#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104210.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104210_Fobs loop_ _publ_author_name 'Michiue, Yuichi' 'Kimizuka, Noboru' 'Kanke, Yasushi' _publ_section_title ; Structure of Ga~2~O~3~(ZnO)~6~: a member of the homologous series Ga~2~O~3~(ZnO)~m~ ; _journal_coeditor_code KD5022 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 521 _journal_page_last 526 _journal_volume 64 _journal_year 2008 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _[local]_cod_data_source_file kd5022Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_intensity_meas _refln_intensity_calc _refln_intensity_sigma _refln_observed_status 4 0 0 14505.1 13633.3 202.6 o 6 0 0 3656.0 3100.7 113.1 o 1 1 0 223.6 266.9 13.7 o 3 1 0 61.2 54.6 9.0 o 5 1 0 8.8 4.3 31.1 < 2 2 0 69.7 33.4 6.7 o 4 2 0 20.5 19.6 13.8 < 6 2 0 23.3 8.0 27.9 < 1 3 0 69.0 62.2 6.2 o 3 3 0 -2.3 27.1 19.9 < 5 3 0 -39.5 6.1 32.4 < 0 4 0 -13.4 0.8 11.5 < 2 4 0 21.9 8.9 6.1 o 4 4 0 -6.4 15.4 25.4 < 6 4 0 -23.7 6.8 35.8 < 1 5 0 1576.8 1566.8 30.6 o 3 5 0 415.6 402.6 26.9 o 5 5 0 101.9 90.3 16.5 o 0 6 0 5.5 1.3 14.4 < 2 6 0 17.5 8.8 6.9 o 4 6 0 -25.3 5.1 26.8 < 6 6 0 4.8 1.3 35.6 < 1 7 0 30.0 25.6 6.0 o 3 7 0 -10.4 11.4 20.0 < 5 7 0 -17.4 0.8 32.5 < 0 8 0 28856.5 27611.3 310.1 o 2 8 0 18917.6 18807.1 221.2 o 4 8 0 5429.9 5376.8 109.7 o 6 8 0 1467.7 1284.5 75.5 o 1 9 0 80.6 71.5 7.7 o 3 9 0 58.8 45.5 9.9 o 5 9 0 -6.0 12.1 34.9 < 0 10 0 213.4 201.6 19.4 o 2 10 0 199.8 186.0 15.2 o 4 10 0 68.6 77.9 13.7 o 6 10 0 -28.3 21.6 44.4 < 1 11 0 43.0 40.9 7.2 o 3 11 0 -3.1 14.8 23.9 < 5 11 0 -44.3 4.0 37.5 < 0 12 0 -31.1 3.6 19.9 < 2 12 0 -7.3 2.7 19.7 < 4 12 0 -3.3 2.0 30.0 < 6 12 0 -28.7 1.7 43.7 < 1 13 0 109.6 123.4 10.4 o 3 13 0 129.2 131.6 12.6 o 5 13 0 6.6 45.5 42.3 < 0 14 0 28.8 6.8 20.3 < 2 14 0 -16.7 2.4 21.4 < 4 14 0 -55.7 0.0 31.1 < 6 14 0 2.3 0.6 43.1 < 1 15 0 65.7 52.3 9.3 o 3 15 0 29.8 49.6 25.9 < 5 15 0 34.8 32.9 16.9 o 0 16 0 12430.4 11962.6 168.3 o 2 16 0 7007.5 7360.9 114.7 o 4 16 0 2448.5 2431.0 80.6 o 1 17 0 25.0 2.5 22.7 < 3 17 0 1.1 0.7 28.7 < 5 17 0 -62.5 1.5 42.2 < 0 18 0 1582.4 1420.4 51.5 o 2 18 0 744.3 886.5 42.1 o 4 18 0 296.0 298.0 24.0 o 1 19 0 229.6 226.3 20.4 o 3 19 0 156.7 159.6 15.0 o 5 19 0 57.5 72.9 44.9 < 0 20 0 2.8 13.5 26.7 < 2 20 0 -32.3 8.6 26.1 < 4 20 0 46.2 3.6 33.1 < 1 21 0 608.7 692.5 41.7 o 3 21 0 334.1 345.2 30.5 o 5 21 0 2.6 120.7 53.4 < 0 22 0 -17.5 17.5 31.2 < 2 22 0 27.4 9.5 28.0 < 4 22 0 29.7 3.6 38.0 < 1 23 0 134.0 144.4 14.3 o 3 23 0 109.6 116.7 16.2 o 5 23 0 52.1 60.9 20.7 o 0 24 0 207.9 191.8 19.5 o 2 24 0 106.2 139.8 15.8 o 4 24 0 33.9 62.0 42.7 < 1 25 0 84.8 77.7 15.0 o 3 25 0 19.2 37.3 36.4 < 0 26 0 627.8 734.6 54.9 o 2 26 0 551.4 540.5 47.1 o 4 26 0 185.3 239.0 22.6 o 1 27 0 -7.7 1.3 33.4 < 3 27 0 43.1 2.9 36.2 < 0 28 0 48.5 1.8 36.8 < 2 28 0 -23.1 0.5 38.1 < 4 28 0 -0.7 0.1 19.1 < 1 29 0 -75.2 3.0 40.6 < 3 29 0 44.0 0.6 40.2 < 0 30 0 35.2 14.0 41.4 < 2 30 0 -53.1 11.2 37.3 < 4 30 0 10.9 4.6 42.1 < 1 31 0 176.6 145.7 18.9 o 3 31 0 62.0 101.4 46.0 < 0 32 0 421.5 359.1 38.5 o 2 32 0 253.0 244.8 25.3 o 1 33 0 71.3 50.4 19.6 o 3 33 0 55.1 31.2 20.4 o 0 34 0 779.7 728.2 74.2 o 2 34 0 529.9 565.2 43.2 o 1 35 0 37.5 62.6 28.9 < 0 36 0 -5.6 0.1 50.5 < 2 36 0 13.6 0.1 45.4 < 1 37 0 -45.7 3.8 50.1 < 0 38 0 -15.7 1.3 49.2 < 1 1 1 8.4 11.9 11.3 < 3 1 1 4.6 2.1 12.8 < 5 1 1 -1.1 0.1 21.4 < 2 2 1 64.8 58.9 4.7 o 4 2 1 44.1 55.1 8.3 o 6 2 1 -48.4 25.6 29.2 < 1 3 1 7095.0 6903.8 109.3 o 3 3 1 1889.7 1890.5 37.5 o 5 3 1 479.5 411.8 27.7 o 0 4 1 7.3 23.0 10.0 < 2 4 1 13.6 23.1 8.1 < 4 4 1 28.6 8.8 17.7 < 6 4 1 19.9 1.3 26.0 < 1 5 1 10421.0 10262.4 166.6 o 3 5 1 3844.9 3708.0 59.2 o 5 5 1 882.3 868.0 39.5 o 0 6 1 214.9 222.4 12.5 o 2 6 1 41.2 54.8 16.6 o 4 6 1 -15.9 2.0 18.9 < 6 6 1 -60.3 0.0 29.4 < 1 7 1 35.8 26.3 4.2 o 3 7 1 12.2 10.4 14.4 < 5 7 1 -14.4 1.4 23.9 < 0 8 1 807.5 760.5 30.1 o 2 8 1 202.0 205.3 11.2 o 4 8 1 11.1 22.2 22.3 < 6 8 1 -242.9 3.6 149.6 < 1 9 1 6.9 1.9 9.9 < 3 9 1 3.3 0.4 14.5 < 5 9 1 -14.1 0.5 23.4 < 0 10 1 508.1 461.0 18.1 o 2 10 1 309.4 244.9 52.7 o 4 10 1 78.8 71.7 9.6 o 6 10 1 -38.3 20.8 32.5 < 1 11 1 180.0 172.5 9.8 o 3 11 1 120.4 128.0 10.5 o 5 11 1 46.2 54.7 15.8 o 0 12 1 23.5 41.6 22.0 < 2 12 1 28.5 36.2 13.9 o 4 12 1 1.0 12.3 37.9 < 6 12 1 28.3 1.6 28.9 < 1 13 1 10720.5 10738.2 124.5 o 3 13 1 3995.5 4053.7 66.7 o 5 13 1 1103.6 1060.3 52.0 o 0 14 1 136.8 131.2 9.1 o 2 14 1 67.1 70.4 7.2 o 4 14 1 5.3 14.9 22.1 < 6 14 1 -5.8 1.5 31.2 < 1 15 1 24.2 11.0 14.1 < 3 15 1 18.0 16.7 18.4 < 5 15 1 -10.4 7.7 27.4 < 0 16 1 -40.8 2.0 18.3 < 2 16 1 -12.5 1.3 17.4 < 4 16 1 -2.3 0.3 24.5 < 1 17 1 -4.5 2.6 15.6 < 3 17 1 3.8 8.4 19.4 < 5 17 1 22.5 5.7 21.5 < 0 18 1 460.3 454.3 25.4 o 2 18 1 309.9 284.6 25.3 o 4 18 1 79.8 102.7 35.3 o 1 19 1 291.8 278.9 18.6 o 3 19 1 69.3 91.5 30.2 o 5 19 1 16.5 20.3 29.8 < 0 20 1 34.4 23.5 9.2 o 2 20 1 4.4 15.1 19.0 < 4 20 1 -1.6 2.6 23.6 < 1 21 1 4804.3 4834.3 91.7 o 3 21 1 1993.5 2084.0 70.9 o 5 21 1 637.8 644.0 39.0 o 0 22 1 -10.7 13.2 22.7 < 2 22 1 17.1 9.0 14.2 < 4 22 1 -34.9 2.7 30.8 < 1 23 1 7.3 2.6 31.3 < 3 23 1 -32.2 1.6 37.7 < 5 23 1 39.8 0.9 31.0 < 0 24 1 -23.3 1.1 23.2 < 2 24 1 -13.3 0.0 22.2 < 4 24 1 -2.3 0.3 27.8 < 1 25 1 12.8 0.0 21.4 < 3 25 1 -15.0 3.0 50.2 < 0 26 1 204.0 175.0 13.9 o 2 26 1 103.6 118.4 12.0 o 4 26 1 17.9 50.0 21.7 < 1 27 1 200.1 211.6 14.8 o 3 27 1 77.7 114.9 22.3 o 0 28 1 -7.4 4.6 27.9 < 2 28 1 -22.0 3.6 25.0 < 4 28 1 -58.2 0.9 33.6 < 1 29 1 799.2 849.8 39.8 o 3 29 1 477.0 459.2 26.5 o 0 30 1 -41.7 2.3 72.5 < 2 30 1 4.9 3.6 27.5 < 4 30 1 -48.5 3.2 33.6 < 1 31 1 6.4 11.7 28.1 < 3 31 1 14.2 9.3 31.1 < 0 32 1 -21.1 17.7 33.8 < 2 32 1 -66.4 14.2 32.3 < 1 33 1 22.4 4.5 29.8 < 3 33 1 24.4 1.8 22.7 < 0 34 1 142.9 110.9 16.1 o 2 34 1 27.9 74.7 29.0 < 1 35 1 84.3 111.6 53.0 < 0 36 1 19.2 10.0 49.2 < 2 36 1 -9.5 10.1 27.1 < 1 37 1 103.9 90.1 15.9 o 0 38 1 49.9 6.8 35.2 < 2 0 2 148.4 137.0 15.3 o 4 0 2 81.7 75.6 9.0 o 6 0 2 19.1 21.4 21.3 < 1 1 2 194.1 184.4 29.9 o 3 1 2 49.3 42.0 6.3 o 5 1 2 20.5 6.5 22.4 < 0 2 2 7.2 1.6 8.9 < 2 2 2 12.0 4.4 9.8 < 4 2 2 7.7 4.4 18.6 < 6 2 2 37.1 3.1 25.9 < 1 3 2 6570.6 6286.2 164.8 o 3 3 2 1589.3 1562.2 33.9 o 5 3 2 339.4 344.4 21.6 o 0 4 2 -2.3 1.6 12.1 < 2 4 2 13.6 5.2 9.7 < 4 4 2 26.1 10.7 18.1 < 6 4 2 5.7 4.4 27.0 < 1 5 2 4640.8 4731.0 59.8 o 3 5 2 1965.3 1860.6 40.8 o 5 5 2 434.7 436.5 24.3 o 0 6 2 282.6 304.9 15.2 o 2 6 2 201.5 203.5 11.3 o 4 6 2 57.8 62.6 8.8 o 6 6 2 -7.4 11.3 30.1 < 1 7 2 164.8 146.4 9.4 o 3 7 2 30.2 43.8 11.8 o 5 7 2 -17.4 6.8 47.1 < 0 8 2 0.3 0.5 12.8 < 2 8 2 15.2 7.0 11.8 < 4 8 2 -5.3 7.7 30.7 < 6 8 2 9.1 2.6 29.1 < 1 9 2 18.3 12.3 4.6 o 3 9 2 26.5 12.6 15.7 < 5 9 2 21.3 4.2 23.8 < 0 10 2 276.0 243.7 22.0 o 2 10 2 217.1 214.5 13.8 o 4 10 2 100.4 93.5 9.8 o 6 10 2 -25.2 29.7 31.5 < 1 11 2 14.3 0.8 10.8 < 3 11 2 10.7 0.3 16.2 < 5 11 2 -14.0 0.2 24.7 < 0 12 2 8.4 27.8 13.4 < 2 12 2 6.5 15.3 14.1 < 4 12 2 6.9 3.9 20.6 < 6 12 2 12.3 0.8 21.5 < 1 13 2 7658.6 7653.8 94.1 o 3 13 2 2521.0 2609.6 51.6 o 5 13 2 682.1 666.3 80.6 o 0 14 2 156.0 132.1 27.3 o 2 14 2 95.9 107.2 7.5 o 4 14 2 64.8 36.9 9.8 o 6 14 2 18.7 7.3 26.1 < 1 15 2 17.4 6.0 12.6 < 3 15 2 -7.5 0.1 18.5 < 5 15 2 -59.9 0.2 27.7 < 0 16 2 -25.7 13.2 18.1 < 2 16 2 -9.1 9.4 31.6 < 4 16 2 29.8 4.8 21.9 < 1 17 2 -1.3 2.1 15.2 < 3 17 2 15.0 5.4 19.1 < 5 17 2 -9.9 3.1 27.3 < 0 18 2 1116.0 1039.9 34.6 o 2 18 2 641.8 679.7 28.2 o 4 18 2 232.0 247.7 15.2 o 1 19 2 1069.8 1043.1 33.3 o 3 19 2 392.6 377.5 24.0 o 5 19 2 82.5 95.6 25.5 o 0 20 2 95.1 72.1 20.0 o 2 20 2 27.7 49.3 19.8 < 4 20 2 -12.0 18.3 30.8 < 1 21 2 1339.1 1306.9 37.7 o 3 21 2 610.7 603.5 35.3 o 5 21 2 149.4 198.2 69.5 o 0 22 2 186.4 192.8 12.2 o 2 22 2 150.9 140.8 10.6 o 4 22 2 52.8 57.9 30.3 < 1 23 2 2.9 9.5 20.4 < 3 23 2 -12.4 17.5 24.4 < 5 23 2 -19.8 12.9 67.0 < 0 24 2 96.8 71.8 11.2 o 2 24 2 59.5 55.2 23.7 o 4 24 2 7.8 26.1 41.8 < 1 25 2 -11.0 4.4 39.2 < 3 25 2 -17.2 2.5 26.4 < 0 26 2 384.1 342.2 28.8 o 2 26 2 256.3 260.1 16.3 o 4 26 2 -11.4 121.7 34.8 < 1 27 2 870.2 850.7 38.8 o 3 27 2 421.4 426.0 39.3 o 0 28 2 51.5 74.7 22.7 o 2 28 2 38.0 62.2 27.2 < 4 28 2 41.1 32.7 23.5 < 1 29 2 168.6 183.6 17.1 o 3 29 2 60.2 120.6 32.7 < 0 30 2 16.5 1.0 31.6 < 2 30 2 6.3 0.5 26.1 < 4 30 2 -70.3 0.2 33.5 < 1 31 2 147.9 127.6 14.0 o 3 31 2 57.7 85.2 14.5 o 0 32 2 176.5 146.3 15.7 o 2 32 2 120.2 132.3 14.8 o 1 33 2 34.8 1.6 23.8 < 3 33 2 53.7 0.5 31.3 < 0 34 2 211.5 203.0 39.4 o 2 34 2 151.1 155.4 19.9 o 1 35 2 590.7 541.1 91.5 o 0 36 2 13.4 26.9 27.8 < 2 36 2 0.5 27.2 34.7 < 1 37 2 -45.8 2.2 33.6 < 0 38 2 19.6 0.9 47.8 < 1 1 3 -1.0 0.1 6.5 < 3 1 3 6.1 1.9 10.4 < 5 1 3 -4.6 1.6 21.4 < 0 2 3 10.3 9.8 10.0 < 2 2 3 36.3 28.3 4.6 o 4 2 3 10.6 22.3 14.1 < 6 2 3 -31.3 7.7 27.6 < 1 3 3 2019.1 1896.2 68.8 o 3 3 3 431.3 407.1 26.7 o 5 3 3 47.1 78.5 19.5 o 0 4 3 -5.3 17.5 15.0 < 2 4 3 19.9 13.7 10.1 < 4 4 3 -34.0 5.1 18.9 < 6 4 3 -3.4 1.1 45.4 < 1 5 3 534.8 573.7 18.9 o 3 5 3 294.2 275.6 22.2 o 5 5 3 47.6 58.5 20.5 o 0 6 3 1843.3 1951.1 116.2 o 2 6 3 787.4 770.6 20.8 o 4 6 3 148.0 147.7 9.9 o 6 6 3 2.8 31.9 31.7 < 1 7 3 8.9 3.8 8.9 < 3 7 3 -0.3 0.5 15.1 < 5 7 3 22.8 0.1 23.0 < 0 8 3 4.2 3.4 10.1 < 2 8 3 -7.3 5.1 12.1 < 4 8 3 -20.1 5.4 35.1 < 6 8 3 0.5 2.2 35.0 < 1 9 3 -19.6 0.0 23.4 < 3 9 3 9.1 0.0 19.3 < 5 9 3 8.6 0.0 20.7 < 0 10 3 1657.7 1536.2 32.1 o 2 10 3 939.3 906.5 39.6 o 4 10 3 269.6 273.0 16.6 o 6 10 3 -11.0 73.6 48.7 < 1 11 3 22.3 8.1 8.4 o 3 11 3 32.3 16.1 7.5 o 5 11 3 -16.6 10.9 26.5 < 0 12 3 38.4 24.5 10.5 o 2 12 3 32.2 28.5 6.4 o 4 12 3 17.4 17.1 19.8 < 6 12 3 43.0 6.5 28.0 < 1 13 3 2550.6 2524.2 49.0 o 3 13 3 911.6 916.1 32.1 o 5 13 3 238.2 248.6 15.3 o 0 14 3 841.8 809.0 66.3 o 2 14 3 519.8 513.6 25.6 o 4 14 3 154.6 154.0 12.2 o 6 14 3 -57.7 38.0 109.7 < 1 15 3 12.1 14.4 15.0 < 3 15 3 -8.8 17.9 19.3 < 5 15 3 -11.9 8.1 33.1 < 0 16 3 45.9 73.9 18.2 o 2 16 3 32.6 30.2 13.6 o 4 16 3 -8.4 6.9 27.8 < 1 17 3 -18.4 2.2 16.0 < 3 17 3 33.8 3.7 19.4 < 5 17 3 -52.0 1.7 28.1 < 0 18 3 3247.8 2989.0 227.3 o 2 18 3 1880.1 1862.6 43.0 o 4 18 3 649.5 640.3 55.4 o 1 19 3 391.6 389.1 23.3 o 3 19 3 192.4 208.6 13.5 o 5 19 3 47.5 79.6 33.2 < 0 20 3 49.7 31.9 10.8 o 2 20 3 17.2 25.7 19.8 < 4 20 3 44.6 11.2 20.1 o 1 21 3 226.8 223.5 14.7 o 3 21 3 155.4 147.1 11.5 o 5 21 3 31.5 61.1 29.2 < 0 22 3 1135.4 1021.4 127.0 o 2 22 3 712.6 706.1 31.8 o 4 22 3 281.3 288.0 34.6 o 1 23 3 -55.2 3.8 21.1 < 3 23 3 24.3 2.0 22.7 < 5 23 3 -17.1 0.6 35.7 < 0 24 3 -8.8 0.1 24.7 < 2 24 3 -10.7 0.9 22.2 < 4 24 3 -15.8 1.4 26.2 < 1 25 3 -3.7 13.1 23.1 < 3 25 3 3.3 2.4 26.2 < 0 26 3 1348.1 1225.8 70.1 o 2 26 3 827.5 853.8 112.1 o 4 26 3 334.8 365.7 52.2 o 1 27 3 727.5 723.9 84.3 o 3 27 3 428.3 399.9 29.8 o 0 28 3 -22.9 2.2 49.1 < 2 28 3 -43.9 3.0 24.9 < 4 28 3 -4.0 3.0 43.0 < 1 29 3 57.9 66.3 49.0 < 3 29 3 4.4 45.0 31.3 < 0 30 3 77.2 79.4 45.7 < 2 30 3 34.0 69.1 31.5 < 4 30 3 -26.8 40.1 40.6 < 1 31 3 14.3 30.4 23.4 < 3 31 3 28.4 13.9 23.4 < 0 32 3 3.5 2.7 43.2 < 2 32 3 3.9 2.1 24.8 < 1 33 3 28.0 2.3 24.8 < 3 33 3 -10.8 1.0 34.8 < 0 34 3 947.3 721.0 128.7 o 2 34 3 626.1 537.5 39.9 o 1 35 3 369.6 318.7 24.1 o 0 36 3 -6.3 0.1 60.3 < 2 36 3 -10.6 0.2 48.0 < 1 37 3 -10.6 0.1 37.6 < 0 38 3 -19.0 12.6 36.0 < 0 0 4 21.3 9.2 6.3 o 2 0 4 22.6 17.9 7.7 o 4 0 4 13.9 10.2 17.9 < 6 0 4 -10.6 3.2 28.0 < 1 1 4 434.0 454.2 31.2 o 3 1 4 152.4 156.3 9.6 o 5 1 4 48.3 41.2 18.4 o 0 2 4 8.5 12.5 7.4 < 2 2 4 -18.0 4.6 10.6 < 4 2 4 -25.5 0.7 30.8 < 6 2 4 -9.4 0.0 38.3 < 1 3 4 69.6 77.0 5.9 o 3 3 4 23.5 35.6 15.1 < 5 3 4 -20.7 9.9 29.3 < 0 4 4 28.1 41.8 15.4 < 2 4 4 -18.0 7.3 10.9 < 4 4 4 -28.7 0.2 18.7 < 6 4 4 -71.0 0.1 28.6 < 1 5 4 32.5 33.2 4.5 o 3 5 4 47.8 51.3 6.9 o 5 5 4 20.9 15.2 24.8 < 0 6 4 4874.3 4852.1 196.8 o 2 6 4 2109.3 2135.3 35.3 o 4 6 4 537.3 481.1 26.6 o 6 6 4 96.9 115.5 32.9 o 1 7 4 1.0 9.2 10.3 < 3 7 4 0.0 7.9 22.5 < 5 7 4 -3.9 1.9 23.6 < 0 8 4 63.3 40.3 7.2 o 2 8 4 19.8 22.0 12.5 < 4 8 4 0.2 6.2 21.1 < 6 8 4 54.8 1.1 28.7 < 1 9 4 135.3 140.1 7.9 o 3 9 4 87.9 84.8 7.8 o 5 9 4 36.8 27.5 13.1 o 0 10 4 2573.4 2457.5 72.6 o 2 10 4 1129.1 1165.9 41.1 o 4 10 4 289.0 267.8 18.1 o 6 10 4 35.0 61.8 57.1 < 1 11 4 49.8 45.2 5.6 o 3 11 4 15.1 24.3 14.6 < 5 11 4 1.8 7.9 26.2 < 0 12 4 9.2 2.3 15.9 < 2 12 4 10.8 2.1 13.7 < 4 12 4 -18.5 1.0 20.4 < 6 12 4 -0.9 0.2 31.5 < 1 13 4 424.6 422.7 18.7 o 3 13 4 202.1 191.7 19.2 o 5 13 4 56.5 60.9 12.3 o 0 14 4 2752.1 2612.7 191.5 o 2 14 4 1529.1 1551.5 54.7 o 4 14 4 420.3 447.8 28.7 o 6 14 4 9.6 117.4 79.6 < 1 15 4 -5.8 5.4 15.3 < 3 15 4 10.1 5.6 17.8 < 5 15 4 44.5 1.9 16.0 o 0 16 4 6.2 4.9 18.2 < 2 16 4 19.2 3.1 13.8 < 4 16 4 25.1 0.8 23.4 < 1 17 4 5.9 4.2 16.6 < 3 17 4 -0.6 0.1 21.2 < 5 17 4 -2.6 0.1 23.9 < 0 18 4 2421.3 2160.0 248.6 o 2 18 4 1268.9 1312.1 37.6 o 4 18 4 435.4 432.9 41.7 o 1 19 4 267.5 278.2 18.5 o 3 19 4 149.9 158.1 11.1 o 5 19 4 -19.0 56.9 31.1 < 0 20 4 28.9 20.2 15.2 < 2 20 4 15.3 9.2 18.9 < 4 20 4 -20.9 1.3 26.3 < 1 21 4 21.0 4.7 18.2 < 3 21 4 -21.0 1.5 22.8 < 5 21 4 -46.3 0.6 56.1 < 0 22 4 3036.9 2676.8 399.3 o 2 22 4 1764.4 1740.6 46.5 o 4 22 4 633.5 651.4 35.7 o 1 23 4 57.8 75.2 13.1 o 3 23 4 68.2 57.3 24.4 o 5 23 4 10.9 26.8 24.4 < 0 24 4 19.8 9.4 16.7 < 2 24 4 -15.0 3.8 22.9 < 4 24 4 22.8 0.5 27.3 < 1 25 4 -17.5 7.4 23.5 < 3 25 4 24.0 4.2 25.6 < 0 26 4 1227.9 965.4 295.1 o 2 26 4 610.5 666.5 64.4 o 4 26 4 242.6 277.7 20.8 o 1 27 4 437.0 392.2 24.3 o 3 27 4 220.4 244.6 15.4 o 0 28 4 -22.9 6.1 50.0 < 2 28 4 -17.1 2.2 26.7 < 4 28 4 -28.4 0.1 36.0 < 1 29 4 -34.7 7.2 28.5 < 3 29 4 -11.4 5.7 25.1 < 0 30 4 569.4 422.1 157.4 o 2 30 4 350.3 314.1 22.1 o 4 30 4 -80.3 151.3 191.2 < 1 31 4 77.3 96.0 26.8 o 3 31 4 62.3 65.8 21.3 o 0 32 4 -4.4 0.3 32.1 < 2 32 4 -3.9 0.1 29.4 < 1 33 4 65.2 58.1 14.1 o 3 33 4 36.3 43.2 28.3 < 0 34 4 436.1 351.7 62.0 o 2 34 4 150.2 276.6 178.1 < 1 35 4 196.0 150.7 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