#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104041.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104041_Fobs loop_ _publ_author_name 'Redhammer, G\"unther J.' 'Ohashi, Haruo' 'Roth, Georg' _publ_section_title ; Single-crystal structure refinement of NaTiSi~2~O~6~ clinopyroxene at low temperatures (298<T<100K) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 730 _journal_page_last 746 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.660 _cell_angle_beta 77.699 _cell_angle_gamma 77.758 _cell_length_a 5.2988 _cell_length_b 6.5383 _cell_length_c 6.6021 _exptl_crystal_F_000 218.00 _reflns_d_resolution_high 0.8500 _[local]_cod_data_source_file ws5001150sup13.hkl _[local]_cod_data_source_block 150 #BEGIN Tags that were not found in dictionaries: _shelx_title ' NaTiSi2O6, 150 K, 60 mm Abstand, MODELL' _shelx_refln_list_code 4 _shelx_F_calc_maximum 82.14 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.12 -2.19 7.34 o 3 0 0 0.97 -0.98 4.32 o 4 0 0 3978.63 3920.54 58.07 o 5 0 0 1.90 1.63 4.76 o -5 1 0 132.66 135.34 4.91 o -4 1 0 14.65 12.39 5.80 o -3 1 0 276.33 273.20 7.96 o -2 1 0 2191.60 2296.62 39.14 o -1 1 0 302.12 323.13 7.79 o 0 1 0 325.33 313.10 11.65 o 1 1 0 423.17 428.28 16.86 o 2 1 0 103.44 92.72 5.60 o 3 1 0 144.79 154.75 4.50 o 4 1 0 143.68 152.55 4.80 o 5 1 0 60.75 68.56 9.97 o 6 1 0 20.17 15.93 5.13 o -5 2 0 1699.53 1695.77 22.65 o -4 2 0 284.25 266.95 7.60 o -3 2 0 1861.80 1872.86 17.11 o -2 2 0 151.54 147.63 5.46 o -1 2 0 3718.74 3524.48 27.84 o 0 2 0 359.86 332.90 9.21 o 2 2 0 5.60 3.73 5.03 o 3 2 0 4714.18 4814.32 52.21 o 4 2 0 98.35 95.69 4.44 o 5 2 0 1350.01 1343.34 22.26 o 6 2 0 73.96 73.60 5.21 o -5 3 0 14.93 12.63 5.22 o -4 3 0 68.78 70.22 9.16 o -3 3 0 10.68 1.47 9.50 o -2 3 0 87.88 99.46 5.01 o -1 3 0 522.29 511.14 7.92 o 0 3 0 439.32 460.79 9.01 o 1 3 0 2480.49 2572.86 14.73 o 2 3 0 256.90 311.22 23.28 o 3 3 0 573.33 568.38 7.45 o 4 3 0 121.60 114.67 5.07 o 5 3 0 17.13 24.17 4.73 o -4 4 0 1185.36 1205.98 8.50 o -3 4 0 139.89 135.15 4.86 o -2 4 0 576.81 590.77 6.74 o -1 4 0 10.62 10.63 5.57 o 0 4 0 2222.71 2247.45 42.94 o 1 4 0 92.63 85.01 9.31 o 2 4 0 364.20 391.29 9.96 o 3 4 0 77.65 84.52 5.33 o 4 4 0 671.00 682.99 7.64 o 5 4 0 77.35 69.21 7.11 o -3 5 0 2.41 -3.41 5.59 o -2 5 0 10.83 8.17 5.33 o -1 5 0 183.75 195.04 5.81 o 0 5 0 6.90 2.70 6.41 o 1 5 0 139.80 139.24 9.45 o 2 5 0 24.23 35.41 6.12 o 3 5 0 226.18 227.90 6.68 o 4 5 0 104.59 119.00 7.30 o 5 5 0 118.44 133.41 9.80 o -2 6 0 35.81 28.66 5.92 o -1 6 0 7.07 11.72 8.71 o 0 6 0 88.33 91.93 6.53 o 1 6 0 6.02 5.80 9.62 o 2 6 0 1611.27 1584.48 14.71 o 3 6 0 26.95 30.60 5.96 o 4 6 0 509.70 519.82 6.73 o -1 7 0 121.29 127.41 6.75 o 0 7 0 850.39 902.25 34.92 o 1 7 0 76.24 83.28 11.49 o 2 7 0 358.78 369.48 7.71 o 3 7 0 74.52 74.54 6.93 o -3 -7 1 151.92 156.80 6.30 o -2 -7 1 44.05 33.79 6.29 o -1 -7 1 272.67 289.76 9.44 o 0 -7 1 68.26 73.79 8.05 o 1 -7 1 752.22 734.83 43.59 o -4 -6 1 10.24 11.94 5.72 o -3 -6 1 1370.48 1347.27 58.92 o -2 -6 1 175.34 168.01 5.78 o -1 -6 1 1987.32 2107.45 125.99 o 0 -6 1 524.98 523.89 8.88 o 1 -6 1 1023.09 1016.72 43.40 o 2 -6 1 270.77 263.55 10.03 o -5 -5 1 15.24 12.97 5.84 o -4 -5 1 964.73 1007.81 71.09 o -3 -5 1 15.30 12.72 5.22 o -2 -5 1 60.21 79.29 11.33 o -1 -5 1 14.73 22.62 5.65 o 0 -5 1 286.33 302.70 7.35 o 1 -5 1 2.64 1.73 5.38 o 2 -5 1 132.24 147.90 4.88 o 3 -5 1 8.94 5.63 4.97 o -5 -4 1 116.46 117.58 13.12 o -4 -4 1 1492.44 1626.93 139.10 o -3 -4 1 121.64 137.26 11.23 o -2 -4 1 3699.10 3631.97 112.67 o -1 -4 1 85.05 88.29 5.48 o 0 -4 1 1555.10 1515.60 7.22 o 1 -4 1 180.73 179.87 5.25 o 2 -4 1 4011.01 3999.55 31.53 o 3 -4 1 40.54 42.61 4.72 o 4 -4 1 1187.28 1221.14 22.25 o -5 -3 1 272.46 263.68 7.18 o -4 -3 1 221.47 205.39 6.90 o -3 -3 1 1368.73 1456.78 131.25 o -2 -3 1 13.78 22.06 4.98 o -1 -3 1 1133.75 1198.49 50.29 o 0 -3 1 74.35 89.41 5.46 o 1 -3 1 437.97 449.31 5.51 o 2 -3 1 28.45 33.55 5.76 o 3 -3 1 192.40 193.83 5.18 o 4 -3 1 140.65 151.73 13.90 o 5 -3 1 556.42 546.71 5.26 o -5 -2 1 2186.02 2177.51 9.02 o -4 -2 1 10.36 15.36 6.65 o -3 -2 1 3389.54 3353.42 10.15 o -2 -2 1 183.85 205.35 24.94 o -1 -2 1 1885.42 1824.99 11.51 o 0 -2 1 50.80 65.12 6.21 o 1 -2 1 27.40 7.32 5.45 o 2 -2 1 332.37 349.04 5.21 o 3 -2 1 249.43 252.69 12.25 o 4 -2 1 46.55 46.74 4.39 o 5 -2 1 420.40 427.00 6.95 o -5 -1 1 49.33 51.13 4.43 o -4 -1 1 195.99 201.64 12.56 o -3 -1 1 81.40 76.60 7.28 o -2 -1 1 358.72 409.61 7.03 o -1 -1 1 120.37 149.75 10.16 o 0 -1 1 1131.31 1091.16 9.96 o 1 -1 1 128.68 139.12 7.18 o 2 -1 1 340.46 404.41 5.32 o 3 -1 1 67.86 60.77 4.71 o 4 -1 1 224.16 231.92 4.35 o 5 -1 1 40.45 45.85 9.25 o -5 0 1 165.42 153.00 8.07 o -4 0 1 12.04 7.30 7.12 o -3 0 1 326.78 327.97 4.37 o -2 0 1 2112.80 2167.38 33.75 o -1 0 1 329.55 338.37 8.20 o 0 0 1 321.50 307.81 8.78 o 1 0 1 404.78 426.18 8.05 o 2 0 1 122.96 111.10 6.60 o 3 0 1 118.34 127.03 4.57 o 4 0 1 109.69 112.60 4.75 o 5 0 1 42.26 39.61 4.78 o 6 0 1 21.79 27.05 9.01 o -5 1 1 8.28 6.01 4.87 o -4 1 1 339.99 345.90 4.40 o -3 1 1 2.80 2.04 4.56 o -2 1 1 1721.77 1763.30 46.45 o -1 1 1 2.31 -2.46 6.78 o 0 1 1 36.69 41.05 10.94 o 1 1 1 0.94 24.52 9.13 o 2 1 1 108.21 156.26 5.90 o 3 1 1 7.29 2.86 4.67 o 4 1 1 274.30 297.62 14.58 o 5 1 1 11.49 13.57 4.63 o 6 1 1 131.39 130.07 8.63 o -5 2 1 7.84 7.73 5.04 o -4 2 1 1581.54 1594.35 6.00 o -3 2 1 169.40 160.59 4.83 o -2 2 1 926.81 906.17 6.05 o -1 2 1 613.46 634.52 6.79 o 1 2 1 626.44 631.18 18.01 o 2 2 1 63.95 36.67 5.74 o 3 2 1 449.26 457.50 5.28 o 4 2 1 2274.64 2268.62 51.91 o 5 2 1 231.46 220.83 4.88 o 6 2 1 685.31 669.74 20.15 o -4 3 1 72.13 76.86 7.06 o -3 3 1 20.44 20.76 4.98 o -2 3 1 1013.21 1043.32 7.29 o -1 3 1 642.25 653.52 6.79 o 0 3 1 3.92 7.41 8.17 o 1 3 1 1457.61 1510.08 29.43 o 2 3 1 467.10 518.52 10.14 o 3 3 1 302.14 295.70 5.33 o 4 3 1 9.14 7.89 4.70 o 5 3 1 101.16 104.19 5.10 o 6 3 1 16.71 12.53 5.14 o -4 4 1 61.18 65.36 5.39 o -3 4 1 2961.14 2956.60 7.56 o -2 4 1 12.02 18.70 5.35 o -1 4 1 6608.51 6719.93 115.88 o 0 4 1 61.71 57.14 7.72 o 2 4 1 80.88 86.64 7.18 o 3 4 1 1609.21 1631.83 10.96 o 4 4 1 11.03 19.18 7.40 o 5 4 1 738.43 797.39 8.07 o -3 5 1 219.88 224.19 5.82 o -2 5 1 181.19 192.16 5.74 o -1 5 1 143.05 148.43 6.48 o 0 5 1 4.75 4.69 7.89 o 2 5 1 382.46 417.85 8.80 o 3 5 1 112.81 117.71 6.23 o 4 5 1 17.48 22.99 5.34 o 5 5 1 15.62 13.89 8.06 o -2 6 1 981.12 989.45 7.30 o -1 6 1 9.07 10.58 6.60 o 0 6 1 3728.37 3887.19 47.42 o 2 6 1 2240.52 2332.64 28.11 o 3 6 1 29.90 32.13 7.25 o 4 6 1 2316.72 2513.92 70.73 o -1 7 1 4.82 7.79 8.26 o 3 7 1 28.03 32.71 9.52 o -2 -7 2 24.29 21.18 9.31 o -1 -7 2 982.50 1019.97 55.04 o 0 -7 2 22.22 24.22 6.67 o -3 -6 2 165.22 158.73 5.77 o -2 -6 2 7.31 13.84 7.82 o -1 -6 2 175.37 196.08 6.33 o 0 -6 2 242.96 224.61 18.13 o 1 -6 2 154.96 160.67 7.42 o 2 -6 2 53.20 44.94 10.89 o -4 -5 2 74.76 70.46 5.08 o -3 -5 2 21.02 23.67 5.03 o -2 -5 2 234.58 232.82 7.13 o -1 -5 2 15.73 17.75 5.09 o 0 -5 2 3.58 8.55 5.06 o 1 -5 2 37.76 49.40 5.37 o 2 -5 2 606.53 585.30 5.61 o 3 -5 2 28.28 35.29 8.75 o -5 -4 2 116.92 127.10 6.68 o -4 -4 2 224.97 225.43 7.08 o -3 -4 2 39.07 40.99 7.09 o -2 -4 2 1078.02 1105.94 8.44 o -1 -4 2 126.93 124.96 4.92 o 0 -4 2 51.23 58.14 4.85 o 1 -4 2 17.40 14.10 4.81 o 2 -4 2 24.65 36.23 4.84 o 3 -4 2 94.76 104.33 5.10 o 4 -4 2 1.99 3.93 5.03 o -5 -3 2 21.40 21.93 5.96 o -4 -3 2 136.33 143.40 10.04 o -3 -3 2 44.14 58.17 10.77 o -2 -3 2 234.84 251.07 7.25 o -1 -3 2 193.72 200.52 8.72 o 0 -3 2 2643.57 2582.23 12.69 o 1 -3 2 45.12 44.11 7.69 o 2 -3 2 835.09 846.49 5.70 o 3 -3 2 186.56 180.14 6.39 o 4 -3 2 844.97 865.39 5.21 o 5 -3 2 97.08 92.03 7.42 o -5 -2 2 51.03 44.31 6.11 o -4 -2 2 255.37 248.32 6.93 o -3 -2 2 221.88 247.59 28.29 o -2 -2 2 1836.88 1957.42 197.47 o -1 -2 2 1509.54 1590.38 31.65 o 0 -2 2 112.78 72.49 5.31 o 1 -2 2 1455.27 1464.96 6.72 o 2 -2 2 1703.90 1723.27 13.11 o 3 -2 2 188.19 194.79 4.63 o 4 -2 2 197.84 210.36 4.92 o 5 -2 2 38.29 46.76 7.24 o -5 -1 2 404.00 387.24 7.40 o -4 -1 2 61.90 60.38 6.63 o -3 -1 2 242.42 219.91 6.77 o -2 -1 2 303.63 342.82 37.03 o -1 -1 2 30.31 1.72 7.53 o 0 -1 2 48.55 47.84 5.68 o 1 -1 2 2012.84 1824.21 7.46 o 2 -1 2 204.61 206.03 4.97 o 3 -1 2 3587.63 3562.45 12.73 o 4 -1 2 13.29 24.57 4.76 o 5 -1 2 2306.81 2357.72 17.20 o -5 0 2 1803.24 1793.90 10.77 o -4 0 2 297.69 285.58 9.62 o -3 0 2 1928.29 1842.01 8.80 o -2 0 2 155.55 143.32 6.93 o -1 0 2 3774.35 3601.52 317.48 o 0 0 2 364.92 341.78 7.16 o 1 0 2 6687.69 5905.62 112.37 o 2 0 2 6.52 3.81 4.82 o 3 0 2 4545.03 4508.68 8.45 o 4 0 2 78.47 81.68 4.77 o 5 0 2 1259.26 1287.66 16.02 o 6 0 2 95.50 87.05 5.21 o -5 1 2 7.34 18.08 4.69 o -4 1 2 1513.36 1485.45 5.59 o -3 1 2 147.04 148.66 4.48 o -2 1 2 883.98 831.42 16.87 o -1 1 2 613.27 598.66 8.45 o 0 1 2 3279.11 3255.81 152.46 o 1 1 2 678.83 671.85 13.71 o 2 1 2 89.76 58.34 5.25 o 3 1 2 522.64 533.21 12.83 o 4 1 2 2489.91 2525.36 63.13 o 5 1 2 285.98 278.75 4.57 o 6 1 2 785.15 792.22 9.52 o -4 2 2 1372.75 1409.05 5.96 o -3 2 2 2.01 12.27 4.69 o -2 2 2 2930.79 2872.12 7.56 o -1 2 2 0.20 -4.73 7.64 o 0 2 2 55.64 9.89 7.39 o 1 2 2 0.57 1.08 8.06 o 2 2 2 2839.41 2774.44 9.74 o 3 2 2 4.92 2.82 4.67 o 4 2 2 1904.64 1909.45 13.82 o 5 2 2 9.42 7.24 4.38 o 6 2 2 1616.23 1626.45 12.94 o -4 3 2 9.29 14.02 4.91 o -3 3 2 40.67 35.69 5.79 o -2 3 2 361.59 370.86 6.13 o -1 3 2 297.28 315.28 6.14 o 0 3 2 484.36 561.59 43.84 o 2 3 2 41.75 36.41 6.78 o 3 3 2 624.32 642.95 13.34 o 4 3 2 37.48 38.13 7.28 o 5 3 2 532.93 546.27 5.27 o 6 3 2 23.18 19.89 5.50 o -4 4 2 45.02 48.80 5.57 o -3 4 2 938.33 968.20 11.28 o -2 4 2 139.71 134.59 5.59 o -1 4 2 1336.01 1323.95 8.13 o 2 4 2 330.04 344.16 12.07 o 3 4 2 183.82 189.56 6.31 o 4 4 2 50.36 50.78 7.63 o 5 4 2 206.01 222.72 12.40 o -3 5 2 7.18 6.54 6.03 o -2 5 2 56.02 56.17 8.10 o -1 5 2 75.33 67.58 6.71 o 3 5 2 250.33 257.92 13.20 o 4 5 2 94.08 103.69 9.19 o 5 5 2 25.27 30.35 8.10 o -2 6 2 3.34 6.14 6.54 o -1 6 2 97.87 115.53 11.17 o 4 6 2 48.31 48.17 7.25 o -3 -6 3 0.87 -0.78 5.51 o -2 -6 3 88.09 84.65 8.20 o -1 -6 3 24.00 28.24 5.27 o 0 -6 3 483.39 441.43 8.24 o 1 -6 3 5.99 5.80 5.68 o 2 -6 3 53.45 48.54 5.55 o -3 -5 3 1529.74 1326.67 37.73 o -2 -5 3 9.50 12.52 6.90 o -1 -5 3 2514.01 2399.61 7.03 o 0 -5 3 21.64 16.20 4.72 o 1 -5 3 1330.80 1228.75 38.82 o 2 -5 3 3.79 6.64 5.56 o 3 -5 3 1476.75 1291.50 181.29 o -4 -4 3 116.89 121.85 11.61 o -3 -4 3 984.30 1011.91 67.87 o -2 -4 3 160.91 152.96 7.06 o -1 -4 3 958.21 1028.28 36.21 o 0 -4 3 191.81 183.77 5.03 o 1 -4 3 1363.60 1339.90 13.10 o 2 -4 3 10.17 9.55 4.75 o 3 -4 3 752.51 761.88 21.35 o 4 -4 3 63.22 59.79 7.22 o -4 -3 3 479.71 485.37 30.70 o -3 -3 3 47.97 52.46 12.74 o -2 -3 3 4384.77 4290.08 10.85 o -1 -3 3 38.36 47.36 4.83 o 0 -3 3 3777.39 3600.98 35.69 o 1 -3 3 43.45 46.33 4.86 o 2 -3 3 4430.86 4305.12 35.15 o 3 -3 3 61.94 56.52 4.16 o 4 -3 3 518.88 525.14 6.31 o -5 -2 3 82.68 88.63 13.78 o -4 -2 3 788.02 864.56 79.92 o -3 -2 3 175.55 196.97 23.29 o -2 -2 3 774.93 805.16 58.08 o -1 -2 3 48.62 48.94 6.05 o 0 -2 3 2490.24 2459.38 26.70 o 1 -2 3 230.37 222.78 10.26 o 2 -2 3 201.53 193.99 4.62 o 3 -2 3 60.92 50.70 4.52 o 4 -2 3 115.59 113.44 5.81 o 5 -2 3 30.35 33.73 8.37 o -5 -1 3 489.77 449.22 6.86 o -4 -1 3 114.47 122.81 4.88 o -3 -1 3 155.40 165.01 6.72 o -2 -1 3 23.76 17.03 4.65 o -1 -1 3 427.86 468.16 5.06 o 0 -1 3 70.42 81.07 4.77 o 1 -1 3 1173.79 1147.98 16.06 o 2 -1 3 18.02 17.60 4.84 o 3 -1 3 1407.85 1395.20 22.68 o 4 -1 3 189.45 176.11 5.86 o 5 -1 3 295.97 311.98 12.38 o -5 0 3 17.17 5.99 6.44 o -4 0 3 52.74 45.56 6.68 o -3 0 3 10.06 24.66 6.64 o -2 0 3 104.28 115.66 9.63 o -1 0 3 498.56 526.13 7.73 o 0 0 3 446.02 488.36 20.17 o 1 0 3 2522.07 2524.78 96.57 o 2 0 3 235.35 264.81 5.20 o 3 0 3 606.16 603.96 9.01 o 4 0 3 149.78 142.54 4.95 o 5 0 3 12.21 19.37 4.41 o -4 1 3 57.23 58.83 6.87 o -3 1 3 25.50 25.32 6.61 o -2 1 3 970.32 945.36 7.94 o -1 1 3 650.80 678.13 41.59 o 0 1 3 3.71 0.41 5.31 o 1 1 3 1437.99 1439.94 23.35 o 2 1 3 508.36 537.07 7.11 o 3 1 3 272.34 262.88 7.74 o 4 1 3 8.89 11.67 6.66 o 5 1 3 81.40 80.42 4.86 o 6 1 3 24.03 22.22 5.17 o -4 2 3 7.70 0.80 7.02 o -3 2 3 52.15 38.42 6.65 o -2 2 3 380.69 389.38 7.24 o -1 2 3 314.37 351.22 28.26 o 0 2 3 458.45 496.78 9.54 o 1 2 3 533.03 538.36 7.25 o 2 2 3 29.24 27.25 5.54 o 3 2 3 543.44 543.82 5.93 o 4 2 3 26.59 18.24 5.37 o 5 2 3 449.82 455.90 9.91 o 6 2 3 18.12 26.86 5.15 o -4 3 3 194.59 186.20 7.51 o -3 3 3 3.60 -0.14 6.63 o -2 3 3 71.17 66.96 6.82 o -1 3 3 0.02 4.33 5.28 o 0 3 3 2758.79 2763.30 10.98 o 1 3 3 1.46 4.66 11.37 o 2 3 3 2880.00 2819.84 29.09 o 3 3 3 6.29 1.39 5.86 o 4 3 3 3860.94 3850.12 44.30 o 5 3 3 7.81 3.92 5.09 o 6 3 3 425.10 425.28 6.37 o -3 4 3 5.29 4.78 7.89 o -2 4 3 1402.86 1427.01 10.19 o -1 4 3 1.99 12.51 8.84 o 0 4 3 1011.88 1004.36 14.53 o 3 4 3 55.71 60.51 6.83 o 4 4 3 621.84 630.39 20.91 o 5 4 3 33.70 35.71 5.54 o -2 5 3 275.13 278.76 9.13 o -1 5 3 897.84 1025.97 64.99 o 3 5 3 1502.34 1527.12 18.24 o 4 5 3 34.03 40.54 9.94 o 5 5 3 1426.14 1457.72 34.65 o -1 6 3 646.69 721.54 66.53 o 4 6 3 67.76 61.88 9.56 o -1 -6 4 509.42 343.67 45.39 o 0 -6 4 45.51 53.18 5.24 o -2 -5 4 145.44 105.07 7.36 o -1 -5 4 43.43 42.22 4.95 o 0 -5 4 17.64 18.87 4.90 o 1 -5 4 18.58 12.24 6.93 o 2 -5 4 201.63 162.35 10.81 o -3 -4 4 6.97 11.58 4.96 o -2 -4 4 132.20 123.96 7.01 o -1 -4 4 34.27 29.55 4.75 o 0 -4 4 6.73 -10.83 10.83 o 1 -4 4 28.80 17.50 5.10 o 2 -4 4 136.72 131.36 5.00 o 3 -4 4 7.65 0.35 4.62 o -4 -3 4 49.41 55.82 7.24 o -3 -3 4 823.76 797.13 75.00 o -2 -3 4 7.08 9.28 6.75 o -1 -3 4 1476.74 1496.16 25.16 o 0 -3 4 159.81 156.64 6.86 o 1 -3 4 1028.70 1025.14 9.27 o 2 -3 4 179.82 188.28 4.92 o 3 -3 4 1012.43 1014.61 15.01 o 4 -3 4 118.48 127.42 6.19 o -4 -2 4 1.85 0.90 5.02 o -3 -2 4 119.81 125.36 7.30 o -2 -2 4 26.75 16.49 6.86 o -1 -2 4 19.50 16.25 4.77 o 0 -2 4 39.09 36.36 11.92 o 1 -2 4 110.06 101.63 5.49 o 2 -2 4 990.93 1003.76 31.51 o 3 -2 4 27.19 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