#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/40/2104044.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104044_Fobs loop_ _publ_author_name 'Redhammer, G\"unther J.' 'Ohashi, Haruo' 'Roth, Georg' _publ_section_title ; Single-crystal structure refinement of NaTiSi~2~O~6~ clinopyroxene at low temperatures (298<T<100K) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 730 _journal_page_last 746 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.600 _cell_angle_beta 77.729 _cell_angle_gamma 77.750 _cell_length_a 5.2976 _cell_length_b 6.5159 _cell_length_c 6.6123 _exptl_crystal_F_000 218.00 _reflns_d_resolution_high 0.8504 _[local]_cod_data_source_file ws5001110sup16.hkl _[local]_cod_data_source_block 110 #BEGIN Tags that were not found in dictionaries: _shelx_title ' NaTiSi2O6, 110 K, kleiner Abstand, MODELL' _shelx_refln_list_code 4 _shelx_F_calc_maximum 83.02 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.78 -1.92 9.58 o 3 0 0 2.60 -4.23 5.96 o 4 0 0 4083.61 3898.11 30.61 o 5 0 0 4.36 14.82 4.99 o -5 1 0 133.60 112.23 5.51 o -4 1 0 18.66 27.04 11.35 o -3 1 0 272.05 264.80 8.84 o -2 1 0 2224.67 2318.72 30.90 o -1 1 0 295.91 351.87 10.00 o 1 1 0 424.52 442.91 10.66 o 2 1 0 104.84 89.99 7.94 o 3 1 0 144.47 137.46 5.78 o 4 1 0 150.50 160.49 5.90 o 5 1 0 69.84 68.01 4.95 o 6 1 0 23.85 25.79 5.63 o -5 2 0 1758.69 1773.82 6.76 o -4 2 0 277.46 266.07 5.56 o -3 2 0 1893.50 1889.31 30.05 o -2 2 0 149.01 144.19 6.00 o -1 2 0 3727.15 3567.31 97.07 o 0 2 0 352.78 304.96 11.68 o 1 2 0 6807.56 7128.25 24.69 o 2 2 0 7.89 3.59 6.61 o 3 2 0 4844.85 4689.03 127.86 o 4 2 0 114.16 120.25 7.26 o 5 2 0 1422.83 1404.18 6.00 o 6 2 0 74.75 56.10 5.73 o -5 3 0 15.92 15.53 6.49 o -4 3 0 74.56 65.63 5.44 o -3 3 0 10.86 17.15 5.57 o -2 3 0 84.01 97.53 6.03 o -1 3 0 528.66 514.58 7.37 o 0 3 0 454.63 473.18 9.19 o 1 3 0 2500.80 2576.17 16.12 o 2 3 0 253.64 307.27 22.35 o 3 3 0 589.65 587.41 9.52 o 4 3 0 126.16 135.85 8.08 o 5 3 0 15.40 13.18 5.34 o -4 4 0 1238.92 1252.31 6.52 o -3 4 0 139.59 131.21 5.53 o -2 4 0 584.64 604.17 6.94 o -1 4 0 7.54 14.44 6.75 o 0 4 0 2246.38 2263.65 40.27 o 1 4 0 88.91 83.49 11.28 o 2 4 0 383.10 394.55 7.38 o 3 4 0 87.82 90.66 6.37 o 4 4 0 711.30 716.47 9.40 o 5 4 0 89.56 89.37 8.81 o -3 5 0 3.36 7.41 8.88 o -2 5 0 12.01 17.09 6.04 o -1 5 0 191.07 205.56 7.10 o 0 5 0 6.29 6.24 7.65 o 1 5 0 144.82 137.05 11.21 o 2 5 0 25.83 33.68 7.30 o 3 5 0 233.70 240.07 6.61 o 4 5 0 116.23 125.37 8.72 o 5 5 0 121.41 124.54 6.10 o -2 6 0 37.50 42.37 9.80 o -1 6 0 7.17 8.57 6.71 o 0 6 0 89.81 95.72 7.26 o 1 6 0 6.94 2.98 11.14 o 2 6 0 1619.05 1625.64 15.38 o 3 6 0 35.93 38.48 11.56 o 4 6 0 507.88 521.73 7.06 o -1 7 0 127.13 135.89 11.36 o 0 7 0 883.47 941.97 35.37 o 1 7 0 81.03 83.40 12.77 o 2 7 0 370.91 377.35 8.47 o 3 7 0 78.54 84.55 7.60 o -3 -7 1 171.36 165.13 8.20 o -2 -7 1 49.07 53.27 6.98 o -1 -7 1 297.22 313.99 10.42 o 0 -7 1 65.90 62.18 7.05 o 1 -7 1 818.08 802.98 7.92 o -4 -6 1 10.23 10.22 6.32 o -3 -6 1 1422.20 1444.69 40.94 o -2 -6 1 180.00 174.10 6.48 o -1 -6 1 2069.06 2173.93 121.88 o 0 -6 1 525.83 551.51 19.08 o 1 -6 1 1082.35 1083.57 7.26 o 2 -6 1 268.72 278.92 10.23 o -5 -5 1 19.28 12.72 9.37 o -4 -5 1 996.49 1053.49 50.64 o -3 -5 1 18.07 15.45 6.03 o -2 -5 1 62.34 77.35 6.34 o -1 -5 1 15.72 24.93 6.74 o 0 -5 1 299.03 319.99 7.37 o 1 -5 1 3.40 3.49 6.62 o 2 -5 1 142.42 150.20 5.56 o 3 -5 1 10.71 9.84 8.96 o -5 -4 1 119.29 134.84 5.72 o -4 -4 1 1529.50 1691.05 139.25 o -3 -4 1 118.84 133.79 12.24 o -2 -4 1 3747.97 3777.52 60.87 o -1 -4 1 79.55 91.65 7.16 o 0 -4 1 1579.90 1549.44 10.97 o 1 -4 1 172.69 175.82 6.62 o 2 -4 1 4117.63 4129.09 36.86 o 3 -4 1 38.69 39.51 5.43 o 4 -4 1 1252.94 1280.95 9.12 o -5 -3 1 282.89 290.06 7.96 o -4 -3 1 231.41 215.35 6.84 o -3 -3 1 1393.63 1472.86 115.42 o -2 -3 1 15.15 18.19 5.77 o -1 -3 1 1134.02 1201.48 48.91 o 0 -3 1 74.03 89.50 7.07 o 1 -3 1 441.44 448.19 6.45 o 2 -3 1 29.90 50.66 6.16 o 3 -3 1 201.44 209.48 5.35 o 4 -3 1 153.15 147.55 5.16 o 5 -3 1 571.30 604.40 5.73 o -5 -2 1 2237.72 2220.87 9.75 o -4 -2 1 15.03 17.09 7.83 o -3 -2 1 3388.44 3318.89 11.45 o -2 -2 1 188.46 205.46 16.05 o -1 -2 1 1864.64 1814.35 13.24 o 0 -2 1 50.31 48.64 13.48 o 2 -2 1 342.44 359.64 6.23 o 3 -2 1 257.27 258.62 5.83 o 4 -2 1 45.75 41.63 13.22 o 5 -2 1 457.31 462.72 5.81 o -5 -1 1 57.02 61.86 5.01 o -4 -1 1 195.91 204.66 5.66 o -3 -1 1 85.35 72.37 4.81 o -2 -1 1 362.53 411.43 9.49 o -1 -1 1 119.66 160.82 11.38 o 0 -1 1 1131.23 1112.01 11.08 o 1 -1 1 130.34 135.64 9.32 o 2 -1 1 338.36 391.04 6.79 o 3 -1 1 67.99 67.67 5.62 o 4 -1 1 234.58 247.88 5.04 o 5 -1 1 43.18 39.63 6.40 o -5 0 1 173.51 158.17 5.55 o -4 0 1 15.60 35.25 8.71 o -3 0 1 342.94 336.97 9.19 o -2 0 1 2117.23 2186.64 62.54 o -1 0 1 329.11 357.55 8.90 o 1 0 1 395.02 425.65 10.88 o 2 0 1 131.69 123.68 6.58 o 3 0 1 114.86 110.16 5.84 o 4 0 1 106.47 114.25 8.47 o 5 0 1 44.76 46.40 5.41 o 6 0 1 25.85 17.02 6.22 o -5 1 1 11.02 16.43 5.41 o -4 1 1 359.79 352.81 5.05 o -3 1 1 2.87 2.02 7.85 o -2 1 1 1731.63 1774.91 30.13 o -1 1 1 2.99 -8.16 8.16 o 0 1 1 37.16 40.03 13.79 o 1 1 1 0.34 35.72 11.44 o 3 1 1 8.81 -4.43 9.26 o 4 1 1 284.19 290.74 5.83 o 5 1 1 8.91 -4.90 5.31 o 6 1 1 138.90 129.08 13.06 o -5 2 1 11.88 9.81 9.08 o -4 2 1 1644.92 1646.89 16.71 o -3 2 1 187.47 180.00 5.70 o -2 2 1 941.74 925.60 10.52 o -1 2 1 627.82 638.16 8.09 o 1 2 1 621.31 618.58 19.81 o 2 2 1 61.34 33.40 7.08 o 3 2 1 444.82 459.23 10.34 o 4 2 1 2270.82 2312.02 18.17 o 5 2 1 239.02 235.09 5.53 o 6 2 1 696.17 693.90 19.99 o -4 3 1 73.71 69.39 8.64 o -3 3 1 23.22 23.16 5.80 o -2 3 1 1033.43 1056.26 14.26 o -1 3 1 651.57 652.98 7.93 o 0 3 1 3.89 8.79 10.26 o 1 3 1 1473.76 1515.26 43.36 o 2 3 1 464.24 504.40 11.98 o 3 3 1 310.50 304.97 6.55 o 4 3 1 8.46 12.67 5.52 o 5 3 1 109.09 111.32 17.04 o 6 3 1 18.32 10.98 5.66 o -4 4 1 73.46 77.51 11.44 o -3 4 1 3062.22 3056.97 44.34 o -2 4 1 15.17 23.24 6.33 o -1 4 1 6690.25 6918.83 18.98 o 0 4 1 68.55 59.03 9.33 o 2 4 1 84.16 90.38 8.39 o 3 4 1 1642.45 1677.83 12.20 o 4 4 1 12.95 17.14 8.67 o 5 4 1 757.71 783.45 9.64 o -3 5 1 231.49 230.45 6.11 o -2 5 1 177.73 174.90 7.86 o -1 5 1 147.10 148.80 7.60 o 0 5 1 5.25 6.95 9.26 o 2 5 1 394.61 423.77 11.58 o 3 5 1 120.10 123.16 7.52 o 4 5 1 20.57 28.32 6.58 o 5 5 1 15.74 16.07 8.99 o -2 6 1 1022.01 1034.58 11.27 o -1 6 1 12.22 9.98 7.46 o 0 6 1 3857.58 3996.03 15.38 o 2 6 1 2335.79 2410.99 27.46 o 3 6 1 29.77 35.37 8.01 o 4 6 1 2446.25 2605.86 63.45 o -1 7 1 3.88 4.02 9.06 o 3 7 1 28.01 33.48 10.52 o -2 -7 2 28.87 25.60 9.42 o -1 -7 2 1014.86 1085.04 56.57 o 0 -7 2 20.54 26.21 6.81 o -3 -6 2 169.15 157.85 6.41 o -2 -6 2 6.77 10.92 8.82 o -1 -6 2 183.74 188.99 18.87 o 0 -6 2 260.79 262.35 12.34 o 1 -6 2 162.76 173.63 7.37 o 2 -6 2 56.25 51.76 5.76 o -4 -5 2 71.03 79.77 5.67 o -3 -5 2 28.47 42.04 8.93 o -2 -5 2 234.72 217.94 8.21 o -1 -5 2 18.63 33.15 5.96 o 0 -5 2 3.73 4.02 5.90 o 1 -5 2 42.67 42.70 6.22 o 2 -5 2 628.32 625.95 13.95 o 3 -5 2 28.58 38.27 5.62 o -5 -4 2 131.64 131.07 5.90 o -4 -4 2 244.60 256.47 31.09 o -3 -4 2 38.05 37.91 5.49 o -2 -4 2 1111.21 1144.42 9.52 o -1 -4 2 131.60 137.07 7.30 o 0 -4 2 48.02 51.57 5.82 o 1 -4 2 15.86 12.74 5.75 o 2 -4 2 26.42 40.33 5.96 o 3 -4 2 90.65 87.31 9.69 o 4 -4 2 2.50 -5.57 5.57 o -5 -3 2 21.58 15.72 5.23 o -4 -3 2 147.45 148.89 5.12 o -3 -3 2 44.76 50.19 10.02 o -2 -3 2 256.91 250.10 8.53 o -1 -3 2 195.93 205.70 10.06 o 0 -3 2 2708.12 2645.55 8.27 o 1 -3 2 51.14 54.97 5.82 o 2 -3 2 856.26 865.86 6.56 o 3 -3 2 195.91 205.20 10.96 o 4 -3 2 877.61 886.68 5.72 o 5 -3 2 112.14 112.21 5.39 o -5 -2 2 59.70 57.25 6.75 o -4 -2 2 267.93 255.92 7.87 o -3 -2 2 239.19 252.56 21.36 o -2 -2 2 1876.61 1945.05 179.80 o -1 -2 2 1525.15 1638.29 24.50 o 1 -2 2 1453.65 1464.77 7.69 o 2 -2 2 1718.55 1723.54 7.25 o 3 -2 2 190.53 189.77 5.81 o 4 -2 2 195.50 189.53 8.49 o 5 -2 2 40.74 56.33 15.10 o -5 -1 2 427.61 416.29 8.18 o -4 -1 2 66.01 66.37 7.63 o -3 -1 2 252.73 234.64 7.91 o -2 -1 2 309.26 341.68 35.56 o 0 -1 2 48.03 28.00 7.86 o 1 -1 2 2035.86 1840.86 8.60 o 2 -1 2 220.88 216.15 6.01 o 3 -1 2 3664.35 3640.53 14.56 o 4 -1 2 20.62 32.67 5.75 o 5 -1 2 2381.33 2444.68 31.19 o -5 0 2 1892.48 1887.07 15.54 o -4 0 2 304.98 295.56 14.63 o -3 0 2 1961.17 1892.84 8.97 o -2 0 2 159.10 136.26 8.40 o -1 0 2 3801.96 3719.28 229.51 o 0 0 2 358.06 317.07 10.29 o 1 0 2 6726.46 5957.68 124.10 o 2 0 2 9.55 6.20 6.47 o 3 0 2 4595.83 4573.12 57.21 o 4 0 2 84.05 69.91 5.68 o 5 0 2 1310.46 1323.68 8.41 o 6 0 2 104.67 96.97 5.28 o -5 1 2 10.18 11.77 5.60 o -4 1 2 1557.29 1514.32 6.13 o -3 1 2 154.43 150.83 6.80 o -2 1 2 894.96 845.54 7.83 o -1 1 2 622.29 612.68 10.14 o 0 1 2 3304.34 3291.99 200.99 o 1 1 2 691.82 658.05 9.68 o 3 1 2 538.93 542.64 8.21 o 4 1 2 2541.11 2601.30 17.48 o 5 1 2 320.68 322.65 7.35 o 6 1 2 823.24 828.13 9.97 o -4 2 2 1422.19 1416.88 6.44 o -3 2 2 5.58 8.37 5.47 o -2 2 2 2994.84 2951.42 16.96 o -1 2 2 0.36 -2.27 9.35 o 1 2 2 0.60 -4.72 10.42 o 2 2 2 2885.80 2802.94 64.35 o 3 2 2 4.91 4.07 5.98 o 4 2 2 1973.25 1996.28 17.11 o 5 2 2 15.52 13.51 5.39 o 6 2 2 1713.63 1722.73 14.15 o -4 3 2 10.84 8.20 5.49 o -3 3 2 40.22 34.88 5.60 o -2 3 2 369.76 381.39 6.60 o -1 3 2 302.22 312.73 7.23 o 0 3 2 489.77 547.56 31.92 o 2 3 2 46.57 41.18 8.28 o 3 3 2 649.48 668.11 17.04 o 4 3 2 45.28 50.96 5.89 o 5 3 2 538.33 553.85 5.88 o 6 3 2 30.65 22.35 5.73 o -3 4 2 982.43 986.52 6.95 o -2 4 2 142.23 137.40 6.80 o -1 4 2 1386.05 1353.42 9.13 o 2 4 2 342.39 366.44 15.44 o 3 4 2 199.29 199.39 7.66 o 4 4 2 49.86 47.98 10.64 o 5 4 2 234.44 237.12 5.98 o -3 5 2 8.52 13.99 6.64 o -2 5 2 60.53 58.58 6.73 o -1 5 2 71.12 57.49 7.95 o 3 5 2 261.94 271.86 14.00 o 4 5 2 96.78 110.69 9.62 o 5 5 2 27.45 35.08 9.00 o -2 6 2 3.77 9.17 7.19 o -1 6 2 97.53 104.88 12.52 o 4 6 2 61.23 62.89 8.30 o -2 -6 3 89.34 67.60 9.18 o -1 -6 3 25.84 27.25 6.74 o 0 -6 3 496.27 467.56 11.29 o 1 -6 3 6.56 2.33 5.94 o 2 -6 3 54.45 50.05 6.13 o -3 -5 3 1607.62 1552.06 81.57 o -2 -5 3 10.10 20.07 7.81 o -1 -5 3 2600.22 2676.73 168.62 o 0 -5 3 27.06 18.15 5.43 o 1 -5 3 1374.91 1360.58 14.30 o 2 -5 3 3.39 -4.60 5.52 o 3 -5 3 1539.71 1544.40 6.83 o -4 -4 3 119.59 131.73 9.18 o -3 -4 3 1030.86 1043.00 58.09 o -2 -4 3 154.46 136.63 8.14 o -1 -4 3 977.95 1048.54 46.37 o 0 -4 3 207.07 200.31 11.50 o 1 -4 3 1370.35 1385.35 6.88 o 2 -4 3 14.05 9.87 9.89 o 3 -4 3 775.73 782.94 10.29 o 4 -4 3 74.56 79.07 17.46 o -4 -3 3 492.49 509.91 55.07 o -3 -3 3 53.01 43.41 5.43 o -2 -3 3 4471.83 4375.87 12.36 o -1 -3 3 44.90 51.45 9.36 o 0 -3 3 3814.56 3675.72 8.51 o 1 -3 3 52.06 51.94 8.59 o 2 -3 3 4513.01 4422.74 56.87 o 3 -3 3 74.14 66.54 5.14 o 4 -3 3 534.95 547.37 5.89 o -5 -2 3 89.62 95.36 5.74 o -4 -2 3 816.47 892.74 91.27 o -3 -2 3 183.90 191.83 19.72 o -2 -2 3 786.07 807.07 40.72 o -1 -2 3 52.96 52.91 6.47 o 0 -2 3 2524.29 2476.22 31.28 o 1 -2 3 237.56 232.12 8.66 o 2 -2 3 208.48 200.13 5.51 o 3 -2 3 65.95 69.94 8.86 o 4 -2 3 120.19 117.18 5.50 o 5 -2 3 32.30 45.18 7.94 o -5 -1 3 495.87 485.29 7.42 o -4 -1 3 115.89 125.27 17.34 o -3 -1 3 152.96 177.22 18.63 o -2 -1 3 22.00 17.93 5.60 o -1 -1 3 429.16 448.00 15.37 o 0 -1 3 70.47 85.02 5.54 o 1 -1 3 1193.56 1183.99 20.66 o 2 -1 3 21.67 20.66 6.71 o 3 -1 3 1432.89 1429.37 11.53 o 4 -1 3 185.75 159.16 5.65 o 5 -1 3 323.39 324.78 8.64 o -5 0 3 18.70 10.59 7.04 o -4 0 3 54.38 42.41 7.55 o -3 0 3 9.89 21.13 7.74 o -2 0 3 103.09 108.13 19.04 o -1 0 3 509.85 550.86 9.25 o 0 0 3 465.02 492.85 12.03 o 1 0 3 2559.82 2544.57 70.75 o 2 0 3 225.67 255.88 20.33 o 3 0 3 635.50 619.28 9.08 o 4 0 3 162.82 141.81 5.04 o 5 0 3 10.24 3.15 5.42 o -4 1 3 55.78 52.96 7.76 o -3 1 3 33.19 17.53 7.71 o -2 1 3 981.17 995.94 9.15 o -1 1 3 669.97 681.16 52.05 o 0 1 3 4.11 -3.41 6.55 o 1 1 3 1450.54 1403.96 13.96 o 2 1 3 515.47 538.26 10.67 o 3 1 3 273.40 254.61 14.78 o 4 1 3 8.29 22.20 5.62 o 5 1 3 80.54 85.54 5.48 o 6 1 3 28.53 29.51 5.68 o -4 2 3 8.51 11.65 7.78 o -3 2 3 52.84 41.64 7.63 o -2 2 3 395.98 413.25 8.46 o -1 2 3 319.72 353.15 22.47 o 0 2 3 457.21 486.81 11.32 o 1 2 3 534.50 537.15 20.42 o 2 2 3 30.37 21.69 6.81 o 3 2 3 533.66 543.86 13.62 o 4 2 3 30.29 49.11 7.92 o 5 2 3 441.48 453.35 7.58 o 6 2 3 24.01 10.69 10.65 o -4 3 3 214.59 213.06 8.23 o -3 3 3 4.18 4.80 7.58 o -2 3 3 80.10 86.96 7.88 o -1 3 3 0.11 1.29 6.57 o 0 3 3 2813.04 2840.23 21.71 o 1 3 3 1.88 2.12 14.38 o 2 3 3 2914.43 2856.95 16.42 o 3 3 3 5.61 -5.55 6.35 o 4 3 3 3958.67 3962.64 85.65 o 5 3 3 12.25 11.51 6.04 o 6 3 3 440.30 433.20 6.38 o -3 4 3 7.55 16.30 8.88 o -2 4 3 1446.82 1461.39 11.26 o -1 4 3 2.08 8.38 10.39 o 0 4 3 1020.60 1013.05 13.03 o 3 4 3 61.78 68.30 8.03 o 4 4 3 636.66 630.57 32.37 o 5 4 3 39.50 38.11 5.86 o -2 5 3 283.65 283.39 10.14 o -1 5 3 936.43 1053.57 79.76 o 3 5 3 1552.64 1539.17 20.32 o 4 5 3 39.14 35.54 11.28 o 5 5 3 1486.14 1505.21 37.96 o -1 6 3 686.09 723.05 61.12 o 4 6 3 75.37 74.70 10.29 o -1 -6 4 541.91 495.95 22.07 o 0 -6 4 49.95 51.84 6.11 o -3 -5 4 654.48 605.52 37.61 o -2 -5 4 154.26 138.62 8.20 o -1 -5 4 47.72 60.37 10.21 o 0 -5 4 20.78 18.45 5.10 o 1 -5 4 23.00 27.38 5.58 o 2 -5 4 214.85 213.64 19.03 o -3 -4 4 7.04 3.14 5.58 o -2 -4 4 143.86 145.95 7.89 o -1 -4 4 35.27 32.85 5.45 o 0 -4 4 5.91 -4.48 7.79 o 1 -4 4 27.54 23.78 5.05 o 2 -4 4 152.13 153.47 11.58 o 3 -4 4 8.43 -6.17 6.17 o -4 -3 4 53.71 58.87 7.17 o -3 -3 4 868.87 849.17 61.34 o -2 -3 4 9.10 4.92 7.81 o -1 -3 4 1522.40 1593.57 57.23 o 0 -3 4 165.78 161.42 6.18 o 1 -3 4 1062.99 1068.53 22.22 o 2 -3 4 179.91 172.75 5.32 o 3 -3 4 1057.83 1044.10 22.19 o 4 -3 4 117.13 133.07 5.66 o -4 -2 4 1.90 -4.28 5.58 o -3 -2 4 122.43 124.75 5.49 o -2 -2 4 28.47 48.70 8.23 o -1 -2 4 17.92 11.37 9.19 o 0 -2 4 36.35 39.30 5.66 o 1 -2 4 108.52 111.20 5.02 o 2 -2 4 1001.30 985.92 17.18 o 3 -2 4 24.45 31.15 7.07 o 4 -2 4 173.74 161.56 5.24 o 5 -2 4 85.70 90.08 5.33 o -4 -1 4 1321.49 1397.59 130.28 o -3 -1 4 49.49 38.27 5.01 o -2 -1 4 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