#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104035.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104035_Fobs loop_ _publ_author_name 'Redhammer, G\"unther J.' 'Ohashi, Haruo' 'Roth, Georg' _publ_section_title ; Single-crystal structure refinement of NaTiSi~2~O~6~ clinopyroxene at low temperatures (298<T<100K) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 730 _journal_page_last 746 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.825 _cell_angle_gamma 90.000 _cell_length_a 9.7069 _cell_length_b 8.8735 _cell_length_c 5.3023 _exptl_crystal_F_000 436.00 _reflns_d_resolution_high 0.6714 _[local]_cod_data_source_file ws5001210sup7.hkl _[local]_cod_data_source_block 210 #BEGIN Tags that were not found in dictionaries: _shelx_title ' NaTiSi2O6 Haruo OHASI' _shelx_refln_list_code 4 _shelx_F_calc_maximum 135.02 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 159.93 138.55 16.99 o 8 0 0 5177.40 4993.00 29.14 o 10 0 0 4170.44 4367.35 31.87 o 1 1 0 1250.71 1250.84 26.71 o 5 1 0 1831.17 1909.67 29.42 o 7 1 0 3954.43 3812.13 24.19 o 9 1 0 398.25 412.12 12.10 o 11 1 0 1296.50 1336.94 16.03 o 0 2 0 4436.81 4383.47 34.27 o 2 2 0 1508.67 1474.11 41.34 o 4 2 0 24.05 39.84 8.10 o 6 2 0 2.89 6.80 7.57 o 8 2 0 64.68 65.04 8.24 o 10 2 0 357.10 370.37 12.49 o 12 2 0 102.79 101.25 13.31 o 1 3 0 216.09 271.22 9.22 o 3 3 0 1616.71 1690.59 48.41 o 5 3 0 180.50 147.90 7.61 o 7 3 0 547.79 539.21 23.12 o 9 3 0 206.43 194.28 9.23 o 11 3 0 58.51 61.23 13.00 o 13 3 0 177.18 179.66 15.82 o 2 4 0 324.95 369.43 12.23 o 4 4 0 8597.57 8846.06 27.91 o 6 4 0 8.38 9.85 7.17 o 8 4 0 19.47 19.31 7.48 o 10 4 0 4804.83 4808.37 112.33 o 12 4 0 5.47 15.09 11.20 o 1 5 0 10100.53 9796.09 159.94 o 3 5 0 6155.61 5830.25 38.03 o 5 5 0 34.11 37.39 6.52 o 7 5 0 13907.84 14063.88 431.79 o 9 5 0 406.49 402.21 18.85 o 11 5 0 1163.32 1195.46 95.39 o 0 6 0 14477.63 14405.20 30.78 o 2 6 0 172.26 191.11 10.62 o 4 6 0 953.02 1019.22 30.76 o 6 6 0 304.27 307.24 11.33 o 8 6 0 430.04 436.84 14.75 o 10 6 0 3706.52 3687.98 127.84 o 12 6 0 623.78 621.52 21.95 o 1 7 0 461.67 488.10 8.79 o 3 7 0 5.64 32.85 9.92 o 5 7 0 2101.06 2141.58 18.30 o 7 7 0 2968.34 2881.28 88.34 o 9 7 0 63.85 56.17 7.99 o 11 7 0 0.53 12.25 10.46 o 0 8 0 22.52 7.10 10.95 o 2 8 0 34.17 24.34 7.69 o 4 8 0 747.60 755.98 15.40 o 6 8 0 235.05 222.77 7.27 o 8 8 0 71.87 73.06 7.17 o 10 8 0 806.25 817.74 17.50 o 1 9 0 78.60 95.15 6.58 o 3 9 0 1817.58 1830.08 10.34 o 5 9 0 106.65 109.88 10.70 o 7 9 0 422.60 439.63 20.34 o 9 9 0 134.13 146.44 8.63 o 0 10 0 5778.90 6024.22 20.33 o 2 10 0 206.35 209.32 9.75 o 4 10 0 2821.18 2902.32 11.23 o 6 10 0 1362.60 1293.52 57.34 o 8 10 0 360.92 373.90 20.07 o 1 11 0 119.08 123.40 7.90 o 3 11 0 2685.02 2686.66 47.47 o 5 11 0 279.90 280.85 14.30 o 7 11 0 1595.14 1614.12 47.89 o 0 12 0 4244.43 4189.84 17.68 o 2 12 0 451.48 471.40 25.22 o 4 12 0 43.13 72.35 8.23 o 1 13 0 13.45 26.34 10.57 o -9 1 1 226.60 223.23 13.90 o -7 1 1 71.97 72.08 11.25 o -5 1 1 2224.58 2198.43 25.08 o -3 1 1 2467.40 2474.95 56.74 o -1 1 1 1695.82 1701.06 28.24 o 1 1 1 1245.19 1301.82 21.74 o 3 1 1 2355.21 2390.88 42.03 o 5 1 1 1247.89 1250.49 13.53 o 7 1 1 2.41 7.65 6.76 o 9 1 1 486.40 480.30 8.31 o 11 1 1 127.73 125.02 11.06 o 13 1 1 103.87 122.14 22.31 o -10 2 1 11.37 8.87 11.13 o -8 2 1 3142.19 3113.23 72.89 o -6 2 1 2577.29 2319.04 21.09 o -4 2 1 5860.16 5844.81 29.22 o 0 2 1 471.09 526.17 13.82 o 2 2 1 14707.01 13437.28 114.84 o 4 2 1 2541.76 2504.33 24.12 o 6 2 1 5148.99 5031.06 70.60 o 8 2 1 3406.46 3533.66 49.65 o 10 2 1 50.37 56.38 8.06 o 12 2 1 3676.28 3814.36 65.36 o -11 3 1 2246.26 2192.18 35.01 o -9 3 1 4950.14 4810.63 166.81 o -7 3 1 1753.61 1639.03 72.69 o -3 3 1 9759.18 10075.03 113.94 o -1 3 1 7664.81 6809.78 365.71 o 3 3 1 1916.27 1867.45 52.00 o 7 3 1 259.76 250.70 7.60 o 9 3 1 2314.01 2353.56 47.24 o 11 3 1 834.51 823.90 13.74 o -12 4 1 2544.21 2492.88 74.99 o -10 4 1 274.65 274.28 18.28 o -8 4 1 136.08 146.71 8.55 o -6 4 1 1.30 -4.75 9.14 o -4 4 1 300.96 310.35 14.82 o -2 4 1 4385.09 4527.32 56.51 o 0 4 1 5932.38 6009.66 46.73 o 2 4 1 1620.15 1581.07 63.71 o 4 4 1 3.85 10.34 5.98 o 6 4 1 487.27 488.86 23.18 o 8 4 1 420.74 443.43 7.75 o 10 4 1 648.03 640.06 19.26 o 12 4 1 1250.49 1301.92 49.88 o -13 5 1 70.08 63.89 14.09 o -11 5 1 35.62 39.10 10.25 o -9 5 1 28.65 25.58 8.53 o -7 5 1 7.93 20.28 10.93 o -5 5 1 491.51 477.22 24.66 o -3 5 1 403.79 395.38 8.92 o -1 5 1 690.85 682.70 8.46 o 1 5 1 134.25 126.17 8.16 o 3 5 1 811.66 777.41 32.46 o 5 5 1 669.31 683.80 30.63 o 7 5 1 13.56 8.41 6.95 o 9 5 1 30.86 33.61 7.58 o 11 5 1 140.13 153.09 8.53 o -12 6 1 82.48 69.81 11.06 o -10 6 1 1.27 6.71 8.73 o -8 6 1 297.50 282.36 8.40 o -6 6 1 0.60 12.81 8.36 o -4 6 1 45.61 47.45 10.22 o -2 6 1 439.95 397.82 25.17 o 0 6 1 87.36 61.33 6.11 o 2 6 1 94.18 85.24 6.41 o 4 6 1 1.45 0.81 5.98 o 6 6 1 38.05 47.99 6.68 o 8 6 1 32.67 28.89 7.39 o 10 6 1 7.39 11.52 7.25 o -11 7 1 445.18 422.81 26.51 o -9 7 1 1588.17 1518.25 32.76 o -7 7 1 289.06 318.20 8.23 o -5 7 1 7318.82 7293.10 42.82 o -3 7 1 30.08 51.47 8.16 o -1 7 1 3896.68 3853.16 94.57 o 1 7 1 5442.46 5486.27 134.30 o 3 7 1 154.20 186.42 6.04 o 5 7 1 3818.08 3837.10 135.15 o 7 7 1 451.98 451.03 8.84 o 9 7 1 2732.89 2799.05 61.27 o -10 8 1 1.85 3.12 8.13 o -8 8 1 2461.51 2414.73 100.21 o -6 8 1 885.27 894.22 36.64 o -4 8 1 742.73 706.33 18.51 o -2 8 1 9253.78 9133.91 134.84 o 0 8 1 121.05 133.41 10.32 o 2 8 1 4830.61 4934.09 131.29 o 4 8 1 610.90 601.79 20.27 o 6 8 1 2563.98 2571.92 71.15 o 8 8 1 1623.31 1575.97 56.49 o 10 8 1 34.20 32.57 9.36 o -9 9 1 576.11 575.22 17.40 o -7 9 1 2140.64 2179.83 12.33 o -5 9 1 3519.49 3566.31 65.14 o -3 9 1 39.35 49.08 8.02 o -1 9 1 88.01 116.68 7.96 o 1 9 1 23.71 23.70 7.25 o 3 9 1 29.80 44.44 6.11 o 5 9 1 3641.69 3620.85 142.70 o 7 9 1 745.11 751.34 25.80 o 9 9 1 472.78 481.82 16.70 o -8 10 1 100.61 97.09 11.35 o -6 10 1 38.43 39.00 9.04 o -4 10 1 17.76 39.94 6.89 o -2 10 1 1662.06 1620.31 36.16 o 0 10 1 1019.58 1034.44 14.84 o 2 10 1 149.83 169.82 8.28 o 4 10 1 39.10 45.39 6.47 o 6 10 1 293.98 294.00 17.65 o 8 10 1 5.43 15.60 7.50 o -7 11 1 43.25 34.68 11.02 o -5 11 1 61.25 66.12 8.55 o -3 11 1 151.77 145.31 9.39 o -1 11 1 25.90 21.73 7.79 o 1 11 1 12.09 14.18 6.12 o 3 11 1 145.73 159.97 6.59 o 5 11 1 29.59 37.28 8.04 o -6 12 1 750.20 728.45 10.70 o -4 12 1 581.90 563.84 9.76 o -2 12 1 1153.68 1142.15 10.04 o 0 12 1 222.30 224.94 10.57 o 2 12 1 2252.73 2280.04 19.18 o 4 12 1 316.49 309.12 8.03 o 1 13 1 1150.91 1097.86 11.34 o 2 0 2 6738.85 6926.91 64.48 o 4 0 2 11663.54 11900.28 142.60 o 6 0 2 258.56 291.29 8.47 o 8 0 2 1013.93 999.72 10.17 o 10 0 2 8438.56 8813.42 29.58 o 12 0 2 9.79 7.58 17.46 o -5 1 2 56.79 58.92 9.00 o -1 1 2 388.90 364.07 7.08 o 1 1 2 8434.35 9189.09 129.48 o 3 1 2 3585.82 3509.64 56.50 o 5 1 2 1421.69 1425.49 14.37 o 7 1 2 5229.14 5349.58 41.23 o 9 1 2 5.56 16.64 7.27 o 11 1 2 841.20 872.40 27.96 o -10 2 2 2007.89 2000.38 41.54 o -8 2 2 215.38 202.84 16.09 o -6 2 2 1108.85 1119.55 18.36 o -4 2 2 1850.41 1984.50 57.31 o -2 2 2 0.37 7.99 6.10 o 0 2 2 1407.89 1578.82 37.85 o 2 2 2 635.55 581.31 10.81 o 4 2 2 3772.22 3842.80 48.93 o 6 2 2 536.68 520.05 6.05 o 8 2 2 1021.09 1003.95 11.06 o 10 2 2 1337.17 1318.41 9.77 o 12 2 2 3.49 5.99 12.60 o -11 3 2 89.86 86.21 13.30 o -9 3 2 31.75 32.16 9.39 o -7 3 2 326.39 321.45 14.42 o -5 3 2 247.53 275.81 8.93 o -3 3 2 1031.31 1195.49 24.70 o -1 3 2 672.82 672.25 27.24 o 1 3 2 1180.99 1226.51 29.35 o 3 3 2 356.76 386.68 5.50 o 5 3 2 20.69 32.02 6.52 o 7 3 2 144.05 136.48 7.07 o 9 3 2 0.14 3.08 7.13 o 11 3 2 100.27 96.09 9.80 o -12 4 2 15.45 23.47 14.07 o -10 4 2 1694.73 1640.82 79.94 o -8 4 2 129.21 117.05 12.95 o -6 4 2 1505.43 1501.51 24.62 o -4 4 2 1286.99 1297.36 31.87 o -2 4 2 3.25 15.88 5.75 o 0 4 2 6846.57 6775.80 317.89 o 2 4 2 67.18 79.19 6.13 o 4 4 2 2291.88 2255.11 62.96 o 6 4 2 713.73 738.28 8.61 o 8 4 2 18.17 21.64 6.55 o 10 4 2 1062.83 1074.81 11.18 o -13 5 2 893.34 847.07 46.65 o -11 5 2 1377.05 1312.30 47.36 o -9 5 2 800.50 792.93 14.94 o -7 5 2 8545.51 8600.31 156.53 o -5 5 2 95.20 113.81 7.45 o -3 5 2 14351.45 13947.17 405.20 o -1 5 2 831.77 736.83 19.11 o 1 5 2 3224.12 3108.95 117.28 o 3 5 2 15484.83 15360.85 566.20 o 5 5 2 21.34 44.68 7.28 o 7 5 2 3533.84 3578.51 99.14 o 9 5 2 405.44 422.70 8.23 o 11 5 2 3458.87 3458.34 61.03 o -12 6 2 189.92 187.29 11.94 o -10 6 2 494.93 484.14 18.22 o -8 6 2 169.22 175.47 8.57 o -6 6 2 6228.34 6016.16 170.97 o -4 6 2 213.12 242.04 12.98 o -2 6 2 3935.50 3930.39 109.91 o 0 6 2 16452.42 16174.48 509.44 o 2 6 2 79.53 84.00 6.05 o 4 6 2 418.55 431.55 24.82 o 6 6 2 110.61 115.76 6.14 o 8 6 2 539.89 541.62 17.85 o 10 6 2 1896.45 1981.82 50.29 o -11 7 2 6.53 12.74 11.35 o -9 7 2 33.65 42.83 9.30 o -7 7 2 1258.89 1253.72 35.34 o -5 7 2 708.57 696.58 25.76 o -3 7 2 870.48 869.32 30.26 o -1 7 2 746.60 713.91 44.31 o 1 7 2 2.74 8.99 5.79 o 3 7 2 2163.39 2095.03 87.52 o 5 7 2 1088.79 1054.91 39.75 o 7 7 2 115.63 121.11 8.20 o 9 7 2 8.68 7.94 8.11 o -10 8 2 8.81 22.32 15.63 o -8 8 2 3.73 15.50 8.03 o -6 8 2 125.94 117.47 6.75 o -4 8 2 3.75 7.12 6.41 o -2 8 2 61.11 53.88 5.56 o 0 8 2 447.35 456.30 16.60 o 2 8 2 6.12 15.79 7.98 o 4 8 2 105.01 107.17 5.86 o 6 8 2 8.03 16.16 6.98 o 8 8 2 56.29 68.67 7.72 o -9 9 2 10.43 11.95 9.35 o -7 9 2 1462.04 1418.44 21.09 o -5 9 2 80.80 75.07 6.77 o -3 9 2 364.15 360.72 13.87 o -1 9 2 499.97 484.68 16.50 o 1 9 2 765.36 787.92 18.18 o 3 9 2 211.42 212.62 5.17 o 5 9 2 26.18 21.03 5.86 o 7 9 2 1639.84 1703.30 43.05 o -8 10 2 253.19 271.60 13.89 o -6 10 2 495.66 492.88 12.79 o -4 10 2 3787.53 3651.00 99.75 o -2 10 2 747.33 737.86 14.63 o 0 10 2 2478.74 2416.11 100.24 o 2 10 2 114.07 118.64 7.12 o 4 10 2 5107.47 5092.60 133.19 o 6 10 2 561.83 580.08 21.12 o -7 11 2 3556.78 3559.01 108.73 o -5 11 2 85.72 92.71 7.30 o -3 11 2 1054.88 1043.38 42.28 o -1 11 2 70.78 82.48 6.37 o 1 11 2 726.69 695.01 19.29 o 3 11 2 1470.22 1464.50 43.81 o 5 11 2 190.80 200.90 8.69 o -4 12 2 162.25 157.85 7.97 o -2 12 2 824.71 820.20 10.59 o 0 12 2 1309.58 1307.36 10.97 o 2 12 2 6.93 4.25 7.69 o -7 1 3 154.76 162.00 9.51 o -5 1 3 2220.01 2235.01 13.82 o -3 1 3 1766.85 1812.57 29.12 o -1 1 3 525.05 531.85 7.07 o 1 1 3 1113.84 1099.31 11.31 o 3 1 3 569.12 568.01 8.74 o 5 1 3 170.92 165.79 5.41 o 7 1 3 13.29 19.68 5.24 o 9 1 3 1160.79 1150.96 10.24 o 11 1 3 107.30 101.35 15.39 o -10 2 3 138.26 129.57 16.46 o -8 2 3 5660.70 5642.17 29.35 o -6 2 3 516.34 516.00 11.85 o -4 2 3 1182.21 1077.60 21.39 o -2 2 3 18230.22 18580.66 37.09 o 0 2 3 294.95 257.59 14.99 o 2 2 3 7375.49 7353.85 99.32 o 4 2 3 75.10 79.14 6.62 o 6 2 3 3572.31 3555.68 62.43 o 8 2 3 3061.19 3036.47 41.41 o 10 2 3 1.31 2.32 8.84 o -11 3 3 2305.85 2194.93 74.04 o -9 3 3 7544.09 7653.20 32.10 o -7 3 3 804.04 805.89 12.56 o -5 3 3 6471.45 6514.87 86.86 o -3 3 3 2170.79 2139.21 25.55 o -1 3 3 13683.96 14047.60 189.38 o 3 3 3 1.77 81.74 33.73 o 5 3 3 10839.48 11019.47 114.75 o 7 3 3 29.49 29.92 6.13 o 9 3 3 2765.79 2810.23 56.24 o -12 4 3 1321.74 1264.66 33.39 o -10 4 3 42.06 35.87 13.30 o -8 4 3 1454.14 1422.92 16.53 o -6 4 3 418.50 396.67 25.97 o -4 4 3 186.15 183.91 7.16 o -2 4 3 5230.45 5129.54 68.60 o 0 4 3 811.73 750.95 21.90 o 2 4 3 614.87 617.75 13.42 o 4 4 3 552.05 541.76 7.92 o 6 4 3 721.44 736.52 15.12 o 8 4 3 617.32 618.64 18.60 o 10 4 3 269.61 259.76 9.23 o -13 5 3 18.94 19.29 17.50 o -11 5 3 42.25 36.01 11.00 o -9 5 3 3.25 11.13 13.36 o -7 5 3 77.26 77.48 7.63 o -5 5 3 817.21 773.98 22.25 o -3 5 3 576.26 541.70 13.30 o -1 5 3 143.80 155.85 7.16 o 1 5 3 640.36 600.49 17.85 o 3 5 3 225.20 209.28 5.98 o 5 5 3 0.18 4.53 6.94 o 7 5 3 8.06 4.59 6.60 o 9 5 3 521.71 544.61 10.04 o -12 6 3 256.81 242.27 12.88 o -10 6 3 0.83 -3.08 14.56 o -8 6 3 77.21 75.45 8.31 o -6 6 3 45.21 48.48 6.73 o -4 6 3 30.83 47.61 9.67 o -2 6 3 51.92 86.53 14.66 o 0 6 3 111.83 132.26 5.53 o 2 6 3 405.23 408.56 15.58 o 4 6 3 0.89 12.68 6.45 o 6 6 3 7.63 5.96 6.84 o 8 6 3 75.88 87.99 9.30 o -11 7 3 494.10 461.24 12.33 o -9 7 3 1743.85 1752.94 13.32 o -7 7 3 276.01 265.89 7.64 o -5 7 3 4956.33 5122.29 155.94 o -3 7 3 13.41 0.22 5.56 o -1 7 3 3818.65 3797.76 190.73 o 1 7 3 2891.96 2831.17 108.38 o 3 7 3 147.68 144.17 6.26 o 5 7 3 2651.18 2615.21 68.88 o 7 7 3 217.38 224.32 13.38 o -10 8 3 51.87 44.21 14.33 o -8 8 3 2392.84 2378.45 24.48 o -6 8 3 489.62 522.07 20.19 o -4 8 3 644.40 668.71 18.52 o -2 8 3 5603.63 5605.52 220.56 o 0 8 3 2.83 -6.39 6.39 o 2 8 3 5141.45 5040.15 187.86 o 4 8 3 3.69 -0.17 6.30 o 6 8 3 1514.85 1530.10 74.64 o -9 9 3 2187.17 2172.98 37.16 o -7 9 3 1019.93 1006.08 17.87 o -5 9 3 520.83 507.50 7.57 o -3 9 3 1.85 10.98 5.21 o -1 9 3 2239.32 2186.80 80.86 o 1 9 3 57.80 56.84 5.55 o 3 9 3 591.40 602.74 27.84 o 5 9 3 3023.66 3036.37 133.03 o -8 10 3 165.89 167.65 8.75 o -6 10 3 96.65 96.98 7.84 o -4 10 3 0.17 7.29 7.37 o -2 10 3 944.96 920.50 27.52 o 0 10 3 216.13 226.93 11.59 o 2 10 3 354.33 357.20 6.73 o 4 10 3 184.19 173.54 9.46 o -5 11 3 40.56 34.32 7.58 o -3 11 3 150.71 143.01 6.89 o -1 11 3 37.77 35.04 7.78 o 1 11 3 0.44 11.77 6.90 o 3 11 3 281.36 283.48 11.78 o -4 12 3 343.05 338.46 7.83 o -2 12 3 1608.41 1626.95 41.93 o 0 12 3 175.06 190.04 12.65 o -8 0 4 15.15 27.48 10.91 o -6 0 4 14947.25 15104.48 38.86 o -4 0 4 7311.80 7385.82 235.60 o -2 0 4 965.50 1004.99 23.80 o 0 0 4 15382.23 15917.80 438.20 o 2 0 4 1227.22 1220.39 8.73 o 4 0 4 5330.31 5266.95 100.56 o 6 0 4 751.96 704.94 8.24 o 8 0 4 951.45 976.12 9.62 o -9 1 4 6.15 5.21 16.84 o -7 1 4 2463.38 2495.10 65.40 o -5 1 4 35.96 36.54 5.61 o -3 1 4 9361.65 9439.72 194.81 o -1 1 4 429.48 421.70 5.72 o 1 1 4 4.49 23.12 8.33 o 3 1 4 5823.47 5738.31 56.60 o 5 1 4 6.55 21.30 13.11 o 7 1 4 910.16 897.19 6.90 o 9 1 4 78.05 81.45 7.20 o -10 2 4 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5849.28 118.23 o -1 5 4 437.65 422.30 12.66 o 1 5 4 3137.20 3153.87 100.76 o 3 5 4 4521.09 4501.77 94.48 o 5 5 4 76.73 82.38 6.47 o 7 5 4 4818.84 4820.84 163.45 o -12 6 4 5.17 4.16 13.21 o -10 6 4 2011.99 1977.93 19.52 o -8 6 4 365.50 352.79 8.65 o -6 6 4 1986.38 2017.41 26.24 o -4 6 4 3507.27 3645.59 151.21 o -2 6 4 603.26 599.58 10.16 o 0 6 4 1802.26 1896.99 55.12 o 2 6 4 1.07 8.32 7.04 o 4 6 4 4220.22 4163.81 148.95 o 6 6 4 9.36 18.00 10.10 o -11 7 4 0.32 -6.39 15.17 o -9 7 4 798.02 812.23 11.75 o -7 7 4 1571.67 1530.79 19.83 o -5 7 4 31.58 48.37 6.08 o -3 7 4 275.03 275.44 14.86 o -1 7 4 507.94 508.74 22.35 o 1 7 4 125.01 139.72 6.38 o 3 7 4 448.33 444.82 23.44 o 5 7 4 334.97 345.80 15.37 o 7 7 4 736.96 752.39 24.58 o -10 8 4 314.71 316.07 15.58 o -8 8 4 16.57 21.88 8.65 o -6 8 4 142.02 151.48 9.32 o -4 8 4 278.00 281.27 8.54 o -2 8 4 157.42 162.17 5.97 o 0 8 4 82.73 73.59 5.97 o 2 8 4 195.90 208.90 14.21 o 4 8 4 928.84 920.87 38.73 o 6 8 4 4.16 14.67 8.57 o -9 9 4 360.23 343.17 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