#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/41/2104172.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104172_Fobs loop_ _publ_author_name 'Thaimattam, Ram' 'Szafran, Miroslaw' 'Dega-Szafran, Zofia' 'Jaskolski, Mariusz' _publ_section_title ; Conformational richness and multiple Z' in salt co-crystal of N-methylpiperidine betaine with N-methylpiperidine betaine hexafluorosilicate ; _journal_coeditor_code RY5019 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 483 _journal_page_last 490 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.870 _cell_angle_beta 84.810 _cell_angle_gamma 63.857 _cell_length_a 11.5538 _cell_length_b 12.6207 _cell_length_c 22.7632 _exptl_crystal_F_000 1302.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file ry5019PBETSIF6-IIsup2.hkl _[local]_cod_data_source_block PBETSIF6-II #BEGIN Tags that were not found in dictionaries: _shelx_title 'PBETSIF6-II in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 379.08 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8251.90 6317.20 48.80 o 3 0 0 5546.26 4738.85 62.63 o 4 0 0 295.46 234.16 13.77 o 5 0 0 3712.27 3611.67 31.73 o 6 0 0 131.78 141.88 11.29 o 7 0 0 194.82 156.77 13.11 o 8 0 0 0.09 11.46 7.87 o 9 0 0 697.51 629.65 48.40 o 10 0 0 157.42 169.81 46.45 o 11 0 0 438.75 448.13 60.12 o 12 0 0 0.29 47.86 25.23 o 13 0 0 57.43 38.01 25.95 o -13 1 0 333.73 410.66 59.73 o -12 1 0 162.06 96.03 40.60 o -11 1 0 15.13 28.50 26.93 o -10 1 0 88.10 90.56 46.45 o -9 1 0 89.74 74.56 27.72 o -8 1 0 53.23 72.71 17.73 o -7 1 0 44.32 57.33 13.02 o -6 1 0 67.95 42.98 11.47 o -5 1 0 595.88 552.37 19.07 o -4 1 0 3042.68 2949.99 58.23 o -3 1 0 172.08 151.11 10.73 o -2 1 0 12405.68 11189.78 72.99 o 3 1 0 2930.31 2579.46 19.15 o 4 1 0 375.34 315.76 12.81 o 5 1 0 4844.60 4909.43 32.25 o 6 1 0 6293.62 6982.07 66.59 o 7 1 0 265.33 278.68 13.94 o 8 1 0 503.81 439.76 25.77 o 9 1 0 17.08 52.70 30.45 o 10 1 0 66.23 41.77 21.86 o 11 1 0 178.00 242.41 35.71 o 12 1 0 71.80 115.24 39.43 o 13 1 0 18.05 39.91 24.06 o -12 2 0 1.80 21.47 17.18 o -11 2 0 331.11 282.23 44.11 o -10 2 0 0.18 12.10 17.96 o -9 2 0 90.61 97.59 39.04 o -8 2 0 173.79 179.98 22.28 o -7 2 0 72.80 83.92 14.02 o -6 2 0 326.55 333.90 19.09 o -5 2 0 985.89 990.61 31.11 o -4 2 0 3585.60 3486.43 34.75 o -3 2 0 116.27 124.13 12.73 o -2 2 0 5670.78 4984.23 49.99 o -1 2 0 137.84 238.76 25.57 o 2 2 0 86468.02 81895.82 1276.87 o 3 2 0 39862.67 37591.20 235.19 o 4 2 0 367.87 484.10 11.45 o 5 2 0 5815.20 6151.70 32.90 o 6 2 0 563.09 572.61 15.39 o 7 2 0 41.39 61.04 9.35 o 8 2 0 30.56 23.23 11.88 o 9 2 0 264.84 260.37 34.35 o 10 2 0 172.54 178.71 27.54 o 11 2 0 194.49 162.73 32.20 o 12 2 0 24.47 46.38 23.73 o 13 2 0 286.51 373.67 71.05 o 14 2 0 9.29 10.12 25.88 o -12 3 0 247.02 178.39 44.89 o -11 3 0 135.66 160.83 45.67 o -10 3 0 14.54 24.59 30.06 o -9 3 0 30.09 15.22 14.05 o -8 3 0 123.43 99.34 17.32 o -7 3 0 301.20 270.09 24.09 o -6 3 0 527.46 580.64 31.06 o -5 3 0 79.87 86.73 14.52 o -4 3 0 29.32 30.14 10.66 o -3 3 0 7026.97 7459.67 123.60 o -2 3 0 1312.16 1478.23 38.63 o -1 3 0 4143.24 3723.85 35.67 o 0 3 0 3422.16 2972.52 27.16 o 1 3 0 16935.76 16187.61 83.93 o 2 3 0 64.08 109.33 10.02 o 3 3 0 5018.18 4499.17 39.46 o 4 3 0 41258.96 41501.48 117.53 o 5 3 0 471.89 491.71 18.87 o 6 3 0 187.66 156.76 14.09 o 7 3 0 1534.40 1540.77 29.48 o 8 3 0 231.65 225.21 19.40 o 9 3 0 4.06 18.62 10.97 o 10 3 0 146.42 123.20 24.37 o 11 3 0 174.83 186.10 22.61 o 12 3 0 37.65 30.91 20.89 o 13 3 0 14.58 32.02 18.08 o 14 3 0 3.08 33.62 28.17 o -11 4 0 51.52 73.00 29.28 o -10 4 0 23.33 46.84 30.06 o -9 4 0 171.14 170.20 43.33 o -8 4 0 330.73 316.45 22.89 o -7 4 0 382.42 323.73 21.62 o -6 4 0 14.99 23.66 10.13 o -5 4 0 353.22 404.72 21.95 o -4 4 0 208.04 200.17 16.60 o -3 4 0 502.42 486.78 19.41 o -2 4 0 49.21 58.28 13.31 o -1 4 0 12.94 12.26 8.44 o 0 4 0 5371.14 5495.77 64.75 o 1 4 0 883.64 1079.61 15.67 o 3 4 0 2642.99 2564.63 58.25 o 4 4 0 12453.79 12616.27 92.13 o 5 4 0 1836.19 1909.54 40.79 o 6 4 0 1101.94 1105.96 34.60 o 7 4 0 669.72 659.18 30.44 o 8 4 0 645.25 603.05 24.67 o 9 4 0 1020.54 1065.69 29.94 o 10 4 0 71.75 105.40 29.10 o 11 4 0 470.04 524.46 38.09 o 12 4 0 19.58 14.40 13.83 o 13 4 0 6.48 29.74 24.09 o 14 4 0 14.66 50.00 25.46 o -10 5 0 46.33 17.18 30.45 o -9 5 0 68.68 84.71 33.57 o -8 5 0 48.33 35.76 14.41 o -7 5 0 337.23 322.22 25.04 o -6 5 0 81.69 72.74 14.81 o -5 5 0 29.03 30.81 13.90 o -4 5 0 39.39 67.38 14.69 o -3 5 0 16.28 29.49 10.43 o -2 5 0 5.47 41.15 11.96 o -1 5 0 926.78 920.74 27.00 o 0 5 0 4245.15 4167.75 38.06 o 1 5 0 303.52 398.11 12.02 o 2 5 0 3373.86 3747.82 29.06 o 3 5 0 8900.06 9053.79 82.95 o 4 5 0 4444.66 4393.45 41.33 o 5 5 0 5.88 36.20 16.13 o 6 5 0 6880.14 7436.72 69.07 o 7 5 0 43.52 44.72 19.90 o 8 5 0 1940.09 1975.92 48.37 o 9 5 0 303.09 283.89 33.96 o 10 5 0 95.66 102.51 24.52 o 11 5 0 260.60 241.87 34.23 o 12 5 0 25.59 15.34 16.68 o 13 5 0 18.08 19.00 20.50 o 14 5 0 29.94 18.97 15.19 o -10 6 0 11.92 3.51 21.47 o -9 6 0 10.32 16.79 26.54 o -8 6 0 2.24 9.40 16.31 o -7 6 0 77.07 98.05 27.87 o -6 6 0 14.08 11.98 10.17 o -5 6 0 165.26 143.68 19.10 o -4 6 0 46.63 35.14 10.70 o -3 6 0 668.28 708.62 24.81 o -2 6 0 1580.43 1712.63 33.83 o -1 6 0 977.90 1014.44 29.71 o 0 6 0 8.75 8.97 5.72 o 1 6 0 1037.39 1242.80 20.27 o 2 6 0 11450.03 11491.20 105.68 o 3 6 0 11867.29 12641.07 147.36 o 4 6 0 1910.75 2032.76 31.43 o 5 6 0 430.75 486.73 19.38 o 6 6 0 2210.77 2267.53 46.09 o 7 6 0 3.00 34.75 19.32 o 8 6 0 1770.63 1930.50 48.61 o 9 6 0 24.63 27.02 19.88 o 10 6 0 49.27 28.10 12.67 o 11 6 0 36.39 31.85 16.40 o 12 6 0 105.43 63.04 24.01 o 13 6 0 14.89 25.27 21.69 o 14 6 0 16.95 29.87 22.55 o -9 7 0 15.35 20.69 29.67 o -8 7 0 29.71 20.02 15.73 o -7 7 0 492.72 543.43 30.61 o -6 7 0 216.60 166.55 24.17 o -5 7 0 1127.02 1114.50 40.12 o -4 7 0 324.50 289.09 23.81 o -3 7 0 108.84 94.30 16.65 o -2 7 0 9.15 18.63 9.79 o -1 7 0 20.62 21.40 11.55 o 0 7 0 10.91 28.63 11.66 o 1 7 0 74.37 72.73 8.16 o 2 7 0 5063.59 5393.15 39.57 o 3 7 0 6025.05 6161.53 41.99 o 4 7 0 14375.89 16232.13 129.86 o 5 7 0 1759.88 1919.98 30.48 o 6 7 0 480.89 598.73 22.39 o 7 7 0 665.71 603.26 24.34 o 8 7 0 722.31 666.54 28.11 o 9 7 0 3696.19 3875.99 124.53 o 10 7 0 3703.02 4005.66 93.69 o 11 7 0 121.58 121.82 26.54 o 12 7 0 27.05 32.90 17.79 o 13 7 0 1.81 23.01 21.80 o 14 7 0 3.77 38.56 20.82 o -8 8 0 83.58 36.69 31.23 o -7 8 0 211.06 214.92 26.11 o -6 8 0 2.12 13.87 16.21 o -5 8 0 4.51 15.95 15.57 o -4 8 0 142.05 124.23 19.24 o -3 8 0 0.34 23.09 15.15 o -2 8 0 837.66 906.99 28.18 o -1 8 0 192.04 147.31 21.27 o 0 8 0 25.28 41.61 9.48 o 1 8 0 172.49 163.69 16.66 o 2 8 0 778.15 746.00 26.23 o 3 8 0 1005.61 1017.75 20.59 o 4 8 0 288.40 272.42 15.38 o 5 8 0 2291.67 2425.74 35.03 o 6 8 0 54.57 41.74 13.60 o 7 8 0 5716.73 5429.64 106.61 o 8 8 0 101.81 98.54 23.45 o 9 8 0 323.20 378.48 25.85 o 10 8 0 894.36 861.32 42.55 o 11 8 0 391.20 420.88 33.50 o 12 8 0 25.91 31.89 15.10 o 13 8 0 1.68 33.48 18.94 o 14 8 0 2.08 54.49 26.29 o -7 9 0 3.90 20.69 16.00 o -6 9 0 114.62 90.33 27.90 o -5 9 0 2.01 32.49 18.47 o -4 9 0 93.16 105.58 16.39 o -3 9 0 109.97 82.18 15.61 o -2 9 0 89.79 74.25 20.81 o -1 9 0 144.98 117.90 20.07 o 0 9 0 0.00 24.05 15.96 o 1 9 0 161.88 158.12 16.45 o 2 9 0 441.59 463.21 28.69 o 3 9 0 371.78 353.61 20.26 o 4 9 0 101.91 84.28 16.67 o 5 9 0 864.67 847.22 25.62 o 6 9 0 419.01 423.54 20.79 o 7 9 0 1094.21 1027.08 30.15 o 8 9 0 1370.20 1276.55 37.34 o 9 9 0 179.48 174.12 19.94 o 10 9 0 731.82 819.35 34.36 o 11 9 0 202.73 186.35 29.59 o 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4.32 0.78 38.65 o 8 16 0 207.66 229.92 53.87 o -8 -16 1 135.64 101.49 40.60 o -7 -16 1 220.57 152.63 39.04 o -6 -16 1 1.71 3.89 16.87 o -5 -16 1 222.35 230.27 35.60 o -11 -15 1 1.64 12.12 24.65 o -10 -15 1 30.85 27.93 23.78 o -9 -15 1 129.57 127.65 42.55 o -8 -15 1 45.09 21.47 26.54 o -7 -15 1 55.58 37.08 34.35 o -6 -15 1 74.13 49.28 22.73 o -5 -15 1 13.08 52.09 29.78 o -4 -15 1 5.39 38.67 22.99 o -3 -15 1 15.41 43.90 23.45 o -2 -15 1 68.97 54.67 25.88 o -1 -15 1 10.65 22.18 25.21 o -12 -14 1 2.42 25.25 25.76 o -11 -14 1 158.71 136.62 31.60 o -10 -14 1 161.80 162.30 30.45 o -9 -14 1 38.15 47.11 23.12 o -8 -14 1 344.43 393.82 38.81 o -7 -14 1 0.44 31.23 32.79 o -6 -14 1 11.42 40.24 20.56 o -5 -14 1 369.72 326.15 33.12 o -4 -14 1 61.99 52.58 24.01 o -3 -14 1 226.48 200.98 38.84 o -2 -14 1 88.70 163.32 34.51 o -1 -14 1 63.12 41.58 24.73 o 0 -14 1 244.15 293.94 45.87 o 1 -14 1 26.68 65.53 27.34 o -13 -13 1 2.78 22.55 23.15 o -12 -13 1 0.01 34.90 20.17 o -11 -13 1 71.19 59.59 27.38 o -10 -13 1 34.64 40.60 20.72 o -9 -13 1 11.83 31.21 16.34 o -8 -13 1 10.35 10.37 19.90 o -7 -13 1 8.29 20.72 15.59 o -6 -13 1 97.56 124.74 22.52 o -5 -13 1 0.01 20.25 18.58 o -4 -13 1 30.25 25.00 18.74 o -3 -13 1 40.35 46.45 22.02 o -2 -13 1 27.77 32.84 21.19 o -1 -13 1 14.93 15.22 14.32 o 0 -13 1 13.34 41.38 35.52 o 1 -13 1 18.86 43.42 23.11 o 2 -13 1 7.54 30.50 21.21 o -13 -12 1 20.00 34.82 20.54 o -12 -12 1 377.36 408.85 43.89 o -11 -12 1 24.55 40.13 33.18 o -10 -12 1 21.29 22.20 23.66 o -9 -12 1 102.98 102.45 24.45 o -8 -12 1 67.53 77.68 24.12 o -7 -12 1 138.64 132.93 33.18 o -6 -12 1 0.59 17.22 12.66 o -5 -12 1 149.32 109.90 17.98 o -4 -12 1 141.55 118.19 23.82 o -3 -12 1 4.63 21.65 16.79 o -2 -12 1 240.17 256.83 33.65 o -1 -12 1 210.98 205.72 50.75 o 0 -12 1 8.29 56.99 33.57 o 1 -12 1 149.46 212.05 36.68 o 2 -12 1 234.26 299.37 43.51 o 3 -12 1 304.18 301.64 40.14 o 4 -12 1 69.51 40.28 25.62 o -14 -11 1 159.35 200.47 30.08 o -13 -11 1 2.17 11.63 15.96 o -12 -11 1 4.13 8.79 16.60 o -11 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