#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104236.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104236_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Parkin, Sean' 'Selegue, John P.' 'Brock, Carolyn Pratt' _publ_section_title ; The elusive [Ni(H~2~O)~2~(15-crown-5)]^2+^ cation and related co-crystals of nickel(II) hydrates and 15-crown-5 ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 725 _journal_page_last 737 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.710 _cell_angle_beta 122.530 _cell_angle_gamma 83.580 _cell_length_a 16.0360 _cell_length_b 24.7650 _cell_length_c 10.1630 _exptl_crystal_F_000 1680.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file bs50682bsup4.hkl _[local]_cod_data_source_block 2b #BEGIN Tags that were not found in dictionaries: _shelx_title ' k05253 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 471.73 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1146.65 1178.87 17.32 o 2 0 0 11.76 22.20 6.44 o 3 0 0 3991.09 3821.24 46.40 o 4 0 0 282.13 513.73 18.87 o 5 0 0 171.55 159.63 19.54 o 6 0 0 13103.60 12692.11 192.26 o 7 0 0 67.69 11.32 31.30 o 8 0 0 20884.43 21187.55 379.64 o 9 0 0 6419.16 6251.59 130.10 o 10 0 0 932.75 836.09 66.16 o 11 0 0 207.65 189.15 69.49 o 12 0 0 38.08 -31.30 81.92 o 13 0 0 5083.65 5779.15 189.60 o 14 0 0 1212.59 1259.69 266.41 o 15 0 0 441.94 267.74 217.79 o 16 0 0 473.91 393.62 253.09 o 17 0 0 414.77 592.77 380.53 o -17 1 0 45.73 163.18 308.82 o -16 1 0 1597.61 1756.99 314.37 o -15 1 0 435.66 138.76 343.01 o -14 1 0 110.57 -153.19 213.13 o -13 1 0 83.84 315.25 190.93 o -12 1 0 348.49 353.88 84.59 o -11 1 0 5.03 28.64 57.94 o -10 1 0 551.41 668.03 73.04 o -9 1 0 50.57 34.63 41.07 o -8 1 0 3877.79 3952.45 80.37 o -7 1 0 183.82 127.43 33.08 o -6 1 0 70.37 88.36 25.09 o -5 1 0 2.15 0.00 18.87 o -4 1 0 111.62 170.28 15.76 o -3 1 0 5261.73 5117.12 65.05 o -2 1 0 352.61 441.36 11.77 o -1 1 0 67.64 63.49 4.22 o 1 1 0 1134.53 1010.59 15.98 o 2 1 0 752.36 616.30 13.76 o 3 1 0 225.53 271.30 9.99 o 4 1 0 3821.34 4031.26 52.39 o 5 1 0 2888.68 2815.09 45.96 o 6 1 0 22802.52 24613.40 384.97 o 7 1 0 671.50 583.44 36.41 o 8 1 0 622.17 641.61 43.74 o 9 1 0 33.26 11.54 42.63 o 10 1 0 335.61 529.72 56.39 o 11 1 0 969.97 846.30 88.14 o 12 1 0 1965.42 1987.44 114.78 o 13 1 0 410.69 267.30 92.80 o 14 1 0 65.84 -81.70 244.88 o 15 1 0 1466.90 1202.41 243.32 o 16 1 0 5.45 171.84 238.00 o 17 1 0 470.57 595.21 288.84 o -17 2 0 372.42 -165.40 292.83 o -16 2 0 19.77 -42.18 257.98 o -15 2 0 755.68 1315.86 272.85 o -14 2 0 461.15 671.36 251.32 o -13 2 0 9.46 146.97 206.91 o -12 2 0 1134.06 1091.85 100.13 o -11 2 0 4.52 21.31 60.16 o -10 2 0 658.20 608.31 61.27 o -9 2 0 1334.90 1253.47 65.49 o -8 2 0 14.08 20.65 39.52 o -7 2 0 287.42 327.69 36.41 o -6 2 0 17.33 66.83 23.98 o -5 2 0 13779.55 13225.38 179.83 o -4 2 0 5279.12 6767.98 82.14 o -3 2 0 5.50 33.30 11.77 o -2 2 0 4145.37 4413.34 53.73 o -1 2 0 1230.42 1388.67 21.53 o 0 2 0 512.12 408.94 9.10 o 1 2 0 1384.00 1531.43 20.42 o 2 2 0 45.03 65.72 6.66 o 3 2 0 2682.58 2507.83 35.52 o 4 2 0 139.14 164.95 7.55 o 5 2 0 11108.45 10759.51 170.28 o 6 2 0 91.51 29.53 20.42 o 7 2 0 7687.04 7726.18 147.19 o 8 2 0 66.59 193.15 32.41 o 9 2 0 239.08 197.59 38.41 o 10 2 0 4878.64 4660.00 135.43 o 11 2 0 3171.08 3025.11 118.78 o 12 2 0 1360.27 1278.34 104.79 o 13 2 0 1720.99 1600.92 118.55 o 14 2 0 909.70 1030.79 229.78 o 15 2 0 2284.48 2215.44 333.90 o 16 2 0 1260.51 1446.84 339.45 o 17 2 0 6.74 457.34 579.67 o -17 3 0 165.54 -90.14 306.15 o -16 3 0 732.06 391.63 326.58 o -15 3 0 229.29 291.50 262.86 o -14 3 0 2330.96 2612.17 291.72 o -13 3 0 2018.57 2227.87 276.40 o -12 3 0 22.51 92.13 84.36 o -11 3 0 31.19 207.36 67.05 o -10 3 0 11.39 50.40 54.84 o -9 3 0 2246.75 2100.22 76.59 o -8 3 0 12654.23 12550.91 259.31 o -7 3 0 86.96 52.17 33.97 o -6 3 0 550.17 608.09 34.41 o -5 3 0 5142.44 4786.76 77.04 o -4 3 0 101.70 134.54 17.54 o -3 3 0 3.71 9.10 13.54 o -2 3 0 2820.61 3058.86 40.85 o -1 3 0 1912.56 2263.17 29.97 o 0 3 0 60655.12 62270.79 775.93 o 1 3 0 1908.85 1955.47 31.75 o 2 3 0 3684.95 3464.69 46.62 o 3 3 0 1567.36 1648.43 27.75 o 4 3 0 7636.52 8908.16 140.75 o 5 3 0 8763.62 8235.92 147.41 o 6 3 0 3773.46 3744.87 94.80 o 7 3 0 1886.99 1851.12 67.27 o 8 3 0 9129.78 8867.31 196.48 o 9 3 0 4462.28 4371.83 138.31 o 10 3 0 165.85 69.71 64.83 o 11 3 0 59.42 110.34 74.60 o 12 3 0 3.72 18.87 81.70 o 13 3 0 378.77 271.07 98.79 o 14 3 0 1660.21 1764.32 189.60 o 15 3 0 8.68 -141.20 187.38 o 16 3 0 288.95 511.96 333.46 o 17 3 0 526.97 262.86 413.38 o -16 4 0 627.03 439.36 273.29 o -15 4 0 1457.29 1675.96 330.35 o -14 4 0 62.19 270.85 227.56 o -13 4 0 101.66 16.65 196.26 o -12 4 0 483.91 345.45 94.35 o -11 4 0 9.74 2.89 63.72 o -10 4 0 289.71 109.45 57.94 o -9 4 0 764.37 745.51 60.83 o -8 4 0 5198.59 5422.82 128.77 o -7 4 0 238.19 145.64 34.41 o -6 4 0 930.82 892.93 41.29 o -5 4 0 4004.15 4216.42 71.93 o -4 4 0 1772.65 1933.71 39.30 o -3 4 0 377.87 277.07 15.76 o -2 4 0 110450.50 123200.20 1359.81 o -1 4 0 1634.95 1705.48 26.64 o 0 4 0 410.86 573.23 13.76 o 1 4 0 94.30 71.04 6.88 o 2 4 0 7830.11 8271.22 107.23 o 3 4 0 17820.84 17287.94 209.13 o 4 4 0 17160.06 17162.95 218.90 o 5 4 0 2238.82 1871.77 48.40 o 6 4 0 1256.59 1004.82 49.73 o 7 4 0 45.32 42.18 36.41 o 8 4 0 2452.56 2370.18 81.70 o 9 4 0 2.69 -53.28 55.28 o 10 4 0 6.33 -3.77 66.16 o 11 4 0 6617.38 6552.86 198.26 o 12 4 0 32.77 -68.16 83.92 o 13 4 0 1003.23 1041.67 122.55 o 14 4 0 5.81 -39.07 106.79 o 15 4 0 905.75 983.73 257.53 o 16 4 0 722.78 530.83 299.71 o 17 4 0 563.66 46.18 489.53 o -16 5 0 85.41 158.74 285.28 o -15 5 0 1548.15 1249.70 308.37 o -14 5 0 259.17 390.52 255.98 o -13 5 0 513.87 187.38 205.36 o -12 5 0 1646.43 857.40 277.73 o -11 5 0 229.30 207.36 73.26 o -10 5 0 1712.19 1797.40 85.03 o -9 5 0 1.48 -33.30 49.06 o -8 5 0 228.57 230.45 49.73 o -7 5 0 1234.26 1117.16 55.50 o -6 5 0 1901.48 2058.92 60.61 o -5 5 0 153.52 155.85 24.42 o -4 5 0 912.65 882.94 31.30 o -3 5 0 3550.38 3452.48 50.84 o -2 5 0 5982.44 6705.82 79.92 o -1 5 0 40.72 87.69 9.32 o 0 5 0 69.41 107.45 10.43 o 1 5 0 187.06 130.76 12.21 o 2 5 0 99899.58 103509.20 1170.44 o 3 5 0 108.36 51.95 12.88 o 4 5 0 869.23 782.14 24.87 o 5 5 0 1314.21 1245.70 31.75 o 6 5 0 374.67 357.88 36.19 o 7 5 0 1305.09 1405.10 62.16 o 8 5 0 2089.25 2351.98 91.02 o 9 5 0 160.48 172.95 59.05 o 10 5 0 3992.67 3825.02 143.20 o 11 5 0 3502.91 3680.49 141.64 o 12 5 0 3.69 25.31 108.56 o 13 5 0 545.43 526.83 114.34 o 14 5 0 34.38 -33.08 105.45 o 15 5 0 3370.14 3766.85 260.64 o 16 5 0 483.58 637.39 196.04 o 17 5 0 28.04 22.87 321.91 o -16 6 0 1623.63 1608.69 313.03 o -15 6 0 410.59 150.52 287.73 o -14 6 0 1208.82 1903.07 321.03 o -13 6 0 30.82 -126.99 217.57 o -12 6 0 3.72 -165.62 168.06 o -11 6 0 92.34 44.40 74.82 o -10 6 0 99.33 85.25 63.94 o -9 6 0 1017.10 932.67 73.26 o -8 6 0 1906.00 1732.12 75.04 o -7 6 0 1526.63 1207.51 60.39 o -6 6 0 7832.11 7581.43 162.29 o -5 6 0 497.28 406.94 30.64 o -4 6 0 6598.53 7350.98 111.45 o -3 6 0 51.10 132.10 18.43 o -2 6 0 7836.67 9085.33 140.53 o -1 6 0 2212.12 2010.75 39.07 o 0 6 0 1751.37 1510.11 26.64 o 1 6 0 2761.94 2280.49 38.19 o 2 6 0 15814.38 16850.81 254.42 o 3 6 0 273.68 315.70 15.54 o 4 6 0 2011.43 2121.31 47.07 o 5 6 0 838.69 817.66 31.08 o 6 6 0 705.93 661.15 29.97 o 7 6 0 115.68 72.15 38.19 o 8 6 0 9270.77 9032.27 212.69 o 9 6 0 3588.65 3432.95 106.79 o 10 6 0 5691.77 5946.77 165.62 o 11 6 0 1118.06 1279.89 101.46 o 12 6 0 291.60 389.18 95.69 o 13 6 0 143.99 114.56 85.70 o 14 6 0 175.58 159.40 104.57 o 15 6 0 71.33 -36.19 159.18 o 16 6 0 452.17 857.18 301.27 o 17 6 0 204.48 -530.83 530.83 o -16 7 0 1095.99 1084.08 331.68 o -15 7 0 472.65 328.58 297.49 o -14 7 0 848.58 811.23 274.40 o -13 7 0 3.14 -0.22 214.46 o -12 7 0 66.23 247.54 178.72 o -11 7 0 102.11 -3.33 79.26 o -10 7 0 2525.88 2631.93 106.56 o -9 7 0 1313.28 1213.95 76.59 o -8 7 0 1672.31 1617.35 77.93 o -7 7 0 0.13 -0.44 39.07 o -6 7 0 778.87 713.32 46.18 o -5 7 0 1313.72 1079.41 42.63 o -4 7 0 1772.79 1998.54 44.62 o -3 7 0 314.56 280.62 20.42 o -2 7 0 2963.08 3337.70 53.95 o -1 7 0 15623.70 14484.62 178.27 o 0 7 0 0.50 63.94 13.32 o 1 7 0 4848.08 4372.49 73.26 o 2 7 0 1000.40 1125.59 36.63 o 3 7 0 6520.31 5921.46 93.02 o 4 7 0 59.91 110.78 19.09 o 5 7 0 60.33 72.38 22.87 o 6 7 0 519.73 397.84 30.86 o 7 7 0 415.54 368.54 44.18 o 8 7 0 834.05 648.71 59.72 o 9 7 0 766.61 690.45 68.16 o 10 7 0 2658.43 2454.32 115.89 o 11 7 0 3394.65 3377.67 142.53 o 12 7 0 199.27 29.31 84.14 o 13 7 0 1218.95 1348.93 118.11 o 14 7 0 66.80 -59.72 131.87 o 15 7 0 88.41 320.14 248.87 o 16 7 0 911.35 706.44 305.93 o -16 8 0 0.26 -257.09 357.21 o -15 8 0 247.54 378.53 309.70 o -14 8 0 927.49 799.68 291.50 o -13 8 0 1.30 -97.91 359.21 o -12 8 0 4065.65 4730.82 327.91 o -11 8 0 204.99 226.67 81.70 o -10 8 0 3.04 -32.41 74.15 o -9 8 0 537.79 526.39 65.05 o 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5972.30 161.18 o -7 9 0 248.78 253.98 47.51 o -6 9 0 11752.23 12657.47 236.44 o -5 9 0 21.97 16.21 31.53 o -4 9 0 643.95 585.00 41.07 o -3 9 0 4824.62 5179.50 107.68 o -2 9 0 3761.42 4706.84 87.03 o -1 9 0 2954.22 2754.48 57.50 o 0 9 0 92242.20 97048.93 1711.26 o 1 9 0 2320.31 2301.58 55.95 o 2 9 0 2492.23 2491.18 65.05 o 3 9 0 954.22 880.71 39.07 o 4 9 0 2564.98 2698.98 70.16 o 5 9 0 403.59 358.32 30.64 o 6 9 0 1857.38 1973.01 53.73 o 7 9 0 7161.11 7328.56 134.09 o 8 9 0 2913.29 3077.29 90.36 o 9 9 0 2750.47 2550.68 93.47 o 10 9 0 3164.38 3147.88 109.01 o 11 9 0 181.55 167.40 76.15 o 12 9 0 790.00 716.43 109.90 o 13 9 0 2254.23 2236.09 143.42 o 14 9 0 514.32 338.79 155.19 o 15 9 0 7.58 9.77 134.76 o 16 9 0 291.79 -68.82 246.43 o 17 9 0 167.75 63.27 321.03 o -15 10 0 325.09 285.06 319.92 o -14 10 0 929.45 670.47 352.11 o -13 10 0 91.78 198.70 231.56 o -12 10 0 15.16 -135.65 186.04 o -11 10 0 1521.00 1791.85 198.26 o -10 10 0 2763.54 3039.10 131.21 o -9 10 0 385.13 416.49 70.60 o -8 10 0 1624.45 1694.16 77.93 o -7 10 0 0.57 62.61 42.63 o -6 10 0 1960.18 1863.33 65.94 o -5 10 0 3813.15 3997.52 111.89 o -4 10 0 4371.81 4433.99 102.12 o -3 10 0 1668.62 1787.18 55.28 o -2 10 0 24507.37 26850.15 424.26 o -1 10 0 1191.90 1079.19 37.74 o 0 10 0 18.83 738.18 54.17 o 1 10 0 711.99 671.14 33.30 o 2 10 0 2888.37 4081.66 124.99 o 3 10 0 530.02 595.88 40.85 o 4 10 0 2818.65 2724.73 73.04 o 5 10 0 6.68 32.19 30.42 o 6 10 0 465.77 441.13 40.63 o 7 10 0 6261.54 6363.26 131.87 o 8 10 0 133.60 116.33 34.41 o 9 10 0 79.94 21.53 57.28 o 10 10 0 2296.83 2471.42 108.12 o 11 10 0 467.27 449.57 91.91 o 12 10 0 1174.69 1259.69 107.45 o 13 10 0 205.43 228.45 122.55 o 14 10 0 30.61 42.85 121.66 o 15 10 0 12.38 58.83 155.63 o 16 10 0 1331.36 1263.68 281.29 o 17 10 0 275.95 603.65 308.82 o -15 11 0 726.41 797.46 354.99 o -14 11 0 577.35 978.18 332.79 o -13 11 0 120.87 245.10 189.82 o -12 11 0 4563.40 5536.72 257.31 o -11 11 0 36.74 -70.82 116.78 o -10 11 0 72.55 61.27 67.71 o -9 11 0 196.46 240.66 66.83 o -8 11 0 2726.63 2861.71 94.58 o -7 11 0 0.40 1.11 48.18 o -6 11 0 11424.71 12667.02 216.46 o -5 11 0 159.35 164.51 52.39 o -4 11 0 19863.93 22762.05 358.10 o -3 11 0 10684.99 11697.28 191.59 o -2 11 0 638.49 868.06 41.52 o -1 11 0 2415.86 2567.33 73.26 o 0 11 0 14668.56 14288.58 252.43 o 1 11 0 8951.22 8947.02 165.84 o 2 11 0 17197.68 17289.72 295.27 o 3 11 0 1145.34 1118.93 63.27 o 4 11 0 2859.12 2872.15 100.13 o 5 11 0 3190.00 3107.03 76.59 o 6 11 0 3006.80 2644.14 83.03 o 7 11 0 4170.75 4538.78 114.78 o 8 11 0 665.59 705.10 51.51 o 9 11 0 42.68 0.00 57.50 o 10 11 0 1215.95 1146.24 89.03 o 11 11 0 1838.22 1901.52 107.68 o 12 11 0 444.79 576.56 117.22 o 13 11 0 160.00 77.93 116.78 o 14 11 0 865.39 1140.47 172.95 o 15 11 0 381.47 268.63 198.48 o 16 11 0 437.57 601.43 293.50 o 17 11 0 26.64 499.75 291.06 o -15 12 0 109.98 388.52 331.24 o -14 12 0 3393.92 3157.21 468.22 o -13 12 0 480.89 480.87 179.16 o -12 12 0 99.34 230.22 144.75 o -11 12 0 65.58 -1.33 130.54 o -10 12 0 1907.12 2417.25 151.41 o -9 12 0 5.39 89.03 63.27 o -8 12 0 3268.38 3237.35 113.23 o -7 12 0 354.19 415.38 55.72 o -6 12 0 9579.22 10482.00 197.37 o -5 12 0 68.56 -12.43 45.29 o -4 12 0 11.75 -7.99 31.08 o -3 12 0 154.40 191.15 37.74 o -2 12 0 5342.92 6842.80 129.65 o -1 12 0 15744.00 16329.08 291.72 o 0 12 0 21763.70 26048.91 534.38 o 1 12 0 3210.44 3113.47 75.04 o 2 12 0 2826.15 2853.28 77.04 o 3 12 0 9356.90 8978.10 200.48 o 4 12 0 2735.90 2720.74 88.58 o 5 12 0 11546.20 11209.97 262.19 o 6 12 0 3350.42 3338.37 91.02 o 7 12 0 154.89 215.35 48.18 o 8 12 0 1090.23 941.55 59.72 o 9 12 0 3334.70 3535.29 104.12 o 10 12 0 2582.80 2511.38 102.79 o 11 12 0 98.42 46.40 97.91 o 12 12 0 447.78 553.03 120.11 o 13 12 0 2046.37 2011.19 155.41 o 14 12 0 9.82 -28.20 146.30 o 15 12 0 258.49 65.94 166.06 o 16 12 0 247.39 -114.56 223.79 o 17 12 0 255.45 -113.00 370.31 o -14 13 0 98.21 5.33 325.02 o -13 13 0 4.06 -10.43 173.17 o -12 13 0 11.23 193.15 139.87 o -11 13 0 135.31 57.50 134.98 o -10 13 0 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