#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/41/2104166.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104166_Fobs loop_ _publ_author_name 'Rychlewska, Urszula' 'Wa\'scinska, Natalia' 'War\.zajtis, Beata' 'Gawro\'nski, Jacek' _publ_section_title ; Role of the gauche effect and local 1,3-dipole--dipole interactions in stabilizing an unusual conformation of tartarodinitriles ; _journal_coeditor_code BS5062 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 497 _journal_page_last 503 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.2155 _cell_length_b 6.2725 _cell_length_c 10.8275 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.8080 _[local]_cod_data_source_file bs50621asup2.hkl _[local]_cod_data_source_block 1a #BEGIN Tags that were not found in dictionaries: _shelx_title ' HHCN in Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 82.95 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 745.32 793.26 5.68 o 4 0 0 44.31 41.13 3.18 o 6 0 0 385.03 419.77 10.82 o 8 0 0 43.78 28.70 15.92 o 2 1 0 6881.45 6855.76 21.13 o 4 1 0 25.45 28.28 2.50 o 6 1 0 111.95 108.14 4.57 o 8 1 0 4.39 1.30 1.69 o 0 2 0 80.71 93.69 4.48 o 2 2 0 1032.12 1057.47 7.19 o 4 2 0 2215.24 2455.84 13.77 o 6 2 0 225.32 227.26 14.15 o 8 2 0 26.54 19.31 10.01 o 2 3 0 174.13 188.08 3.70 o 4 3 0 118.32 108.45 6.89 o 6 3 0 436.23 468.82 14.27 o 8 3 0 26.94 13.42 11.01 o 0 4 0 694.63 730.29 12.73 o 2 4 0 611.84 629.31 7.82 o 4 4 0 0.20 1.44 1.74 o 6 4 0 7.84 9.23 5.85 o 2 5 0 134.40 121.36 5.77 o 4 5 0 55.77 52.31 8.81 o 6 5 0 4.78 7.47 5.92 o 0 6 0 27.60 25.12 6.99 o 2 6 0 54.19 44.21 6.19 o 4 6 0 20.93 24.84 8.29 o 2 7 0 1.12 5.10 4.85 o 1 1 1 1863.06 1769.22 7.88 o 2 1 1 34.52 33.02 1.25 o 3 1 1 35.75 32.61 1.50 o 4 1 1 62.70 67.57 2.09 o 5 1 1 12.88 13.41 1.93 o 6 1 1 30.10 29.78 2.67 o 7 1 1 233.42 251.42 5.37 o 8 1 1 2.00 7.14 3.55 o 0 2 1 140.69 116.06 3.24 o 1 2 1 1176.50 1129.83 4.73 o 2 2 1 95.69 89.34 1.91 o 3 2 1 187.09 197.95 2.61 o 4 2 1 28.88 29.08 1.92 o 5 2 1 263.42 271.09 4.59 o 6 2 1 3.36 2.65 2.80 o 7 2 1 16.98 15.51 4.52 o 8 2 1 0.00 0.29 1.80 o 1 3 1 155.58 159.06 2.58 o 2 3 1 9.96 9.72 1.45 o 3 3 1 52.08 50.47 2.04 o 4 3 1 2.82 4.78 1.99 o 5 3 1 206.53 220.25 6.59 o 6 3 1 5.08 4.47 2.03 o 7 3 1 8.45 5.23 2.74 o 8 3 1 42.17 27.51 7.35 o 0 4 1 65.66 56.48 4.02 o 1 4 1 212.34 203.45 3.31 o 2 4 1 10.54 8.77 2.12 o 3 4 1 132.36 133.53 3.62 o 4 4 1 12.26 8.19 4.60 o 5 4 1 159.38 151.44 8.09 o 6 4 1 66.13 68.82 6.23 o 7 4 1 10.78 5.36 3.69 o 1 5 1 8.66 9.06 2.39 o 2 5 1 0.52 0.63 0.79 o 3 5 1 51.61 42.28 4.44 o 4 5 1 46.38 50.35 4.82 o 5 5 1 1.56 6.79 4.44 o 6 5 1 1.82 2.08 2.04 o 0 6 1 33.06 35.44 5.60 o 1 6 1 115.45 116.30 4.64 o 2 6 1 42.71 42.44 4.91 o 3 6 1 51.82 58.63 4.98 o 4 6 1 7.09 2.00 2.33 o 5 6 1 8.02 12.45 6.14 o 1 7 1 29.15 28.45 4.79 o 2 7 1 2.43 5.80 3.16 o 3 7 1 3.27 1.63 1.74 o 0 0 2 2450.48 2254.42 10.53 o 1 0 2 31.52 26.84 1.55 o 2 0 2 18.11 15.89 1.78 o 3 0 2 2915.66 3142.47 13.18 o 4 0 2 900.35 988.68 8.36 o 5 0 2 752.15 815.20 8.54 o 6 0 2 518.19 567.74 8.46 o 7 0 2 7.68 10.91 4.13 o 8 0 2 36.88 28.69 7.23 o 1 1 2 1031.53 1062.89 4.76 o 2 1 2 106.85 130.31 2.10 o 3 1 2 554.97 595.59 4.43 o 4 1 2 291.66 305.19 3.78 o 5 1 2 252.86 273.61 4.16 o 6 1 2 112.35 105.18 3.62 o 7 1 2 39.45 36.01 3.47 o 8 1 2 41.52 38.85 5.91 o 0 2 2 3347.58 3526.34 13.55 o 1 2 2 3570.15 3662.04 12.19 o 2 2 2 576.31 619.09 4.10 o 3 2 2 3.23 1.21 0.91 o 4 2 2 1.61 0.49 0.86 o 5 2 2 4.43 4.26 1.72 o 6 2 2 9.72 6.80 2.39 o 7 2 2 118.17 127.82 5.45 o 8 2 2 6.45 1.04 1.35 o 1 3 2 372.39 371.90 6.93 o 2 3 2 816.46 883.09 6.44 o 3 3 2 261.39 258.47 4.10 o 4 3 2 15.26 10.94 3.02 o 5 3 2 14.56 9.09 2.88 o 6 3 2 17.15 15.38 4.04 o 7 3 2 0.20 3.70 2.93 o 8 3 2 1.83 2.16 6.70 o 0 4 2 129.04 138.86 4.88 o 1 4 2 7.38 4.80 1.95 o 2 4 2 188.96 184.95 3.86 o 3 4 2 240.47 249.94 5.16 o 4 4 2 192.00 196.36 5.55 o 5 4 2 93.58 85.80 5.94 o 6 4 2 6.26 1.50 1.75 o 7 4 2 2.77 2.71 5.62 o 1 5 2 0.81 0.13 0.25 o 2 5 2 22.79 20.12 3.38 o 3 5 2 0.99 0.71 1.05 o 4 5 2 0.68 0.36 1.12 o 5 5 2 9.54 4.87 3.73 o 6 5 2 41.21 31.44 6.74 o 0 6 2 1.93 0.67 1.22 o 1 6 2 12.68 7.52 2.37 o 2 6 2 86.67 89.46 4.72 o 3 6 2 36.79 30.17 4.91 o 4 6 2 2.13 2.49 2.52 o 5 6 2 0.40 2.59 2.21 o 1 7 2 8.26 3.25 2.19 o 2 7 2 0.18 1.02 1.41 o 3 7 2 3.69 3.95 3.49 o 1 1 3 520.99 535.25 3.37 o 2 1 3 9.12 8.39 1.08 o 3 1 3 8.35 10.29 1.72 o 4 1 3 106.20 117.68 3.06 o 5 1 3 0.51 0.59 0.59 o 6 1 3 187.11 206.84 5.09 o 7 1 3 54.72 53.14 5.07 o 8 1 3 30.99 31.68 6.73 o 0 2 3 11.17 8.33 1.34 o 1 2 3 129.26 136.40 2.25 o 2 2 3 98.61 91.09 1.83 o 3 2 3 128.99 119.63 3.20 o 4 2 3 315.44 342.87 4.90 o 5 2 3 77.52 67.59 3.56 o 6 2 3 5.23 2.28 1.36 o 7 2 3 13.18 8.61 2.87 o 8 2 3 5.89 1.71 5.90 o 1 3 3 10.06 8.31 1.46 o 2 3 3 479.19 530.98 5.91 o 3 3 3 0.24 0.90 0.54 o 4 3 3 24.23 24.70 2.84 o 5 3 3 0.00 2.41 1.86 o 6 3 3 0.43 0.10 0.99 o 7 3 3 3.95 0.75 1.11 o 0 4 3 1150.35 1217.56 9.80 o 1 4 3 28.94 25.71 2.66 o 2 4 3 124.78 138.30 4.33 o 3 4 3 40.40 38.57 3.81 o 4 4 3 11.95 11.28 3.32 o 5 4 3 103.19 102.60 7.13 o 6 4 3 84.00 81.70 7.45 o 7 4 3 5.42 4.47 4.03 o 1 5 3 87.54 84.48 4.01 o 2 5 3 169.25 169.57 5.24 o 3 5 3 41.88 36.60 3.77 o 4 5 3 53.08 51.61 6.03 o 5 5 3 46.42 51.59 5.64 o 6 5 3 81.23 94.34 9.02 o 0 6 3 3.32 2.20 2.42 o 1 6 3 8.58 10.38 3.87 o 2 6 3 101.26 121.39 5.35 o 3 6 3 51.23 53.98 5.94 o 4 6 3 238.11 262.20 8.80 o 5 6 3 12.51 12.54 5.40 o 1 7 3 13.04 13.84 4.89 o 2 7 3 59.85 56.47 7.49 o 3 7 3 0.70 -0.29 0.74 o 0 0 4 12.55 18.63 3.88 o 1 0 4 3923.83 4042.99 14.53 o 2 0 4 267.94 284.40 4.18 o 3 0 4 403.14 452.97 5.11 o 4 0 4 3.08 5.37 2.01 o 5 0 4 40.66 35.09 4.38 o 6 0 4 4.10 6.53 3.97 o 7 0 4 8.61 4.01 6.61 o 8 0 4 92.06 100.41 9.19 o 1 1 4 379.94 400.02 3.11 o 2 1 4 0.60 0.88 0.66 o 3 1 4 208.99 202.97 3.16 o 4 1 4 0.48 0.39 0.47 o 5 1 4 13.49 14.52 2.59 o 6 1 4 46.90 39.92 4.37 o 7 1 4 25.75 21.82 4.39 o 8 1 4 36.05 31.46 6.21 o 0 2 4 60.25 61.78 1.98 o 1 2 4 283.13 292.42 2.47 o 2 2 4 206.47 218.93 3.61 o 3 2 4 537.42 558.28 5.66 o 4 2 4 42.00 42.63 2.92 o 5 2 4 539.19 564.64 6.91 o 6 2 4 50.90 51.08 3.87 o 7 2 4 69.31 84.53 5.20 o 8 2 4 0.73 7.20 3.21 o 1 3 4 12.95 13.86 1.63 o 2 3 4 121.36 126.80 3.45 o 3 3 4 63.07 51.91 3.10 o 4 3 4 260.51 266.84 5.18 o 5 3 4 3.43 2.64 2.05 o 6 3 4 10.53 6.90 2.49 o 7 3 4 119.09 143.12 7.40 o 0 4 4 101.68 97.23 4.76 o 1 4 4 501.76 523.50 6.87 o 2 4 4 34.85 36.24 3.47 o 3 4 4 106.13 104.82 4.76 o 4 4 4 1.97 1.54 1.36 o 5 4 4 1.61 1.43 1.83 o 6 4 4 51.07 53.18 6.46 o 7 4 4 9.37 7.06 5.99 o 1 5 4 50.35 44.30 4.18 o 2 5 4 13.17 11.92 3.31 o 3 5 4 88.56 102.21 4.69 o 4 5 4 1.13 1.11 1.00 o 5 5 4 8.43 8.22 3.75 o 6 5 4 2.17 4.72 4.71 o 0 6 4 180.26 205.18 9.87 o 1 6 4 1.27 0.98 1.20 o 2 6 4 20.33 13.32 4.31 o 3 6 4 73.63 66.51 5.84 o 4 6 4 10.76 15.65 4.66 o 5 6 4 20.37 21.96 14.81 o 1 7 4 16.34 13.68 5.06 o 2 7 4 98.75 131.27 11.79 o 1 1 5 20.25 22.28 1.83 o 2 1 5 121.77 122.03 2.29 o 3 1 5 204.35 226.45 3.63 o 4 1 5 7.90 9.75 2.42 o 5 1 5 30.01 31.23 4.07 o 6 1 5 58.75 59.22 4.74 o 7 1 5 5.97 5.80 3.68 o 8 1 5 31.59 36.66 6.18 o 0 2 5 349.56 356.21 4.22 o 1 2 5 128.38 124.97 2.20 o 2 2 5 2.00 0.89 1.24 o 3 2 5 38.31 38.26 2.86 o 4 2 5 9.52 7.31 2.49 o 5 2 5 103.62 100.43 4.19 o 6 2 5 31.31 25.48 4.02 o 7 2 5 60.52 68.39 5.97 o 1 3 5 103.13 93.99 2.94 o 2 3 5 0.32 0.27 0.51 o 3 3 5 39.41 31.74 3.07 o 4 3 5 48.59 48.53 3.47 o 5 3 5 122.19 127.22 4.67 o 6 3 5 36.16 27.64 4.01 o 7 3 5 53.93 54.51 6.78 o 0 4 5 74.56 68.00 4.77 o 1 4 5 82.57 81.52 6.11 o 2 4 5 73.37 68.04 3.53 o 3 4 5 521.16 553.97 7.10 o 4 4 5 72.06 58.42 3.91 o 5 4 5 16.92 18.76 3.48 o 6 4 5 18.82 18.02 5.40 o 1 5 5 456.69 474.55 7.20 o 2 5 5 4.40 3.84 2.18 o 3 5 5 52.28 59.07 4.86 o 4 5 5 18.96 18.46 4.17 o 5 5 5 79.63 82.99 7.70 o 0 6 5 93.11 101.63 9.66 o 1 6 5 241.61 263.83 7.52 o 2 6 5 54.59 63.00 5.10 o 3 6 5 57.72 43.94 6.02 o 4 6 5 15.75 14.19 5.20 o 1 7 5 17.41 21.21 5.22 o 0 0 6 216.17 213.64 9.73 o 1 0 6 83.22 90.97 4.00 o 2 0 6 738.25 819.19 7.03 o 3 0 6 4.34 4.49 3.13 o 4 0 6 144.36 124.22 6.47 o 5 0 6 392.41 400.34 21.73 o 6 0 6 29.59 29.13 7.07 o 7 0 6 78.47 84.96 10.70 o 1 1 6 6.68 11.10 1.87 o 2 1 6 3.12 2.97 1.32 o 3 1 6 136.35 129.33 3.84 o 4 1 6 8.91 10.15 3.28 o 5 1 6 29.56 22.16 3.96 o 6 1 6 15.43 16.57 3.89 o 7 1 6 75.93 87.09 6.63 o 0 2 6 137.42 129.71 4.09 o 1 2 6 439.57 431.67 5.70 o 2 2 6 593.78 603.61 6.50 o 3 2 6 76.28 69.30 3.42 o 4 2 6 159.85 165.78 4.55 o 5 2 6 0.53 1.08 1.20 o 6 2 6 0.73 1.58 1.54 o 7 2 6 3.65 2.90 2.08 o 1 3 6 83.05 69.39 3.13 o 2 3 6 43.68 42.94 2.99 o 3 3 6 63.06 58.81 3.53 o 4 3 6 205.95 194.42 5.16 o 5 3 6 4.75 1.50 1.01 o 6 3 6 1.39 1.66 1.99 o 7 3 6 0.72 6.08 3.37 o 0 4 6 316.51 332.68 10.21 o 1 4 6 2.31 2.28 1.63 o 2 4 6 11.32 10.44 3.19 o 3 4 6 91.73 93.28 4.04 o 4 4 6 47.01 40.46 3.71 o 5 4 6 44.49 44.76 4.20 o 6 4 6 77.82 90.37 5.41 o 1 5 6 13.32 7.08 2.77 o 2 5 6 0.59 1.19 1.15 o 3 5 6 20.28 13.29 3.95 o 4 5 6 11.46 10.32 4.57 o 5 5 6 7.88 2.39 2.55 o 0 6 6 182.03 188.56 10.33 o 1 6 6 38.08 36.91 5.30 o 2 6 6 0.86 1.84 2.22 o 3 6 6 0.32 1.85 1.40 o 1 1 7 72.90 66.54 2.71 o 2 1 7 97.53 88.87 3.08 o 3 1 7 61.37 61.38 3.62 o 4 1 7 28.57 21.93 3.93 o 5 1 7 120.93 105.70 6.01 o 6 1 7 0.02 0.47 1.06 o 7 1 7 4.54 3.87 2.37 o 0 2 7 366.11 353.72 6.38 o 1 2 7 1.01 1.53 1.46 o 2 2 7 17.67 18.04 3.21 o 3 2 7 268.93 261.54 5.47 o 4 2 7 38.43 33.82 3.53 o 5 2 7 1.27 0.39 0.81 o 6 2 7 32.52 24.29 4.93 o 7 2 7 10.36 17.74 4.87 o 1 3 7 51.28 42.32 3.46 o 2 3 7 161.78 148.10 4.65 o 3 3 7 69.10 64.46 3.76 o 4 3 7 13.98 12.82 2.93 o 5 3 7 7.31 5.18 2.06 o 6 3 7 30.21 27.08 5.15 o 0 4 7 67.11 69.30 6.34 o 1 4 7 131.26 137.56 5.93 o 2 4 7 0.95 1.48 1.26 o 3 4 7 95.49 107.17 5.12 o 4 4 7 109.40 102.73 4.95 o 5 4 7 4.87 7.86 2.44 o 6 4 7 0.11 2.98 1.88 o 1 5 7 22.53 23.12 4.62 o 2 5 7 62.96 58.61 4.94 o 3 5 7 20.45 13.15 4.59 o 4 5 7 2.00 6.20 5.05 o 0 6 7 87.82 91.86 8.52 o 1 6 7 28.44 31.66 5.63 o 2 6 7 1.96 6.41 3.61 o 3 6 7 39.11 37.19 7.32 o 0 0 8 187.10 157.29 7.99 o 1 0 8 136.94 128.54 5.35 o 2 0 8 830.14 838.42 9.62 o 3 0 8 440.80 472.46 10.37 o 4 0 8 147.56 142.48 9.36 o 5 0 8 23.49 25.92 8.35 o 6 0 8 24.79 26.70 7.36 o 7 0 8 6.34 3.66 6.53 o 1 1 8 274.81 268.41 4.39 o 2 1 8 0.56 0.72 0.55 o 3 1 8 84.22 78.29 4.53 o 4 1 8 154.01 149.97 5.95 o 5 1 8 74.63 74.49 5.79 o 6 1 8 2.77 5.76 5.29 o 7 1 8 4.00 2.92 2.33 o 0 2 8 69.78 66.23 5.35 o 1 2 8 223.02 215.23 4.73 o 2 2 8 204.14 212.29 4.93 o 3 2 8 7.77 4.41 2.46 o 4 2 8 137.04 144.29 6.31 o 5 2 8 31.34 26.32 4.87 o 6 2 8 112.23 129.94 6.82 o 1 3 8 5.89 5.49 2.67 o 2 3 8 65.51 58.11 4.50 o 3 3 8 93.36 89.51 4.87 o 4 3 8 29.93 25.60 3.80 o 5 3 8 1.14 1.48 1.54 o 6 3 8 0.04 2.20 2.49 o 0 4 8 412.11 426.67 10.97 o 1 4 8 0.23 0.90 1.99 o 2 4 8 36.25 37.61 3.95 o 3 4 8 5.18 6.41 3.04 o 4 4 8 10.38 5.02 2.77 o 5 4 8 62.61 69.08 5.31 o 1 5 8 4.56 11.42 4.49 o 2 5 8 31.20 29.04 5.48 o 3 5 8 3.54 6.10 3.08 o 4 5 8 24.72 20.48 4.85 o 0 6 8 15.01 20.57 7.14 o 1 6 8 14.29 21.91 4.45 o 1 1 9 59.49 55.97 3.00 o 2 1 9 0.01 0.14 0.40 o 3 1 9 24.04 23.12 3.65 o 4 1 9 92.25 84.78 6.51 o 5 1 9 75.51 80.43 6.61 o 6 1 9 1.54 1.46 1.35 o 0 2 9 0.28 0.16 4.32 o 1 2 9 2.07 1.01 1.14 o 2 2 9 57.15 56.73 3.80 o 3 2 9 224.66 209.22 6.13 o 4 2 9 0.76 0.62 0.91 o 5 2 9 7.18 4.20 3.22 o 6 2 9 10.25 7.78 4.66 o 1 3 9 54.06 42.79 5.15 o 2 3 9 0.07 0.94 1.32 o 3 3 9 14.73 16.76 4.14 o 4 3 9 0.13 0.76 1.52 o 5 3 9 9.74 3.71 2.16 o 0 4 9 7.10 6.39 3.95 o 1 4 9 63.82 65.38 5.19 o 2 4 9 33.37 29.29 5.36 o 3 4 9 10.89 8.81 3.10 o 4 4 9 30.71 35.16 8.99 o 1 5 9 3.38 5.53 2.18 o 2 5 9 59.71 63.13 6.49 o 3 5 9 6.02 14.25 4.50 o 0 0 10 445.74 431.62 12.68 o 1 0 10 228.59 243.67 7.42 o 2 0 10 107.93 97.27 6.95 o 3 0 10 141.81 151.52 9.80 o 4 0 10 347.87 380.72 14.59 o 5 0 10 0.46 0.49 1.66 o 1 1 10 3.46 0.45 0.78 o 2 1 10 403.70 419.48 7.91 o 3 1 10 19.67 19.32 4.51 o 4 1 10 9.23 3.75 3.24 o 5 1 10 2.25 8.02 4.15 o 0 2 10 349.09 350.64 10.95 o 1 2 10 52.38 38.82 4.27 o 2 2 10 60.00 64.77 5.26 o 3 2 10 224.48 251.60 6.81 o 4 2 10 55.13 55.96 5.62 o 5 2 10 35.77 37.65 6.11 o 1 3 10 58.96 64.92 5.16 o 2 3 10 50.17 52.77 4.80 o 3 3 10 3.84 4.99 3.35 o 4 3 10 64.58 65.01 6.58 o 0 4 10 0.36 1.28 1.77 o 1 4 10 101.27 117.58 6.24 o 2 4 10 3.83 2.92 2.17 o 3 4 10 0.75 2.72 3.92 o 1 5 10 0.41 1.67 1.49 o 1 1 11 32.83 28.06 3.90 o 2 1 11 0.01 1.22 1.69 o 3 1 11 1.28 1.48 1.94 o 4 1 11 61.03 57.05 6.31 o 0 2 11 0.53 2.86 2.57 o 1 2 11 5.61 2.22 1.90 o 2 2 11 40.69 40.97 4.87 o 3 2 11 44.50 25.67 6.21 o 4 2 11 3.39 1.23 1.96 o 1 3 11 5.31 7.41 4.08 o 2 3 11 0.51 0.76 0.99 o 3 3 11 0.69 3.19 3.36 o 0 4 11 0.01 0.55 1.30 o 1 4 11 0.06 4.08 3.92 o 2 4 11 108.55 133.01 7.10 o 0 0 12 0.00 0.14 2.51 o 1 0 12 232.24 249.29 11.76 o 2 0 12 0.44 -0.36 8.28 o 3 0 12 51.48 47.19 9.19 o 1 1 12 20.84 18.33 4.80 o 2 1 12 47.72 57.95 5.46 o 3 1 12 51.46 53.01 6.51 o 0 2 12 226.02 263.21 12.95 o 1 2 12 3.16 1.15 1.34 o 2 2 12 13.39 7.19 3.10 o 3 2 12 208.63 265.01 9.68 o 1 3 12 82.55 100.17 7.47 o 1 1 13 12.78 8.08 6.47 o