#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:01:02 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180900 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/40/2104043.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104043_Fobs loop_ _publ_author_name 'Redhammer, G\"unther J.' 'Ohashi, Haruo' 'Roth, Georg' _publ_section_title ; Single-crystal structure refinement of NaTiSi~2~O~6~ clinopyroxene at low temperatures (298<T<100K) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 730 _journal_page_last 746 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.630 _cell_angle_beta 77.721 _cell_angle_gamma 77.750 _cell_length_a 5.2976 _cell_length_b 6.5230 _cell_length_c 6.6073 _exptl_crystal_F_000 218.00 _reflns_d_resolution_high 0.8505 _cod_data_source_file ws5001130sup15.hkl _cod_data_source_block 130 #BEGIN Tags that were not found in dictionaries: _shelx_title ' NaTiSi2O6, 130 K, kleiner Abstand, MODELL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 82.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.41 -7.96 9.46 o 3 0 0 2.30 -5.14 5.14 o 4 0 0 4072.97 4002.69 36.26 o 5 0 0 2.89 6.86 5.65 o -5 1 0 136.22 127.06 5.49 o -4 1 0 19.23 25.04 5.21 o -3 1 0 275.37 284.17 12.21 o -2 1 0 2226.32 2352.47 30.09 o -1 1 0 298.67 358.68 9.97 o 1 1 0 424.20 442.46 16.70 o 2 1 0 104.02 91.24 9.35 o 3 1 0 144.00 152.24 9.63 o 4 1 0 149.02 156.68 5.69 o 5 1 0 66.24 60.36 4.96 o 6 1 0 21.90 26.11 13.89 o -5 2 0 1766.31 1778.82 17.16 o -4 2 0 282.81 264.78 5.58 o -3 2 0 1895.06 1884.10 17.57 o -2 2 0 149.36 146.57 5.98 o -1 2 0 3729.56 3559.60 61.85 o 0 2 0 356.87 311.00 11.64 o 2 2 0 6.06 2.49 6.58 o 3 2 0 4819.64 4750.09 34.44 o 4 2 0 105.28 105.22 5.64 o 5 2 0 1412.84 1408.53 6.24 o 6 2 0 79.31 78.00 5.70 o -5 3 0 19.14 17.67 12.66 o -4 3 0 72.87 67.21 5.43 o -3 3 0 11.21 15.05 5.59 o -2 3 0 86.68 94.95 6.97 o -1 3 0 533.40 520.40 7.36 o 0 3 0 453.28 469.74 9.18 o 1 3 0 2505.88 2598.58 16.17 o 2 3 0 255.09 308.93 20.13 o 3 3 0 589.46 577.86 9.50 o 4 3 0 126.88 126.23 9.72 o 5 3 0 15.91 17.36 5.34 o -4 4 0 1243.89 1268.52 8.10 o -3 4 0 138.01 124.69 5.53 o -2 4 0 583.23 600.02 6.59 o -1 4 0 9.32 9.86 6.76 o 0 4 0 2245.69 2279.75 39.04 o 1 4 0 90.35 90.40 11.23 o 2 4 0 372.45 396.82 25.72 o 3 4 0 84.36 85.01 6.34 o 4 4 0 704.26 711.08 9.38 o 5 4 0 82.45 84.24 8.78 o -3 5 0 1.72 -3.86 5.56 o -2 5 0 11.86 18.17 6.06 o -1 5 0 187.04 200.48 7.11 o 0 5 0 5.54 6.35 7.61 o 1 5 0 142.59 147.84 11.15 o 2 5 0 27.55 42.69 7.26 o 3 5 0 232.89 232.77 18.81 o 4 5 0 118.47 132.03 6.14 o 5 5 0 121.76 120.84 8.06 o -2 6 0 36.77 35.10 6.58 o -1 6 0 6.77 17.33 8.69 o 0 6 0 89.11 92.91 8.97 o 1 6 0 6.45 11.14 11.13 o 2 6 0 1643.42 1636.99 13.40 o 3 6 0 29.77 37.23 6.70 o 4 6 0 512.85 530.13 8.99 o -1 7 0 128.48 135.91 7.42 o 0 7 0 880.99 926.09 25.57 o 1 7 0 79.99 86.05 12.78 o 2 7 0 364.24 361.41 8.47 o 3 7 0 82.51 84.01 7.62 o -3 -7 1 167.45 178.77 6.90 o -2 -7 1 49.81 46.35 6.97 o -1 -7 1 300.00 314.46 10.42 o 0 -7 1 67.96 63.46 7.03 o 1 -7 1 813.17 766.78 29.63 o -4 -6 1 10.09 3.59 8.84 o -3 -6 1 1425.39 1441.35 31.10 o -2 -6 1 177.23 168.09 6.48 o -1 -6 1 2065.05 2159.12 141.30 o 0 -6 1 527.21 543.40 20.61 o 1 -6 1 1073.80 1073.61 7.22 o 2 -6 1 272.66 277.88 6.53 o -5 -5 1 14.05 21.73 6.24 o -4 -5 1 999.23 1034.97 65.18 o -3 -5 1 14.42 12.03 6.03 o -2 -5 1 60.63 81.48 6.34 o -1 -5 1 15.46 26.63 6.73 o 0 -5 1 299.14 317.79 7.35 o 1 -5 1 3.57 17.20 6.32 o 2 -5 1 142.45 147.43 5.55 o 3 -5 1 10.39 8.97 6.15 o -5 -4 1 116.67 120.34 16.02 o -4 -4 1 1537.35 1651.01 126.39 o -3 -4 1 117.18 144.63 6.02 o -2 -4 1 3774.66 3724.87 86.01 o -1 -4 1 81.04 87.25 6.46 o 0 -4 1 1581.90 1530.63 8.04 o 1 -4 1 174.64 194.99 12.29 o 2 -4 1 4123.57 4116.59 9.12 o 3 -4 1 38.50 32.00 5.42 o 4 -4 1 1238.96 1268.83 6.55 o -5 -3 1 279.60 244.51 8.02 o -4 -3 1 233.00 222.61 7.92 o -3 -3 1 1387.10 1462.69 107.12 o -2 -3 1 14.58 18.19 6.08 o -1 -3 1 1133.55 1216.04 39.87 o 0 -3 1 74.66 86.38 6.66 o 1 -3 1 436.62 456.69 10.80 o 2 -3 1 30.36 34.05 6.49 o 3 -3 1 199.16 203.04 13.49 o 4 -3 1 150.36 149.36 5.57 o 5 -3 1 572.13 590.04 5.73 o -5 -2 1 2253.43 2370.20 9.90 o -4 -2 1 11.34 8.86 7.84 o -3 -2 1 3417.33 3374.26 10.83 o -2 -2 1 190.55 200.22 27.35 o -1 -2 1 1880.39 1840.44 13.13 o 0 -2 1 50.39 55.65 15.54 o 1 -2 1 28.26 -2.60 6.92 o 2 -2 1 336.19 347.36 6.24 o 3 -2 1 257.03 252.54 5.83 o 4 -2 1 45.70 39.27 5.06 o 5 -2 1 447.76 445.13 12.04 o -5 -1 1 56.93 47.53 13.00 o -4 -1 1 198.99 207.06 5.63 o -3 -1 1 87.19 78.91 5.12 o -2 -1 1 361.78 415.79 8.37 o -1 -1 1 118.51 134.79 13.09 o 0 -1 1 1128.83 1115.23 11.72 o 1 -1 1 126.14 129.11 9.40 o 2 -1 1 345.23 399.53 6.36 o 3 -1 1 71.06 63.57 12.03 o 4 -1 1 228.62 251.67 9.57 o 5 -1 1 45.27 57.38 5.43 o -5 0 1 173.72 162.75 5.74 o -4 0 1 16.09 17.81 12.46 o -3 0 1 334.66 327.67 5.10 o -2 0 1 2124.14 2164.49 43.11 o -1 0 1 328.70 360.11 9.44 o 1 0 1 403.54 450.69 11.87 o 2 0 1 126.90 107.39 7.00 o 3 0 1 118.47 117.10 8.60 o 4 0 1 109.51 115.78 9.01 o 5 0 1 44.19 47.87 5.40 o 6 0 1 24.36 23.15 9.89 o -5 1 1 8.11 1.10 5.46 o -4 1 1 358.31 343.20 7.53 o -3 1 1 1.19 12.87 6.10 o -2 1 1 1742.56 1784.39 37.96 o -1 1 1 1.86 -8.51 8.51 o 0 1 1 36.67 37.18 14.12 o 1 1 1 0.23 37.82 11.40 o 2 1 1 107.01 153.11 7.29 o 3 1 1 5.27 -1.05 6.73 o 4 1 1 276.33 303.37 13.60 o 5 1 1 6.64 6.15 5.26 o 6 1 1 145.18 131.23 8.19 o -5 2 1 9.24 3.25 5.14 o -4 2 1 1641.69 1646.97 12.32 o -3 2 1 181.92 174.01 5.69 o -2 2 1 935.97 931.61 7.29 o -1 2 1 620.78 647.91 8.06 o 0 2 1 3229.49 3114.92 27.86 o 1 2 1 623.92 617.69 18.32 o 2 2 1 58.88 31.23 7.04 o 3 2 1 449.76 468.39 8.74 o 4 2 1 2310.63 2337.13 68.95 o 5 2 1 237.18 231.74 5.55 o 6 2 1 703.44 707.31 21.33 o -4 3 1 72.05 76.04 5.49 o -3 3 1 23.45 31.33 7.43 o -2 3 1 1029.09 1058.24 6.70 o -1 3 1 650.27 657.62 7.90 o 0 3 1 4.05 7.17 10.25 o 1 3 1 1472.88 1519.20 37.76 o 2 3 1 474.18 511.94 12.01 o 3 3 1 309.90 304.51 6.57 o 4 3 1 7.73 15.38 6.96 o 5 3 1 110.72 110.19 7.12 o 6 3 1 17.63 15.79 11.09 o -4 4 1 69.91 78.39 5.65 o -3 4 1 3053.81 3065.27 8.10 o -2 4 1 14.11 28.59 6.32 o -1 4 1 6706.24 6875.12 18.94 o 0 4 1 67.21 57.27 9.30 o 2 4 1 83.51 91.23 8.36 o 3 4 1 1639.66 1672.18 12.25 o 4 4 1 9.87 15.44 8.61 o 5 4 1 761.71 794.49 8.81 o -3 5 1 230.49 233.00 6.12 o -2 5 1 183.28 182.61 11.60 o -1 5 1 149.73 147.55 7.56 o 0 5 1 6.20 7.71 9.25 o 2 5 1 395.09 431.12 10.08 o 3 5 1 113.20 125.19 7.53 o 4 5 1 17.13 24.50 6.26 o 5 5 1 14.11 16.74 8.97 o -2 6 1 1014.12 1018.59 7.95 o -1 6 1 10.99 13.18 7.46 o 0 6 1 3864.89 3975.98 17.14 o 2 6 1 2323.81 2401.18 37.48 o 3 6 1 29.85 30.42 8.24 o 4 6 1 2439.96 2603.72 57.62 o -1 7 1 3.89 9.94 9.04 o 3 7 1 26.38 33.33 10.72 o -2 -7 2 27.14 24.58 10.27 o -1 -7 2 1005.28 1066.79 70.66 o 0 -7 2 21.58 23.91 6.51 o -3 -6 2 170.36 176.91 6.40 o -2 -6 2 7.32 3.15 8.77 o -1 -6 2 183.73 199.00 17.44 o 0 -6 2 261.72 254.66 10.63 o 1 -6 2 164.65 172.53 9.37 o 2 -6 2 55.06 50.07 7.42 o -4 -5 2 71.41 66.52 5.66 o -3 -5 2 26.45 37.83 5.72 o -2 -5 2 235.45 230.89 8.15 o -1 -5 2 18.54 27.37 7.51 o 0 -5 2 3.73 0.83 7.81 o 1 -5 2 40.62 42.49 5.88 o 2 -5 2 623.06 611.06 9.25 o 3 -5 2 30.19 47.26 5.61 o -5 -4 2 118.16 128.58 28.82 o -4 -4 2 240.92 245.83 24.51 o -3 -4 2 35.50 23.27 5.43 o -2 -4 2 1104.30 1148.17 9.53 o -1 -4 2 129.34 135.16 8.04 o 0 -4 2 47.04 56.77 10.96 o 1 -4 2 16.23 10.68 10.96 o 2 -4 2 26.09 44.56 13.23 o 3 -4 2 91.89 98.26 7.25 o 4 -4 2 2.51 6.85 5.60 o -5 -3 2 20.67 34.40 19.99 o -4 -3 2 149.39 156.40 8.61 o -3 -3 2 45.57 56.06 7.58 o -2 -3 2 256.31 258.48 8.48 o -1 -3 2 197.90 214.03 9.00 o 0 -3 2 2710.77 2639.47 19.70 o 1 -3 2 49.13 41.18 6.85 o 2 -3 2 851.77 877.36 6.55 o 3 -3 2 195.16 210.64 5.76 o 4 -3 2 875.82 875.25 10.94 o 5 -3 2 106.07 111.47 6.88 o -5 -2 2 57.20 55.57 6.77 o -4 -2 2 262.92 296.90 7.86 o -3 -2 2 233.02 247.12 19.48 o -2 -2 2 1880.65 1955.53 159.85 o -1 -2 2 1532.17 1605.51 44.65 o 1 -2 2 1459.97 1477.07 8.18 o 2 -2 2 1729.08 1744.59 31.43 o 3 -2 2 190.30 190.71 5.41 o 4 -2 2 197.52 199.52 6.09 o 5 -2 2 40.08 49.58 5.55 o -5 -1 2 425.13 424.49 8.17 o -4 -1 2 61.48 54.39 7.65 o -3 -1 2 248.18 229.56 7.89 o -2 -1 2 308.07 338.53 43.17 o -1 -1 2 31.58 2.36 9.40 o 0 -1 2 49.14 48.10 7.20 o 1 -1 2 2035.49 1826.26 12.58 o 2 -1 2 214.46 209.22 6.00 o 3 -1 2 3661.37 3601.03 8.31 o 4 -1 2 15.38 31.56 14.24 o 5 -1 2 2378.53 2397.03 22.65 o -5 0 2 1888.16 1863.70 36.77 o -4 0 2 304.64 291.99 6.43 o -3 0 2 1963.61 1872.67 9.76 o -2 0 2 158.70 144.15 8.39 o -1 0 2 3816.46 3660.43 288.47 o 0 0 2 366.09 317.36 11.89 o 2 0 2 7.33 7.42 6.48 o 3 0 2 4596.02 4567.48 18.37 o 4 0 2 80.44 85.68 5.67 o 5 0 2 1298.71 1311.14 5.98 o 6 0 2 106.38 106.74 5.72 o -5 1 2 8.36 15.38 18.04 o -4 1 2 1560.04 1525.37 6.13 o -3 1 2 151.66 143.61 8.05 o -2 1 2 885.01 843.21 6.38 o -1 1 2 613.95 600.40 10.15 o 0 1 2 3275.18 3279.60 203.02 o 1 1 2 677.67 662.26 10.42 o 2 1 2 84.87 60.80 6.86 o 3 1 2 533.19 535.99 5.79 o 4 1 2 2541.30 2622.03 52.35 o 5 1 2 303.43 300.83 5.63 o 6 1 2 812.82 816.97 8.01 o -4 2 2 1420.75 1424.78 15.21 o -3 2 2 2.65 12.58 5.49 o -2 2 2 2987.53 2917.65 8.25 o -1 2 2 0.58 -0.10 9.31 o 1 2 2 0.12 -6.49 10.10 o 2 2 2 2887.07 2785.27 26.27 o 3 2 2 3.27 4.47 5.95 o 4 2 2 1960.64 1992.22 15.77 o 5 2 2 12.40 2.79 5.36 o 6 2 2 1708.05 1659.96 41.09 o -4 3 2 13.46 19.05 5.49 o -3 3 2 40.53 40.56 5.59 o -2 3 2 365.85 380.53 6.61 o -1 3 2 298.87 316.23 7.23 o 0 3 2 479.37 551.91 30.56 o 2 3 2 39.83 40.10 8.50 o 3 3 2 633.04 659.42 20.44 o 4 3 2 40.79 45.16 5.86 o 5 3 2 538.47 568.89 11.54 o 6 3 2 28.86 40.29 14.58 o -3 4 2 979.71 988.31 8.52 o -2 4 2 144.22 138.42 6.48 o -1 4 2 1374.66 1331.56 9.12 o 2 4 2 335.31 358.42 13.54 o 3 4 2 190.23 188.82 7.65 o 4 4 2 50.70 34.92 6.06 o 5 4 2 221.96 215.64 6.31 o -3 5 2 10.04 12.01 8.09 o -2 5 2 58.28 60.64 6.72 o -1 5 2 71.55 65.01 7.71 o 3 5 2 252.31 264.85 10.50 o 4 5 2 92.78 108.89 10.39 o 5 5 2 27.74 21.04 9.04 o -2 6 2 3.14 8.71 7.20 o -1 6 2 96.97 109.14 13.09 o 4 6 2 53.61 49.71 8.29 o -2 -6 3 88.95 79.35 9.17 o -1 -6 3 25.57 28.91 5.91 o 0 -6 3 499.52 452.96 9.64 o 1 -6 3 5.72 6.96 6.32 o 2 -6 3 55.66 51.65 7.34 o -3 -5 3 1596.10 1548.24 95.76 o -2 -5 3 7.62 13.87 7.78 o -1 -5 3 2589.02 2671.68 115.04 o 0 -5 3 28.41 17.38 8.31 o 1 -5 3 1368.78 1368.76 22.75 o 2 -5 3 3.87 -5.53 5.53 o 3 -5 3 1540.37 1502.88 6.81 o -4 -4 3 118.45 119.91 12.14 o -3 -4 3 1039.92 1042.89 54.84 o -2 -4 3 160.28 172.33 8.11 o -1 -4 3 986.75 1043.70 38.49 o 0 -4 3 204.31 211.34 6.22 o 1 -4 3 1387.51 1366.10 10.47 o 2 -4 3 11.89 -2.90 5.52 o 3 -4 3 780.13 775.91 27.99 o 4 -4 3 72.42 66.95 5.71 o -4 -3 3 482.93 500.40 18.70 o -3 -3 3 52.27 44.91 5.43 o -2 -3 3 4459.64 4354.44 11.56 o -1 -3 3 45.28 63.74 5.76 o 0 -3 3 3791.28 3656.49 8.47 o 1 -3 3 52.67 50.06 5.83 o 2 -3 3 4492.56 4402.61 36.67 o 3 -3 3 70.03 57.38 9.83 o 4 -3 3 524.22 523.74 5.84 o -5 -2 3 89.22 86.61 13.62 o -4 -2 3 826.12 872.27 88.19 o -3 -2 3 184.20 189.50 20.23 o -2 -2 3 792.52 812.64 52.90 o -1 -2 3 53.62 50.42 5.77 o 0 -2 3 2527.65 2486.78 35.16 o 1 -2 3 239.72 230.33 5.66 o 2 -2 3 208.38 205.34 16.23 o 3 -2 3 65.07 77.64 5.31 o 4 -2 3 123.15 123.46 6.47 o 5 -2 3 29.39 18.52 6.05 o -5 -1 3 498.79 485.31 7.48 o -4 -1 3 115.74 118.28 8.05 o -3 -1 3 153.43 169.08 17.03 o -2 -1 3 23.08 33.82 5.54 o -1 -1 3 426.18 463.05 5.95 o 0 -1 3 70.24 75.35 5.85 o 1 -1 3 1187.21 1169.14 19.80 o 2 -1 3 20.00 21.84 5.83 o 3 -1 3 1427.50 1397.91 14.14 o 4 -1 3 194.27 174.87 10.25 o 5 -1 3 311.44 312.24 5.37 o -5 0 3 21.61 17.22 7.04 o -4 0 3 55.13 46.29 7.56 o -3 0 3 10.27 3.85 7.72 o -2 0 3 103.70 110.88 11.91 o -1 0 3 509.80 535.10 9.14 o 0 0 3 465.22 501.04 18.11 o 1 0 3 2554.34 2559.35 81.73 o 2 0 3 229.56 242.25 11.73 o 3 0 3 621.13 622.94 9.88 o 4 0 3 158.51 159.33 5.76 o 5 0 3 10.91 13.64 12.22 o -4 1 3 55.86 43.32 7.74 o -3 1 3 32.49 29.19 7.71 o -2 1 3 981.49 982.41 9.14 o -1 1 3 672.69 688.72 51.10 o 0 1 3 4.03 7.31 6.50 o 1 1 3 1448.82 1422.46 30.75 o 2 1 3 520.85 548.05 7.03 o 3 1 3 275.53 259.42 6.41 o 4 1 3 7.63 14.76 6.00 o 5 1 3 85.10 88.09 5.49 o 6 1 3 26.20 29.65 5.70 o -4 2 3 10.90 14.07 7.79 o -3 2 3 52.70 44.75 8.52 o -2 2 3 398.39 409.90 8.46 o -1 2 3 320.29 350.55 35.60 o 0 2 3 459.59 503.93 11.33 o 1 2 3 531.79 546.31 12.78 o 2 2 3 26.88 24.77 7.10 o 3 2 3 539.33 550.63 12.82 o 4 2 3 28.32 39.73 9.64 o 5 2 3 453.48 454.66 9.93 o 6 2 3 23.22 11.78 5.67 o -4 3 3 210.74 211.93 8.27 o -3 3 3 4.87 4.27 7.53 o -2 3 3 74.90 80.82 7.92 o -1 3 3 0.01 2.50 6.27 o 0 3 3 2818.30 2824.05 28.56 o 1 3 3 2.02 3.71 14.33 o 2 3 3 2927.00 2827.20 17.08 o 3 3 3 7.85 2.55 6.94 o 4 3 3 3972.95 3932.70 53.53 o 5 3 3 10.08 8.98 5.68 o 6 3 3 441.98 450.82 6.10 o -3 4 3 6.99 16.54 7.92 o -2 4 3 1452.02 1438.47 11.25 o -1 4 3 1.58 4.39 10.37 o 0 4 3 1028.22 1019.87 13.02 o 3 4 3 54.69 66.56 8.01 o 4 4 3 630.64 632.38 23.54 o 5 4 3 34.37 23.09 5.87 o -2 5 3 282.59 280.83 10.14 o -1 5 3 922.79 1039.25 73.13 o 3 5 3 1556.60 1564.76 19.97 o 4 5 3 35.51 25.78 11.30 o 5 5 3 1496.05 1515.27 29.33 o -1 6 3 680.43 713.38 52.04 o 4 6 3 74.83 77.33 10.29 o -1 -6 4 536.55 489.30 29.47 o 0 -6 4 52.48 47.75 5.82 o -3 -5 4 656.92 595.73 37.06 o -2 -5 4 151.74 133.95 8.17 o -1 -5 4 48.80 53.13 10.00 o 0 -5 4 19.25 20.18 5.51 o 1 -5 4 20.63 26.85 7.65 o 2 -5 4 218.69 217.41 9.65 o -3 -4 4 10.18 30.80 6.71 o -2 -4 4 145.63 132.26 7.91 o -1 -4 4 33.38 17.17 6.17 o 0 -4 4 6.48 7.21 17.57 o 1 -4 4 26.50 16.82 6.49 o 2 -4 4 147.04 159.11 5.54 o 3 -4 4 12.01 5.28 6.65 o -4 -3 4 54.32 60.07 5.25 o -3 -3 4 868.83 847.08 51.05 o -2 -3 4 7.95 1.41 7.79 o -1 -3 4 1526.81 1561.76 56.62 o 0 -3 4 165.39 171.48 10.15 o 1 -3 4 1075.82 1059.00 43.92 o 2 -3 4 184.75 185.52 5.72 o 3 -3 4 1067.61 1039.18 18.37 o 4 -3 4 117.32 123.92 5.67 o -4 -2 4 2.13 6.15 5.54 o -3 -2 4 118.19 122.43 6.20 o -2 -2 4 27.54 27.03 8.15 o -1 -2 4 17.20 18.18 7.75 o 0 -2 4 36.92 36.01 5.66 o 1 -2 4 110.39 109.45 5.36 o 2 -2 4 1004.66 1020.80 23.23 o 3 -2 4 23.69 29.64 5.52 o 4 -2 4 174.71 167.58 5.70 o 5 -2 4 81.75 71.11 5.33 o -4 -1 4 1299.36 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