#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104103.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104103_Fobs loop_ _publ_author_name 'Trzop, El\.zbieta' 'Turowska-Tyrk, Ilona' _publ_section_title ; Monitoring structural transformations in crystals. 12. Course of an intramolecular [4+4] photocycloaddition in a crystal ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 375 _journal_page_last 382 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.990 _cell_angle_gamma 90.000 _cell_length_a 10.2740 _cell_length_b 12.7740 _cell_length_c 8.4460 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bk50724.3Psup3.hkl _[local]_cod_data_source_block 4.3P #BEGIN Tags that were not found in dictionaries: _shelx_title 4.3%P _shelx_refln_list_code 4 _shelx_F_calc_maximum 98.99 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 652.52 667.82 3.93 o 3 0 0 91.65 81.57 1.63 o 4 0 0 1758.16 1858.30 8.84 o 5 0 0 220.17 257.86 8.06 o 6 0 0 8.44 7.58 0.82 o 7 0 0 0.16 -0.51 0.51 o 8 0 0 14.56 14.02 1.14 o 9 0 0 17.52 12.58 1.67 o 10 0 0 6.92 12.70 1.85 o 2 1 0 1724.05 1542.50 3.96 o 3 1 0 78.91 74.95 0.74 o 4 1 0 1311.33 1244.86 3.08 o 5 1 0 185.16 207.62 1.25 o 6 1 0 41.62 42.45 0.77 o 7 1 0 1.42 2.39 0.63 o 8 1 0 0.00 -0.35 0.35 o 9 1 0 2.95 2.57 1.24 o 10 1 0 1.57 4.46 2.00 o 11 1 0 0.07 0.29 7.32 o 0 2 0 3076.59 3142.68 11.56 o 1 2 0 570.08 521.45 1.40 o 2 2 0 231.20 186.78 1.59 o 3 2 0 1.71 2.42 0.34 o 4 2 0 332.71 362.55 3.81 o 5 2 0 532.12 540.08 6.79 o 6 2 0 73.70 71.26 1.78 o 7 2 0 6.02 5.20 0.70 o 8 2 0 76.44 75.00 1.33 o 9 2 0 3.50 1.63 1.18 o 10 2 0 0.01 1.64 1.86 o 11 2 0 0.07 -0.19 0.95 o 1 3 0 943.87 909.45 7.41 o 2 3 0 4.45 2.85 0.35 o 3 3 0 0.02 1.18 0.30 o 4 3 0 207.86 191.42 1.68 o 5 3 0 55.33 58.96 1.36 o 6 3 0 4.92 3.44 0.67 o 7 3 0 106.70 99.41 1.40 o 8 3 0 30.87 33.55 1.10 o 9 3 0 60.71 60.89 2.66 o 10 3 0 2.62 2.02 1.98 o 11 3 0 1.31 0.11 0.66 o 0 4 0 315.30 292.86 3.40 o 1 4 0 6.21 5.37 0.42 o 2 4 0 76.74 78.08 0.78 o 3 4 0 159.88 149.08 1.39 o 4 4 0 55.55 51.33 0.58 o 5 4 0 1.27 3.00 0.48 o 6 4 0 0.08 0.20 0.51 o 7 4 0 157.32 166.86 1.75 o 8 4 0 96.46 92.38 1.49 o 9 4 0 54.31 44.82 1.56 o 10 4 0 0.00 0.37 0.89 o 1 5 0 716.06 734.83 3.46 o 2 5 0 41.32 47.04 0.65 o 3 5 0 427.36 453.63 3.44 o 4 5 0 4.09 7.16 0.53 o 5 5 0 0.63 0.40 0.26 o 6 5 0 29.08 23.61 1.37 o 7 5 0 10.38 11.39 0.88 o 8 5 0 0.63 -0.64 1.03 o 9 5 0 11.02 16.92 1.37 o 10 5 0 4.93 1.85 3.17 o 0 6 0 105.35 116.21 1.92 o 1 6 0 475.07 498.91 2.38 o 2 6 0 484.90 523.00 5.51 o 3 6 0 45.41 51.31 0.77 o 4 6 0 91.54 98.83 1.43 o 5 6 0 10.10 6.44 0.73 o 6 6 0 128.42 116.49 1.31 o 7 6 0 39.02 44.74 1.20 o 8 6 0 0.47 -0.06 0.37 o 9 6 0 25.23 26.69 1.60 o 10 6 0 2.47 1.75 3.54 o 1 7 0 364.73 369.52 3.55 o 2 7 0 96.81 98.23 0.98 o 3 7 0 2.30 2.63 0.59 o 4 7 0 74.50 77.78 1.26 o 5 7 0 222.59 225.62 1.67 o 6 7 0 108.37 114.51 1.53 o 7 7 0 70.16 79.56 1.48 o 8 7 0 0.39 -0.01 0.37 o 9 7 0 29.74 33.27 3.36 o 0 8 0 292.71 290.45 3.73 o 1 8 0 105.95 112.82 1.09 o 2 8 0 19.09 20.87 0.69 o 3 8 0 75.89 84.10 1.06 o 4 8 0 0.94 0.68 0.47 o 5 8 0 27.12 29.41 1.01 o 6 8 0 100.15 117.53 1.44 o 7 8 0 93.06 99.27 1.69 o 8 8 0 35.53 39.20 1.74 o 9 8 0 0.01 -0.10 1.09 o 1 9 0 1.21 1.13 0.58 o 2 9 0 40.18 41.12 0.85 o 3 9 0 186.27 185.41 1.55 o 4 9 0 11.34 10.02 0.77 o 5 9 0 53.51 48.46 1.07 o 6 9 0 104.59 105.02 1.43 o 7 9 0 33.96 26.85 1.22 o 8 9 0 2.24 -1.04 1.04 o 9 9 0 0.63 -0.57 1.55 o 0 10 0 98.58 99.72 2.11 o 1 10 0 16.36 17.65 0.90 o 2 10 0 19.96 18.21 0.77 o 3 10 0 10.59 8.19 0.87 o 4 10 0 48.66 41.71 1.01 o 5 10 0 64.51 62.14 1.21 o 6 10 0 63.12 72.83 1.61 o 7 10 0 42.93 48.94 1.45 o 8 10 0 0.26 0.56 1.31 o 1 11 0 105.42 104.43 1.62 o 2 11 0 160.27 155.35 1.90 o 3 11 0 51.44 50.78 1.17 o 4 11 0 23.52 22.99 1.02 o 5 11 0 1.12 1.10 0.83 o 6 11 0 17.01 14.83 1.25 o 7 11 0 0.68 0.70 1.14 o 0 12 0 3.78 3.15 2.24 o 1 12 0 4.49 3.64 1.32 o 2 12 0 1.68 2.37 1.24 o 3 12 0 0.33 0.39 0.98 o 4 12 0 4.79 2.28 1.08 o 5 12 0 1.81 0.61 0.69 o 6 12 0 32.36 34.05 1.57 o 1 13 0 79.68 80.74 1.67 o 2 13 0 4.08 4.62 1.60 o 3 13 0 22.94 24.55 1.46 o 4 13 0 0.19 -0.16 0.58 o 5 13 0 6.40 5.67 1.42 o 0 14 0 95.65 96.94 3.16 o 1 14 0 0.53 -0.06 0.34 o 2 14 0 12.27 10.27 1.61 o 3 14 0 4.39 4.21 1.61 o 4 14 0 4.17 0.43 1.65 o 1 15 0 52.78 57.92 2.68 o -11 1 1 0.09 -0.09 0.82 o -10 1 1 0.00 -0.28 0.74 o -9 1 1 3.90 2.86 0.96 o -8 1 1 0.20 -0.17 0.70 o -7 1 1 14.92 14.81 0.71 o -6 1 1 0.56 -0.06 0.45 o -5 1 1 144.72 188.85 2.37 o -4 1 1 70.14 82.43 1.03 o -3 1 1 1333.07 1228.11 8.29 o -2 1 1 0.00 2.14 0.57 o -1 1 1 2588.34 2080.61 8.70 o 0 1 1 4796.89 4393.98 78.23 o 1 1 1 24.71 25.23 2.75 o 2 1 1 152.42 144.11 1.17 o 3 1 1 24.64 23.95 0.83 o 4 1 1 200.95 202.73 7.06 o 5 1 1 0.45 0.67 0.41 o 6 1 1 8.54 10.83 0.58 o 7 1 1 7.63 7.35 0.98 o 8 1 1 74.50 66.81 1.49 o 9 1 1 30.03 22.58 1.87 o 10 1 1 2.24 2.76 2.23 o -11 2 1 3.35 4.51 2.08 o -10 2 1 6.58 4.54 1.23 o -9 2 1 8.72 6.59 1.06 o -8 2 1 31.04 33.91 1.11 o -7 2 1 0.15 0.39 0.73 o -6 2 1 49.10 46.88 0.83 o -5 2 1 500.36 515.10 2.75 o -4 2 1 176.15 175.55 3.98 o -3 2 1 238.71 246.74 1.00 o -2 2 1 1091.70 991.49 3.76 o -1 2 1 80.52 57.08 0.73 o 0 2 1 2196.90 2161.57 2.79 o 1 2 1 3652.23 3549.57 6.63 o 2 2 1 208.76 199.08 0.78 o 3 2 1 9.98 5.21 0.30 o 4 2 1 776.19 858.30 4.43 o 5 2 1 0.73 1.66 0.46 o 6 2 1 0.34 0.77 0.49 o 7 2 1 6.76 5.23 1.13 o 8 2 1 5.20 3.87 1.96 o 9 2 1 1.88 3.62 1.93 o 10 2 1 0.05 0.41 1.63 o -11 3 1 0.02 0.66 1.15 o -10 3 1 0.11 0.20 1.04 o -9 3 1 45.14 44.91 1.28 o -8 3 1 369.06 385.95 3.30 o -7 3 1 0.39 1.85 0.59 o -6 3 1 6.80 5.20 0.69 o -5 3 1 14.86 10.66 0.44 o -4 3 1 34.95 32.51 0.57 o -3 3 1 636.78 578.55 2.19 o -2 3 1 1.13 1.49 0.32 o -1 3 1 6905.31 7338.99 40.00 o 0 3 1 2948.43 3015.88 3.22 o 1 3 1 621.95 595.34 4.70 o 2 3 1 71.72 64.21 1.29 o 3 3 1 86.06 61.17 1.16 o 4 3 1 5.80 6.02 0.37 o 5 3 1 0.01 0.18 0.38 o 6 3 1 0.11 0.66 0.48 o 7 3 1 1.46 1.11 1.05 o 8 3 1 0.40 0.31 0.53 o 9 3 1 0.56 -0.05 0.35 o 10 3 1 1.67 2.29 2.08 o -11 4 1 0.09 -1.31 1.31 o -10 4 1 9.86 8.82 1.23 o -9 4 1 2.25 1.70 1.11 o -8 4 1 404.47 434.09 2.89 o -7 4 1 113.88 110.55 1.86 o -6 4 1 16.28 14.72 0.54 o -5 4 1 376.32 356.07 1.67 o -4 4 1 128.97 140.07 1.30 o -3 4 1 291.82 289.87 3.32 o -2 4 1 101.69 95.50 1.42 o -1 4 1 2418.43 2399.85 5.65 o 0 4 1 589.14 635.11 2.16 o 1 4 1 152.52 155.16 0.99 o 2 4 1 115.35 106.93 1.85 o 3 4 1 116.66 105.42 2.17 o 4 4 1 1.44 1.93 0.42 o 5 4 1 7.91 11.28 0.75 o 6 4 1 24.39 23.33 1.14 o 7 4 1 27.75 27.17 1.19 o 8 4 1 21.78 23.04 1.99 o 9 4 1 4.00 4.42 2.10 o 10 4 1 2.58 3.78 3.30 o -11 5 1 1.44 1.51 3.06 o -10 5 1 5.61 5.16 1.30 o -9 5 1 11.18 9.16 1.14 o -8 5 1 189.53 188.62 5.54 o -7 5 1 144.98 135.33 2.11 o -6 5 1 50.86 55.02 0.88 o -5 5 1 169.71 184.92 2.40 o -4 5 1 434.16 498.82 4.87 o -3 5 1 273.99 283.94 2.43 o -2 5 1 16.86 18.42 0.51 o -1 5 1 111.62 113.23 0.97 o 0 5 1 39.45 38.87 0.53 o 1 5 1 187.59 189.87 0.94 o 2 5 1 4.24 3.52 0.35 o 3 5 1 148.62 129.80 1.94 o 4 5 1 49.72 42.19 1.26 o 5 5 1 1.75 1.16 0.57 o 6 5 1 42.45 41.04 1.09 o 7 5 1 57.87 61.78 1.30 o 8 5 1 41.11 44.07 1.56 o 9 5 1 1.65 0.54 1.66 o 10 5 1 3.71 3.93 2.84 o -10 6 1 1.72 0.24 0.81 o -9 6 1 17.39 16.55 1.54 o -8 6 1 0.26 -0.08 0.36 o -7 6 1 0.66 0.10 0.25 o -6 6 1 1.68 2.37 0.72 o -5 6 1 67.88 71.06 0.96 o -4 6 1 73.82 72.26 0.91 o -3 6 1 549.49 563.45 5.33 o -2 6 1 37.43 31.82 0.49 o -1 6 1 164.14 145.32 1.65 o 0 6 1 104.20 118.38 1.08 o 1 6 1 77.49 81.95 0.79 o 2 6 1 435.21 396.61 1.79 o 3 6 1 0.58 0.32 0.43 o 4 6 1 11.01 10.96 0.66 o 5 6 1 105.13 111.05 1.42 o 6 6 1 121.18 118.94 1.89 o 7 6 1 123.94 151.20 1.84 o 8 6 1 1.02 0.06 1.31 o 9 6 1 1.94 1.12 4.50 o -10 7 1 17.60 24.04 1.95 o -9 7 1 1.47 -0.20 0.95 o -8 7 1 3.75 4.13 1.36 o -7 7 1 0.07 0.11 0.63 o -6 7 1 29.89 29.17 0.85 o -5 7 1 1.98 1.77 0.59 o -4 7 1 26.35 28.61 0.74 o -3 7 1 330.28 374.70 3.48 o -2 7 1 82.15 100.33 0.81 o -1 7 1 12.29 9.12 0.40 o 0 7 1 12.73 13.41 0.38 o 1 7 1 883.85 915.45 6.27 o 2 7 1 1.85 2.98 0.46 o 3 7 1 98.62 115.56 1.35 o 4 7 1 40.89 37.36 0.87 o 5 7 1 46.73 44.73 1.17 o 6 7 1 92.98 100.85 2.11 o 7 7 1 247.92 257.95 4.01 o 8 7 1 20.10 17.00 2.37 o 9 7 1 0.53 -1.11 2.07 o -9 8 1 0.59 -1.42 1.42 o -8 8 1 0.03 -0.60 0.60 o -7 8 1 34.08 29.99 1.18 o -6 8 1 10.91 11.22 0.87 o -5 8 1 19.41 20.66 0.81 o -4 8 1 0.18 -0.07 0.43 o -3 8 1 44.72 36.74 0.79 o -2 8 1 71.28 73.59 0.93 o -1 8 1 106.13 97.47 0.83 o 0 8 1 2.87 1.91 0.45 o 1 8 1 41.36 36.77 0.79 o 2 8 1 231.77 254.44 2.55 o 3 8 1 64.16 70.72 1.07 o 4 8 1 4.71 5.24 0.78 o 5 8 1 149.14 141.20 1.52 o 6 8 1 134.90 136.22 1.80 o 7 8 1 0.40 0.06 0.79 o 8 8 1 33.73 38.99 2.29 o 9 8 1 2.77 6.34 2.46 o -9 9 1 3.47 3.21 1.83 o -8 9 1 5.38 5.35 1.50 o -7 9 1 92.15 101.51 1.73 o -6 9 1 15.98 17.46 1.13 o -5 9 1 0.29 0.26 0.51 o -4 9 1 13.20 11.09 0.75 o -3 9 1 73.43 64.75 1.00 o -2 9 1 48.09 56.16 0.98 o -1 9 1 39.29 42.20 1.05 o 0 9 1 34.59 34.85 0.72 o 1 9 1 9.23 7.40 0.70 o 2 9 1 147.16 145.48 1.40 o 3 9 1 58.81 60.30 1.09 o 4 9 1 1.95 1.97 0.88 o 5 9 1 20.93 22.46 0.95 o 6 9 1 34.60 41.94 1.10 o 7 9 1 1.91 0.86 2.34 o 8 9 1 14.25 13.96 2.31 o -8 10 1 7.55 4.73 1.65 o -7 10 1 14.65 16.85 1.29 o -6 10 1 99.36 98.89 1.68 o -5 10 1 14.53 16.55 0.97 o -4 10 1 8.52 6.76 0.87 o -3 10 1 43.72 45.50 0.95 o -2 10 1 123.31 123.43 1.62 o -1 10 1 7.15 6.24 0.87 o 0 10 1 2.39 0.72 1.06 o 1 10 1 2.56 4.09 0.82 o 2 10 1 40.57 48.08 1.02 o 3 10 1 43.51 48.49 1.07 o 4 10 1 13.70 13.45 0.94 o 5 10 1 41.53 36.80 1.10 o 6 10 1 51.73 49.37 1.22 o 7 10 1 0.67 -0.11 0.97 o -8 11 1 30.85 28.33 1.61 o -7 11 1 1.61 0.77 0.87 o -6 11 1 2.91 4.52 1.27 o -5 11 1 0.08 0.88 0.71 o -4 11 1 1.25 1.96 0.94 o -3 11 1 28.27 30.32 1.16 o -2 11 1 75.05 83.77 1.51 o -1 11 1 45.05 41.36 1.25 o 0 11 1 24.37 22.40 1.34 o 1 11 1 4.46 3.19 1.21 o 2 11 1 28.40 31.95 0.94 o 3 11 1 22.61 22.01 1.00 o 4 11 1 79.33 83.91 1.36 o 5 11 1 14.32 13.26 1.14 o 6 11 1 2.05 0.41 0.77 o 7 11 1 0.37 -1.36 3.16 o -7 12 1 30.21 30.91 1.85 o -6 12 1 37.84 36.75 1.44 o -5 12 1 2.52 0.08 0.58 o -4 12 1 45.57 48.00 1.40 o -3 12 1 94.18 97.69 1.71 o -2 12 1 125.43 128.25 1.86 o -1 12 1 4.56 4.12 1.14 o 0 12 1 139.94 157.39 2.43 o 1 12 1 35.20 35.62 1.22 o 2 12 1 3.67 3.80 1.43 o 3 12 1 7.85 5.02 1.16 o 4 12 1 35.55 33.91 1.20 o 5 12 1 1.83 2.53 1.33 o 6 12 1 0.13 0.03 0.42 o -6 13 1 27.42 28.37 1.95 o -5 13 1 2.67 1.60 2.58 o -4 13 1 0.55 0.00 0.22 o -3 13 1 6.22 6.06 1.41 o -2 13 1 22.53 17.72 1.40 o -1 13 1 42.92 41.23 1.43 o 0 13 1 11.03 10.90 1.54 o 1 13 1 0.45 -0.30 0.92 o 2 13 1 1.92 0.13 0.77 o 3 13 1 1.43 1.48 1.75 o 4 13 1 0.66 0.00 0.35 o 5 13 1 15.86 18.29 1.52 o -4 14 1 0.81 0.16 0.50 o -3 14 1 9.34 8.05 1.64 o -2 14 1 3.82 5.18 1.62 o -1 14 1 8.34 7.23 1.74 o 0 14 1 6.16 6.37 1.86 o 1 14 1 29.17 32.45 1.91 o 2 14 1 9.69 6.85 1.96 o 3 14 1 0.02 0.06 0.56 o -1 15 1 27.84 30.81 1.99 o 0 15 1 0.01 -0.88 1.57 o -11 0 2 1.79 3.47 1.72 o -10 0 2 18.05 20.16 2.42 o -9 0 2 279.11 282.26 11.01 o -8 0 2 335.65 321.60 2.97 o -7 0 2 29.51 30.21 2.61 o -6 0 2 65.66 70.06 1.55 o -5 0 2 126.05 145.82 2.32 o -4 0 2 325.89 300.86 4.14 o -3 0 2 21.71 17.13 0.63 o -2 0 2 67.34 81.42 0.84 o -1 0 2 810.07 742.53 1.99 o 0 0 2 3055.07 2928.08 4.58 o 1 0 2 0.08 0.54 1.11 o 2 0 2 673.19 605.90 5.45 o 3 0 2 365.21 374.29 2.51 o 4 0 2 1574.49 1644.09 6.06 o 5 0 2 0.16 -0.27 2.87 o 6 0 2 37.53 29.13 1.41 o 7 0 2 33.92 31.32 1.18 o 8 0 2 131.44 124.94 2.69 o -11 1 2 0.14 -1.16 1.16 o -10 1 2 0.54 -0.36 1.03 o -9 1 2 37.87 36.01 1.14 o -8 1 2 201.88 205.41 3.56 o -7 1 2 1.09 0.01 0.09 o -6 1 2 16.61 21.52 0.84 o -5 1 2 12.60 13.66 0.80 o -4 1 2 477.81 422.70 1.29 o -3 1 2 70.16 56.52 1.01 o -2 1 2 3486.74 3388.94 4.88 o -1 1 2 963.43 872.24 3.02 o 0 1 2 1315.37 1320.14 3.65 o 1 1 2 76.26 55.23 0.59 o 2 1 2 108.01 112.47 1.89 o 3 1 2 228.23 217.91 1.07 o 4 1 2 149.98 150.20 1.38 o 5 1 2 0.38 0.01 0.08 o 6 1 2 0.23 -0.42 0.62 o 7 1 2 0.71 0.58 0.85 o 8 1 2 21.35 21.56 1.69 o 9 1 2 0.58 0.91 1.68 o -11 2 2 0.81 -0.67 0.67 o -10 2 2 0.66 0.61 1.04 o -9 2 2 0.61 0.25 0.71 o -8 2 2 85.86 72.83 1.85 o -7 2 2 5.02 8.60 0.74 o -6 2 2 34.74 35.65 0.94 o -5 2 2 19.06 13.99 0.41 o -4 2 2 1094.78 1070.30 3.63 o -3 2 2 5.26 5.24 0.45 o -2 2 2 923.59 844.96 2.81 o -1 2 2 9799.72 10828.45 62.67 o 0 2 2 3653.53 3845.00 3.48 o 1 2 2 263.33 242.36 1.77 o 2 2 2 82.04 76.19 0.87 o 3 2 2 385.03 406.43 3.03 o 4 2 2 180.57 196.88 1.43 o 5 2 2 6.14 8.50 0.61 o 6 2 2 0.37 0.21 0.89 o 7 2 2 1.82 2.78 1.51 o 8 2 2 0.00 1.18 1.03 o 9 2 2 5.01 3.17 2.01 o -11 3 2 5.41 5.76 1.47 o -10 3 2 5.08 4.93 1.33 o -9 3 2 0.12 -0.09 0.99 o -8 3 2 5.77 8.61 1.04 o -7 3 2 31.11 31.29 1.03 o -6 3 2 3.35 1.80 0.81 o -5 3 2 308.23 336.91 3.78 o -4 3 2 541.91 593.19 5.78 o -3 3 2 613.88 578.24 1.26 o -2 3 2 280.01 283.09 3.45 o -1 3 2 9598.90 10673.57 25.72 o 0 3 2 467.51 494.13 4.10 o 1 3 2 40.42 54.23 0.90 o 2 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