.64 0.28 0.41 o -5 2 0 50.43 48.43 1.72 o -4 2 0 22.96 22.93 0.95 o -3 2 0 761.85 741.59 20.18 o -2 2 0 287.52 249.08 8.21 o -1 2 0 2863.83 2813.75 109.68 o 0 2 0 387.37 308.42 11.63 o 1 2 0 158.24 145.37 4.55 o 2 2 0 320.46 359.74 10.71 o 3 2 0 521.20 516.54 14.97 o 4 2 0 4.01 0.99 0.35 o 5 2 0 113.84 121.49 3.54 o 6 2 0 31.31 29.20 1.18 o 7 2 0 136.47 147.03 7.61 o 8 2 0 57.50 58.90 4.74 o 9 2 0 0.61 -1.73 1.95 o -9 3 0 3.15 0.44 2.45 o -8 3 0 6.70 5.79 2.07 o -7 3 0 84.06 78.85 4.30 o -6 3 0 208.68 202.08 7.49 o -5 3 0 554.96 561.67 16.17 o -4 3 0 228.23 228.99 6.43 o -3 3 0 1995.02 1901.93 49.35 o -2 3 0 2271.45 2256.22 63.98 o -1 3 0 118.70 101.15 4.09 o 0 3 0 48.95 38.78 1.37 o 1 3 0 2349.19 2359.25 76.68 o 2 3 0 4.91 2.33 0.36 o 3 3 0 49.57 56.79 1.79 o 4 3 0 98.71 86.09 2.70 o 5 3 0 317.58 332.60 9.11 o 6 3 0 255.86 261.74 7.73 o 7 3 0 106.80 101.18 5.74 o 8 3 0 4.16 2.97 3.23 o -8 4 0 22.07 18.93 1.36 o -7 4 0 11.38 9.93 0.96 o -6 4 0 17.40 18.72 1.21 o -5 4 0 335.95 340.86 10.31 o -4 4 0 49.63 49.60 1.47 o -3 4 0 164.44 157.70 4.44 o -2 4 0 1.25 0.97 0.37 o -1 4 0 309.09 293.01 11.41 o 0 4 0 505.08 569.51 20.24 o 1 4 0 35.87 37.64 1.16 o 2 4 0 9.73 7.21 0.88 o 3 4 0 526.67 547.03 13.28 o 4 4 0 164.87 166.98 4.33 o 5 4 0 6.06 5.38 0.52 o 6 4 0 90.79 95.72 3.15 o 7 4 0 179.45 189.89 7.78 o 8 4 0 36.63 36.97 4.07 o -8 5 0 5.94 3.91 1.51 o -7 5 0 34.15 31.94 1.93 o -6 5 0 129.08 134.64 4.88 o -5 5 0 43.55 47.71 1.74 o -4 5 0 1152.08 1158.51 28.27 o -3 5 0 53.21 48.24 2.16 o -2 5 0 36.11 36.25 4.25 o -1 5 0 8.55 11.16 1.30 o 0 5 0 801.14 765.43 26.54 o 1 5 0 133.93 125.93 3.40 o 2 5 0 202.89 210.50 6.10 o 3 5 0 239.57 233.40 6.23 o 4 5 0 73.33 77.63 2.16 o 5 5 0 120.36 124.48 3.59 o 6 5 0 68.70 64.05 3.19 o 7 5 0 135.05 140.54 6.51 o 8 5 0 107.26 103.55 11.81 o -8 6 0 59.01 52.15 7.72 o -7 6 0 41.79 41.58 2.99 o -6 6 0 625.05 664.63 25.89 o -5 6 0 13.59 14.76 0.95 o -4 6 0 300.83 298.21 8.75 o -3 6 0 358.87 337.43 11.43 o -2 6 0 178.50 169.88 5.54 o -1 6 0 123.65 131.35 4.56 o 0 6 0 19.54 17.34 1.66 o 1 6 0 442.00 418.25 10.44 o 2 6 0 149.02 167.89 4.61 o 3 6 0 107.34 114.46 3.31 o 4 6 0 154.82 153.59 5.10 o 5 6 0 3.59 2.66 0.66 o 6 6 0 36.78 35.42 2.00 o 7 6 0 197.27 207.79 10.05 o -7 7 0 140.04 130.41 7.99 o -6 7 0 0.01 1.35 0.79 o -5 7 0 79.02 83.92 3.70 o -4 7 0 13.90 13.60 1.19 o -3 7 0 1.98 1.55 1.15 o -2 7 0 142.83 140.18 5.67 o -1 7 0 13.03 13.04 1.19 o 0 7 0 37.18 32.06 2.01 o 1 7 0 696.68 686.95 20.61 o 2 7 0 121.64 120.86 3.81 o 3 7 0 132.17 135.53 4.74 o 4 7 0 99.07 87.62 4.61 o 5 7 0 107.97 115.11 5.42 o 6 7 0 56.55 61.15 2.88 o -6 8 0 1.77 1.81 1.13 o -5 8 0 203.82 211.68 9.79 o -4 8 0 11.90 11.27 1.60 o -3 8 0 174.27 180.45 11.32 o -2 8 0 73.85 74.57 4.05 o -1 8 0 41.61 38.09 2.26 o 0 8 0 39.01 48.63 3.24 o 1 8 0 7.72 4.92 1.88 o 2 8 0 89.89 95.20 3.22 o 3 8 0 12.63 9.52 0.91 o 4 8 0 0.08 0.87 0.67 o 5 8 0 0.01 0.32 0.85 o -5 9 0 242.39 252.05 13.54 o -4 9 0 14.28 11.45 1.60 o -3 9 0 17.61 15.31 2.12 o -2 9 0 0.06 -0.58 1.25 o -1 9 0 6.07 3.40 1.35 o 0 9 0 140.17 132.69 5.98 o 1 9 0 8.13 4.32 1.19 o 2 9 0 101.22 100.46 4.52 o 3 9 0 2.56 3.50 0.80 o 4 9 0 106.98 105.98 4.68 o -3 10 0 4.45 0.23 1.54 o -2 10 0 133.00 123.32 11.55 o -1 10 0 46.93 44.86 5.82 o 0 10 0 0.63 0.66 1.41 o 1 10 0 4.17 1.72 1.25 o 2 10 0 40.55 34.67 3.75 o 3 10 0 210.74 213.69 20.66 o -1 -10 1 67.92 59.07 4.15 o 0 -10 1 2.80 2.04 1.41 o 1 -10 1 2.79 0.61 1.72 o 2 -10 1 2.87 5.53 2.80 o 3 -10 1 77.08 79.14 6.50 o -4 -9 1 62.78 61.86 4.33 o -3 -9 1 131.20 134.22 7.44 o -2 -9 1 160.40 161.52 8.28 o -1 -9 1 150.44 161.36 7.51 o 0 -9 1 4.97 4.45 1.33 o 1 -9 1 8.86 14.56 2.42 o 2 -9 1 18.92 13.48 2.08 o 3 -9 1 5.11 2.25 1.56 o 4 -9 1 210.15 225.88 13.34 o 5 -9 1 12.88 12.62 1.87 o -5 -8 1 18.62 19.94 1.51 o -4 -8 1 26.85 31.00 3.20 o -3 -8 1 0.81 1.98 0.75 o -2 -8 1 188.02 196.79 8.44 o -1 -8 1 112.75 121.60 5.20 o 0 -8 1 146.34 148.13 6.71 o 1 -8 1 101.48 101.72 5.48 o 2 -8 1 194.09 189.95 10.31 o 3 -8 1 65.39 66.37 4.63 o 4 -8 1 31.59 33.10 2.47 o 5 -8 1 56.57 55.74 3.08 o 6 -8 1 44.31 39.60 2.82 o -6 -7 1 39.12 36.52 2.33 o -5 -7 1 20.06 26.42 1.73 o -4 -7 1 110.36 111.45 4.59 o -3 -7 1 0.69 1.37 0.62 o -2 -7 1 69.67 69.71 2.76 o -1 -7 1 31.67 31.13 1.33 o 0 -7 1 157.43 155.83 5.34 o 1 -7 1 100.96 116.46 6.81 o 2 -7 1 606.52 582.83 25.06 o 3 -7 1 16.52 14.21 3.05 o 4 -7 1 1.42 2.45 1.54 o 5 -7 1 5.08 7.78 1.45 o 6 -7 1 1.27 1.78 1.35 o 7 -7 1 60.06 51.21 3.12 o -7 -6 1 21.11 18.49 1.51 o -6 -6 1 62.58 65.94 4.83 o -5 -6 1 67.34 77.15 4.58 o -4 -6 1 91.77 93.28 4.34 o -3 -6 1 378.14 420.67 12.30 o -2 -6 1 920.98 904.58 25.70 o -1 -6 1 117.86 111.86 3.17 o 0 -6 1 169.73 160.58 4.29 o 1 -6 1 242.15 229.46 7.61 o 2 -6 1 63.91 57.64 3.68 o 3 -6 1 116.24 118.17 5.03 o 4 -6 1 140.44 131.62 10.74 o 5 -6 1 509.55 549.71 17.80 o 6 -6 1 20.47 18.16 1.22 o 7 -6 1 20.10 21.45 2.00 o 8 -6 1 97.73 93.39 6.64 o -7 -5 1 28.75 28.83 2.00 o -6 -5 1 44.48 44.74 2.75 o -5 -5 1 85.01 93.00 3.56 o -4 -5 1 249.69 243.45 7.69 o -3 -5 1 152.30 156.75 4.66 o -2 -5 1 12.46 14.00 1.23 o -1 -5 1 283.91 282.80 8.42 o 0 -5 1 101.47 95.80 4.61 o 1 -5 1 55.20 51.52 2.26 o 2 -5 1 8.29 7.11 1.10 o 3 -5 1 36.72 35.06 1.83 o 4 -5 1 95.38 87.82 2.83 o 5 -5 1 158.15 150.85 5.80 o 6 -5 1 460.18 465.54 18.44 o 7 -5 1 0.28 -0.42 0.89 o 8 -5 1 125.67 138.06 8.93 o -8 -4 1 24.00 22.75 3.38 o -7 -4 1 125.75 129.35 7.41 o -6 -4 1 127.32 135.55 5.40 o -5 -4 1 233.62 224.94 8.94 o -4 -4 1 55.46 59.73 2.34 o -3 -4 1 23.04 24.97 1.03 o -2 -4 1 604.46 578.23 15.84 o -1 -4 1 456.84 510.29 15.72 o 0 -4 1 44.89 44.16 2.10 o 1 -4 1 195.30 179.82 5.74 o 2 -4 1 190.00 190.49 7.02 o 3 -4 1 38.23 37.25 1.40 o 4 -4 1 238.74 227.02 6.11 o 5 -4 1 39.47 36.42 1.25 o 6 -4 1 226.08 229.60 6.86 o 7 -4 1 17.00 14.39 1.12 o 8 -4 1 78.05 83.42 5.84 o 9 -4 1 10.69 2.75 2.82 o -8 -3 1 52.86 47.05 5.08 o -7 -3 1 68.40 67.06 3.19 o -6 -3 1 17.46 16.55 0.92 o -5 -3 1 760.75 763.29 30.48 o -4 -3 1 179.54 175.98 6.59 o -3 -3 1 38.57 42.17 1.27 o -2 -3 1 861.87 844.64 21.12 o -1 -3 1 110.65 117.37 4.56 o 0 -3 1 381.90 346.91 12.61 o 1 -3 1 523.04 552.45 17.01 o 2 -3 1 9.22 5.58 0.38 o 3 -3 1 898.86 881.51 33.56 o 4 -3 1 178.36 187.51 5.03 o 5 -3 1 1545.03 1557.24 37.23 o 6 -3 1 27.59 29.12 1.83 o 7 -3 1 70.79 76.35 3.57 o 8 -3 1 17.02 15.38 1.90 o 9 -3 1 5.17 0.52 1.93 o -8 -2 1 185.34 182.25 11.97 o -7 -2 1 14.41 12.65 0.89 o -6 -2 1 394.56 407.92 13.95 o -5 -2 1 11.35 12.24 1.07 o -4 -2 1 172.32 172.88 8.72 o -3 -2 1 14.08 21.21 1.50 o -2 -2 1 513.44 572.76 15.43 o -1 -2 1 442.45 410.33 10.77 o 0 -2 1 687.85 664.23 26.73 o 1 -2 1 598.61 509.72 17.21 o 2 -2 1 21.37 21.57 0.70 o 3 -2 1 25.29 18.23 0.79 o 4 -2 1 76.36 84.10 2.34 o 5 -2 1 304.46 282.83 7.96 o 6 -2 1 50.70 50.78 1.92 o 7 -2 1 150.56 168.69 12.46 o 8 -2 1 19.47 17.75 2.16 o 9 -2 1 52.83 45.44 4.42 o -9 -1 1 13.92 9.15 2.92 o -8 -1 1 1.07 -0.36 1.58 o -7 -1 1 226.19 229.17 7.88 o -6 -1 1 170.89 177.96 7.89 o -5 -1 1 70.59 74.10 2.56 o -4 -1 1 391.90 405.91 15.27 o -3 -1 1 63.78 73.17 3.35 o -2 -1 1 10.68 15.58 0.81 o -1 -1 1 925.68 927.10 30.67 o 0 -1 1 1145.69 1021.79 32.03 o 1 -1 1 744.34 692.17 25.90 o 2 -1 1 54.77 58.68 1.59 o 3 -1 1 319.20 255.62 7.31 o 4 -1 1 856.75 873.78 23.62 o 5 -1 1 950.01 966.61 35.25 o 6 -1 1 1.17 1.38 1.68 o 7 -1 1 244.76 249.72 15.13 o 8 -1 1 28.00 29.68 2.68 o 9 -1 1 1.43 1.20 2.01 o -9 0 1 62.63 51.01 8.14 o -8 0 1 282.87 288.37 18.14 o -7 0 1 779.16 804.12 41.00 o -6 0 1 189.11 193.66 6.43 o -5 0 1 13.00 18.88 0.82 o -4 0 1 66.40 85.13 2.84 o -3 0 1 39.77 37.83 1.68 o -2 0 1 77.86 83.38 3.83 o 1 0 1 126.57 105.23 7.66 o 2 0 1 1961.28 1835.14 76.08 o 3 0 1 1851.82 1958.04 78.92 o 4 0 1 141.27 144.27 5.46 o 5 0 1 10.53 13.36 1.25 o 6 0 1 79.00 75.44 3.34 o 7 0 1 57.37 62.16 4.05 o 8 0 1 8.96 5.41 1.44 o 9 0 1 262.69 285.55 37.46 o -9 1 1 33.41 28.90 5.06 o -8 1 1 2.52 4.94 1.63 o -7 1 1 4.70 5.13 2.15 o -6 1 1 139.59 152.27 5.16 o -5 1 1 1.96 2.02 0.43 o -4 1 1 0.01 0.40 0.36 o -3 1 1 344.39 378.10 13.16 o -2 1 1 695.00 666.09 25.53 o -1 1 1 848.32 863.06 36.26 o 0 1 1 682.46 669.40 54.85 o 1 1 1 127.80 123.58 4.25 o 2 1 1 4917.58 4894.30 252.93 o 3 1 1 90.39 86.05 2.87 o 4 1 1 142.93 146.79 5.06 o 5 1 1 19.59 18.74 2.52 o 6 1 1 459.61 473.28 22.68 o 7 1 1 159.89 168.38 8.28 o 8 1 1 159.19 153.01 12.31 o 9 1 1 25.23 25.81 4.16 o -9 2 1 49.84 42.68 6.17 o -8 2 1 66.98 57.60 5.30 o -7 2 1 1.64 2.18 0.89 o -6 2 1 8.81 7.25 0.78 o -5 2 1 55.90 55.44 2.55 o -4 2 1 509.64 554.99 20.45 o -3 2 1 100.82 118.34 4.66 o -2 2 1 29.20 38.21 2.32 o -1 2 1 364.29 394.49 14.46 o 0 2 1 1817.66 1846.05 83.28 o 1 2 1 509.39 469.64 13.36 o 2 2 1 114.97 108.12 2.91 o 3 2 1 2.77 8.12 0.38 o 4 2 1 460.67 470.51 11.60 o 5 2 1 60.92 52.39 1.89 o 6 2 1 27.76 29.01 3.17 o 7 2 1 118.27 131.06 8.26 o 8 2 1 0.00 0.66 1.02 o 9 2 1 0.67 1.04 1.94 o -8 3 1 17.59 16.68 2.30 o -7 3 1 41.98 39.53 2.27 o -6 3 1 332.19 340.18 12.37 o -5 3 1 8.04 6.99 1.15 o -4 3 1 204.51 186.00 8.72 o -3 3 1 1433.09 1492.64 43.78 o -2 3 1 145.71 180.57 5.22 o -1 3 1 3870.13 3943.33 115.50 o 0 3 1 88.76 98.25 3.45 o 1 3 1 313.60 282.52 7.52 o 2 3 1 620.34 668.74 19.64 o 3 3 1 176.57 165.47 4.54 o 4 3 1 230.32 225.07 4.99 o 5 3 1 315.47 324.91 8.84 o 6 3 1 234.09 248.74 8.94 o 7 3 1 11.41 10.05 1.47 o 8 3 1 12.50 12.95 2.55 o 9 3 1 6.70 6.52 2.25 o -8 4 1 61.60 54.58 4.10 o -7 4 1 12.92 14.91 1.28 o -6 4 1 22.27 21.07 2.05 o -5 4 1 67.58 63.52 2.27 o -4 4 1 68.06 65.56 3.69 o -3 4 1 8.97 6.98 0.58 o -2 4 1 37.50 35.90 1.33 o -1 4 1 195.17 160.00 6.98 o 0 4 1 1041.60 1039.50 39.32 o 1 4 1 1041.31 1057.42 30.32 o 2 4 1 853.00 884.66 25.25 o 3 4 1 1388.61 1456.00 36.79 o 4 4 1 21.22 17.63 0.67 o 5 4 1 1.59 2.49 0.44 o 6 4 1 297.40 298.99 10.20 o 7 4 1 0.71 0.55 0.67 o 8 4 1 174.29 178.52 13.38 o -7 5 1 245.38 250.68 16.64 o -6 5 1 84.43 87.27 3.63 o -5 5 1 452.65 444.68 15.23 o -4 5 1 39.62 41.56 1.59 o -3 5 1 333.46 315.52 7.79 o -2 5 1 222.61 233.07 7.82 o -1 5 1 4.58 2.99 0.83 o 0 5 1 236.21 236.72 8.10 o 1 5 1 1139.40 1100.87 33.48 o 2 5 1 253.74 235.09 5.92 o 3 5 1 1.43 1.57 0.52 o 4 5 1 5.68 4.66 0.52 o 5 5 1 114.51 109.58 3.58 o 6 5 1 9.27 10.51 0.68 o 7 5 1 3.56 2.18 0.71 o 8 5 1 1.20 0.91 1.44 o -7 6 1 3.58 4.45 1.06 o -6 6 1 214.11 220.58 10.21 o -5 6 1 30.77 26.04 1.35 o -4 6 1 0.09 -0.47 0.51 o -3 6 1 410.59 437.41 11.22 o -2 6 1 427.52 409.25 13.52 o -1 6 1 0.80 0.36 0.66 o 0 6 1 903.36 878.28 25.13 o 1 6 1 111.16 98.62 3.81 o 2 6 1 53.66 54.16 1.70 o 3 6 1 55.86 49.37 1.71 o 4 6 1 74.75 66.18 2.24 o 5 6 1 99.57 103.82 4.39 o 6 6 1 192.35 217.80 8.98 o 7 6 1 91.96 95.37 5.85 o -7 7 1 3.57 3.35 2.27 o -6 7 1 137.39 136.80 7.90 o -5 7 1 90.58 89.82 3.24 o -4 7 1 326.07 345.56 10.46 o -3 7 1 131.55 118.77 4.13 o -2 7 1 67.76 68.46 3.21 o -1 7 1 90.70 90.13 3.46 o 0 7 1 1284.70 1265.91 47.48 o 1 7 1 238.81 238.84 9.04 o 2 7 1 42.44 41.53 1.33 o 3 7 1 142.59 140.76 4.67 o 4 7 1 95.29 111.51 3.56 o 5 7 1 17.70 14.35 1.45 o 6 7 1 76.36 64.58 3.84 o 7 7 1 96.42 96.90 5.97 o -6 8 1 13.05 10.59 1.64 o -5 8 1 206.13 216.46 9.82 o -4 8 1 12.72 12.74 1.23 o -3 8 1 174.64 168.94 6.98 o -2 8 1 70.28 66.77 4.23 o -1 8 1 114.19 125.44 6.53 o 0 8 1 296.38 274.26 12.48 o 1 8 1 22.58 17.45 1.68 o 2 8 1 16.53 15.96 1.29 o 3 8 1 3.16 3.11 0.71 o 4 8 1 39.34 37.54 1.75 o 5 8 1 17.62 21.02 1.74 o 6 8 1 31.81 28.27 2.16 o -5 9 1 59.60 57.27 3.66 o -4 9 1 10.77 7.19 1.75 o -3 9 1 148.10 156.03 9.69 o -2 9 1 14.20 18.04 1.52 o -1 9 1 50.38 52.07 3.44 o 0 9 1 14.14 12.71 1.95 o 1 9 1 65.67 58.30 2.83 o 2 9 1 5.89 8.40 1.93 o 3 9 1 44.99 45.09 3.21 o 4 9 1 63.42 74.57 3.53 o 5 9 1 18.45 15.10 2.62 o -4 10 1 32.63 37.42 3.01 o -3 10 1 554.16 641.04 37.78 o -2 10 1 49.87 50.17 3.15 o -1 10 1 23.50 18.32 1.84 o 0 10 1 11.48 13.05 2.22 o 1 10 1 1.80 0.82 1.02 o 2 10 1 194.86 207.24 9.66 o 3 10 1 33.61 31.36 4.70 o 1 -10 2 10.96 8.03 2.09 o -3 -9 2 176.77 164.82 10.96 o -2 -9 2 13.26 13.33 3.09 o -1 -9 2 4.06 -0.54 1.28 o 0 -9 2 5.74 6.69 1.66 o 1 -9 2 58.09 58.01 3.38 o 2 -9 2 60.23 56.08 3.94 o 3 -9 2 101.80 94.41 6.59 o 4 -9 2 0.09 0.44 1.63 o -4 -8 2 84.55 83.76 3.83 o -3 -8 2 39.46 38.17 2.31 o -2 -8 2 0.32 0.57 1.23 o -1 -8 2 267.51 276.68 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