#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:01:09 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180901 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/41/2104104.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104104_Fobs loop_ _publ_author_name 'Trzop, El\.zbieta' 'Turowska-Tyrk, Ilona' _publ_section_title ; Monitoring structural transformations in crystals. 12. Course of an intramolecular [4+4] photocycloaddition in a crystal ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 375 _journal_page_last 382 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.050 _cell_angle_gamma 90.000 _cell_length_a 10.2850 _cell_length_b 12.7910 _cell_length_c 8.4484 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file bk50729.9Psup4.hkl _cod_data_source_block 9.9P #BEGIN Tags that were not found in dictionaries: _shelx_title 9.9%P _shelx_refln_list_code 4 _shelx_f_calc_maximum 97.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 638.85 660.41 6.08 o 3 0 0 121.02 117.83 6.89 o 4 0 0 1761.34 1874.81 17.76 o 5 0 0 218.55 266.27 9.08 o 6 0 0 5.20 5.22 0.79 o 7 0 0 0.10 0.48 0.94 o 8 0 0 11.80 11.11 1.10 o 9 0 0 10.67 8.07 1.66 o 10 0 0 4.65 10.44 2.01 o 2 1 0 1646.67 1429.64 4.95 o 3 1 0 92.10 86.39 2.57 o 4 1 0 1236.28 1156.48 6.30 o 5 1 0 178.54 207.26 3.56 o 6 1 0 38.01 36.48 0.72 o 7 1 0 1.22 2.01 0.71 o 8 1 0 0.08 0.19 0.33 o 9 1 0 4.10 1.65 1.68 o 10 1 0 1.38 1.39 8.53 o 11 1 0 0.12 -0.54 2.02 o 0 2 0 3118.82 3262.02 4.56 o 1 2 0 598.22 533.04 2.32 o 2 2 0 209.27 160.98 1.82 o 3 2 0 0.96 1.79 0.32 o 4 2 0 302.94 319.58 1.52 o 5 2 0 478.62 469.92 4.57 o 6 2 0 67.35 60.70 1.16 o 7 2 0 6.96 5.81 0.62 o 8 2 0 64.54 62.73 1.23 o 9 2 0 3.70 1.57 1.42 o 10 2 0 0.01 -1.38 2.18 o 11 2 0 0.06 1.41 1.67 o 1 3 0 940.62 905.95 2.90 o 2 3 0 4.62 2.36 0.37 o 3 3 0 3.21 6.02 0.34 o 4 3 0 206.41 188.40 2.56 o 5 3 0 42.06 46.00 1.68 o 6 3 0 8.28 6.94 0.74 o 7 3 0 84.67 74.79 2.03 o 8 3 0 32.57 35.08 1.06 o 9 3 0 53.37 51.83 1.60 o 10 3 0 2.86 0.42 5.56 o 11 3 0 1.01 0.53 2.40 o 0 4 0 359.04 334.60 2.83 o 1 4 0 4.46 4.24 0.39 o 2 4 0 95.15 92.12 1.21 o 3 4 0 119.83 110.44 2.62 o 4 4 0 74.15 66.63 1.65 o 5 4 0 0.02 1.60 0.52 o 6 4 0 1.04 0.73 0.78 o 7 4 0 141.07 149.74 3.76 o 8 4 0 100.70 97.72 2.59 o 9 4 0 40.84 33.24 1.57 o 10 4 0 0.00 -0.34 12.76 o 1 5 0 674.93 682.17 2.38 o 2 5 0 42.73 48.23 0.80 o 3 5 0 434.21 450.92 3.72 o 4 5 0 5.25 7.63 0.65 o 5 5 0 0.33 0.74 0.54 o 6 5 0 16.77 14.88 1.10 o 7 5 0 14.15 15.90 0.90 o 8 5 0 0.20 2.22 1.85 o 9 5 0 10.09 14.53 1.38 o 10 5 0 5.02 4.84 2.40 o 0 6 0 112.86 124.85 2.52 o 1 6 0 421.40 439.00 2.95 o 2 6 0 413.15 451.27 4.25 o 3 6 0 46.61 54.91 0.86 o 4 6 0 94.64 101.11 1.39 o 5 6 0 6.22 3.79 0.65 o 6 6 0 123.88 105.27 1.25 o 7 6 0 20.68 26.93 1.07 o 8 6 0 0.01 -0.10 1.24 o 9 6 0 19.48 22.87 1.58 o 10 6 0 3.15 2.21 2.69 o 1 7 0 336.42 337.17 2.83 o 2 7 0 80.98 81.46 1.14 o 3 7 0 3.65 3.98 0.57 o 4 7 0 72.09 73.85 1.02 o 5 7 0 201.29 198.26 2.43 o 6 7 0 83.11 88.13 2.67 o 7 7 0 49.06 59.15 1.52 o 8 7 0 0.01 -0.04 0.62 o 9 7 0 28.55 31.15 1.79 o 0 8 0 287.62 280.07 3.29 o 1 8 0 106.34 115.23 1.10 o 2 8 0 27.70 30.02 0.74 o 3 8 0 56.08 61.74 1.14 o 4 8 0 0.56 0.75 0.67 o 5 8 0 20.39 21.72 0.85 o 6 8 0 89.17 100.60 1.72 o 7 8 0 69.14 75.43 1.51 o 8 8 0 27.20 32.71 1.51 o 9 8 0 0.04 0.28 0.94 o 1 9 0 3.21 4.01 0.59 o 2 9 0 36.52 38.96 0.96 o 3 9 0 170.95 169.43 1.49 o 4 9 0 12.34 11.76 0.74 o 5 9 0 51.80 46.83 1.06 o 6 9 0 88.72 87.50 1.65 o 7 9 0 31.78 23.64 1.20 o 8 9 0 1.88 -1.02 2.10 o 9 9 0 0.35 -0.66 0.86 o 0 10 0 90.48 88.95 1.69 o 1 10 0 15.66 17.05 0.89 o 2 10 0 15.54 15.78 0.76 o 3 10 0 9.50 7.82 0.82 o 4 10 0 41.90 34.81 0.95 o 5 10 0 47.65 45.69 1.10 o 6 10 0 47.45 56.65 1.24 o 7 10 0 39.34 47.26 1.41 o 8 10 0 0.07 -0.42 1.71 o 1 11 0 95.25 92.00 1.54 o 2 11 0 153.12 145.58 1.99 o 3 11 0 54.73 56.07 1.38 o 4 11 0 25.80 25.55 1.01 o 5 11 0 0.64 0.31 1.10 o 6 11 0 15.39 13.44 1.32 o 7 11 0 0.68 0.23 0.42 o 0 12 0 9.12 12.55 1.98 o 1 12 0 2.66 3.09 1.09 o 2 12 0 1.23 1.38 1.16 o 3 12 0 0.10 0.14 0.35 o 4 12 0 2.37 0.40 0.52 o 5 12 0 0.97 0.05 0.12 o 6 12 0 27.26 28.09 1.49 o 1 13 0 78.78 82.94 1.69 o 2 13 0 6.62 7.62 1.45 o 3 13 0 22.63 25.00 1.44 o 4 13 0 0.11 0.41 1.16 o 5 13 0 7.02 6.24 1.54 o 0 14 0 82.21 82.97 2.99 o 1 14 0 0.30 1.94 1.28 o 2 14 0 11.23 11.22 1.59 o 3 14 0 3.59 2.65 1.80 o 4 14 0 5.05 3.96 1.94 o 1 15 0 43.26 47.01 2.08 o -11 1 1 0.03 0.71 1.20 o -10 1 1 0.01 0.38 0.67 o -9 1 1 0.60 2.80 0.96 o -8 1 1 2.16 6.29 0.76 o -7 1 1 12.60 12.68 0.67 o -6 1 1 0.72 0.27 0.42 o -5 1 1 104.37 142.58 4.16 o -4 1 1 54.19 58.71 1.94 o -3 1 1 1275.97 1131.87 9.18 o -2 1 1 4.32 11.62 0.86 o -1 1 1 2615.54 2156.04 10.50 o 0 1 1 4834.37 4633.45 22.63 o 1 1 1 32.90 33.79 5.73 o 2 1 1 143.82 136.21 0.66 o 3 1 1 35.94 39.54 2.35 o 4 1 1 103.65 129.99 11.04 o 5 1 1 0.42 3.32 0.41 o 6 1 1 5.74 7.41 0.56 o 7 1 1 5.14 6.04 0.93 o 8 1 1 50.10 50.89 1.34 o 9 1 1 21.40 15.88 1.82 o 10 1 1 1.67 2.42 2.20 o -11 2 1 1.80 -0.01 0.08 o -10 2 1 6.09 3.91 1.53 o -9 2 1 11.08 9.16 0.98 o -8 2 1 12.28 23.11 1.18 o -7 2 1 0.63 0.34 0.61 o -6 2 1 46.68 50.68 1.08 o -5 2 1 403.38 416.68 5.97 o -4 2 1 117.49 133.98 1.68 o -3 2 1 217.41 230.51 2.06 o -2 2 1 1332.16 1237.36 3.06 o -1 2 1 58.63 43.35 0.57 o 0 2 1 2116.14 2078.96 3.69 o 1 2 1 3846.54 3835.24 9.66 o 2 2 1 182.49 164.05 2.69 o 3 2 1 5.91 4.53 0.30 o 4 2 1 769.72 843.24 6.49 o 5 2 1 0.15 1.38 0.44 o 6 2 1 0.96 1.53 0.47 o 7 2 1 4.17 4.12 1.00 o 8 2 1 4.84 3.65 1.78 o 9 2 1 0.76 2.55 2.01 o 10 2 1 0.01 -1.03 2.25 o -11 3 1 0.07 -1.34 2.90 o -10 3 1 0.07 0.08 0.16 o -9 3 1 27.74 29.03 1.76 o -8 3 1 267.43 270.33 2.77 o -7 3 1 0.04 0.53 0.50 o -6 3 1 3.69 2.98 0.73 o -5 3 1 5.53 4.45 0.43 o -4 3 1 44.50 40.59 1.21 o -3 3 1 645.37 578.00 2.75 o -2 3 1 0.08 4.14 0.39 o -1 3 1 6782.58 7289.31 49.26 o 0 3 1 2870.65 2966.08 4.34 o 1 3 1 706.64 667.95 4.92 o 2 3 1 95.84 82.58 2.27 o 3 3 1 93.67 64.23 1.55 o 4 3 1 5.89 6.99 0.41 o 5 3 1 0.00 0.46 0.28 o 6 3 1 0.46 2.69 0.99 o 7 3 1 3.22 4.00 0.92 o 8 3 1 2.25 1.75 1.39 o 9 3 1 1.64 -0.36 6.72 o 10 3 1 1.06 0.93 1.65 o -11 4 1 0.29 -1.56 1.56 o -10 4 1 8.31 6.50 1.37 o -9 4 1 1.11 0.23 0.68 o -8 4 1 333.03 344.17 4.35 o -7 4 1 71.52 73.00 6.90 o -6 4 1 14.23 12.00 0.53 o -5 4 1 392.51 370.29 4.11 o -4 4 1 101.08 103.68 1.76 o -3 4 1 220.96 222.88 3.46 o -2 4 1 100.27 87.10 1.12 o -1 4 1 2376.40 2296.86 5.31 o 0 4 1 594.82 647.89 3.18 o 1 4 1 145.90 148.75 1.35 o 2 4 1 86.82 79.71 1.76 o 3 4 1 81.32 84.48 1.40 o 4 4 1 4.10 4.39 0.54 o 5 4 1 3.08 7.38 0.94 o 6 4 1 18.34 18.72 1.04 o 7 4 1 17.47 15.92 1.32 o 8 4 1 13.97 15.54 2.04 o 9 4 1 3.39 4.91 2.31 o 10 4 1 2.39 1.76 9.50 o -11 5 1 1.71 0.79 8.61 o -10 5 1 2.74 3.88 1.21 o -9 5 1 5.98 5.29 1.05 o -8 5 1 171.00 170.25 2.40 o -7 5 1 120.04 115.19 4.95 o -6 5 1 45.80 47.50 0.84 o -5 5 1 150.52 163.38 1.88 o -4 5 1 424.70 455.26 7.06 o -3 5 1 215.96 224.23 3.31 o -2 5 1 30.81 32.07 1.09 o -1 5 1 103.84 103.40 1.01 o 0 5 1 34.60 32.80 0.72 o 1 5 1 164.67 167.29 1.28 o 2 5 1 5.63 6.04 0.43 o 3 5 1 124.80 109.17 2.04 o 4 5 1 35.79 32.08 0.94 o 5 5 1 1.35 1.05 0.74 o 6 5 1 46.98 44.48 2.05 o 7 5 1 37.11 41.65 1.16 o 8 5 1 26.03 29.59 1.60 o 9 5 1 2.44 2.50 2.27 o 10 5 1 3.17 2.57 2.49 o -10 6 1 1.89 0.02 0.73 o -9 6 1 14.92 13.22 1.55 o -8 6 1 1.31 1.33 1.35 o -7 6 1 1.08 0.00 0.21 o -6 6 1 0.64 2.05 0.66 o -5 6 1 63.86 68.98 0.95 o -4 6 1 78.38 72.39 1.05 o -3 6 1 489.76 498.29 4.39 o -2 6 1 33.17 29.21 0.58 o -1 6 1 153.92 135.79 1.37 o 0 6 1 125.19 143.30 1.81 o 1 6 1 76.91 82.83 1.45 o 2 6 1 452.52 420.93 3.50 o 3 6 1 1.45 1.58 0.65 o 4 6 1 15.86 13.87 0.67 o 5 6 1 71.15 80.75 2.66 o 6 6 1 111.26 110.99 1.53 o 7 6 1 90.65 111.47 2.78 o 8 6 1 0.16 0.54 0.70 o 9 6 1 2.74 2.55 2.40 o -10 7 1 15.62 17.58 1.93 o -9 7 1 0.80 1.40 1.77 o -8 7 1 3.15 4.17 1.31 o -7 7 1 0.18 0.32 0.60 o -6 7 1 25.12 24.59 0.80 o -5 7 1 1.00 0.93 0.90 o -4 7 1 33.09 34.61 0.76 o -3 7 1 324.97 367.41 1.79 o -2 7 1 60.27 79.81 1.05 o -1 7 1 16.73 13.48 0.48 o 0 7 1 16.76 18.20 0.47 o 1 7 1 848.44 874.30 7.37 o 2 7 1 3.23 5.73 0.47 o 3 7 1 86.99 97.77 1.10 o 4 7 1 32.38 29.86 0.81 o 5 7 1 54.08 51.55 1.03 o 6 7 1 62.14 66.66 1.65 o 7 7 1 214.00 220.66 3.65 o 8 7 1 16.25 13.61 1.68 o 9 7 1 0.29 1.05 2.08 o -9 8 1 0.61 -0.76 1.27 o -8 8 1 0.00 -0.21 0.57 o -7 8 1 26.47 24.47 1.14 o -6 8 1 6.19 6.63 0.82 o -5 8 1 16.10 17.41 0.78 o -4 8 1 0.63 -0.09 0.32 o -3 8 1 45.40 35.48 0.79 o -2 8 1 62.05 63.54 0.87 o -1 8 1 107.92 99.78 1.18 o 0 8 1 3.84 3.17 0.46 o 1 8 1 31.47 29.23 0.74 o 2 8 1 195.98 217.76 1.57 o 3 8 1 56.91 64.41 1.15 o 4 8 1 1.87 3.32 0.73 o 5 8 1 140.96 135.78 1.90 o 6 8 1 118.72 117.63 1.69 o 7 8 1 0.35 -0.13 0.32 o 8 8 1 23.67 29.08 2.21 o 9 8 1 1.20 3.41 2.28 o -9 9 1 3.02 2.18 2.18 o -8 9 1 5.36 4.62 1.26 o -7 9 1 67.48 79.34 1.58 o -6 9 1 8.14 10.52 1.10 o -5 9 1 0.01 0.51 0.74 o -4 9 1 14.17 12.80 0.74 o -3 9 1 67.95 60.92 0.97 o -2 9 1 48.85 52.98 0.88 o -1 9 1 35.16 40.55 1.03 o 0 9 1 37.25 37.10 0.74 o 1 9 1 4.49 5.03 0.68 o 2 9 1 119.08 118.72 2.22 o 3 9 1 56.87 56.80 1.06 o 4 9 1 4.56 5.56 0.84 o 5 9 1 20.67 23.16 0.94 o 6 9 1 27.54 31.74 1.17 o 7 9 1 2.14 1.48 1.62 o 8 9 1 12.39 12.82 2.27 o -8 10 1 9.31 5.37 1.56 o -7 10 1 12.42 14.86 1.55 o -6 10 1 80.99 79.48 2.67 o -5 10 1 10.27 11.70 0.98 o -4 10 1 4.72 4.25 0.87 o -3 10 1 37.15 37.26 0.90 o -2 10 1 92.13 93.90 1.46 o -1 10 1 6.23 4.81 0.95 o 0 10 1 1.50 0.76 0.57 o 1 10 1 1.17 3.40 0.77 o 2 10 1 36.40 45.74 1.00 o 3 10 1 32.37 37.77 1.46 o 4 10 1 7.63 8.06 0.90 o 5 10 1 38.94 35.12 1.06 o 6 10 1 50.63 45.69 1.17 o 7 10 1 0.99 -0.37 1.09 o -8 11 1 25.45 24.45 1.57 o -7 11 1 1.27 1.01 1.07 o -6 11 1 2.54 3.62 1.48 o -5 11 1 0.04 1.33 1.05 o -4 11 1 1.84 3.02 1.08 o -3 11 1 23.08 23.98 1.10 o -2 11 1 56.74 61.58 1.36 o -1 11 1 46.73 40.72 1.20 o 0 11 1 24.23 20.97 1.03 o 1 11 1 3.74 2.96 1.01 o 2 11 1 22.44 25.59 0.88 o 3 11 1 20.60 20.83 0.96 o 4 11 1 71.00 72.21 1.61 o 5 11 1 10.31 10.89 1.11 o 6 11 1 1.18 0.08 0.41 o 7 11 1 0.27 -1.27 2.37 o -7 12 1 26.49 25.96 1.58 o -6 12 1 32.91 31.76 1.44 o -5 12 1 2.91 1.65 1.62 o -4 12 1 39.55 43.64 1.59 o -3 12 1 90.19 93.86 1.67 o -2 12 1 108.66 114.39 1.91 o -1 12 1 2.08 2.88 1.26 o 0 12 1 126.16 138.04 4.09 o 1 12 1 34.92 36.46 1.24 o 2 12 1 5.62 6.76 1.25 o 3 12 1 4.34 3.58 1.09 o 4 12 1 30.27 30.57 1.21 o 5 12 1 2.88 2.43 1.21 o 6 12 1 0.01 -0.68 0.76 o -6 13 1 18.34 18.38 1.94 o -5 13 1 1.95 0.99 0.99 o -4 13 1 0.73 -0.15 1.78 o -3 13 1 4.55 3.71 1.42 o -2 13 1 18.36 12.62 1.43 o -1 13 1 33.55 31.86 1.37 o 0 13 1 7.80 5.62 1.50 o 1 13 1 0.25 0.85 1.12 o 2 13 1 1.03 0.40 0.55 o 3 13 1 0.68 0.00 0.27 o 4 13 1 0.90 1.31 1.21 o 5 13 1 14.20 14.75 1.52 o -4 14 1 0.79 0.39 0.82 o -3 14 1 8.32 7.95 1.52 o -2 14 1 5.76 7.81 1.49 o -1 14 1 8.52 8.63 1.50 o 0 14 1 4.18 5.86 1.78 o 1 14 1 24.01 24.78 1.97 o 2 14 1 7.32 7.24 1.55 o 3 14 1 0.05 0.58 1.34 o -1 15 1 28.00 31.87 1.89 o 0 15 1 0.10 0.14 0.57 o 1 15 1 32.61 28.04 2.05 o -11 0 2 1.59 2.73 1.62 o -10 0 2 11.17 13.79 1.43 o -9 0 2 248.85 242.48 2.85 o -8 0 2 304.57 291.43 3.40 o -7 0 2 12.66 17.25 3.09 o -6 0 2 63.17 60.82 2.20 o -5 0 2 122.52 143.66 2.27 o -4 0 2 288.47 261.28 1.67 o -3 0 2 9.22 14.39 0.59 o -2 0 2 108.30 145.30 4.71 o -1 0 2 895.51 831.97 2.10 o 0 0 2 2829.35 2722.77 7.72 o 1 0 2 0.00 0.82 0.35 o 2 0 2 700.98 624.41 7.76 o 3 0 2 325.81 316.52 4.35 o 4 0 2 1366.97 1398.35 11.59 o 5 0 2 1.97 1.73 0.91 o 6 0 2 35.57 25.70 1.31 o 7 0 2 27.22 27.73 1.34 o 8 0 2 115.58 108.27 2.48 o -11 1 2 0.08 -0.59 0.66 o -10 1 2 0.62 -0.18 0.81 o -9 1 2 48.85 50.66 3.14 o -8 1 2 183.71 189.03 2.23 o -7 1 2 3.14 1.53 0.75 o -6 1 2 14.32 21.19 0.84 o -5 1 2 26.85 32.61 0.95 o -4 1 2 467.37 372.86 2.81 o -3 1 2 94.85 86.25 2.60 o -2 1 2 3438.57 3330.43 7.64 o -1 1 2 1038.28 939.96 6.07 o 0 1 2 1183.42 1138.06 5.48 o 1 1 2 76.33 55.46 1.61 o 2 1 2 123.34 119.17 2.83 o 3 1 2 217.46 200.65 1.46 o 4 1 2 143.61 145.32 1.08 o 5 1 2 1.17 1.45 0.49 o 6 1 2 0.45 1.10 0.85 o 7 1 2 0.90 0.30 0.74 o 8 1 2 14.20 14.82 1.70 o 9 1 2 0.38 0.90 1.58 o -11 2 2 0.25 -0.01 1.25 o -10 2 2 1.02 0.25 1.43 o -9 2 2 3.01 1.57 0.98 o -8 2 2 96.76 82.71 2.09 o -7 2 2 5.02 7.89 0.72 o -6 2 2 25.93 24.79 1.18 o -5 2 2 12.21 11.95 0.55 o -4 2 2 1089.21 1019.39 7.85 o -3 2 2 20.82 23.79 0.61 o -2 2 2 851.78 729.32 3.18 o -1 2 2 9572.01 10779.81 56.69 o 0 2 2 3326.79 3569.21 9.90 o 1 2 2 278.78 246.97 3.87 o 2 2 2 81.87 75.72 0.97 o 3 2 2 354.48 362.69 3.01 o 4 2 2 155.53 170.21 1.21 o 5 2 2 3.93 6.47 0.61 o 6 2 2 0.02 0.12 0.96 o 7 2 2 1.89 2.59 1.50 o 8 2 2 0.01 0.78 0.94 o 9 2 2 3.70 2.60 2.00 o -11 3 2 3.38 3.30 1.42 o -10 3 2 2.03 0.45 0.68 o -9 3 2 0.40 2.18 1.14 o -8 3 2 0.06 3.86 0.83 o -7 3 2 26.79 25.98 0.97 o -6 3 2 1.94 1.29 0.58 o -5 3 2 332.13 352.71 2.36 o -4 3 2 636.46 685.32 8.21 o -3 3 2 587.95 534.88 1.59 o -2 3 2 351.36 368.12 8.78 o -1 3 2 8929.15 10090.85 53.82 o 0 3 2 424.27 459.47 3.31 o 1 3 2 31.20 46.43 0.98 o 2 3 2 0.58 0.56 0.29 o 3 3 2 95.99 91.86 1.92 o 4 3 2 74.18 74.44 1.70 o 5 3 2 70.73 66.53 2.36 o 6 3 2 0.33 0.26 1.10 o 7 3 2 0.10 0.93 2.96 o 8 3 2 6.29 7.11 1.81 o 9 3 2 0.63 0.49 6.16 o -11 4 2 18.09 19.31 1.46 o -10 4 2 8.32 8.82 1.38 o -9 4 2 3.42 3.46 1.37 o -8 4 2 74.70 75.56 4.97 o -7 4 2 27.06 23.86 1.37 o -6 4 2 22.39 27.57 0.79 o -5 4 2 122.85 140.30 3.04 o -4 4 2 115.43 105.49 0.96 o -3 4 2 27.87 40.63 1.37 o -2 4 2 100.24 118.92 1.90 o -1 4 2 780.13 794.13 4.72 o 0 4 2 3819.35 3989.80 7.23 o 1 4 2 1774.27 1883.19 4.88 o 2 4 2 0.21 2.24 0.39 o 3 4 2 327.11 265.66 2.46 o 4 4 2 43.06 39.16 1.02 o 5 4 2 180.38 186.33 1.94 o 6 4 2 0.02 1.77 1.57 o 7 4 2 10.28 10.31 1.83 o 8 4 2 2.53 2.53 1.73 o 9 4 2 0.02 0.86 1.84 o -11 5 2 0.01 0.35 1.27 o -10 5 2 4.26 3.48 1.51 o -9 5 2 5.90 4.96 1.50 o -8 5 2 63.08 58.42 2.16 o -7 5 2 0.34 -0.01 0.26 o -6 5 2 114.82 118.87 1.40 o -5 5 2 285.71 296.67 3.11 o -4 5 2 1.89 10.37 0.48 o -3 5 2 42.67 29.46 1.34 o -2 5 2 143.31 146.85 1.74 o -1 5 2 31.10 25.53 0.73 o 0 5 2 69.41 74.35 0.68 o 1 5 2 123.46 123.03 3.81 o 2 5 2 19.20 23.22 1.50 o 3 5 2 23.59 34.31 0.83 o 4 5 2 79.20 86.74 1.99 o 5 5 2 445.93 444.13 6.02 o 6 5 2 0.70 0.58 0.92 o 7 5 2 29.39 31.92 1.48 o 8 5 2 0.01 -0.54 1.41 o 9 5 2 0.83 -0.18 0.58 o -11 6 2 0.01 0.34 0.79 o -10 6 2 10.89 9.14 1.38 o -9 6 2 17.38 18.49 1.58 o -8 6 2 3.08 1.78 0.88 o -7 6 2 7.74 10.01 0.84 o -6 6 2 40.87 47.98 1.43 o -5 6 2 4.37 2.87 0.54 o -4 6 2 286.80 285.06 2.91 o -3 6 2 66.19 78.36 0.84 o -2 6 2 32.91 33.77 1.08 o -1 6 2 99.87 88.92 0.85 o 0 6 2 209.41 213.98 1.17 o 1 6 2 140.11 162.40 1.62 o 2 6 2 50.42 50.14 0.68 o 3 6 2 57.06 53.84 1.33 o 4 6 2 3.78 3.30 0.76 o 5 6 2 263.14 248.89 2.51 o 6 6 2 171.28 168.16 3.45 o 7 6 2 29.51 30.35 1.44 o 8 6 2 18.26 16.95 2.21 o 9 6 2 2.43 3.27 1.98 o -10 7 2 0.01 0.01 0.23 o -9 7 2 0.56 -0.59 0.76 o -8 7 2 0.96 0.26 0.59 o -7 7 2 4.27 2.62 1.02 o -6 7 2 0.27 0.39 1.18 o -5 7 2 13.34 14.18 0.71 o -4 7 2 23.77 23.86 0.71 o -3 7 2 3.48 3.65 0.88 o -2 7 2 1.83 2.78 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