#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104045.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104045_Fobs loop_ _publ_author_name 'Redhammer, G\"unther J.' 'Ohashi, Haruo' 'Roth, Georg' _publ_section_title ; Single-crystal structure refinement of NaTiSi~2~O~6~ clinopyroxene at low temperatures (298<T<100K) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 730 _journal_page_last 746 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.590 _cell_angle_beta 77.732 _cell_angle_gamma 77.760 _cell_length_a 5.2967 _cell_length_b 6.5099 _cell_length_c 6.6153 _exptl_crystal_F_000 218.00 _reflns_d_resolution_high 0.8504 _[local]_cod_data_source_file ws5001100sup17.hkl _[local]_cod_data_source_block 100 #BEGIN Tags that were not found in dictionaries: _shelx_title ' NaTiSi2O6, 100 K, kleiner Abstand, MODELL' _shelx_refln_list_code 4 _shelx_F_calc_maximum 82.26 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.14 -1.19 8.07 o 3 0 0 0.94 -2.40 4.74 o 4 0 0 3969.67 3938.33 12.30 o 5 0 0 3.44 -2.07 4.12 o -5 1 0 123.50 124.68 4.58 o -4 1 0 17.54 16.55 4.76 o -3 1 0 262.86 274.36 4.95 o -2 1 0 2210.34 2348.68 35.85 o -1 1 0 296.40 319.90 7.96 o 0 1 0 326.24 317.36 11.36 o 1 1 0 424.68 429.64 9.46 o 2 1 0 101.87 92.79 9.58 o 3 1 0 151.56 149.54 4.49 o 4 1 0 155.04 167.21 8.88 o 5 1 0 67.42 70.31 4.68 o 6 1 0 25.27 18.17 8.80 o -5 2 0 1659.31 1709.46 9.00 o -4 2 0 269.60 261.62 6.25 o -3 2 0 1831.73 1832.09 6.27 o -2 2 0 148.01 144.41 5.01 o -1 2 0 3685.81 3507.14 39.72 o 0 2 0 347.54 327.19 8.47 o 2 2 0 6.03 9.60 5.06 o 3 2 0 4774.74 4812.36 24.30 o 4 2 0 107.19 103.42 4.76 o 5 2 0 1389.32 1416.33 26.88 o 6 2 0 68.04 67.44 5.21 o -5 3 0 14.45 7.40 7.22 o -4 3 0 72.46 77.01 4.82 o -3 3 0 10.60 17.00 10.08 o -2 3 0 83.15 90.83 4.94 o -1 3 0 510.97 521.52 5.61 o 0 3 0 432.11 478.99 6.65 o 1 3 0 2461.53 2589.69 14.13 o 2 3 0 262.51 277.58 8.12 o 3 3 0 573.25 564.18 7.55 o 4 3 0 119.00 112.84 6.16 o 5 3 0 16.69 18.76 4.79 o -4 4 0 1149.43 1212.64 18.50 o -3 4 0 133.76 137.81 4.85 o -2 4 0 559.81 569.56 7.61 o -1 4 0 9.41 7.77 5.00 o 0 4 0 2225.10 2269.01 23.05 o 1 4 0 84.14 87.39 8.56 o 2 4 0 370.00 373.31 8.14 o 3 4 0 78.87 84.24 7.47 o 4 4 0 690.52 726.81 7.76 o 5 4 0 87.99 95.02 7.09 o -3 5 0 1.21 -5.19 5.19 o -2 5 0 11.51 8.69 5.00 o -1 5 0 178.28 199.70 5.60 o 0 5 0 6.80 7.60 5.64 o 1 5 0 136.07 135.59 8.08 o 2 5 0 24.66 38.34 5.65 o 3 5 0 218.72 207.33 8.40 o 4 5 0 107.78 102.49 7.65 o 5 5 0 110.47 113.05 8.21 o -2 6 0 35.25 35.79 5.03 o -1 6 0 6.28 9.48 5.36 o 0 6 0 82.62 83.57 7.62 o 1 6 0 6.31 4.78 8.25 o 2 6 0 1542.86 1558.81 45.98 o 3 6 0 30.54 35.56 6.39 o 4 6 0 471.81 494.28 9.38 o -1 7 0 115.41 121.73 5.97 o 0 7 0 816.42 876.29 9.30 o 1 7 0 79.83 84.25 8.91 o 2 7 0 337.69 345.72 23.89 o 3 7 0 76.31 87.28 6.89 o -2 -7 1 43.34 41.51 8.19 o -1 -7 1 276.10 315.21 9.25 o 0 -7 1 66.01 61.01 8.22 o 1 -7 1 754.81 778.35 9.28 o -4 -6 1 11.49 13.02 7.18 o -3 -6 1 1396.38 1414.85 39.97 o -2 -6 1 177.70 174.77 7.95 o -1 -6 1 1996.93 2049.77 10.38 o 0 -6 1 510.75 539.64 7.63 o 1 -6 1 1014.42 1006.47 49.13 o 2 -6 1 244.25 241.66 5.30 o -5 -5 1 20.11 15.92 7.36 o -4 -5 1 940.65 941.97 8.20 o -3 -5 1 17.05 21.85 7.30 o -2 -5 1 57.96 64.41 10.63 o -1 -5 1 16.56 19.12 6.93 o 0 -5 1 294.43 307.91 8.19 o 1 -5 1 3.80 1.59 4.80 o 2 -5 1 142.89 146.03 4.86 o 3 -5 1 10.73 13.74 4.58 o -5 -4 1 109.41 97.67 7.19 o -4 -4 1 1472.01 1508.17 8.57 o -3 -4 1 113.53 114.63 7.51 o -2 -4 1 3677.97 3390.29 11.28 o -1 -4 1 79.25 81.73 6.99 o 0 -4 1 1562.20 1515.08 9.23 o 1 -4 1 174.56 176.84 5.24 o 2 -4 1 3993.03 4073.28 7.91 o 3 -4 1 35.27 33.58 4.75 o 4 -4 1 1180.27 1247.94 6.31 o -5 -3 1 261.37 266.25 7.18 o -4 -3 1 227.79 223.89 6.97 o -3 -3 1 1338.34 1302.82 8.41 o -2 -3 1 17.39 20.71 7.34 o -1 -3 1 1106.30 1170.31 9.22 o 0 -3 1 70.01 82.91 5.39 o 1 -3 1 435.12 448.07 5.36 o 2 -3 1 34.61 33.27 6.73 o 3 -3 1 200.79 201.95 5.03 o 4 -3 1 161.15 156.18 4.88 o 5 -3 1 569.36 580.47 7.27 o -5 -2 1 2130.86 2189.36 10.52 o -4 -2 1 9.86 12.50 10.04 o -3 -2 1 3325.21 3230.06 23.22 o -2 -2 1 185.25 176.68 7.24 o 0 -2 1 48.58 54.17 6.32 o 2 -2 1 348.67 361.08 5.55 o 3 -2 1 268.98 257.29 6.33 o 4 -2 1 42.85 39.18 4.13 o 5 -2 1 445.93 446.57 15.81 o -5 -1 1 58.53 64.98 4.43 o -4 -1 1 188.01 193.03 4.59 o -3 -1 1 85.53 79.13 4.09 o -2 -1 1 363.71 429.25 7.49 o -1 -1 1 121.34 122.56 9.66 o 0 -1 1 1126.00 1123.17 13.83 o 1 -1 1 132.88 149.08 7.23 o 2 -1 1 337.37 394.08 5.07 o 3 -1 1 64.53 57.45 4.81 o 4 -1 1 227.64 247.65 8.67 o 5 -1 1 39.99 42.13 4.83 o -5 0 1 172.15 165.21 4.95 o -4 0 1 14.45 26.65 5.20 o -3 0 1 333.93 335.85 6.71 o -2 0 1 2088.61 2212.37 41.11 o -1 0 1 334.33 334.62 21.04 o 1 0 1 394.94 415.61 10.51 o 2 0 1 134.37 120.27 5.79 o 3 0 1 108.94 118.13 4.84 o 4 0 1 101.46 117.95 4.88 o 5 0 1 39.76 35.99 4.73 o 6 0 1 28.44 31.96 4.79 o -5 1 1 5.56 -4.52 4.91 o -4 1 1 350.16 354.12 4.67 o -3 1 1 1.60 3.86 4.29 o -2 1 1 1725.72 1752.09 22.03 o -1 1 1 0.87 -1.36 6.62 o 0 1 1 39.75 37.46 10.71 o 1 1 1 0.70 18.05 10.48 o 3 1 1 6.68 7.06 4.74 o 4 1 1 271.58 303.58 5.03 o 5 1 1 11.10 7.25 5.82 o 6 1 1 134.30 140.54 5.17 o -5 2 1 11.15 14.37 5.04 o -4 2 1 1605.25 1619.31 7.70 o -3 2 1 176.97 188.18 4.92 o -2 2 1 953.92 928.12 5.73 o -1 2 1 622.63 643.16 6.53 o 0 2 1 3219.04 3227.90 20.55 o 1 2 1 620.95 639.25 20.01 o 2 2 1 58.31 42.02 8.30 o 3 2 1 439.56 446.47 9.76 o 4 2 1 2194.81 2228.86 48.87 o 5 2 1 225.59 218.40 11.34 o 6 2 1 640.25 685.03 12.05 o -4 3 1 70.44 75.39 4.88 o -3 3 1 20.80 8.71 4.70 o -2 3 1 1010.42 1067.16 24.36 o -1 3 1 639.50 651.51 15.87 o 0 3 1 5.23 1.70 6.76 o 1 3 1 1468.13 1485.28 17.16 o 2 3 1 456.01 488.65 10.32 o 3 3 1 320.14 305.28 5.91 o 4 3 1 10.34 9.50 8.92 o 5 3 1 109.77 108.17 5.06 o 6 3 1 16.03 20.40 5.12 o -4 4 1 67.54 71.30 5.11 o -3 4 1 2948.34 3023.19 46.48 o -2 4 1 12.59 17.76 6.92 o -1 4 1 6582.47 6752.19 83.10 o 0 4 1 67.83 62.90 6.80 o 2 4 1 81.98 80.85 10.01 o 3 4 1 1596.70 1632.05 11.13 o 4 4 1 11.19 20.08 8.16 o 5 4 1 718.41 755.50 14.59 o -3 5 1 218.60 233.62 10.02 o -2 5 1 173.28 179.00 5.23 o -1 5 1 143.10 149.80 5.93 o 0 5 1 4.38 3.06 6.14 o 1 5 1 0.32 9.73 10.23 o 2 5 1 381.87 410.34 7.87 o 3 5 1 121.13 123.34 8.97 o 4 5 1 24.65 23.27 8.24 o 5 5 1 21.83 15.32 8.82 o -2 6 1 980.40 1000.65 8.57 o -1 6 1 11.54 9.44 5.67 o 0 6 1 3721.75 3906.70 14.19 o 1 6 1 3.51 7.83 9.53 o 2 6 1 2247.69 2323.04 35.43 o 3 6 1 28.46 28.30 6.84 o 4 6 1 2350.64 2478.30 13.07 o -1 7 1 4.26 4.47 6.38 o 0 7 1 122.27 130.68 9.66 o 1 7 1 70.02 69.92 10.18 o 2 7 1 49.07 53.13 8.38 o 3 7 1 29.08 39.88 7.90 o -2 -7 2 21.98 27.64 8.39 o -1 -7 2 974.38 943.88 9.42 o 0 -7 2 18.58 20.03 8.30 o -3 -6 2 153.53 142.66 9.38 o -2 -6 2 8.01 10.95 7.03 o -1 -6 2 167.40 176.64 7.85 o 0 -6 2 244.58 256.87 7.27 o 1 -6 2 148.80 149.56 9.66 o 2 -6 2 53.20 52.91 5.15 o -4 -5 2 67.78 65.31 7.11 o -3 -5 2 24.30 30.85 6.74 o -2 -5 2 228.01 223.56 7.02 o -1 -5 2 11.76 22.80 6.92 o 0 -5 2 1.35 2.68 6.84 o 1 -5 2 32.53 46.40 5.07 o 2 -5 2 614.90 592.88 11.01 o 3 -5 2 24.38 25.77 4.67 o -5 -4 2 123.94 123.13 7.46 o -4 -4 2 237.82 231.23 7.04 o -3 -4 2 40.89 48.72 6.68 o -2 -4 2 1064.15 1003.95 7.96 o -1 -4 2 130.63 141.85 7.05 o 0 -4 2 40.23 41.51 6.96 o 1 -4 2 17.65 20.81 8.03 o 2 -4 2 28.80 32.21 5.27 o 3 -4 2 89.33 92.00 4.16 o 4 -4 2 2.76 0.41 5.04 o -5 -3 2 18.96 26.55 7.07 o -4 -3 2 139.39 138.85 6.81 o -3 -3 2 39.31 39.37 6.59 o -2 -3 2 245.36 230.74 6.95 o 0 -3 2 2651.47 2621.30 9.79 o 1 -3 2 48.17 49.23 4.49 o 2 -3 2 812.52 844.30 5.24 o 3 -3 2 194.53 205.12 13.80 o 4 -3 2 828.07 863.06 17.45 o 5 -3 2 104.67 102.20 6.62 o -5 -2 2 56.49 57.30 4.33 o -4 -2 2 272.47 262.78 6.06 o -3 -2 2 235.50 227.09 6.88 o -2 -2 2 1885.00 1712.01 8.88 o 0 -2 2 114.36 67.60 7.63 o 1 -2 2 1399.69 1457.66 13.97 o 2 -2 2 1672.56 1688.34 12.72 o 3 -2 2 175.33 178.21 4.62 o 4 -2 2 186.71 204.13 9.90 o 5 -2 2 36.07 44.55 5.33 o -5 -1 2 405.99 393.52 4.85 o -4 -1 2 66.28 64.62 4.08 o -3 -1 2 242.44 222.55 5.67 o -2 -1 2 303.78 296.87 7.16 o -1 -1 2 31.22 12.10 6.38 o 0 -1 2 46.90 53.56 8.75 o 1 -1 2 2047.59 1884.53 55.71 o 2 -1 2 216.97 222.74 4.93 o 3 -1 2 3607.13 3636.32 25.41 o 4 -1 2 14.90 15.11 4.51 o 5 -1 2 2297.07 2376.60 23.92 o -5 0 2 1813.15 1858.06 42.49 o -4 0 2 295.62 275.20 4.57 o -3 0 2 1945.33 1937.33 9.93 o -2 0 2 159.52 150.57 7.20 o -1 0 2 3792.42 3345.74 12.83 o 1 0 2 6692.63 6051.45 54.62 o 2 0 2 7.61 7.16 5.27 o 3 0 2 4503.68 4524.74 10.40 o 4 0 2 76.30 83.32 4.52 o 5 0 2 1239.40 1293.55 12.60 o 6 0 2 100.02 95.01 4.54 o -5 1 2 9.78 16.35 6.74 o -4 1 2 1487.00 1524.98 22.66 o -3 1 2 143.64 138.76 4.22 o -2 1 2 874.58 845.88 5.29 o -1 1 2 608.85 623.61 6.61 o 0 1 2 3277.66 2985.74 15.94 o 1 1 2 693.33 689.54 8.99 o 2 1 2 95.80 64.74 5.96 o 3 1 2 552.72 577.34 5.76 o 4 1 2 2521.49 2613.45 19.33 o 5 1 2 314.59 317.62 5.00 o 6 1 2 794.36 803.52 22.15 o -4 2 2 1363.03 1394.45 12.50 o -3 2 2 2.41 9.49 6.36 o -2 2 2 2945.41 2912.92 18.21 o -1 2 2 0.88 0.28 5.42 o 2 2 2 2868.30 2773.81 20.51 o 3 2 2 6.14 4.41 5.19 o 4 2 2 1923.99 1945.41 14.91 o 5 2 2 10.55 12.59 4.71 o 6 2 2 1634.86 1675.26 19.45 o -4 3 2 14.92 23.65 11.19 o -3 3 2 38.20 31.96 4.96 o -2 3 2 354.77 390.86 5.42 o -1 3 2 287.04 313.44 6.12 o 0 3 2 477.74 512.45 8.57 o 2 3 2 50.22 49.86 13.16 o 3 3 2 635.50 677.49 22.18 o 4 3 2 47.30 42.79 5.36 o 5 3 2 535.50 573.19 15.41 o 6 3 2 31.80 26.42 5.18 o -3 4 2 922.51 981.52 20.65 o -2 4 2 135.00 130.62 8.91 o -1 4 2 1327.45 1343.23 25.61 o 0 4 2 5.06 4.40 6.65 o 3 4 2 196.00 212.37 10.07 o 4 4 2 43.94 43.36 5.90 o 5 4 2 223.06 238.26 7.00 o -3 5 2 9.71 17.72 9.52 o -2 5 2 56.58 56.71 6.62 o -1 5 2 65.26 68.62 5.81 o 0 5 2 129.91 142.68 7.20 o 3 5 2 252.87 268.25 13.77 o 4 5 2 96.27 115.38 9.78 o 5 5 2 25.67 33.63 8.84 o -2 6 2 2.19 14.57 6.10 o -1 6 2 96.33 110.25 6.10 o 0 6 2 11.10 9.51 6.93 o 4 6 2 55.00 62.77 11.90 o 0 7 2 102.12 123.18 11.02 o -2 -6 3 93.87 87.59 7.29 o -1 -6 3 22.94 13.29 7.04 o 0 -6 3 482.88 416.68 7.60 o 1 -6 3 2.04 -0.03 7.25 o 2 -6 3 50.09 24.17 9.20 o -2 -5 3 7.25 -1.98 6.84 o -1 -5 3 2490.85 2569.15 9.65 o 0 -5 3 27.55 12.67 6.77 o 1 -5 3 1326.87 1332.50 8.36 o 2 -5 3 3.98 8.66 4.91 o 3 -5 3 1487.02 1191.78 241.65 o -4 -4 3 110.50 101.38 7.13 o -3 -4 3 979.74 918.80 7.84 o -2 -4 3 145.75 112.48 6.71 o -1 -4 3 940.25 967.42 8.12 o 0 -4 3 202.01 196.03 7.23 o 1 -4 3 1330.74 1355.58 43.71 o 2 -4 3 8.26 12.67 15.14 o 3 -4 3 735.37 731.62 5.43 o 4 -4 3 61.87 64.24 9.89 o -4 -3 3 467.41 429.97 7.31 o -3 -3 3 50.85 40.27 5.73 o -2 -3 3 4381.10 3926.03 10.75 o -1 -3 3 43.16 29.96 6.77 o 0 -3 3 3759.74 3681.72 10.98 o 1 -3 3 50.86 46.09 4.60 o 2 -3 3 4410.62 4332.74 118.41 o 3 -3 3 74.23 73.68 10.52 o 4 -3 3 525.70 520.29 13.98 o -5 -2 3 82.04 86.21 7.33 o -4 -2 3 783.47 760.30 7.56 o -3 -2 3 176.18 161.28 6.79 o -2 -2 3 760.10 725.29 6.68 o 0 -2 3 2453.05 2410.35 9.98 o 1 -2 3 240.32 241.11 5.12 o 2 -2 3 195.50 194.32 10.58 o 3 -2 3 61.47 64.97 4.85 o 4 -2 3 114.62 103.93 12.78 o 5 -2 3 31.21 32.45 4.65 o -5 -1 3 463.88 459.11 6.79 o -4 -1 3 114.31 114.77 6.84 o -3 -1 3 146.71 139.67 6.80 o -2 -1 3 24.64 40.65 6.52 o 0 -1 3 61.68 74.74 7.35 o 1 -1 3 1201.64 1216.04 16.24 o 2 -1 3 25.97 25.62 4.77 o 3 -1 3 1415.83 1427.89 6.08 o 4 -1 3 174.67 170.66 12.00 o 5 -1 3 302.95 323.19 5.79 o -5 0 3 17.76 18.97 5.85 o -4 0 3 49.62 48.35 7.79 o -3 0 3 9.82 10.80 4.38 o -2 0 3 104.09 101.19 6.59 o -1 0 3 500.00 467.84 7.48 o 1 0 3 2551.60 2567.92 11.48 o 2 0 3 225.75 244.34 8.21 o 3 0 3 623.78 604.70 17.73 o 4 0 3 159.90 156.24 4.90 o 5 0 3 10.12 2.56 4.84 o -4 1 3 49.73 55.29 4.45 o -3 1 3 29.96 38.81 5.16 o -2 1 3 958.86 973.40 20.51 o -1 1 3 659.81 644.17 7.87 o 0 1 3 4.07 3.54 7.86 o 1 1 3 1419.68 1384.72 11.13 o 2 1 3 525.45 549.70 7.99 o 3 1 3 261.37 253.20 8.02 o 4 1 3 9.58 10.30 5.32 o 5 1 3 76.55 80.49 5.74 o 6 1 3 27.20 34.72 8.53 o -4 2 3 11.35 13.20 4.56 o -3 2 3 56.41 50.81 4.69 o -2 2 3 393.16 405.80 5.10 o -1 2 3 310.94 325.71 7.10 o 0 2 3 442.40 472.39 9.30 o 1 2 3 508.58 519.65 11.95 o 2 2 3 30.30 27.71 6.54 o 3 2 3 506.37 532.24 6.30 o 4 2 3 29.65 38.73 5.37 o 5 2 3 414.07 448.74 10.39 o 6 2 3 23.32 14.99 5.20 o -4 3 3 200.70 195.52 5.25 o -3 3 3 3.86 -0.07 7.26 o -2 3 3 76.21 75.13 5.32 o -1 3 3 0.01 3.04 5.45 o 0 3 3 2752.51 2859.44 15.16 o 3 3 3 8.29 5.54 6.41 o 4 3 3 3853.40 3903.51 79.92 o 5 3 3 8.37 5.24 5.38 o 6 3 3 419.75 428.91 12.86 o -3 4 3 8.45 12.08 9.31 o -2 4 3 1390.99 1436.81 6.69 o -1 4 3 2.16 17.55 5.73 o 0 4 3 981.26 997.12 12.43 o 3 4 3 57.25 65.28 15.98 o 4 4 3 588.76 609.97 24.46 o 5 4 3 34.59 38.00 6.08 o -2 5 3 278.32 292.70 5.88 o -1 5 3 900.93 958.92 9.84 o 0 5 3 20.74 18.63 7.77 o 4 5 3 39.63 44.74 13.26 o 5 5 3 1439.96 1548.88 12.33 o -1 6 3 645.87 672.80 7.43 o -1 -6 4 490.99 446.45 7.90 o 0 -6 4 43.20 28.01 7.45 o -2 -5 4 142.37 124.36 5.09 o -1 -5 4 42.47 40.27 6.99 o 0 -5 4 15.09 22.03 6.99 o 1 -5 4 11.69 7.62 7.07 o 2 -5 4 191.62 173.93 54.98 o -3 -4 4 8.23 9.34 6.97 o -2 -4 4 129.79 119.99 6.82 o -1 -4 4 37.50 34.64 5.84 o 0 -4 4 8.32 1.20 5.86 o 1 -4 4 27.44 23.49 6.78 o 2 -4 4 132.88 138.54 4.96 o 3 -4 4 9.14 5.43 4.96 o -4 -3 4 47.02 35.82 7.18 o -3 -3 4 822.27 730.57 7.64 o -2 -3 4 5.12 6.20 5.71 o -1 -3 4 1471.75 1486.53 8.59 o 0 -3 4 158.49 147.61 6.14 o 1 -3 4 1022.88 1020.38 8.00 o 2 -3 4 171.20 181.92 4.94 o 3 -3 4 992.33 1036.92 44.46 o 4 -3 4 104.46 104.09 5.08 o -4 -2 4 2.11 15.52 6.04 o -3 -2 4 122.53 109.40 5.91 o -2 -2 4 28.20 25.79 6.57 o 0 -2 4 32.45 43.58 6.85 o 1 -2 4 107.68 92.88 6.01 o 2 -2 4 957.14 1010.97 29.15 o 3 -2 4 24.24 30.50 7.19 o 4 -2 4 158.25 167.90 4.97 o 5 -2 4 75.34 69.14 4.90 o -4 -1 4 1242.59 1260.63 8.29 o -3 -1 4 41.67 36.19 6.65 o -2 -1 4 4118.53 3790.60 10.50 o -1 -1 4 167.00 162.56 5.77 o 0 -1 4 1589.52 1553.17 8.89 o 1 -1 4 76.05 80.04 6.88 o 2 -1 4 3820.47 3862.63 70.25 o 3 -1 4 109.94 125.19 4.60 o 4 -1 4 1540.75 1578.66 45.08 o 5 -1 4 95.83 84.58 5.09 o -4 0 4 1253.03 1229.51 8.23 o -3 0 4 120.64 123.36 6.60 o -2 0 4 579.53 560.87 7.37 o -1 0 4 10.32 5.97 6.57 o 1 0 4 124.80 117.97 7.03 o 2 0 4 297.59 312.55 6.41 o 3 0 4 49.77 45.21 6.32 o 4 0 4 554.52 558.63 17.88 o 5 0 4 52.66 54.92 5.88 o -4 1 4 60.97 58.69 7.16 o -3 1 4 2949.67 2888.23 9.71 o -2 1 4 14.70 22.73 6.54 o -1 1 4 6766.53 6355.19 13.66 o 0 1 4 80.94 75.03 7.37 o 1 1 4 4585.32 4270.73 13.66 o 2 1 4 108.69 118.23 5.57 o 3 1 4 1727.53 1726.41 32.14 o 4 1 4 18.90 16.44 5.01 o 5 1 4 832.56 885.00 5.91 o -4 2 4 40.31 43.20 4.81 o -3 2 4 947.99 1001.46 5.63 o -2 2 4 131.42 109.03 6.69 o -1 2 4 1299.79 1236.08 9.27 o 0 2 4 7.17 10.74 7.32 o 1 2 4 640.44 577.65 10.18 o 2 2 4 294.99 283.91 8.83 o 3 2 4 140.66 137.63 5.85 o 4 2 4 67.97 64.59 5.32 o 5 2 4 163.71 165.87 5.58 o -3 3 4 5.82 18.81 5.67 o -2 3 4 1387.40 1424.49 34.41 o -1 3 4 3.49 10.41 7.48 o 0 3 4 1059.15 1047.65 10.88 o 1 3 4 44.46 46.55 7.87 o 3 3 4 93.45 105.70 7.35 o 4 3 4 720.23 746.13 8.95 o 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