#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2103906.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2103906_Fobs loop_ _publ_author_name 'Pinheiro, Carlos Bas\'ilio' 'Gardon, Manuel' 'Chapuis, Gervais' _publ_section_title ; Structural changes of hexamethylenetetramine and undecanedioic acid co-crystal (HMT-C11) as a function of the temperature ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 416 _journal_page_last 427 _journal_volume 59 _journal_year 2003 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-B 2b 2' _symmetry_space_group_name_H-M 'B m m b' _exptl_crystal_F_000 776.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file na0146324Ksup10.hkl _[local]_cod_data_source_block 324K #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_F_calc_maximum 303.74 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 92255.27 102069.77 100.13 o 4 0 0 656.27 423.92 27.65 o 6 0 0 122.02 147.74 8.49 o 8 0 0 765.22 774.93 38.85 o 10 0 0 9.87 13.88 3.32 o 2 2 0 373.19 292.70 15.94 o 4 2 0 1145.43 1204.39 52.02 o 6 2 0 774.65 661.73 27.51 o 8 2 0 970.74 1033.21 44.71 o 10 2 0 24.47 25.18 3.85 o 2 4 0 24.42 14.92 2.46 o 4 4 0 32.97 43.51 2.31 o 6 4 0 832.58 837.14 33.65 o 8 4 0 269.44 286.81 6.73 o 10 4 0 4.40 9.71 2.22 o 0 6 0 4719.14 4115.20 291.15 o 2 6 0 489.99 365.08 14.29 o 4 6 0 24.03 19.16 0.98 o 6 6 0 396.70 395.79 17.57 o 8 6 0 133.57 149.14 10.22 o 10 6 0 0.13 0.52 1.61 o 0 8 0 4705.51 3958.42 369.23 o 2 8 0 842.36 611.84 24.06 o 4 8 0 121.20 124.21 6.18 o 6 8 0 14.08 11.66 1.25 o 8 8 0 50.97 72.31 5.06 o 10 8 0 1.46 0.13 2.20 o 0 10 0 478.24 402.56 31.89 o 2 10 0 318.51 269.85 11.17 o 4 10 0 86.15 65.55 2.89 o 6 10 0 36.06 38.34 1.54 o 8 10 0 1.04 1.56 1.47 o 10 10 0 0.00 0.60 1.98 o 0 12 0 1565.45 1363.99 110.20 o 2 12 0 52.60 41.73 1.44 o 4 12 0 4.58 7.08 1.06 o 6 12 0 23.40 29.14 1.42 o 8 12 0 49.28 49.80 3.43 o 10 12 0 2.18 3.94 2.49 o 0 14 0 1688.35 1562.08 138.38 o 2 14 0 146.40 124.89 6.14 o 4 14 0 22.16 27.55 1.37 o 6 14 0 1.22 1.07 0.76 o 8 14 0 30.05 31.02 4.80 o 10 14 0 1.49 2.01 2.89 o 0 16 0 1.17 0.04 1.30 o 2 16 0 6.88 5.67 0.78 o 4 16 0 12.49 16.48 1.33 o 6 16 0 36.32 46.74 2.12 o 8 16 0 22.75 12.90 3.50 o 0 18 0 1079.20 1147.79 106.34 o 2 18 0 403.64 382.45 20.48 o 4 18 0 2.10 0.81 0.65 o 6 18 0 2.08 3.23 1.16 o 8 18 0 34.08 39.93 5.10 o 0 20 0 237.40 199.72 23.71 o 2 20 0 0.86 1.38 0.70 o 4 20 0 199.30 255.55 18.58 o 6 20 0 73.44 93.12 4.87 o 8 20 0 2.30 2.45 1.75 o 0 22 0 94.21 82.49 5.08 o 2 22 0 15.70 25.03 3.41 o 4 22 0 6.82 8.39 1.36 o 6 22 0 43.36 46.40 2.81 o 8 22 0 36.67 37.20 4.12 o 0 24 0 531.00 741.79 78.63 o 2 24 0 237.87 321.31 21.79 o 4 24 0 68.54 80.18 4.56 o 6 24 0 62.14 86.94 4.70 o 8 24 0 30.19 30.00 4.38 o 0 26 0 311.01 352.86 48.11 o 2 26 0 51.88 51.28 2.80 o 4 26 0 3.33 3.97 1.22 o 6 26 0 3.82 3.64 1.34 o 0 28 0 14.88 7.47 2.57 o 2 28 0 1.27 2.55 1.13 o 4 28 0 7.19 6.37 1.41 o 6 28 0 6.64 3.80 1.59 o 0 30 0 0.00 2.85 2.24 o 2 30 0 1.68 2.20 1.25 o 4 30 0 0.53 1.25 1.38 o 0 32 0 3.33 3.70 2.14 o 2 32 0 0.82 0.79 1.36 o 4 32 0 0.00 2.46 1.36 o 0 34 0 0.53 0.00 3.75 o 2 34 0 0.28 0.95 1.41 o 1 0 1 702.86 656.74 63.38 o 3 0 1 0.54 1.17 1.08 o 5 0 1 87.85 97.62 3.48 o 7 0 1 100.07 115.76 15.00 o 9 0 1 22.01 16.96 2.43 o 11 0 1 0.20 4.50 2.28 o 1 1 1 1174.05 1203.10 27.81 o 3 1 1 3232.47 3030.34 74.78 o 5 1 1 25.29 23.71 0.74 o 7 1 1 540.85 531.43 16.05 o 9 1 1 25.26 18.62 1.25 o 11 1 1 34.96 50.09 2.78 o 1 2 1 2380.42 2194.86 105.48 o 3 2 1 20.87 29.13 1.98 o 5 2 1 92.72 104.93 3.23 o 7 2 1 108.41 107.58 6.91 o 9 2 1 32.71 30.69 1.50 o 11 2 1 2.44 4.34 1.60 o 1 3 1 7020.22 6566.69 366.03 o 3 3 1 3301.17 3161.85 80.49 o 5 3 1 564.91 648.42 15.22 o 7 3 1 417.30 419.05 11.68 o 9 3 1 78.56 105.91 3.31 o 11 3 1 10.00 5.90 1.60 o 1 4 1 10344.08 9321.18 444.79 o 3 4 1 1074.42 1038.35 26.88 o 5 4 1 180.45 202.98 5.46 o 7 4 1 30.45 35.53 2.54 o 9 4 1 3.29 2.31 0.76 o 1 5 1 37077.27 35375.73 1456.82 o 3 5 1 34.62 29.86 1.09 o 5 5 1 358.63 330.47 8.05 o 7 5 1 97.51 115.22 3.45 o 9 5 1 16.54 22.58 1.57 o 1 6 1 6681.79 5747.38 259.12 o 3 6 1 391.80 336.06 9.70 o 5 6 1 12.98 7.17 0.70 o 7 6 1 4.47 2.74 0.73 o 9 6 1 0.67 1.58 0.80 o 1 7 1 3278.18 2879.14 128.91 o 3 7 1 1004.23 852.82 26.95 o 5 7 1 18.66 24.98 0.90 o 7 7 1 40.19 38.21 2.12 o 9 7 1 0.44 1.88 0.88 o 1 8 1 358.71 250.15 11.15 o 3 8 1 376.50 320.60 9.06 o 5 8 1 0.42 0.09 0.42 o 7 8 1 68.18 54.91 2.00 o 9 8 1 21.09 20.16 1.53 o 1 9 1 2361.86 2225.07 86.33 o 3 9 1 6.48 8.59 0.60 o 5 9 1 50.55 51.04 1.51 o 7 9 1 5.36 4.67 1.03 o 9 9 1 41.64 53.64 2.12 o 1 10 1 731.26 883.58 34.88 o 3 10 1 28.68 27.25 0.88 o 5 10 1 58.74 64.89 1.90 o 7 10 1 94.85 93.07 3.03 o 9 10 1 15.74 12.40 1.45 o 1 11 1 533.02 551.18 22.25 o 3 11 1 0.78 1.18 0.46 o 5 11 1 60.13 51.33 1.57 o 7 11 1 7.86 7.70 1.08 o 9 11 1 2.28 1.16 0.85 o 1 12 1 3499.12 3694.32 126.68 o 3 12 1 138.05 131.05 3.37 o 5 12 1 2.33 3.51 0.64 o 7 12 1 29.07 36.72 1.86 o 9 12 1 8.76 9.53 1.27 o 1 13 1 180.47 212.73 13.13 o 3 13 1 8.63 8.24 0.86 o 5 13 1 1.31 0.98 0.51 o 7 13 1 3.85 5.48 1.08 o 9 13 1 2.51 2.35 0.95 o 1 14 1 608.80 540.40 20.13 o 3 14 1 60.60 58.24 1.92 o 5 14 1 28.36 31.54 1.33 o 7 14 1 7.03 4.74 1.02 o 9 14 1 2.68 3.43 1.13 o 1 15 1 7.41 10.50 1.96 o 3 15 1 78.67 84.62 3.46 o 5 15 1 222.47 241.15 7.52 o 7 15 1 71.71 86.68 2.80 o 9 15 1 1.76 1.59 1.11 o 1 16 1 4.35 2.89 0.57 o 3 16 1 3.47 3.19 0.57 o 5 16 1 87.46 78.59 2.34 o 7 16 1 96.21 96.01 3.15 o 9 16 1 5.32 2.14 1.49 o 1 17 1 162.69 144.17 6.20 o 3 17 1 19.46 15.22 0.97 o 5 17 1 4.58 8.44 1.02 o 7 17 1 4.23 7.38 1.12 o 9 17 1 0.17 2.68 1.58 o 1 18 1 4.99 2.78 0.63 o 3 18 1 0.39 0.63 0.51 o 5 18 1 7.35 7.78 0.87 o 7 18 1 5.55 4.74 0.97 o 9 18 1 0.24 1.49 1.50 o 1 19 1 11.13 17.02 0.99 o 3 19 1 18.38 13.95 0.92 o 5 19 1 15.02 18.85 1.22 o 7 19 1 10.26 6.68 1.14 o 9 19 1 1.67 3.12 1.96 o 1 20 1 32.64 32.44 1.35 o 3 20 1 79.92 67.33 2.39 o 5 20 1 77.68 66.26 2.34 o 7 20 1 31.50 26.74 1.86 o 9 20 1 6.98 6.12 2.87 o 1 21 1 152.57 168.61 7.67 o 3 21 1 0.31 2.49 0.66 o 5 21 1 4.11 3.54 0.79 o 7 21 1 15.28 13.59 1.64 o 1 22 1 99.44 106.12 4.69 o 3 22 1 42.82 36.11 1.46 o 5 22 1 14.71 14.86 1.29 o 7 22 1 8.78 5.35 1.20 o 1 23 1 98.49 108.77 5.65 o 3 23 1 17.05 20.49 1.31 o 5 23 1 21.38 26.88 1.45 o 7 23 1 8.24 3.82 1.09 o 1 24 1 23.20 25.72 1.74 o 3 24 1 0.19 1.99 0.74 o 5 24 1 0.36 1.61 0.69 o 7 24 1 3.22 2.27 1.11 o 1 25 1 0.59 2.12 0.71 o 3 25 1 65.83 78.99 4.20 o 5 25 1 26.82 34.15 1.95 o 7 25 1 1.07 1.96 1.07 o 1 26 1 37.58 46.28 2.63 o 3 26 1 11.71 15.61 1.37 o 5 26 1 10.02 8.92 1.13 o 7 26 1 7.37 9.00 1.62 o 1 27 1 4.85 3.58 0.84 o 3 27 1 1.46 1.90 0.78 o 5 27 1 0.46 1.72 0.83 o 1 28 1 23.23 25.57 2.15 o 3 28 1 5.28 3.42 0.95 o 5 28 1 1.35 2.47 0.88 o 1 29 1 30.87 31.97 2.22 o 3 29 1 1.68 2.12 0.81 o 5 29 1 1.05 2.26 0.92 o 1 30 1 0.07 1.63 0.88 o 3 30 1 0.03 1.48 0.79 o 5 30 1 0.15 1.80 1.04 o 1 31 1 0.95 2.46 0.93 o 3 31 1 1.08 1.36 0.85 o 1 32 1 0.02 1.78 0.87 o 3 32 1 0.84 3.53 1.13 o 1 33 1 17.95 25.67 2.04 o 3 33 1 9.30 7.96 1.57 o 1 34 1 9.69 6.30 1.35 o 0 0 2 4523.47 4353.07 125.26 o 2 0 2 801.69 694.52 32.67 o 4 0 2 5875.19 6008.13 288.17 o 6 0 2 132.62 151.80 5.11 o 8 0 2 61.54 73.88 2.56 o 10 0 2 12.98 7.84 1.66 o 0 1 2 1641.89 1556.65 52.57 o 2 1 2 53.29 45.53 1.06 o 4 1 2 115.61 198.54 19.74 o 6 1 2 6.24 5.22 0.84 o 8 1 2 15.19 7.72 1.04 o 10 1 2 0.91 1.39 0.94 o 0 2 2 1233.99 996.84 46.17 o 2 2 2 1113.73 1046.81 31.40 o 4 2 2 3853.07 3975.79 126.42 o 6 2 2 86.85 102.22 2.81 o 8 2 2 26.81 26.06 1.33 o 10 2 2 16.05 11.06 1.33 o 0 3 2 123.54 118.97 5.50 o 2 3 2 150.72 146.39 4.72 o 4 3 2 63.69 76.25 8.28 o 6 3 2 0.00 1.42 0.64 o 8 3 2 0.54 1.13 0.66 o 10 3 2 3.18 1.95 1.01 o 0 4 2 391.73 574.72 23.42 o 2 4 2 2085.23 2056.80 66.97 o 4 4 2 1761.88 1788.04 50.60 o 6 4 2 52.92 55.76 2.03 o 8 4 2 0.27 1.30 0.70 o 10 4 2 29.16 30.45 1.79 o 0 5 2 689.87 768.91 34.39 o 2 5 2 875.03 871.75 29.14 o 4 5 2 302.93 295.13 8.98 o 6 5 2 78.09 75.64 2.22 o 8 5 2 31.09 20.84 1.31 o 10 5 2 7.68 4.76 1.09 o 0 6 2 604.38 522.08 25.76 o 2 6 2 957.97 917.68 32.14 o 4 6 2 383.78 434.35 13.76 o 6 6 2 4.49 3.83 0.81 o 8 6 2 4.92 4.60 0.91 o 10 6 2 15.90 17.12 1.53 o 0 7 2 4393.02 4533.01 226.96 o 2 7 2 1364.99 1374.03 40.36 o 4 7 2 54.54 43.52 1.87 o 6 7 2 33.84 41.71 1.48 o 8 7 2 51.69 61.12 2.32 o 10 7 2 4.00 4.51 1.17 o 0 8 2 1065.02 1047.46 35.49 o 2 8 2 72.31 104.69 8.53 o 4 8 2 33.39 43.22 2.69 o 6 8 2 53.91 54.04 1.81 o 8 8 2 63.08 86.84 2.88 o 10 8 2 0.01 1.88 1.07 o 0 9 2 3870.35 3433.77 184.21 o 2 9 2 52.23 62.99 6.47 o 4 9 2 602.44 679.51 21.03 o 6 9 2 20.31 21.14 1.17 o 8 9 2 53.88 62.31 2.70 o 10 9 2 5.68 7.35 1.31 o 0 10 2 4649.23 4673.14 200.39 o 2 10 2 1001.06 987.32 33.03 o 4 10 2 5.30 9.70 1.49 o 6 10 2 14.68 10.55 1.23 o 8 10 2 0.31 4.94 1.10 o 10 10 2 0.46 2.42 1.23 o 0 11 2 6199.39 5874.30 305.96 o 2 11 2 1179.49 1159.83 43.18 o 4 11 2 65.85 54.70 2.52 o 6 11 2 245.21 211.98 6.83 o 8 11 2 190.73 212.27 7.30 o 10 11 2 4.36 3.49 1.21 o 0 12 2 955.99 1046.76 58.58 o 2 12 2 601.53 510.74 23.23 o 4 12 2 26.04 19.22 0.99 o 6 12 2 4.33 6.81 1.18 o 8 12 2 0.53 16.85 1.94 o 10 12 2 0.00 1.07 1.43 o 0 13 2 643.48 708.13 26.26 o 2 13 2 1.38 3.47 0.50 o 4 13 2 4.80 4.41 0.66 o 6 13 2 279.15 300.76 10.05 o 8 13 2 223.01 276.16 11.71 o 10 13 2 5.28 3.57 1.14 o 0 14 2 31.04 47.20 4.38 o 2 14 2 104.43 100.36 3.88 o 4 14 2 212.35 207.06 7.47 o 6 14 2 43.94 49.78 2.63 o 8 14 2 0.17 7.57 1.30 o 0 15 2 1566.95 1771.89 106.20 o 2 15 2 155.34 178.44 7.36 o 4 15 2 30.72 29.76 1.05 o 6 15 2 3.22 4.58 1.09 o 8 15 2 18.47 17.74 1.69 o 0 16 2 302.96 294.32 20.23 o 2 16 2 55.24 42.72 1.80 o 4 16 2 0.08 0.40 0.22 o 6 16 2 0.82 2.23 0.79 o 8 16 2 3.04 3.17 1.01 o 0 17 2 968.63 1016.15 80.15 o 2 17 2 138.81 140.78 5.17 o 4 17 2 14.33 11.87 0.91 o 6 17 2 0.04 1.26 0.78 o 8 17 2 3.34 4.55 1.07 o 0 18 2 60.61 59.85 4.27 o 2 18 2 2.11 4.05 0.66 o 4 18 2 69.87 64.92 2.65 o 6 18 2 8.37 4.63 0.94 o 8 18 2 3.08 1.76 0.95 o 0 19 2 31.72 26.16 2.94 o 2 19 2 3.70 3.09 0.61 o 4 19 2 4.39 2.63 0.62 o 6 19 2 25.49 19.30 1.47 o 8 19 2 2.93 2.73 1.12 o 0 20 2 9.97 10.43 1.47 o 2 20 2 34.93 34.26 1.65 o 4 20 2 67.10 76.24 2.94 o 6 20 2 18.11 23.65 1.60 o 8 20 2 0.38 0.00 1.13 o 0 21 2 38.30 43.90 3.07 o 2 21 2 2.01 3.90 0.75 o 4 21 2 21.79 24.68 1.35 o 6 21 2 23.28 18.24 1.47 o 8 21 2 0.39 0.39 1.12 o 0 22 2 24.63 23.01 2.41 o 2 22 2 44.57 44.08 2.23 o 4 22 2 61.80 67.58 2.65 o 6 22 2 14.55 13.82 1.40 o 8 22 2 0.83 0.81 1.23 o 0 23 2 34.35 43.23 2.67 o 2 23 2 2.87 4.35 0.81 o 4 23 2 1.46 3.27 0.75 o 6 23 2 0.00 1.51 0.94 o 0 24 2 0.08 1.86 0.99 o 2 24 2 13.95 13.33 1.04 o 4 24 2 37.34 31.02 1.42 o 6 24 2 2.62 2.19 0.93 o 0 25 2 10.19 5.53 1.25 o 2 25 2 0.58 1.12 0.65 o 4 25 2 0.33 1.42 0.69 o 6 25 2 7.22 4.00 1.11 o 0 26 2 8.08 4.81 1.45 o 2 26 2 0.37 1.00 0.69 o 4 26 2 10.35 6.25 0.98 o 6 26 2 0.02 2.77 1.14 o 0 27 2 27.21 27.66 2.40 o 2 27 2 7.81 9.42 1.06 o 4 27 2 1.43 3.42 1.01 o 6 27 2 3.27 4.50 1.26 o 0 28 2 14.75 18.62 2.26 o 2 28 2 33.85 38.56 2.68 o 4 28 2 34.89 36.97 2.61 o 6 28 2 3.07 1.89 1.48 o 0 29 2 61.46 52.03 6.00 o 2 29 2 50.37 45.74 2.49 o 4 29 2 13.61 8.07 1.27 o 0 30 2 6.45 2.86 1.22 o 2 30 2 0.00 1.56 0.86 o 4 30 2 5.11 3.20 0.98 o 0 31 2 7.32 3.32 1.33 o 2 31 2 2.53 2.21 0.97 o 4 31 2 0.00 0.56 1.09 o 0 32 2 0.00 1.90 1.42 o 2 32 2 0.00 1.07 1.03 o 0 33 2 0.08 0.00 1.60 o 2 33 2 0.09 1.63 1.35 o 1 0 3 82.80 82.94 2.48 o 3 0 3 1625.44 1616.60 59.79 o 5 0 3 540.74 688.47 27.65 o 7 0 3 14.98 15.20 1.36 o 9 0 3 3.60 2.59 1.15 o 1 1 3 12.36 18.77 0.72 o 3 1 3 1128.92 1103.43 36.34 o 5 1 3 589.02 680.23 21.11 o 7 1 3 12.35 7.88 0.92 o 9 1 3 6.52 3.55 0.90 o 1 2 3 70.60 85.22 2.87 o 3 2 3 787.14 821.45 21.52 o 5 2 3 253.77 282.70 7.30 o 7 2 3 7.45 5.36 0.91 o 9 2 3 3.57 2.63 0.81 o 1 3 3 14.44 20.78 2.44 o 3 3 3 235.61 280.53 10.52 o 5 3 3 6.32 16.07 1.84 o 7 3 3 128.29 149.73 5.89 o 9 3 3 8.80 7.19 1.01 o 1 4 3 52.59 57.22 1.69 o 3 4 3 0.02 11.59 3.03 o 5 4 3 25.04 26.95 1.87 o 7 4 3 7.96 9.91 1.29 o 9 4 3 0.65 1.27 0.83 o 1 5 3 109.33 97.31 2.29 o 3 5 3 495.71 573.05 18.74 o 5 5 3 175.36 181.67 6.31 o 7 5 3 18.98 19.19 1.17 o 9 5 3 3.57 2.21 0.84 o 1 6 3 17.46 15.38 0.86 o 3 6 3 24.51 20.52 1.18 o 5 6 3 2.73 1.59 0.63 o 7 6 3 27.28 20.26 1.29 o 9 6 3 11.86 15.13 1.45 o 1 7 3 106.36 113.88 3.03 o 3 7 3 107.77 109.47 3.43 o 5 7 3 51.66 43.52 1.27 o 7 7 3 6.23 5.16 0.90 o 9 7 3 2.17 2.40 0.89 o 1 8 3 186.53 176.89 6.79 o 3 8 3 35.82 38.77 1.55 o 5 8 3 0.07 0.14 0.67 o 7 8 3 113.06 100.66 4.66 o 9 8 3 28.10 24.83 1.61 o 1 9 3 212.80 245.43 6.62 o 3 9 3 22.69 26.24 1.27 o 5 9 3 57.69 45.60 2.06 o 7 9 3 56.04 56.09 2.63 o 9 9 3 3.72 5.13 1.13 o 1 10 3 446.69 473.93 15.01 o 3 10 3 312.41 324.43 11.23 o 5 10 3 158.16 146.90 5.13 o 7 10 3 29.91 27.35 1.70 o 9 10 3 13.71 7.74 1.36 o 1 11 3 540.35 590.87 16.99 o 3 11 3 15.88 21.42 1.60 o 5 11 3 42.45 50.64 2.88 o 7 11 3 62.79 71.02 2.91 o 9 11 3 5.92 3.59 1.08 o 1 12 3 352.26 374.79 14.82 o 3 12 3 465.34 501.43 16.90 o 5 12 3 287.98 306.06 11.28 o 7 12 3 6.41 9.27 1.67 o 9 12 3 3.24 1.99 1.18 o 1 13 3 761.41 737.79 23.51 o 3 13 3 9.25 15.01 1.11 o 5 13 3 7.58 11.58 1.72 o 7 13 3 46.07 44.01 1.83 o 9 13 3 13.75 8.77 1.55 o 1 14 3 92.48 79.00 4.45 o 3 14 3 342.28 383.40 12.61 o 5 14 3 109.57 128.07 5.37 o 7 14 3 25.76 25.94 1.75 o 9 14 3 2.54 6.22 1.29 o 1 15 3 385.40 447.40 18.75 o 3 15 3 43.10 69.02 2.83 o 5 15 3 23.18 24.21 1.71 o 7 15 3 19.51 15.79 1.60 o 9 15 3 3.03 2.41 1.20 o 1 16 3 161.55 205.29 9.99 o 3 16 3 8.20 7.63 0.77 o 5 16 3 5.19 2.58 0.73 o 7 16 3 61.29 59.64 3.08 o 9 16 3 1.62 1.72 1.34 o 1 17 3 83.57 87.54 4.93 o 3 17 3 65.24 58.65 2.28 o 5 17 3 0.41 1.63 0.71 o 7 17 3 4.31 15.00 5.03 o 1 18 3 38.52 38.38 2.01 o 3 18 3 64.35 70.84 2.57 o 5 18 3 2.61 1.89 0.71 o 7 18 3 36.49 41.64 2.45 o 1 19 3 23.81 21.41 1.27 o 3 19 3 0.00 1.87 0.56 o 5 19 3 1.37 1.29 0.78 o 7 19 3 0.01 1.76 0.84 o 1 20 3 62.21 60.36 3.02 o 3 20 3 15.86 10.67 1.00 o 5 20 3 2.42 1.77 0.80 o 7 20 3 0.12 2.18 0.88 o 1 21 3 41.74 29.52 1.34 o 3 21 3 1.76 1.09 0.59 o 5 21 3 0.56 1.14 0.76 o 7 21 3 0.38 1.43 0.96 o 1 22 3 6.25 7.94 0.97 o 3 22 3 0.42 1.59 0.68 o 5 22 3 0.18 0.80 0.86 o 7 22 3 0.18 2.89 1.05 o 1 23 3 131.90 146.83 8.13 o 3 23 3 66.60 65.26 3.40 o 5 23 3 12.57 6.16 1.02 o 7 23 3 0.01 0.48 1.04 o 1 24 3 86.69 82.20 4.57 o 3 24 3 78.92 76.93 3.73 o 5 24 3 26.53 17.83 1.67 o 7 24 3 0.38 1.22 1.16 o 1 25 3 21.08 19.54 1.42 o 3 25 3 0.03 2.04 0.76 o 5 25 3 6.46 11.25 1.41 o 1 26 3 6.24 4.29 1.06 o 3 26 3 9.97 8.62 1.13 o 5 26 3 19.01 14.85 1.73 o 1 27 3 0.43 1.35 0.88 o 3 27 3 3.98 2.75 0.91 o 5 27 3 1.03 1.38 0.98 o 1 28 3 1.93 0.94 0.81 o 3 28 3 1.18 1.02 0.87 o 5 28 3 0.22 0.18 1.23 o 1 29 3 0.96 1.27 0.84 o 3 29 3 0.86 0.58 0.86 o 1 30 3 1.00 1.45 0.89 o 3 30 3 0.00 0.00 1.05 o 1 31 3 2.28 0.83 1.13 o 3 31 3 0.03 0.00 1.15 o 1 32 3 0.77 2.21 1.06 o 0 0 4 251.66 258.50 18.21 o 2 0 4 174.43 153.22 6.30 o 4 0 4 37.67 28.94 2.28 o 6 0 4 10.95 13.46 2.15 o 8 0 4 2.93 3.61 1.38 o 0 1 4 17.75 16.70 1.24 o 2 1 4 15.08 13.29 0.86 o 4 1 4 2.55 1.25 0.64 o 6 1 4 30.37 46.47 1.54 o 8 1 4 12.41 12.01 1.35 o 0 2 4 5.22 4.66 0.71 o 2 2 4 1.31 2.55 0.79 o 4 2 4 1.91 2.11 0.66 o 6 2 4 7.95 10.09 0.99 o 8 2 4 1.87 2.87 0.94 o 0 3 4 0.15 0.16 0.48 o 2 3 4 22.53 24.38 1.42 o 4 3 4 140.40 154.82 5.36 o 6 3 4 59.21 52.48 2.50 o 8 3 4 8.32 5.62 1.09 o 0 4 4 95.51 97.33 3.51 o 2 4 4 14.33 14.72 0.89 o 4 4 4 47.39 41.80 1.29 o 6 4 4 22.03 14.97 1.23 o 8 4 4 2.29 0.95 0.69 o 0 5 4 20.62 33.68 1.25 o 2 5 4 1.45 1.51 0.43 o 4 5 4 34.88 25.93 1.12 o 6 5 4 11.53 7.38 1.06 o 8 5 4 0.00 1.42 0.86 o 0 6 4 82.52 75.25 3.02 o 2 6 4 4.89 4.49 0.52 o 4 6 4 88.09 92.26 2.98 o 6 6 4 2.76 4.30 0.88 o 8 6 4 0.95 1.44 0.76 o 0 7 4 11.63 14.80 1.80 o 2 7 4 169.85 179.10 5.30 o 4 7 4 631.36 642.12 24.67 o 6 7 4 133.87 149.53 6.22 o 8 7 4 1.15 1.88 0.82 o 0 8 4 13.63 11.39 0.94 o 2 8 4 50.42 58.98 1.79 o 4 8 4 70.61 117.47 4.73 o 6 8 4 7.40 12.43 1.30 o 8 8 4 15.95 13.72 1.39 o 0 9 4 1.41 2.16 0.66 o 2 9 4 323.64 328.15 10.80 o 4 9 4 755.57 827.96 37.23 o 6 9 4 67.00 82.71 3.03 o 8 9 4 1.15 2.13 0.89 o 0 10 4 5.72 4.97 0.96 o 2 10 4 82.54 80.82 2.46 o 4 10 4 134.75 177.95 6.42 o 6 10 4 0.41 2.06 0.88 o 8 10 4 5.71 3.32 1.06 o 0 11 4 0.80 1.34 0.67 o 2 11 4 290.96 310.85 10.35 o 4 11 4 650.15 741.89 35.31 o 6 11 4 27.04 32.03 1.65 o 8 11 4 5.54 3.79 1.06 o 0 12 4 5.14 5.32 0.88 o 2 12 4 104.89 88.11 3.77 o 4 12 4 173.88 228.97 9.41 o 6 12 4 4.43 3.67 0.86 o 8 12 4 1.35 2.13 0.87 o 0 13 4 22.33 27.07 1.61 o 2 13 4 135.53 151.19 7.09 o 4 13 4 470.22 562.60 21.97 o 6 13 4 15.02 13.48 1.38 o 8 13 4 8.98 4.35 1.26 o 0 14 4 4.87 5.52 1.12 o 2 14 4 94.16 88.20 4.41 o 4 14 4 142.49 180.73 7.68 o 6 14 4 0.88 1.40 0.84 o 8 14 4 2.28 2.47 1.02 o 0 15 4 87.99 110.58 6.42 o 2 15 4 21.75 23.34 1.22 o 4 15 4 232.19 276.80 16.24 o 6 15 4 14.95 10.11 1.19 o 8 15 4 0.56 0.57 1.05 o 0 16 4 220.26 232.30 13.10 o 2 16 4 17.84 16.12 1.22 o 4 16 4 9.32 20.41 2.43 o 6 16 4 0.10 2.31 0.91 o 8 16 4 0.05 0.68 1.16 o 0 17 4 172.54 241.20 10.02 o 2 17 4 301.41 370.00 13.34 o 4 17 4 225.73 272.38 15.73 o 6 17 4 8.70 5.17 1.09 o 8 17 4 0.09 0.87 1.13 o 0 18 4 142.50 179.81 6.58 o 2 18 4 104.18 122.80 4.06 o 4 18 4 17.21 10.01 1.26 o 6 18 4 1.12 2.66 0.99 o 8 18 4 0.73 1.10 1.17 o 0 19 4 175.60 174.16 8.99 o 2 19 4 22.01 16.02 1.23 o 4 19 4 6.85 11.67 1.43 o 6 19 4 0.14 2.05 0.89 o 0 20 4 35.67 49.56 2.65 o 2 20 4 19.53 23.58 1.68 o 4 20 4 3.95 4.51 1.01 o 6 20 4 0.09 1.73 0.96 o 0 21 4 10.32 8.33 1.81 o 2 21 4 3.86 2.80 0.76 o 4 21 4 7.56 5.04 1.10 o 6 21 4 13.47 10.80 1.59 o 0 22 4 17.03 10.68 1.89 o 2 22 4 8.72 6.05 0.92 o 4 22 4 0.81 2.02 0.89 o 6 22 4 0.14 1.02 1.08 o 0 23 4 40.03 48.50 4.33 o 2 23 4 11.40 10.07 1.14 o 4 23 4 2.12 3.11 0.98 o 6 23 4 3.02 3.17 1.14 o 0 24 4 0.00 2.00 1.06 o 2 24 4 0.54 1.40 0.75 o 4 24 4 0.71 2.24 0.90 o 6 24 4 0.15 1.74 1.48 o 0 25 4 3.42 2.01 1.17 o 2 25 4 4.33 2.39 0.84 o 4 25 4 1.66 1.91 1.01 o 0 26 4 0.66 1.30 1.07 o 2 26 4 0.00 2.34 0.97 o 4 26 4 0.04 1.02 1.15 o 0 27 4 2.62 1.70 1.13 o 2 27 4 2.72 2.37 0.97 o 4 27 4 0.99 1.71 1.16 o 0 28 4 0.65 1.44 1.25 o 2 28 4 0.35 1.01 1.07 o 4 28 4 0.04 1.01 1.27 o 0 29 4 0.74 0.94 1.64 o 2 29 4 0.00 1.68 1.01 o 0 30 4 1.30 2.05 1.57 o 2 30 4 0.34 0.00 1.27 o 1 0 5 5.72 4.30 0.78 o 3 0 5 0.89 1.83 1.38 o 5 0 5 0.71 1.31 0.94 o 7 0 5 1.75 1.79 1.44 o 9 0 5 0.41 1.56 1.44 o 1 1 5 101.70 101.80 3.08 o 3 1 5 96.47 95.16 4.20 o 5 1 5 21.31 20.09 1.35 o 7 1 5 0.65 0.89 0.94 o 9 1 5 0.56 0.00 1.42 o 1 2 5 0.27 0.81 0.40 o 3 2 5 11.63 9.06 1.08 o 5 2 5 2.04 1.98 0.76 o 7 2 5 0.32 0.55 0.84 o 9 2 5 0.21 1.84 1.20 o 1 3 5 2.61 2.02 0.44 o 3 3 5 4.23 1.68 0.73 o 5 3 5 3.77 2.33 0.86 o 7 3 5 0.50 0.99 0.81 o 9 3 5 0.59 1.20 1.30 o 1 4 5 1.23 0.71 0.42 o 3 4 5 65.61 72.52 3.25 o 5 4 5 39.83 53.93 1.74 o 7 4 5 1.68 3.28 0.98 o 9 4 5 0.09 1.31 1.13 o 1 5 5 64.15 66.13 1.66 o 3 5 5 13.92 8.45 1.31 o 5 5 5 0.22 1.75 0.79 o 7 5 5 0.90 0.99 0.83 o 1 6 5 0.01 0.23 0.46 o 3 6 5 96.98 88.78 4.00 o 5 6 5 36.13 41.07 2.31 o 7 6 5 1.49 1.46 0.98 o 1 7 5 10.10 6.83 0.71 o 3 7 5 49.88 47.40 2.27 o 5 7 5 16.80 11.29 1.26 o 7 7 5 0.05 2.26 0.92 o 1 8 5 83.61 96.85 3.01 o 3 8 5 15.64 19.43 2.71 o 5 8 5 3.69 6.14 1.15 o 7 8 5 25.44 27.59 1.90 o 1 9 5 10.89 12.37 0.91 o 3 9 5 327.00 396.25 20.02 o 5 9 5 210.27 269.71 10.47 o 7 9 5 6.93 6.82 1.23 o 1 10 5 250.82 294.28 11.02 o 3 10 5 13.79 24.90 1.63 o 5 10 5 47.45 75.74 7.28 o 7 10 5 2.24 3.01 1.00 o 1 11 5 111.29 100.38 3.09 o 3 11 5 122.24 156.03 4.39 o 5 11 5 110.79 141.41 6.55 o 7 11 5 0.71 1.78 0.94 o 1 12 5 129.78 193.12 8.16 o 3 12 5 309.34 397.37 18.12 o 5 12 5 86.94 100.49 5.31 o 7 12 5 6.02 5.49 1.25 o 1 13 5 254.69 325.56 11.78 o 3 13 5 309.99 373.75 17.04 o 5 13 5 43.53 34.73 2.01 o 7 13 5 3.64 4.54 1.08 o 1 14 5 103.86 106.51 2.84 o 3 14 5 26.02 38.52 5.92 o 5 14 5 20.22 28.54 4.69 o 7 14 5 6.65 3.87 1.11 o 1 15 5 1.63 1.44 0.61 o 3 15 5 80.07 77.19 5.19 o 5 15 5 31.29 24.57 1.76 o 7 15 5 0.51 1.93 1.25 o 1 16 5 58.60 61.76 2.47 o 3 16 5 13.55 16.04 1.75 o 5 16 5 5.85 4.92 1.07 o 7 16 5 10.17 10.15 1.72 o 1 17 5 0.95 1.90 0.57 o 3 17 5 32.90 30.67 1.95 o 5 17 5 11.94 7.53 1.18 o 7 17 5 0.00 2.13 1.56 o 1 18 5 5.99 6.76 0.85 o 3 18 5 8.04 6.01 1.17 o 5 18 5 0.75 2.19 1.03 o 7 18 5 6.14 5.89 1.68 o 1 19 5 2.18 2.45 0.77 o 3 19 5 6.43 7.52 1.37 o 5 19 5 0.03 1.03 1.01 o 1 20 5 0.22 1.24 0.69 o 3 20 5 6.45 3.64 0.85 o 5 20 5 0.52 1.32 0.93 o 1 21 5 1.25 2.81 0.91 o 3 21 5 0.64 0.72 0.76 o 5 21 5 2.02 2.08 1.04 o 1 22 5 0.07 1.16 0.71 o 3 22 5 1.86 1.95 1.02 o 5 22 5 0.18 1.34 1.09 o 1 23 5 1.40 1.25 0.78 o 3 23 5 8.11 8.77 1.33 o 5 23 5 3.36 3.46 1.31 o 1 24 5 0.43 1.93 0.92 o 3 24 5 0.00 1.75 0.98 o 1 25 5 1.17 0.35 0.97 o 3 25 5 5.55 6.43 1.27 o 1 26 5 0.41 1.42 0.96 o 3 26 5 1.05 2.53 1.05 o 1 27 5 0.65 1.60 1.11 o 1 28 5 1.47 0.69 1.54 o 0 0 6 2.84 1.85 1.24 o 2 0 6 39.45 39.40 3.02 o 4 0 6 172.31 195.25 16.33 o 6 0 6 24.45 32.89 3.37 o 8 0 6 0.14 1.45 1.83 o 0 1 6 4.57 1.86 1.03 o 2 1 6 57.50 54.32 1.67 o 4 1 6 75.02 85.44 3.49 o 6 1 6 3.09 4.22 1.13 o 8 1 6 0.20 0.94 1.45 o 0 2 6 0.00 1.39 0.75 o 2 2 6 31.87 27.91 1.46 o 4 2 6 113.71 138.42 7.30 o 6 2 6 17.87 17.88 1.89 o 8 2 6 0.00 0.00 1.27 o 0 3 6 9.54 10.31 1.48 o 2 3 6 17.55 9.54 1.24 o 4 3 6 58.89 57.19 2.16 o 6 3 6 0.66 0.30 1.04 o 0 4 6 6.66 6.98 2.01 o 2 4 6 14.48 11.36 1.10 o 4 4 6 26.93 28.33 2.79 o 6 4 6 8.44 5.66 1.24 o 0 5 6 189.26 213.79 14.84 o 2 5 6 27.49 25.85 1.51 o 4 5 6 6.20 2.53 0.93 o 6 5 6 0.28 1.66 0.92 o 0 6 6 281.73 308.71 20.71 o 2 6 6 139.74 138.67 7.76 o 4 6 6 18.26 13.76 1.86 o 6 6 6 2.33 1.41 0.94 o 0 7 6 17.53 25.14 2.93 o 2 7 6 42.31 55.33 2.69 o 4 7 6 26.50 25.65 2.14 o 6 7 6 2.46 2.27 0.89 o 0 8 6 4.43 3.42 0.87 o 2 8 6 10.32 12.01 1.82 o 4 8 6 6.55 4.56 1.06 o 6 8 6 3.25 3.77 0.98 o 0 9 6 91.04 88.06 6.51 o 2 9 6 12.31 7.77 1.12 o 4 9 6 3.48 1.44 0.85 o 6 9 6 1.57 1.05 0.97 o 0 10 6 14.18 22.67 2.08 o 2 10 6 0.00 0.87 0.82 o 4 10 6 4.19 2.13 0.93 o 6 10 6 6.63 8.24 1.39 o 0 11 6 185.07 160.30 7.48 o 2 11 6 42.18 50.22 3.89 o 4 11 6 0.05 1.56 0.89 o 6 11 6 7.69 2.83 1.25 o 0 12 6 144.58 166.79 16.81 o 2 12 6 15.93 18.20 1.81 o 4 12 6 8.44 6.80 1.30 o 6 12 6 3.55 2.51 1.12 o 0 13 6 158.08 187.54 17.45 o 2 13 6 51.13 60.68 5.25 o 4 13 6 3.10 2.67 1.01 o 6 13 6 14.44 14.66 1.82 o 0 14 6 82.45 77.65 3.07 o 2 14 6 1.48 1.83 0.92 o 4 14 6 23.61 30.13 2.13 o 6 14 6 0.58 1.47 1.12 o 0 15 6 29.18 28.93 3.31 o 2 15 6 2.24 2.12 0.96 o 4 15 6 3.21 3.12 1.05 o 6 15 6 1.56 1.60 1.25 o 0 16 6 11.61 16.47 4.21 o 2 16 6 0.00 1.68 0.96 o 4 16 6 1.49 2.06 0.96 o 6 16 6 6.41 5.81 1.49 o 0 17 6 5.91 2.78 2.68 o 2 17 6 0.65 1.95 1.02 o 4 17 6 7.48 5.53 1.20 o 0 18 6 4.06 1.27 2.63 o 2 18 6 1.55 0.71 1.07 o 4 18 6 2.96 4.13 1.15 o 0 19 6 7.57 1.44 3.14 o 2 19 6 0.11 1.56 1.03 o 4 19 6 4.30 2.56 1.02 o 0 20 6 2.36 4.84 4.33 o 2 20 6 2.18 2.15 1.25 o 4 20 6 3.69 2.69 1.25 o 0 21 6 6.72 3.74 3.14 o 2 21 6 0.00 3.04 1.28 o 4 21 6 2.74 2.75 1.07 o 0 22 6 0.53 1.10 3.14 o 2 22 6 2.22 2.31 1.38 o 0 23 6 0.33 1.78 2.46 o 2 23 6 0.82 2.06 1.26 o 0 24 6 0.51 0.00 4.67 o 2 24 6 2.66 4.40 1.37 o 0 25 6 3.43 3.06 3.99 o 1 0 7 83.01 74.99 5.35 o 3 0 7 15.82 20.42 2.22 o 5 0 7 26.94 29.27 2.99 o 1 1 7 1.85 3.01 1.13 o 3 1 7 12.45 16.82 1.91 o 5 1 7 7.59 7.15 1.37 o 1 2 7 19.92 22.28 2.24 o 3 2 7 121.66 157.30 7.44 o 5 2 7 36.49 36.69 2.24 o 1 3 7 15.39 9.11 1.96 o 3 3 7 5.78 5.17 1.03 o 5 3 7 7.04 5.32 1.25 o 1 4 7 2.16 1.52 1.29 o 3 4 7 46.80 47.24 2.05 o 5 4 7 14.27 15.77 1.61 o 1 5 7 0.25 2.16 1.19 o 3 5 7 11.49 9.99 1.52 o 5 5 7 8.94 7.16 1.25 o 1 6 7 9.49 5.85 1.67 o 3 6 7 11.26 7.52 1.46 o 5 6 7 6.72 5.30 1.28 o 1 7 7 21.39 20.93 2.25 o 3 7 7 11.77 14.74 2.46 o 5 7 7 6.02 5.41 1.41 o 1 8 7 14.41 9.46 1.87 o 3 8 7 2.78 3.34 1.02 o 5 8 7 2.13 1.69 1.11 o 1 9 7 61.69 57.64 3.95 o 3 9 7 8.20 7.66 1.62 o 5 9 7 3.21 2.49 1.35 o 1 10 7 1.97 2.07 1.33 o 3 10 7 1.06 1.45 0.96 o 5 10 7 0.13 0.55 1.10 o 1 11 7 41.30 34.65 3.83 o 3 11 7 1.57 1.96 1.19 o 5 11 7 1.39 1.63 1.02 o 1 12 7 0.15 1.40 1.39 o 3 12 7 1.14 1.82 1.15 o 5 12 7 0.28 1.61 1.07 o 1 13 7 23.01 16.83 4.40 o 3 13 7 0.68 0.28 1.16 o 5 13 7 1.57 2.05 1.33 o 1 14 7 1.16 1.96 1.72 o 3 14 7 1.95 1.29 1.13 o 1 15 7 16.47 15.24 3.17 o 3 15 7 0.90 0.11 1.26 o 1 16 7 4.22 4.26 2.27 o 3 16 7 0.73 0.98 1.02 o 1 17 7 14.63 9.59 3.16 o 3 17 7 1.67 2.19 1.21 o 1 18 7 5.18 1.22 1.98 o 3 18 7 1.28 0.13 1.48 o 1 19 7 1.47 4.82 2.41 o 1 20 7 0.77 3.47 3.54 o 0 0 8 61.56 52.93 6.97 o 2 0 8 17.40 11.51 3.16 o 4 0 8 0.13 0.00 1.93 o 0 1 8 56.87 60.92 5.72 o 2 1 8 3.98 2.11 1.87 o 4 1 8 3.83 1.90 1.43 o 0 2 8 35.19 37.97 8.96 o 2 2 8 9.39 6.15 1.91 o 4 2 8 0.05 0.57 1.50 o 0 3 8 52.10 52.82 5.84 o 2 3 8 3.22 3.87 1.55 o 4 3 8 5.00 2.82 1.49 o 0 4 8 4.42 5.49 2.49 o 2 4 8 0.38 0.97 1.48 o 4 4 8 0.24 0.00 1.72 o 0 5 8 53.66 61.57 5.38 o 2 5 8 7.93 5.37 1.60 o 4 5 8 0.90 0.00 1.59 o 0 6 8 15.23 10.84 2.47 o 2 6 8 6.04 4.13 1.80 o 0 7 8 2.41 1.51 3.47 o 2 7 8 0.12 1.45 1.95 o 0 8 8 0.23 2.00 2.20 o 2 8 8 0.01 1.88 1.89 o 0 9 8 0.34 0.00 3.18 o 2 9 8 0.05 1.56 1.73 o 0 10 8 1.81 0.74 2.91 o 2 10 8 0.59 0.00 2.17 o 0 11 8 1.01 3.99 6.46 o 2 11 8 0.15 2.22 1.82 o 0 12 8 4.05 1.02 2.80 o 0 13 8 0.68 1.10 2.97 o