#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:01:09 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180901 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/41/2104113.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104113_Fobs loop_ _publ_author_name 'Rychlewska, Urszula' 'War\.zajtis, Beata' 'Joachimiak, Roman' 'Paryzek, Zdzis\/law' _publ_section_title ; Synthesis and structural characteristics of lithocholate triads: steroid-type channels occupied by spacer fragments ; _journal_coeditor_code BK5073 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 383 _journal_page_last 392 _journal_volume 64 _journal_year 2008 _space_group_IT_number 1 _symmetry_space_group_name_Hall 'P 1' _symmetry_space_group_name_H-M 'P 1' _cell_angle_alpha 75.390 _cell_angle_beta 83.250 _cell_angle_gamma 82.770 _cell_length_a 12.8560 _cell_length_b 13.5460 _cell_length_c 17.4210 _exptl_crystal_F_000 1132.00 _reflns_d_resolution_high 0.8392 _cod_data_source_file bk507352Py120Ksup2.hkl _cod_data_source_block 52Py120K #BEGIN Tags that were not found in dictionaries: _shelx_title ' 5+2Py(120K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 355.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 5531.64 5147.56 70.11 o 4 0 0 1894.26 1822.27 34.86 o 5 0 0 8196.93 8086.90 96.78 o 6 0 0 2337.34 2324.92 60.70 o 7 0 0 1304.11 1304.34 55.62 o 8 0 0 494.82 490.15 33.05 o 9 0 0 398.24 349.05 36.72 o 10 0 0 7.48 32.39 17.22 o 11 0 0 408.44 365.30 35.51 o 12 0 0 295.14 293.26 54.40 o 13 0 0 50.83 97.96 44.98 o 14 0 0 109.27 63.10 36.30 o 15 0 0 59.05 61.40 33.69 o -15 1 0 18.59 18.32 36.18 o -14 1 0 38.30 35.20 39.53 o -13 1 0 101.90 94.06 76.71 o -12 1 0 356.00 356.07 57.02 o -11 1 0 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