#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104086.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104086_Fobs loop_ _publ_author_name 'Hansson, Christian' 'Lindqvist, Maria' 'Oskarsson, \%Ake' _publ_section_title ; Cis/trans isomers of PtX~2~L~2~ (X = halogen, L = neutral ligand); the crystal structures of two polymorphs of cis-dichlorobis(dibenzyl sulfido-\kS)platinum(II) in the temperature range 100--295K ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 187 _journal_page_last 195 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.837 _cell_angle_beta 89.261 _cell_angle_gamma 71.456 _cell_length_a 8.2930 _cell_length_b 12.1730 _cell_length_c 15.7892 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.6571 _[local]_cod_data_source_file ry5016abtri200sup4.hkl _[local]_cod_data_source_block abtri200 #BEGIN Tags that were not found in dictionaries: _shelx_title ' abtri200 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 269.24 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14590.84 16026.09 140.85 o 2 0 0 2517.50 2541.80 11.96 o 3 0 0 80.10 74.43 5.11 o 4 0 0 3203.41 3227.19 63.67 o 5 0 0 1563.36 1716.20 80.55 o 6 0 0 2976.26 2825.03 90.68 o 7 0 0 6543.06 5991.94 76.21 o 8 0 0 469.99 416.76 36.66 o 9 0 0 23.60 58.85 34.73 o 10 0 0 359.12 365.63 47.27 o 11 0 0 871.55 893.34 64.64 o -11 1 0 765.30 722.58 63.67 o -10 1 0 711.57 702.32 55.95 o -9 1 0 152.38 159.18 38.59 o -8 1 0 48.49 94.54 31.84 o -7 1 0 2020.47 1792.47 48.24 o -6 1 0 4772.26 4302.70 60.78 o -5 1 0 1780.30 1692.33 25.57 o -4 1 0 9763.45 9334.64 271.09 o -3 1 0 4665.98 4738.53 62.71 o -2 1 0 833.04 884.66 8.68 o -1 1 0 2561.25 2707.26 178.48 o 1 1 0 21682.54 22908.51 447.63 o 2 1 0 20736.11 20930.55 285.08 o 3 1 0 11011.24 11202.50 126.54 o 4 1 0 941.81 829.48 14.37 o 5 1 0 100.55 87.79 7.68 o 6 1 0 1248.71 1234.24 75.25 o 7 1 0 7229.08 6918.84 97.44 o 8 1 0 1146.46 1099.79 45.34 o 9 1 0 379.87 331.87 39.55 o 10 1 0 1.10 35.70 41.48 o 11 1 0 277.20 255.65 53.06 o -10 2 0 473.12 416.76 53.06 o -9 2 0 237.82 302.93 43.41 o -8 2 0 773.43 698.46 44.38 o -7 2 0 43.01 113.84 29.91 o -6 2 0 2243.86 1995.06 45.34 o -5 2 0 2929.90 2611.93 91.65 o -4 2 0 17528.34 16372.17 970.04 o -3 2 0 6412.37 5169.99 47.27 o -2 2 0 1799.78 1738.73 111.91 o 0 2 0 15049.48 15265.09 116.06 o 1 2 0 13430.91 13960.80 135.54 o 2 2 0 1323.92 1616.73 24.59 o 3 2 0 29319.15 29234.09 273.02 o 4 2 0 8978.20 8693.01 30.13 o 5 2 0 251.98 244.68 12.82 o 6 2 0 765.34 677.74 16.94 o 7 2 0 4941.14 4720.47 36.81 o 8 2 0 1661.59 1526.20 50.17 o 9 2 0 433.60 393.61 41.48 o 10 2 0 442.92 405.19 47.27 o 11 2 0 42.92 44.38 49.20 o -10 3 0 347.39 247.94 54.99 o -9 3 0 163.16 185.23 44.38 o -8 3 0 952.19 986.92 50.17 o -7 3 0 1099.98 1092.07 45.34 o -6 3 0 86.21 71.39 25.08 o -5 3 0 451.85 455.35 27.01 o -4 3 0 11954.69 10608.17 79.11 o -3 3 0 19832.65 17114.31 354.06 o -2 3 0 9212.24 8382.54 55.95 o 0 3 0 221.80 274.01 6.72 o 1 3 0 11728.25 11270.52 621.29 o 2 3 0 917.36 966.28 26.05 o 3 3 0 12748.37 12838.06 102.26 o 4 3 0 12384.55 12327.84 188.12 o 5 3 0 6142.80 5793.48 65.60 o 6 3 0 6.74 8.15 13.44 o 7 3 0 2150.08 2088.94 35.69 o 8 3 0 2407.07 2308.48 30.97 o 9 3 0 617.70 682.06 45.34 o 10 3 0 1052.23 984.99 55.95 o 11 3 0 595.83 527.71 57.88 o -9 4 0 213.61 172.69 46.31 o -8 4 0 1291.34 1276.34 56.92 o -7 4 0 1750.88 1654.51 54.02 o -6 4 0 220.84 189.09 30.87 o -5 4 0 6.11 -8.68 22.19 o -4 4 0 942.00 842.21 29.91 o -3 4 0 8220.70 7348.35 64.64 o -2 4 0 11052.74 9850.86 67.53 o 0 4 0 10729.63 10552.38 138.45 o 1 4 0 1449.39 1510.09 57.88 o 2 4 0 109.41 96.55 4.41 o 3 4 0 9665.20 9461.55 100.81 o 4 4 0 11487.57 12236.59 723.67 o 5 4 0 6013.49 6058.35 44.86 o 6 4 0 2190.06 2127.89 30.87 o 7 4 0 353.06 226.10 49.68 o 8 4 0 572.63 464.80 35.69 o 9 4 0 1122.15 1178.90 53.06 o 10 4 0 1903.66 1991.20 70.43 o 11 4 0 1359.56 1290.81 71.39 o 12 4 0 217.40 132.17 59.81 o -9 5 0 45.93 64.64 48.24 o -8 5 0 1002.19 929.04 56.92 o -7 5 0 2528.91 2430.15 65.60 o -6 5 0 1015.31 1012.97 44.38 o -5 5 0 537.88 546.04 32.80 o -4 5 0 422.48 453.42 27.98 o -3 5 0 754.26 668.56 27.98 o -2 5 0 1404.77 1223.28 29.91 o -1 5 0 20446.25 20188.91 351.16 o 0 5 0 22349.57 20819.09 562.44 o 1 5 0 9495.19 8852.65 370.46 o 2 5 0 51.74 48.28 4.56 o 3 5 0 110.95 111.54 8.04 o 4 5 0 2326.29 2262.38 26.81 o 5 5 0 3022.39 3286.00 209.29 o 6 5 0 2800.57 2918.33 27.97 o 7 5 0 2647.56 2648.85 177.51 o 8 5 0 614.60 577.57 23.36 o 9 5 0 156.83 111.73 40.52 o 10 5 0 1430.65 1543.57 66.57 o 11 5 0 2229.14 2270.01 85.86 o 12 5 0 656.59 690.75 68.50 o -9 6 0 12.05 9.65 49.20 o -8 6 0 106.15 120.59 45.34 o -7 6 0 1343.32 1239.68 55.95 o -6 6 0 1749.17 1797.29 55.95 o -5 6 0 1577.54 1551.29 48.24 o -4 6 0 2554.77 2454.27 51.13 o -3 6 0 581.94 607.78 29.91 o -2 6 0 13.65 5.79 11.54 o -1 6 0 2789.73 2936.64 39.55 o 0 6 0 10774.94 10465.76 258.55 o 1 6 0 13545.93 12598.16 729.82 o 2 6 0 4881.87 4709.23 206.45 o 3 6 0 380.35 319.90 19.65 o 4 6 0 1110.13 1072.09 16.40 o 5 6 0 1641.44 1567.00 24.62 o 6 6 0 2959.61 3915.94 95.51 o 7 6 0 3316.66 3935.52 110.46 o 8 6 0 1725.76 1801.40 152.43 o 9 6 0 30.03 7.60 20.70 o 10 6 0 58.83 66.57 46.31 o 11 6 0 972.98 902.99 66.57 o 12 6 0 835.46 805.55 71.39 o -8 7 0 31.93 -5.79 48.24 o -7 7 0 118.21 141.47 26.87 o -6 7 0 655.00 695.57 53.06 o -5 7 0 2058.59 2174.37 74.77 o -4 7 0 4777.25 4857.58 181.85 o -3 7 0 2451.72 2566.31 53.54 o -2 7 0 270.90 289.58 16.62 o -1 7 0 88.98 119.63 18.33 o 0 7 0 2530.94 2538.26 25.68 o 1 7 0 2825.42 2624.06 134.58 o 2 7 0 3886.42 3975.89 271.09 o 3 7 0 8617.04 8107.73 588.00 o 4 7 0 2063.58 1836.48 150.02 o 5 7 0 1004.78 882.07 53.06 o 6 7 0 3586.46 3896.00 282.18 o 7 7 0 5132.66 6672.07 61.67 o 8 7 0 3073.58 3748.88 85.86 o 9 7 0 372.51 349.54 25.52 o 10 7 0 191.50 147.60 48.24 o 12 7 0 228.42 183.30 62.71 o -7 8 0 48.26 60.33 28.49 o -6 8 0 47.10 39.55 30.87 o -5 8 0 507.97 555.52 28.01 o -4 8 0 3464.85 3644.34 46.15 o -3 8 0 5833.39 5838.77 112.39 o -2 8 0 1256.46 1373.84 83.45 o -1 8 0 381.93 370.46 24.12 o 0 8 0 127.11 110.50 13.18 o 1 8 0 740.74 715.45 17.70 o 2 8 0 911.57 907.36 41.48 o 3 8 0 5862.26 5679.80 359.84 o 4 8 0 5484.40 5195.08 328.01 o 5 8 0 960.00 827.29 74.77 o 6 8 0 114.43 100.63 16.70 o 7 8 0 3241.22 4051.91 217.06 o 8 8 0 3401.37 4537.71 122.04 o 9 8 0 910.96 967.38 84.41 o 10 8 0 912.89 836.51 104.19 o 11 8 0 309.44 246.01 62.71 o -7 9 0 314.62 373.14 62.23 o -6 9 0 35.22 58.85 36.66 o -5 9 0 5.36 6.75 36.66 o -4 9 0 549.00 564.41 28.16 o -3 9 0 2684.56 2928.45 42.44 o -2 9 0 2720.40 2969.97 52.10 o -1 9 0 3539.88 3532.84 55.95 o 0 9 0 1118.11 1088.22 35.70 o 1 9 0 312.25 333.93 16.70 o 2 9 0 1014.60 965.83 21.11 o 3 9 0 2841.36 2830.51 116.25 o 4 9 0 3432.58 3238.60 160.15 o 5 9 0 563.76 542.90 34.25 o 6 9 0 498.75 467.30 22.67 o 7 9 0 22.79 13.51 31.84 o 8 9 0 1489.63 1887.25 86.83 o 9 9 0 1484.98 1700.70 326.56 o 10 9 0 1763.51 1987.54 218.51 o 11 9 0 1030.85 1210.74 79.11 o -7 10 0 519.61 597.17 54.99 o -6 10 0 199.14 209.35 33.78 o -5 10 0 93.85 95.07 27.81 o -4 10 0 16.76 22.70 24.44 o -3 10 0 391.04 374.72 27.32 o -2 10 0 481.33 531.12 26.63 o -1 10 0 2350.70 2470.67 53.06 o 0 10 0 5230.17 5251.03 70.43 o 1 10 0 834.48 890.32 23.47 o 2 10 0 7.27 7.24 14.96 o 3 10 0 2072.29 2051.96 125.41 o 4 10 0 4831.91 4806.45 203.56 o 5 10 0 1120.81 1153.99 118.18 o 6 10 0 1545.84 1552.70 38.11 o 7 10 0 750.26 725.23 28.63 o 8 10 0 9.24 0.00 36.66 o 9 10 0 412.15 336.69 39.55 o 10 10 0 1741.79 1739.41 57.88 o 11 10 0 1825.32 1903.44 253.24 o -6 11 0 368.92 410.98 53.06 o -5 11 0 269.90 328.78 57.88 o -4 11 0 274.00 288.66 31.03 o -3 11 0 0.76 15.92 25.25 o -2 11 0 43.36 13.90 23.07 o -1 11 0 373.74 451.49 33.77 o 0 11 0 2289.88 2463.92 54.99 o 1 11 0 1373.88 1360.27 43.41 o 2 11 0 463.67 420.56 28.94 o 3 11 0 5.07 14.80 18.75 o 4 11 0 1391.88 1350.59 73.80 o 5 11 0 1031.79 1060.68 86.34 o 6 11 0 1716.39 1726.83 136.03 o 7 11 0 2117.60 2042.19 119.63 o 8 11 0 434.67 398.32 28.43 o 10 11 0 244.29 160.15 42.45 o 11 11 0 998.89 851.86 56.92 o -5 12 0 350.21 414.83 53.06 o -4 12 0 694.46 755.96 47.75 o -3 12 0 151.88 169.10 30.08 o -2 12 0 2.47 -9.03 25.25 o -1 12 0 64.21 70.43 31.84 o 0 12 0 1080.15 1192.41 45.34 o 1 12 0 667.17 606.82 38.59 o 2 12 0 589.59 629.75 25.52 o 3 12 0 675.58 648.08 27.29 o 4 12 0 30.72 41.48 21.83 o 5 12 0 710.25 652.85 48.24 o 6 12 0 1964.34 1978.41 97.44 o 7 12 0 2736.61 2779.53 263.37 o 8 12 0 921.80 849.69 55.47 o 9 12 0 151.22 199.70 39.55 o -3 13 0 556.43 681.17 40.24 o -2 13 0 123.19 114.65 32.14 o -1 13 0 10.65 46.31 37.62 o 0 13 0 291.02 310.64 38.59 o 1 13 0 428.55 383.00 40.52 o 2 13 0 591.51 623.22 41.48 o 3 13 0 1084.30 1131.73 39.55 o 4 13 0 632.78 636.41 29.31 o 6 13 0 403.57 370.14 27.97 o 7 13 0 2187.66 2150.02 201.63 o 8 13 0 1529.50 1545.41 42.23 o 9 13 0 470.30 529.64 49.20 o 10 13 0 149.35 112.87 46.31 o -2 14 0 276.04 259.93 36.26 o -1 14 0 281.12 305.16 35.01 o 0 14 0 1.38 9.65 39.55 o 1 14 0 206.72 217.06 40.52 o 2 14 0 322.01 343.44 42.45 o 3 14 0 646.13 738.98 48.24 o 4 14 0 945.37 1007.52 51.61 o 5 14 0 351.31 319.02 28.63 o 6 14 0 28.34 30.56 27.62 o 7 14 0 172.14 165.26 29.62 o 8 14 0 892.33 863.43 54.99 o 9 14 0 1007.65 1047.70 59.81 o -1 15 0 243.05 210.03 49.68 o 0 15 0 241.69 250.83 48.24 o 2 15 0 226.40 254.69 45.34 o 3 15 0 688.51 688.82 51.13 o 4 15 0 611.65 680.13 52.10 o 5 15 0 301.52 306.05 31.72 o 6 15 0 136.05 118.89 29.31 o 7 15 0 101.32 100.36 32.40 o 8 15 0 16.05 25.08 46.31 o 2 16 0 3.45 0.00 44.38 o 3 16 0 127.36 144.71 46.31 o 4 16 0 680.18 779.50 59.81 o 5 16 0 907.00 984.02 60.78 o 6 16 0 247.23 274.27 35.13 o 7 16 0 252.85 218.03 53.06 o -7 -16 1 149.61 146.64 54.99 o -6 -16 1 104.72 52.10 48.24 o -5 -16 1 26.30 34.73 48.24 o -4 -16 1 594.02 749.60 57.88 o -3 -16 1 700.71 801.69 60.78 o -8 -15 1 525.93 441.85 58.85 o -7 -15 1 376.36 374.38 36.14 o -6 -15 1 140.16 112.87 32.06 o -5 -15 1 38.23 3.86 43.41 o -4 -15 1 37.91 23.15 41.48 o -3 -15 1 307.73 328.97 47.27 o -2 -15 1 670.67 711.97 54.02 o -1 -15 1 744.87 823.88 58.85 o 0 -15 1 331.78 335.73 50.17 o 1 -15 1 18.70 23.15 49.20 o -8 -14 1 577.03 561.76 45.34 o -7 -14 1 1136.99 1104.27 70.91 o -6 -14 1 506.98 492.34 66.08 o -5 -14 1 173.03 146.55 35.70 o -4 -14 1 4.57 6.75 36.66 o -3 -14 1 35.40 36.66 38.59 o -2 -14 1 209.75 275.91 41.48 o -1 -14 1 673.08 638.65 49.20 o 0 -14 1 1194.89 1229.07 58.85 o 1 -14 1 362.05 401.77 36.38 o 2 -14 1 56.08 6.63 33.34 o -10 -13 1 349.60 316.43 48.24 o -9 -13 1 174.54 150.50 41.48 o -8 -13 1 32.60 21.85 30.21 o -7 -13 1 986.58 910.38 55.95 o -6 -13 1 1467.37 1413.64 45.34 o -5 -13 1 1098.96 1112.17 82.48 o -4 -13 1 563.98 559.79 30.87 o -3 -13 1 19.03 39.55 33.77 o -2 -13 1 78.02 80.07 33.77 o -1 -13 1 259.38 293.28 38.59 o 0 -13 1 1307.43 1389.21 55.95 o 1 -13 1 881.41 975.16 70.43 o 2 -13 1 390.07 417.27 67.53 o 3 -13 1 143.14 153.28 35.01 o -11 -12 1 689.94 729.34 56.92 o -10 -12 1 463.01 480.44 49.20 o -9 -12 1 234.49 196.80 40.52 o -8 -12 1 146.60 152.03 28.95 o -7 -12 1 4.27 23.15 24.56 o -6 -12 1 767.01 738.72 84.41 o -5 -12 1 1518.11 1550.27 117.70 o -4 -12 1 3218.78 3331.62 102.26 o -3 -12 1 1642.89 1698.27 37.62 o -2 -12 1 75.86 60.78 30.87 o -1 -12 1 24.31 47.27 29.91 o 0 -12 1 581.61 620.32 41.48 o 1 -12 1 695.28 723.55 42.45 o 2 -12 1 496.33 552.41 32.66 o 3 -12 1 763.50 785.06 46.31 o 4 -12 1 153.00 210.62 33.78 o -11 -11 1 550.97 413.87 51.13 o -10 -11 1 873.24 910.71 52.10 o -9 -11 1 524.96 551.83 42.45 o -8 -11 1 521.91 482.55 29.39 o -7 -11 1 182.01 161.60 27.98 o -6 -11 1 139.59 102.80 21.48 o -5 -11 1 598.62 579.75 24.89 o -4 -11 1 4724.24 4693.77 282.18 o -3 -11 1 4251.46 4262.26 168.83 o -2 -11 1 1383.01 1366.80 58.37 o -1 -11 1 553.60 549.90 35.70 o 0 -11 1 62.92 6.75 31.84 o 1 -11 1 436.57 415.80 34.73 o 2 -11 1 138.28 167.86 24.72 o 3 -11 1 844.52 1004.06 40.52 o 4 -11 1 549.11 652.01 35.21 o 5 -11 1 80.69 91.69 36.66 o -10 -10 1 564.02 441.85 45.34 o -9 -10 1 795.55 835.46 45.34 o -8 -10 1 2177.29 2262.97 78.63 o -7 -10 1 2570.95 2632.60 44.86 o -6 -10 1 148.52 131.01 19.36 o -5 -10 1 1.93 0.00 24.12 o -4 -10 1 1042.20 1025.36 58.37 o -3 -10 1 5728.40 5745.78 325.11 o -2 -10 1 4421.07 4517.10 121.56 o -1 -10 1 3915.68 4004.59 61.74 o 0 -10 1 1434.83 1454.81 43.41 o 1 -10 1 52.96 70.43 26.05 o 2 -10 1 78.34 87.02 22.10 o 3 -10 1 720.71 742.12 30.39 o 4 -10 1 691.09 720.24 45.82 o 5 -10 1 148.53 164.71 30.08 o 6 -10 1 95.70 115.42 32.83 o -12 -9 1 235.93 249.87 73.32 o -11 -9 1 419.22 441.85 65.60 o -10 -9 1 4.64 86.83 54.99 o -9 -9 1 204.84 198.04 64.64 o -8 -9 1 2514.02 2706.03 327.53 o -7 -9 1 4789.93 4913.77 68.98 o -6 -9 1 1314.64 1347.32 28.55 o -5 -9 1 367.20 345.05 26.53 o -4 -9 1 2.04 0.96 14.33 o -3 -9 1 948.92 882.67 22.16 o -2 -9 1 726.37 737.76 57.88 o -1 -9 1 5310.37 5344.60 63.67 o 0 -9 1 6935.13 6678.83 73.32 o 1 -9 1 1249.07 1304.32 39.55 o 2 -9 1 116.05 89.67 20.60 o 3 -9 1 534.63 521.52 41.97 o 4 -9 1 1098.22 1177.33 59.81 o 5 -9 1 225.17 277.57 27.87 o 6 -9 1 183.94 159.26 29.65 o 7 -9 1 92.88 128.92 33.35 o -12 -8 1 298.26 286.52 70.43 o -11 -8 1 836.43 959.91 72.35 o -10 -8 1 198.42 132.07 34.73 o -9 -8 1 19.32 27.98 42.45 o -8 -8 1 937.17 1137.38 37.63 o -7 -8 1 6575.63 6816.10 380.10 o -6 -8 1 3902.92 3824.04 35.15 o -5 -8 1 2023.80 1890.45 77.18 o -4 -8 1 1754.64 1549.51 28.46 o -3 -8 1 150.68 136.65 14.33 o -2 -8 1 527.73 536.67 30.39 o -1 -8 1 1753.17 1805.08 41.97 o 0 -8 1 6776.71 6520.61 66.57 o 1 -8 1 3301.24 3373.66 51.13 o 2 -8 1 1557.22 1559.83 29.92 o 3 -8 1 172.14 187.40 20.73 o 4 -8 1 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