#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:01:02 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180900 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/40/2104033.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104033_Fobs loop_ _publ_author_name 'Redhammer, G\"unther J.' 'Ohashi, Haruo' 'Roth, Georg' _publ_section_title ; Single-crystal structure refinement of NaTiSi~2~O~6~ clinopyroxene at low temperatures (298<T<100K) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 730 _journal_page_last 746 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.835 _cell_angle_gamma 90.000 _cell_length_a 9.7052 _cell_length_b 8.8747 _cell_length_c 5.3029 _exptl_crystal_F_000 436.00 _reflns_d_resolution_high 0.6714 _cod_data_source_file ws5001220sup5.hkl _cod_data_source_block 220 #BEGIN Tags that were not found in dictionaries: _shelx_title ' NaTiSi2O6 Haruo OHASI 220 K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 134.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 155.87 131.91 17.46 o 8 0 0 5126.66 4976.00 28.80 o 10 0 0 4132.42 4398.54 31.45 o 1 1 0 1254.64 1235.91 35.74 o 5 1 0 1829.10 1906.92 21.93 o 7 1 0 3968.87 3818.71 15.32 o 9 1 0 398.08 419.51 11.67 o 11 1 0 1288.85 1308.77 15.12 o 0 2 0 4425.38 4269.13 31.31 o 2 2 0 1510.89 1470.91 36.78 o 4 2 0 24.21 32.45 7.72 o 6 2 0 2.42 13.52 7.35 o 8 2 0 61.56 65.51 8.13 o 10 2 0 364.18 380.70 13.13 o 12 2 0 101.96 100.51 13.04 o 1 3 0 218.33 257.84 9.15 o 3 3 0 1600.92 1682.39 34.78 o 5 3 0 170.54 142.78 7.43 o 7 3 0 552.86 546.57 9.97 o 9 3 0 201.07 195.82 9.11 o 11 3 0 53.62 55.42 10.91 o 13 3 0 179.16 172.28 15.63 o 2 4 0 326.48 375.59 7.51 o 4 4 0 8597.14 8760.15 34.90 o 6 4 0 8.28 10.51 6.87 o 8 4 0 17.24 17.14 7.42 o 10 4 0 4760.11 4773.45 157.79 o 12 4 0 5.61 2.70 10.93 o 1 5 0 10078.45 9830.17 152.03 o 3 5 0 6147.25 5915.06 121.19 o 5 5 0 33.50 19.77 6.49 o 7 5 0 13819.92 14006.95 452.15 o 9 5 0 399.43 397.84 8.10 o 11 5 0 1153.81 1154.80 52.44 o 0 6 0 14471.34 14477.87 30.85 o 2 6 0 172.45 175.71 10.32 o 4 6 0 954.02 1017.48 8.91 o 6 6 0 307.10 295.42 17.86 o 8 6 0 434.95 432.32 16.17 o 10 6 0 3661.82 3628.55 126.66 o 12 6 0 611.81 602.36 19.29 o 1 7 0 452.18 469.06 8.60 o 3 7 0 6.62 20.55 7.83 o 5 7 0 2097.36 2114.19 13.79 o 7 7 0 2942.05 2820.16 59.56 o 9 7 0 64.89 65.46 7.57 o 11 7 0 0.42 16.96 9.35 o 0 8 0 26.12 24.87 10.88 o 2 8 0 32.04 36.35 11.67 o 4 8 0 736.13 740.83 18.82 o 6 8 0 246.76 237.64 6.52 o 8 8 0 74.60 89.76 9.65 o 10 8 0 789.13 809.95 22.98 o 1 9 0 78.33 77.85 8.34 o 3 9 0 1810.52 1816.90 21.16 o 5 9 0 110.38 127.03 8.90 o 7 9 0 427.15 427.28 7.57 o 9 9 0 131.41 133.67 10.91 o 0 10 0 5716.83 5867.95 20.03 o 2 10 0 207.18 232.85 7.65 o 4 10 0 2833.68 2917.65 56.25 o 6 10 0 1351.42 1305.69 87.06 o 8 10 0 355.16 370.53 17.83 o 1 11 0 116.72 105.77 7.82 o 3 11 0 2681.34 2683.78 49.76 o 5 11 0 272.68 286.07 11.09 o 7 11 0 1584.82 1573.14 38.44 o 0 12 0 4202.34 4174.92 17.51 o 2 12 0 458.56 457.27 9.06 o 4 12 0 45.31 48.01 16.21 o 1 13 0 11.48 14.85 10.49 o -9 1 1 230.57 226.01 13.79 o -7 1 1 70.13 65.54 11.06 o -5 1 1 2235.31 2190.48 24.87 o -3 1 1 2458.59 2442.78 57.10 o -1 1 1 1704.33 1695.18 25.50 o 1 1 1 1240.60 1290.69 23.32 o 3 1 1 2347.62 2369.31 25.25 o 5 1 1 1263.87 1264.11 16.93 o 7 1 1 2.06 2.89 6.60 o 9 1 1 486.80 491.23 8.15 o 11 1 1 121.82 123.10 10.90 o 13 1 1 110.39 115.70 21.93 o -10 2 1 11.37 9.57 11.33 o -8 2 1 3111.05 3082.55 61.71 o -6 2 1 2566.57 2322.32 21.00 o -4 2 1 5834.33 5792.03 29.03 o 0 2 1 467.54 522.65 9.83 o 2 2 1 14690.86 13257.92 257.54 o 4 2 1 2520.66 2480.14 43.53 o 6 2 1 5144.50 5006.71 91.11 o 8 2 1 3364.60 3474.97 49.34 o 10 2 1 51.32 64.02 9.15 o 12 2 1 3638.49 3712.52 94.60 o -11 3 1 2215.42 2142.72 22.71 o -9 3 1 4931.50 4732.09 139.32 o -7 3 1 1753.72 1649.12 66.86 o -3 3 1 9767.80 10062.47 55.14 o -1 3 1 7664.49 6917.12 273.82 o 3 3 1 1931.95 1881.36 60.58 o 7 3 1 263.13 254.55 7.42 o 9 3 1 2310.93 2337.12 24.26 o 11 3 1 815.07 811.45 10.83 o -12 4 1 2536.42 2497.59 85.01 o -10 4 1 266.67 274.03 11.03 o -8 4 1 136.03 149.28 14.52 o -6 4 1 1.20 16.20 8.88 o -4 4 1 300.53 313.17 9.24 o -2 4 1 4369.40 4612.10 76.35 o 0 4 1 5931.58 5996.52 86.72 o 2 4 1 1621.46 1584.77 73.42 o 4 4 1 4.30 3.35 6.94 o 6 4 1 493.33 480.80 18.29 o 8 4 1 420.88 450.24 8.18 o 10 4 1 637.13 622.36 8.90 o 12 4 1 1245.09 1295.56 56.40 o -13 5 1 70.49 70.10 13.89 o -11 5 1 36.28 37.07 10.10 o -9 5 1 25.85 26.15 9.14 o -7 5 1 9.03 12.29 8.55 o -5 5 1 484.39 487.58 22.99 o -3 5 1 412.78 407.36 8.76 o -1 5 1 681.22 696.30 24.22 o 1 5 1 126.00 119.37 8.08 o 3 5 1 827.23 775.12 30.24 o 5 5 1 663.22 673.11 30.36 o 7 5 1 12.62 13.59 6.86 o 9 5 1 28.62 29.10 7.16 o 11 5 1 143.17 154.63 8.08 o -12 6 1 84.33 83.69 11.80 o -10 6 1 1.88 12.14 8.54 o -8 6 1 305.52 281.99 12.60 o -6 6 1 0.66 9.79 8.23 o -4 6 1 44.33 46.83 7.34 o -2 6 1 443.48 419.42 23.86 o 0 6 1 85.64 79.56 6.04 o 2 6 1 99.37 81.18 5.65 o 4 6 1 2.01 9.12 7.51 o 6 6 1 37.23 38.32 6.53 o 8 6 1 34.12 37.03 7.24 o 10 6 1 9.76 22.74 7.10 o -11 7 1 439.20 401.39 20.58 o -9 7 1 1578.78 1498.86 42.33 o -7 7 1 289.99 295.98 15.90 o -5 7 1 7279.17 7330.58 147.61 o -3 7 1 27.42 48.36 8.47 o -1 7 1 3895.04 3878.65 70.55 o 1 7 1 5464.74 5451.71 168.85 o 3 7 1 151.63 180.61 5.92 o 5 7 1 3784.44 3783.72 161.11 o 7 7 1 449.87 440.48 16.76 o 9 7 1 2700.39 2782.25 54.57 o 11 7 1 52.47 38.14 19.90 o -10 8 1 1.95 7.81 7.97 o -8 8 1 2446.30 2364.17 79.05 o -6 8 1 884.99 886.41 35.73 o -4 8 1 734.99 708.84 10.14 o -2 8 1 9234.81 9053.39 184.54 o 0 8 1 116.91 128.54 7.79 o 2 8 1 4825.47 4976.21 135.50 o 4 8 1 609.61 592.21 16.61 o 6 8 1 2554.12 2590.38 70.98 o 8 8 1 1597.77 1565.32 31.16 o 10 8 1 32.71 17.00 9.19 o -9 9 1 580.64 583.29 17.05 o -7 9 1 2131.40 2122.59 37.09 o -5 9 1 3490.28 3529.13 59.65 o -3 9 1 39.09 49.18 9.33 o -1 9 1 85.83 103.88 7.87 o 1 9 1 24.17 36.94 7.12 o 3 9 1 28.73 29.07 6.07 o 5 9 1 3607.49 3595.36 140.90 o 7 9 1 742.47 753.23 19.66 o 9 9 1 473.33 488.50 17.06 o -8 10 1 95.99 96.92 8.70 o -6 10 1 41.14 45.06 9.60 o -4 10 1 15.50 18.33 6.80 o -2 10 1 1634.20 1596.99 73.47 o 0 10 1 1034.16 1051.00 35.97 o 2 10 1 145.12 152.46 15.27 o 4 10 1 36.12 34.30 6.37 o 6 10 1 281.37 283.54 6.84 o 8 10 1 4.34 5.48 7.37 o -7 11 1 43.71 34.54 11.50 o -5 11 1 59.25 62.59 8.40 o -3 11 1 160.41 162.01 8.99 o -1 11 1 26.46 23.58 7.77 o 1 11 1 12.29 11.41 7.75 o 3 11 1 153.64 150.33 12.87 o 5 11 1 32.41 19.34 7.88 o -6 12 1 743.10 723.33 10.56 o -4 12 1 579.09 581.14 22.74 o -2 12 1 1144.13 1141.07 29.68 o 0 12 1 222.76 197.24 13.35 o 2 12 1 2254.40 2276.33 9.77 o 4 12 1 315.92 307.32 7.93 o -1 13 1 1813.10 1827.22 15.45 o 1 13 1 1160.67 1146.64 11.22 o 2 0 2 6680.19 6884.21 100.61 o 4 0 2 11628.61 11893.63 244.59 o 6 0 2 253.69 275.29 8.37 o 8 0 2 1004.59 1007.02 12.19 o 10 0 2 8302.82 8660.85 29.18 o 12 0 2 9.71 24.23 17.21 o -5 1 2 54.60 55.03 8.87 o -1 1 2 383.02 373.73 7.04 o 1 1 2 8437.04 9135.88 149.74 o 3 1 2 3577.50 3443.14 28.29 o 5 1 2 1409.94 1397.16 18.64 o 7 1 2 5198.24 5290.12 33.44 o 9 1 2 5.55 9.04 6.85 o 11 1 2 853.01 891.46 12.55 o -10 2 2 1986.42 2000.49 22.41 o -8 2 2 206.90 208.56 15.80 o -6 2 2 1100.60 1132.01 17.23 o -4 2 2 1838.10 1950.31 56.03 o -2 2 2 0.47 7.01 6.01 o 0 2 2 1419.03 1616.85 22.57 o 2 2 2 630.08 581.05 13.25 o 4 2 2 3768.98 3817.75 44.13 o 6 2 2 542.85 520.03 8.08 o 8 2 2 999.32 983.51 19.76 o 10 2 2 1333.33 1319.56 9.99 o 12 2 2 3.43 7.36 12.25 o -11 3 2 91.52 80.79 13.58 o -9 3 2 33.48 35.73 9.32 o -7 3 2 315.47 301.18 13.98 o -5 3 2 244.08 263.23 16.90 o -3 3 2 1041.57 1204.25 31.62 o -1 3 2 653.64 651.91 18.23 o 1 3 2 1172.83 1223.20 26.95 o 3 3 2 354.95 387.17 5.36 o 5 3 2 18.93 14.20 6.43 o 7 3 2 134.57 134.86 6.94 o 9 3 2 0.11 -3.31 7.02 o 11 3 2 99.53 114.41 9.66 o -12 4 2 14.61 19.65 13.80 o -10 4 2 1694.63 1615.23 83.20 o -8 4 2 128.36 108.87 12.80 o -6 4 2 1495.71 1499.01 20.35 o -4 4 2 1297.73 1277.48 26.90 o -2 4 2 3.11 3.48 5.71 o 0 4 2 6817.06 6692.32 355.70 o 2 4 2 66.57 84.98 5.60 o 4 4 2 2291.41 2258.93 66.61 o 6 4 2 702.86 729.81 9.74 o 8 4 2 19.54 19.14 6.78 o 10 4 2 1067.72 1084.42 14.18 o -13 5 2 883.06 812.76 58.72 o -11 5 2 1352.91 1289.27 51.98 o -9 5 2 785.15 770.75 14.69 o -7 5 2 8498.89 8450.89 173.98 o -5 5 2 93.54 117.94 6.61 o -3 5 2 14339.02 13803.41 388.48 o -1 5 2 827.77 733.68 25.55 o 1 5 2 3212.97 3135.90 90.35 o 3 5 2 15414.01 15336.65 496.12 o 5 5 2 20.44 30.62 6.16 o 7 5 2 3507.64 3601.61 100.13 o 9 5 2 398.73 400.05 8.05 o 11 5 2 3411.12 3410.70 26.24 o -12 6 2 184.13 189.61 14.05 o -10 6 2 494.06 470.46 22.81 o -8 6 2 167.13 171.93 8.28 o -6 6 2 6217.26 5996.71 166.58 o -4 6 2 215.23 246.47 9.31 o -2 6 2 3928.02 3925.76 149.10 o 0 6 2 16436.63 16068.86 398.98 o 2 6 2 78.27 82.75 5.93 o 4 6 2 419.49 443.77 21.13 o 6 6 2 110.02 116.77 11.44 o 8 6 2 541.75 556.96 9.47 o 10 6 2 1878.53 1948.56 41.26 o -11 7 2 6.00 3.94 11.12 o -9 7 2 34.16 30.16 9.01 o -7 7 2 1253.70 1247.38 36.24 o -5 7 2 716.78 700.49 19.79 o -3 7 2 859.13 845.11 16.04 o -1 7 2 749.58 722.99 38.40 o 1 7 2 2.18 12.59 5.72 o 3 7 2 2124.88 2083.88 79.55 o 5 7 2 1080.97 1067.25 69.85 o 7 7 2 116.14 127.69 7.05 o 9 7 2 9.91 20.34 7.97 o -10 8 2 8.10 5.87 9.55 o -8 8 2 2.78 14.33 7.92 o -6 8 2 118.37 115.05 6.62 o -4 8 2 3.23 6.82 6.32 o -2 8 2 64.45 61.67 5.46 o 0 8 2 429.45 419.47 23.44 o 2 8 2 6.99 5.51 5.88 o 4 8 2 104.21 103.66 6.18 o 6 8 2 5.78 9.19 6.36 o 8 8 2 60.59 60.41 12.99 o -9 9 2 10.41 18.51 9.20 o -7 9 2 1450.32 1405.31 24.80 o -5 9 2 82.48 89.62 6.66 o -3 9 2 363.64 367.35 11.54 o -1 9 2 504.83 508.10 28.83 o 1 9 2 765.61 794.85 22.66 o 3 9 2 206.00 217.44 6.49 o 5 9 2 26.53 33.86 5.72 o 7 9 2 1646.28 1684.50 41.47 o -8 10 2 251.04 262.48 10.23 o -6 10 2 482.25 464.60 17.90 o -4 10 2 3777.57 3644.74 140.90 o -2 10 2 761.21 738.12 14.29 o 0 10 2 2455.43 2376.66 80.98 o 2 10 2 109.67 111.41 12.10 o 4 10 2 5085.10 5050.48 154.37 o 6 10 2 559.16 595.17 19.33 o -7 11 2 3507.72 3580.68 101.95 o -5 11 2 82.69 86.02 7.20 o -3 11 2 1059.49 1023.92 32.71 o -1 11 2 69.35 86.25 12.38 o 1 11 2 722.81 691.81 7.93 o 3 11 2 1461.54 1442.65 36.86 o 5 11 2 189.29 206.00 8.59 o -4 12 2 155.06 155.07 7.84 o -2 12 2 824.91 828.76 10.87 o 0 12 2 1295.57 1309.01 34.92 o 2 12 2 8.50 3.43 7.05 o -7 1 3 150.23 154.13 9.42 o -5 1 3 2221.64 2228.31 18.53 o -3 1 3 1768.37 1808.08 21.48 o -1 1 3 533.49 541.37 9.83 o 1 1 3 1112.60 1121.66 10.71 o 3 1 3 570.17 571.05 9.57 o 5 1 3 175.30 177.12 5.32 o 7 1 3 11.48 14.91 5.18 o 9 1 3 1152.92 1131.97 7.42 o 11 1 3 105.21 91.82 15.16 o -10 2 3 136.88 123.34 16.47 o -8 2 3 5624.19 5763.22 29.44 o -6 2 3 508.78 517.99 8.55 o -4 2 3 1171.55 1074.28 20.64 o -2 2 3 18175.00 18422.97 37.75 o 0 2 3 291.19 254.31 5.47 o 2 2 3 7345.05 7328.18 115.68 o 4 2 3 71.93 83.21 6.63 o 6 2 3 3559.54 3543.71 60.96 o 8 2 3 3015.23 2974.02 56.84 o 10 2 3 1.29 3.86 7.90 o -11 3 3 2272.63 2124.47 107.06 o -9 3 3 7499.03 7698.97 32.00 o -7 3 3 801.78 798.72 14.79 o -5 3 3 6444.82 6532.92 55.22 o -3 3 3 2150.75 2139.42 40.42 o -1 3 3 13647.81 13998.02 314.94 o 3 3 3 1.76 72.89 34.57 o 5 3 3 10741.79 10977.58 180.29 o 7 3 3 28.19 35.50 6.05 o 9 3 3 2754.48 2797.63 57.10 o -12 4 3 1318.29 1250.47 28.04 o -10 4 3 39.12 50.72 13.19 o -8 4 3 1450.70 1374.66 16.41 o -6 4 3 419.66 389.77 23.94 o -4 4 3 182.62 180.43 6.42 o -2 4 3 5214.81 5131.35 59.71 o 0 4 3 820.84 752.67 26.92 o 2 4 3 618.53 607.52 14.24 o 4 4 3 548.19 549.67 16.08 o 6 4 3 719.45 724.47 22.06 o 8 4 3 610.91 627.62 16.50 o 10 4 3 256.98 267.98 9.10 o -13 5 3 18.11 23.44 17.20 o -11 5 3 40.97 39.33 10.80 o -9 5 3 2.65 2.58 13.15 o -7 5 3 78.64 83.13 7.56 o -5 5 3 804.97 766.36 15.27 o -3 5 3 595.59 556.36 18.47 o -1 5 3 143.30 154.46 10.97 o 1 5 3 636.69 602.11 16.84 o 3 5 3 235.84 204.08 8.89 o 5 5 3 0.42 -0.15 6.32 o 7 5 3 8.51 11.82 6.28 o 9 5 3 511.39 517.76 11.79 o -12 6 3 258.59 237.49 16.00 o -10 6 3 0.68 14.88 14.37 o -8 6 3 79.52 87.41 8.17 o -6 6 3 49.19 52.76 8.56 o -4 6 3 32.75 32.78 5.92 o -2 6 3 51.14 69.56 5.77 o 0 6 3 110.80 119.09 5.38 o 2 6 3 412.42 427.59 10.90 o 4 6 3 0.66 12.29 6.31 o 6 6 3 8.27 8.92 6.70 o 8 6 3 77.09 68.33 7.18 o -11 7 3 485.49 470.45 11.39 o -9 7 3 1725.35 1696.29 33.77 o -7 7 3 274.39 254.69 7.53 o -5 7 3 4935.84 5078.39 146.35 o -3 7 3 12.98 21.09 5.45 o -1 7 3 3787.83 3750.15 219.61 o 1 7 3 2864.38 2847.53 101.56 o 3 7 3 149.21 159.90 13.21 o 5 7 3 2639.09 2553.80 86.47 o 7 7 3 211.18 211.99 7.21 o -10 8 3 49.90 54.15 13.94 o -8 8 3 2380.22 2375.02 24.25 o -6 8 3 495.03 504.82 12.28 o -4 8 3 635.50 631.30 16.16 o -2 8 3 5552.30 5561.29 192.68 o 0 8 3 3.36 4.86 6.33 o 2 8 3 5119.27 4990.57 172.97 o 4 8 3 3.09 16.31 10.17 o 6 8 3 1522.68 1530.97 58.88 o 8 8 3 2342.33 2406.55 17.57 o -9 9 3 2181.54 2155.95 34.23 o -7 9 3 1016.52 1002.21 18.58 o -5 9 3 513.10 500.66 16.24 o -3 9 3 1.60 9.12 5.52 o -1 9 3 2218.83 2162.10 97.36 o 1 9 3 62.83 67.78 5.45 o 3 9 3 574.96 582.38 30.15 o 5 9 3 3007.09 3048.33 151.47 o -8 10 3 159.07 180.44 11.91 o -6 10 3 98.71 101.82 7.68 o -4 10 3 0.32 -4.44 7.22 o -2 10 3 913.79 904.31 35.11 o 0 10 3 221.74 228.54 5.27 o 2 10 3 350.80 343.70 12.43 o 4 10 3 191.24 180.10 7.47 o -5 11 3 41.57 45.23 8.08 o -3 11 3 155.70 154.77 7.24 o -1 11 3 35.97 30.30 7.68 o 1 11 3 0.40 -6.47 6.78 o 3 11 3 281.97 285.10 6.60 o -4 12 3 346.46 345.33 7.70 o -2 12 3 1602.02 1587.41 47.08 o 0 12 3 166.28 170.58 13.92 o -8 0 4 17.42 25.29 10.67 o -4 0 4 7263.22 7423.10 284.43 o -2 0 4 966.23 999.97 24.87 o 0 0 4 15313.82 15799.14 132.49 o 2 0 4 1198.32 1176.78 24.77 o 4 0 4 5298.72 5366.13 28.16 o 6 0 4 737.00 694.27 19.80 o 8 0 4 932.74 951.90 30.09 o -9 1 4 5.81 5.50 16.23 o -7 1 4 2462.96 2482.57 61.10 o -5 1 4 36.77 39.52 5.53 o -3 1 4 9333.30 9405.66 209.16 o -1 1 4 429.67 420.94 11.52 o 1 1 4 4.72 24.54 7.47 o 3 1 4 5768.71 5734.43 54.57 o 5 1 4 6.71 28.60 10.52 o 7 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8692.04 244.35 o -5 5 4 428.46 418.53 7.03 o -3 5 4 5808.04 5833.98 123.17 o -1 5 4 424.06 423.61 7.15 o 1 5 4 3119.84 3132.41 99.39 o 3 5 4 4491.19 4401.87 105.34 o 5 5 4 73.84 84.80 9.90 o 7 5 4 4734.33 4764.20 132.36 o -12 6 4 4.71 11.21 12.90 o -10 6 4 1985.60 1947.55 19.22 o -8 6 4 360.72 351.24 8.49 o -6 6 4 1981.31 2008.30 58.47 o -4 6 4 3467.12 3555.68 116.88 o -2 6 4 596.58 591.05 18.27 o 0 6 4 1806.40 1830.50 72.11 o 2 6 4 0.92 14.46 6.98 o 4 6 4 4188.89 4147.26 129.79 o 6 6 4 9.14 9.57 8.91 o -11 7 4 0.30 2.82 14.71 o -9 7 4 794.49 808.83 11.33 o -7 7 4 1550.64 1547.76 15.45 o -5 7 4 32.34 40.53 6.00 o -3 7 4 269.57 278.35 9.19 o -1 7 4 513.43 506.15 19.08 o 1 7 4 125.25 122.41 5.79 o 3 7 4 433.05 430.57 17.74 o 5 7 4 334.21 338.64 7.59 o 7 7 4 733.66 720.72 29.11 o -10 8 4 301.46 308.76 15.43 o -8 8 4 17.46 14.63 8.53 o -6 8 4 147.47 155.34 7.16 o -4 8 4 266.74 268.92 6.19 o -2 8 4 157.37 163.29 9.62 o 0 8 4 87.46 80.46 5.91 o 2 8 4 206.40 226.23 7.12 o 4 8 4 920.94 916.73 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