#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104085.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104085_Fobs loop_ _publ_author_name 'Hansson, Christian' 'Lindqvist, Maria' 'Oskarsson, \%Ake' _publ_section_title ; Cis/trans isomers of PtX~2~L~2~ (X = halogen, L = neutral ligand); the crystal structures of two polymorphs of cis-dichlorobis(dibenzyl sulfido-\kS)platinum(II) in the temperature range 100--295K ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 187 _journal_page_last 195 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.022 _cell_angle_beta 89.222 _cell_angle_gamma 71.433 _cell_length_a 8.3411 _cell_length_b 12.2228 _cell_length_c 15.8547 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.6597 _[local]_cod_data_source_file ry5016abtri250sup3.hkl _[local]_cod_data_source_block abtri250 #BEGIN Tags that were not found in dictionaries: _shelx_title ' abtri2500 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 265.98 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14569.49 16262.89 145.49 o 2 0 0 2264.11 2356.90 47.77 o 3 0 0 28.96 12.79 11.67 o 4 0 0 3250.19 3270.37 59.36 o 5 0 0 1522.74 1613.13 27.10 o 6 0 0 2477.31 2444.83 24.22 o 7 0 0 4786.84 4950.86 75.49 o 8 0 0 287.00 325.99 43.24 o 9 0 0 2.53 38.43 44.61 o 10 0 0 343.43 386.38 60.39 o 11 0 0 633.56 622.46 74.12 o -11 1 0 492.05 516.09 75.49 o -10 1 0 554.60 600.50 67.26 o -9 1 0 161.90 236.08 51.47 o -8 1 0 107.46 240.89 43.92 o -7 1 0 1219.06 1308.74 52.16 o -6 1 0 3709.04 3562.50 62.45 o -5 1 0 1614.04 1549.95 31.57 o -4 1 0 9390.09 8693.15 214.12 o -3 1 0 4876.42 4834.19 106.37 o -2 1 0 700.68 796.96 36.03 o -1 1 0 3079.50 3194.42 14.97 o 1 1 0 21840.99 22210.22 739.26 o 2 1 0 19797.31 19569.31 149.91 o 3 1 0 10229.49 10271.81 31.33 o 4 1 0 544.20 438.86 23.05 o 5 1 0 158.12 122.38 9.92 o 6 1 0 1300.78 1300.58 47.01 o 7 1 0 5921.42 6021.50 262.50 o 8 1 0 870.14 915.50 50.10 o 9 1 0 227.06 185.98 45.29 o 10 1 0 3.51 80.98 52.16 o 11 1 0 258.70 317.06 65.88 o -10 2 0 322.37 338.34 68.63 o -9 2 0 195.19 225.79 54.90 o -8 2 0 732.13 779.62 56.96 o -7 2 0 130.60 242.26 41.86 o -6 2 0 1527.93 1540.71 50.10 o -5 2 0 2396.33 2092.16 178.78 o -4 2 0 15641.30 14126.87 1047.61 o -3 2 0 6171.58 5085.02 633.78 o -2 2 0 1652.40 1796.20 16.89 o 0 2 0 14905.84 15352.38 354.81 o 1 2 0 13694.21 14526.79 111.01 o 2 2 0 1477.00 1631.54 23.97 o 3 2 0 27031.98 27566.74 723.81 o 4 2 0 7973.95 7820.30 123.53 o 5 2 0 158.25 120.67 19.28 o 6 2 0 939.59 890.23 23.84 o 7 2 0 4538.51 4491.29 196.62 o 8 2 0 1473.10 1373.94 54.22 o 9 2 0 310.35 313.63 45.98 o 10 2 0 226.31 206.57 52.16 o 11 2 0 7.85 52.84 59.02 o -10 3 0 186.67 55.59 71.37 o -9 3 0 108.04 24.02 58.33 o -8 3 0 781.84 881.19 61.77 o -7 3 0 1098.06 1246.98 57.65 o -6 3 0 27.63 32.26 35.00 o -5 3 0 281.09 300.59 32.94 o -4 3 0 10172.88 8684.90 1167.03 o -3 3 0 18696.74 18725.28 103.63 o -2 3 0 8968.65 9327.98 65.88 o 0 3 0 303.47 344.56 8.08 o 1 3 0 11665.76 11948.54 205.89 o 2 3 0 952.93 957.00 8.72 o 3 3 0 12115.30 12769.22 175.69 o 4 3 0 11527.54 11148.75 83.04 o 5 3 0 5309.91 4741.79 43.62 o 6 3 0 9.54 6.18 25.39 o 7 3 0 2313.94 2188.93 31.22 o 8 3 0 2214.72 2164.01 84.41 o 9 3 0 534.53 548.34 48.04 o 10 3 0 676.89 645.11 56.28 o 11 3 0 323.19 293.73 59.02 o -9 4 0 114.79 93.33 60.39 o -8 4 0 830.23 862.66 65.88 o -7 4 0 1453.35 1503.65 63.82 o -6 4 0 214.98 163.34 40.49 o -5 4 0 22.22 19.90 32.94 o -4 4 0 596.19 601.19 35.00 o -3 4 0 7197.16 7339.13 72.06 o -2 4 0 10301.51 11000.46 78.92 o 0 4 0 11057.61 10688.35 510.60 o 1 4 0 1391.67 1617.33 24.02 o 2 4 0 102.57 83.56 5.43 o 3 4 0 8699.01 9121.66 141.55 o 4 4 0 11208.01 11315.76 272.90 o 5 4 0 5487.10 5457.77 36.94 o 6 4 0 1721.93 1689.07 28.92 o 7 4 0 158.93 156.47 32.26 o 8 4 0 599.26 501.38 25.55 o 9 4 0 915.02 858.54 50.79 o 10 4 0 1364.78 1169.43 63.14 o 11 4 0 904.51 731.58 68.63 o 12 4 0 113.60 2.06 63.14 o -9 5 0 13.45 31.57 63.14 o -8 5 0 551.65 462.56 64.51 o -7 5 0 1753.03 1789.83 71.37 o -6 5 0 803.39 756.29 52.16 o -5 5 0 486.69 573.05 41.86 o -4 5 0 532.00 556.58 37.06 o -3 5 0 580.72 562.75 32.94 o -2 5 0 1249.41 1262.76 36.37 o -1 5 0 18864.37 18030.07 85.10 o 0 5 0 21534.54 21548.85 1105.95 o 1 5 0 9300.77 9307.30 218.92 o 2 5 0 73.79 59.76 7.91 o 3 5 0 87.38 70.26 12.56 o 4 5 0 2464.68 2421.86 17.21 o 5 5 0 2850.18 2896.29 35.06 o 6 5 0 2266.80 2358.36 33.71 o 7 5 0 1916.48 1901.59 32.60 o 8 5 0 373.02 335.26 24.56 o 9 5 0 151.29 108.09 45.64 o 10 5 0 1068.67 1001.98 61.08 o 11 5 0 1517.96 1309.43 75.49 o 12 5 0 388.18 339.71 67.26 o -8 6 0 31.70 120.79 60.39 o -7 6 0 805.93 765.21 63.14 o -6 6 0 1257.53 1353.35 61.08 o -5 6 0 1234.90 1194.14 54.90 o -4 6 0 2343.07 2538.57 60.39 o -3 6 0 588.48 595.70 37.75 o -2 6 0 7.20 -2.94 14.82 o -1 6 0 2400.98 2482.98 39.80 o 0 6 0 9944.26 10055.23 422.75 o 1 6 0 13067.12 12796.84 385.01 o 2 6 0 4597.94 4717.01 100.88 o 3 6 0 369.58 346.24 15.72 o 4 6 0 1176.59 1196.85 21.98 o 5 6 0 1724.57 1670.38 36.06 o 6 6 0 2488.42 2509.35 54.90 o 7 6 0 2714.09 2653.23 77.55 o 8 6 0 1304.23 1310.57 57.65 o 9 6 0 21.89 12.35 38.43 o 10 6 0 71.63 74.12 47.35 o 11 6 0 732.78 631.38 64.51 o 12 6 0 518.23 450.20 67.94 o -8 7 0 40.80 39.80 63.14 o -7 7 0 38.45 70.88 33.64 o -6 7 0 432.41 367.16 54.90 o -5 7 0 1525.76 1675.22 63.82 o -4 7 0 3965.83 3934.09 47.70 o -3 7 0 2365.59 2490.42 68.63 o -2 7 0 293.23 311.57 33.97 o -1 7 0 41.08 51.47 21.96 o 0 7 0 2178.40 2098.12 48.38 o 1 7 0 2569.57 2589.78 27.46 o 2 7 0 3675.39 3844.47 163.68 o 3 7 0 7942.50 8060.58 172.60 o 4 7 0 1713.35 1751.19 27.26 o 5 7 0 957.17 868.79 23.50 o 6 7 0 3138.50 3279.86 37.33 o 7 7 0 4346.43 4591.18 46.22 o 8 7 0 2416.38 2397.89 53.87 o 9 7 0 257.94 241.01 27.20 o 10 7 0 94.21 52.84 46.67 o 11 7 0 24.13 17.84 54.90 o 12 7 0 162.06 120.10 61.77 o -7 8 0 58.34 54.43 36.53 o -6 8 0 18.65 24.71 38.43 o -5 8 0 339.82 372.08 35.34 o -4 8 0 2592.56 2650.40 105.00 o -3 8 0 4866.60 4839.28 187.36 o -2 8 0 1207.62 1395.60 148.92 o -1 8 0 421.44 443.34 29.51 o 0 8 0 42.82 58.33 24.71 o 1 8 0 659.28 645.42 76.52 o 2 8 0 792.04 868.49 25.05 o 3 8 0 4998.51 5213.26 92.31 o 4 8 0 4926.60 5029.76 42.99 o 5 8 0 793.52 719.69 29.17 o 6 8 0 108.92 90.74 19.65 o 7 8 0 2645.78 2713.55 79.95 o 8 8 0 2790.09 3025.29 62.79 o 9 8 0 697.12 707.29 35.00 o 10 8 0 515.10 478.02 35.25 o 11 8 0 143.83 80.30 57.65 o 12 8 0 3.45 5.49 62.45 o -7 9 0 223.46 217.13 41.87 o -6 9 0 34.18 50.10 43.92 o -5 9 0 0.76 3.43 49.41 o -4 9 0 332.25 327.32 32.12 o -3 9 0 2127.16 2203.58 43.58 o -2 9 0 2476.63 2692.98 179.12 o -1 9 0 3083.16 3052.59 58.33 o 0 9 0 1151.55 1087.76 41.86 o 1 9 0 217.26 230.39 19.25 o 2 9 0 777.55 804.36 23.16 o 3 9 0 2268.91 2415.94 33.32 o 4 9 0 2941.36 3119.38 111.86 o 5 9 0 486.13 532.98 23.93 o 6 9 0 369.41 321.52 23.53 o 7 9 0 37.55 3.43 33.63 o 8 9 0 1200.25 1122.83 33.52 o 9 9 0 1100.20 1137.11 38.01 o 10 9 0 1110.63 1153.64 135.20 o 11 9 0 580.23 600.50 65.20 o -7 10 0 310.01 323.93 61.08 o -6 10 0 153.78 117.62 40.23 o -5 10 0 73.92 39.96 34.44 o -4 10 0 24.20 21.57 31.00 o -3 10 0 239.94 238.97 31.63 o -2 10 0 386.73 399.98 31.00 o -1 10 0 1837.89 1922.28 52.84 o 0 10 0 4593.23 4388.79 69.31 o 1 10 0 796.44 895.51 58.68 o 2 10 0 1.29 -1.93 19.13 o 3 10 0 1630.31 1663.33 32.96 o 4 10 0 4046.51 4170.14 139.66 o 5 10 0 1024.72 1124.14 30.88 o 6 10 0 1106.52 1160.19 94.71 o 7 10 0 525.44 493.23 35.34 o 8 10 0 6.54 -5.49 36.37 o 9 10 0 318.08 253.93 45.29 o 10 10 0 1087.76 1176.29 61.08 o 11 10 0 1095.77 1074.23 48.68 o -6 11 0 243.73 177.75 59.71 o -5 11 0 189.72 172.78 41.72 o -4 11 0 241.82 227.28 37.26 o -3 11 0 1.30 21.26 32.43 o -1 11 0 246.91 207.94 38.43 o 0 11 0 1792.56 1754.83 56.28 o 1 11 0 1270.25 1218.16 49.41 o 2 11 0 425.60 403.84 26.08 o 3 11 0 16.49 26.00 24.02 o 4 11 0 1099.33 1096.15 33.88 o 5 11 0 913.01 970.85 32.90 o 6 11 0 1222.32 1354.08 119.76 o 7 11 0 1468.98 1488.80 158.87 o 8 11 0 307.42 258.50 59.02 o 10 11 0 165.12 102.94 50.79 o 11 11 0 588.30 625.89 63.14 o -5 12 0 217.99 231.28 61.08 o -4 12 0 482.87 519.79 45.17 o -3 12 0 145.88 175.62 38.68 o -2 12 0 0.21 -4.12 52.16 o -1 12 0 24.62 61.77 41.86 o 0 12 0 711.62 713.05 48.04 o 1 12 0 532.43 521.58 46.67 o 2 12 0 471.21 460.51 29.61 o 3 12 0 594.33 606.59 32.20 o 4 12 0 14.93 21.67 26.68 o 5 12 0 559.52 499.53 31.76 o 6 12 0 1375.08 1421.14 93.68 o 7 12 0 1806.65 1857.67 163.68 o 8 12 0 625.19 603.79 83.38 o 9 12 0 93.09 103.63 47.35 o -4 13 0 309.67 433.73 74.81 o -3 13 0 427.16 444.21 66.57 o -2 13 0 110.64 110.60 39.17 o -1 13 0 25.28 43.92 48.73 o 0 13 0 154.60 194.90 45.29 o 1 13 0 328.56 275.89 48.04 o 2 13 0 395.94 398.05 46.67 o 3 13 0 759.89 833.80 43.58 o 4 13 0 466.09 469.81 32.69 o 5 13 0 3.00 17.84 39.12 o 6 13 0 263.95 246.72 33.70 o 7 13 0 1455.32 1396.59 53.53 o 8 13 0 1058.52 1159.31 163.68 o 9 13 0 294.23 352.06 54.90 o 10 13 0 61.94 35.69 56.28 o -2 14 0 197.35 167.48 45.42 o -1 14 0 232.49 214.52 45.98 o 0 14 0 6.58 98.82 50.10 o 1 14 0 121.11 137.94 49.41 o 2 14 0 196.34 155.79 48.04 o 3 14 0 435.90 438.54 51.47 o 4 14 0 670.64 649.66 37.62 o 5 14 0 254.05 257.07 34.85 o 6 14 0 20.90 18.26 34.15 o 7 14 0 99.82 109.71 36.15 o 8 14 0 590.63 605.17 73.78 o 9 14 0 625.90 697.27 63.82 o -1 15 0 163.43 81.53 65.20 o 0 15 0 193.35 181.87 57.65 o 2 15 0 127.29 103.63 54.22 o 3 15 0 392.03 341.77 59.02 o 4 15 0 392.44 433.05 60.39 o 5 15 0 205.38 218.14 38.19 o 6 15 0 95.47 81.67 36.52 o 7 15 0 63.35 34.01 38.09 o 8 15 0 8.74 19.22 55.59 o 2 16 0 6.66 19.90 59.71 o 3 16 0 62.34 72.06 57.65 o 4 16 0 428.61 472.85 65.20 o 5 16 0 549.13 590.20 67.26 o 6 16 0 146.02 150.05 51.81 o 7 16 0 127.80 120.79 61.08 o -7 -16 1 87.61 43.24 62.45 o -6 -16 1 57.52 26.08 59.71 o -5 -16 1 12.45 87.84 63.82 o -4 -16 1 361.67 455.01 67.26 o -3 -16 1 455.28 503.05 66.57 o -2 -16 1 206.38 233.34 63.82 o -8 -15 1 317.68 380.88 59.71 o -7 -15 1 204.72 234.88 71.03 o -6 -15 1 77.35 20.12 37.59 o -5 -15 1 20.06 26.08 55.59 o -4 -15 1 27.92 15.10 53.53 o -3 -15 1 212.46 218.24 57.65 o -2 -15 1 467.42 437.85 61.08 o -1 -15 1 494.17 459.12 65.20 o 0 -15 1 187.30 197.65 60.39 o 1 -15 1 5.89 24.71 65.88 o -9 -14 1 2.65 5.49 56.28 o -8 -14 1 403.67 364.12 41.49 o -7 -14 1 719.34 765.28 80.30 o -6 -14 1 316.40 366.45 49.07 o -5 -14 1 125.85 77.07 64.17 o -4 -14 1 2.01 30.88 48.73 o -3 -14 1 40.26 2.75 48.04 o -2 -14 1 169.47 160.59 51.47 o -1 -14 1 493.02 457.75 59.71 o 0 -14 1 772.47 736.38 65.20 o 1 -14 1 206.65 188.27 43.18 o -10 -13 1 217.36 201.77 59.71 o -9 -13 1 138.20 157.85 52.84 o -8 -13 1 13.08 25.39 50.10 o -7 -13 1 635.54 606.62 113.24 o -6 -13 1 1028.21 987.99 103.97 o -5 -13 1 801.71 831.45 61.77 o -4 -13 1 431.29 438.37 33.60 o -3 -13 1 7.58 30.88 43.92 o -2 -13 1 64.94 49.41 44.61 o -1 -13 1 211.21 295.10 48.04 o 0 -13 1 894.24 979.33 59.02 o 1 -13 1 580.67 595.66 44.27 o 2 -13 1 260.64 224.96 42.29 o 3 -13 1 69.67 86.17 43.09 o -11 -12 1 384.09 411.08 64.51 o -10 -12 1 265.54 354.12 56.96 o -9 -12 1 179.23 214.12 48.73 o -8 -12 1 131.91 101.27 33.28 o -7 -12 1 1.71 66.57 43.92 o -6 -12 1 473.05 492.18 33.93 o -5 -12 1 1176.67 1258.27 41.18 o -4 -12 1 2462.68 2723.26 47.16 o -3 -12 1 1142.29 1124.09 36.84 o -2 -12 1 46.28 19.90 37.06 o -1 -12 1 29.02 8.92 38.43 o 0 -12 1 461.35 406.97 47.35 o 1 -12 1 475.43 490.01 50.10 o 2 -12 1 353.17 351.73 38.47 o 3 -12 1 470.89 483.45 42.70 o 4 -12 1 56.28 127.01 41.86 o -11 -11 1 294.79 209.32 60.39 o -10 -11 1 498.14 525.01 55.59 o -9 -11 1 351.00 452.95 49.41 o -8 -11 1 417.88 452.67 87.16 o -7 -11 1 143.72 136.79 29.12 o -6 -11 1 98.81 69.52 26.15 o -5 -11 1 467.78 496.51 29.98 o -4 -11 1 3752.60 3863.67 112.89 o -3 -11 1 3347.68 3436.36 46.88 o -2 -11 1 1034.99 967.66 47.35 o -1 -11 1 409.25 373.34 41.18 o 0 -11 1 69.06 24.71 39.80 o 1 -11 1 323.92 347.95 43.24 o 2 -11 1 125.76 137.39 30.96 o 3 -11 1 585.02 550.05 38.79 o 4 -11 1 292.91 302.80 39.54 o 5 -11 1 32.02 12.35 52.16 o -10 -10 1 302.39 167.45 50.79 o -9 -10 1 557.57 611.48 49.41 o -8 -10 1 1666.65 1687.68 167.80 o -7 -10 1 1838.00 1893.90 66.23 o -6 -10 1 124.66 117.33 23.99 o -5 -10 1 0.33 -2.01 22.18 o -4 -10 1 885.79 895.29 41.18 o -3 -10 1 4649.36 4831.92 87.16 o -2 -10 1 3716.09 3774.14 83.04 o -1 -10 1 3271.41 3347.70 63.82 o 0 -10 1 946.71 1087.07 46.67 o 1 -10 1 61.25 59.02 35.00 o 2 -10 1 91.16 69.13 28.32 o 3 -10 1 596.36 580.69 34.94 o 4 -10 1 425.95 493.62 37.03 o 5 -10 1 77.72 78.86 37.26 o 6 -10 1 45.32 28.25 40.21 o -12 -9 1 179.15 129.02 65.88 o -11 -9 1 329.34 323.24 61.08 o -10 -9 1 15.02 42.55 49.41 o -9 -9 1 123.97 113.44 38.78 o -8 -9 1 1797.44 1802.07 80.64 o -7 -9 1 3653.18 3918.79 170.88 o -6 -9 1 1033.77 1072.50 78.92 o -5 -9 1 335.29 348.33 37.75 o -4 -9 1 0.06 -8.24 28.14 o -3 -9 1 802.53 750.98 24.90 o -2 -9 1 661.39 699.65 23.93 o -1 -9 1 4623.82 4725.07 65.20 o 0 -9 1 5532.05 5534.89 72.06 o 1 -9 1 925.00 994.43 43.24 o 2 -9 1 56.02 35.00 32.94 o 3 -9 1 532.72 565.97 63.14 o 4 -9 1 871.80 882.24 37.08 o 5 -9 1 161.33 170.47 33.80 o 6 -9 1 110.99 97.75 37.75 o 7 -9 1 36.64 52.39 40.73 o -12 -8 1 203.01 108.43 63.14 o -11 -8 1 607.49 541.48 63.14 o -10 -8 1 184.91 139.43 32.05 o -9 -8 1 29.63 24.89 24.73 o -8 -8 1 598.03 502.42 30.20 o -7 -8 1 4812.18 4764.08 259.07 o -6 -8 1 3127.07 3290.02 32.51 o -5 -8 1 1798.32 1922.10 38.62 o -4 -8 1 1486.67 1442.25 30.01 o -3 -8 1 144.98 140.66 17.45 o -2 -8 1 458.20 448.84 19.34 o -1 -8 1 1656.25 1790.53 54.22 o 0 -8 1 5661.29 5390.08 64.51 o 1 -8 1 2583.76 2658.67 51.47 o 2 -8 1 1152.02 1113.22 31.75 o 3 -8 1 44.94 101.87 25.38 o 4 -8 1 632.03 672.66 43.92 o 5 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