#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:01:16 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180902 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/42/2104239.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104239_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Parkin, Sean' 'Selegue, John P.' 'Brock, Carolyn Pratt' _publ_section_title ; The elusive [Ni(H~2~O)~2~(15-crown-5)]^2+^ cation and related co-crystals of nickel(II) hydrates and 15-crown-5 ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 725 _journal_page_last 737 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.120 _cell_angle_beta 105.470 _cell_angle_gamma 90.040 _cell_length_a 12.1440 _cell_length_b 12.1370 _cell_length_c 16.0390 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file bs50685sup7.hkl _cod_data_source_block 5 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k06078 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 343.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5659.98 5409.18 100.87 o 2 0 0 23837.40 23292.46 383.21 o 3 0 0 561.26 685.76 18.73 o 4 0 0 1298.76 1226.97 24.60 o 5 0 0 50110.84 52162.66 725.97 o 6 0 0 1412.50 1354.75 28.71 o 7 0 0 11704.20 12025.45 268.53 o 8 0 0 7379.17 7532.40 179.77 o 9 0 0 951.24 1031.27 39.74 o 10 0 0 356.63 436.87 32.11 o 11 0 0 1910.75 1885.32 74.58 o 12 0 0 3023.74 3175.31 145.86 o 13 0 0 2084.12 2434.43 120.79 o 14 0 0 27.76 37.64 54.30 o 15 0 0 502.10 511.90 89.91 o -15 1 0 21.16 -56.20 93.66 o -14 1 0 366.29 329.15 85.63 o -13 1 0 484.03 553.51 64.00 o -12 1 0 2271.12 2337.57 82.96 o -11 1 0 5243.57 5640.27 146.52 o -10 1 0 507.61 491.33 36.57 o -9 1 0 919.22 948.96 52.97 o -8 1 0 95.17 96.16 25.42 o -7 1 0 3139.49 2930.42 64.22 o -6 1 0 15483.11 15816.56 483.02 o -5 1 0 1884.73 2105.36 43.03 o -4 1 0 18450.07 17946.15 280.80 o -3 1 0 10225.27 9606.96 165.24 o -2 1 0 1133.92 1176.57 22.47 o -1 1 0 44712.24 42588.61 686.76 o 0 1 0 68.15 69.68 3.78 o 1 1 0 43918.40 41605.55 1004.59 o 2 1 0 976.45 1015.64 20.81 o 3 1 0 10095.13 9443.10 157.53 o 4 1 0 17722.80 17657.93 282.66 o 5 1 0 2134.79 2294.71 35.80 o 6 1 0 15005.29 15607.45 450.91 o 7 1 0 2794.59 2735.20 49.51 o 8 1 0 114.46 117.29 17.31 o 9 1 0 1023.65 1062.43 47.19 o 10 1 0 591.36 606.83 31.18 o 11 1 0 5813.51 6002.79 143.21 o 12 1 0 2083.99 2101.53 127.11 o 13 1 0 610.75 600.76 57.69 o 14 1 0 330.85 336.05 70.06 o 15 1 0 27.83 64.22 64.34 o -15 2 0 1163.42 1199.91 122.26 o -14 2 0 103.83 134.87 62.34 o -13 2 0 783.94 859.17 77.70 o -12 2 0 1639.33 1648.91 216.76 o -11 2 0 63.27 75.17 38.50 o -10 2 0 4664.96 5025.93 132.59 o -9 2 0 2109.29 2265.09 69.94 o -8 2 0 5484.87 5471.67 123.41 o -7 2 0 5983.04 6168.49 132.42 o -6 2 0 717.66 710.51 22.71 o -5 2 0 18406.45 18477.07 291.89 o -4 2 0 1504.26 1542.17 76.27 o -3 2 0 9231.64 8579.83 147.18 o -2 2 0 2971.87 3066.79 68.24 o -1 2 0 1145.30 1067.65 16.72 o 0 2 0 10812.92 9813.58 177.13 o 1 2 0 1012.03 957.95 22.47 o 2 2 0 2720.12 2931.44 57.80 o 3 2 0 9767.44 8836.21 174.96 o 4 2 0 1997.35 1910.69 44.96 o 5 2 0 19212.06 18884.86 315.47 o 6 2 0 838.04 802.73 19.80 o 7 2 0 6196.42 6248.46 133.04 o 8 2 0 4998.80 5431.30 93.81 o 9 2 0 2285.63 2449.63 60.87 o 10 2 0 4847.32 5217.81 125.77 o 11 2 0 80.01 50.16 33.07 o 12 2 0 1719.48 1895.38 101.69 o 13 2 0 723.19 840.65 69.05 o 14 2 0 112.34 100.49 44.06 o 15 2 0 1211.12 1246.62 111.06 o -14 3 0 831.64 880.84 272.96 o -13 3 0 40.32 77.91 53.02 o -12 3 0 78.73 132.99 86.97 o -11 3 0 4088.85 4117.60 132.18 o -10 3 0 838.42 808.24 47.31 o -9 3 0 6099.65 6150.59 236.25 o -8 3 0 1546.21 1537.24 52.98 o -7 3 0 1314.04 1367.60 61.55 o -6 3 0 1156.58 979.58 60.21 o -5 3 0 2546.98 2711.49 49.48 o -4 3 0 18877.26 19440.56 327.21 o -3 3 0 9640.08 9437.18 202.04 o -2 3 0 5880.48 5655.55 86.06 o -1 3 0 4493.32 4590.00 78.94 o 0 3 0 15.87 28.27 5.35 o 1 3 0 4427.74 4511.79 101.69 o 2 3 0 5541.86 5395.05 100.90 o 3 3 0 11161.38 10609.21 192.49 o 4 3 0 19771.35 20228.94 317.76 o 5 3 0 2032.08 2245.05 54.30 o 6 3 0 1203.54 985.33 34.06 o 7 3 0 1023.93 1074.18 77.60 o 8 3 0 1470.38 1600.95 34.77 o 9 3 0 5485.79 5709.80 159.21 o 10 3 0 835.03 785.03 81.62 o 11 3 0 3605.98 3565.50 141.58 o 12 3 0 71.82 0.31 38.80 o 13 3 0 32.44 -0.04 53.88 o 14 3 0 772.14 873.90 113.73 o -14 4 0 48.00 14.22 82.96 o -13 4 0 124.43 131.13 41.58 o -12 4 0 291.15 261.64 42.07 o -11 4 0 178.65 191.83 70.91 o -10 4 0 4101.53 4160.38 114.68 o -9 4 0 365.07 316.05 38.80 o -8 4 0 4484.37 4624.96 158.04 o -7 4 0 4802.89 4802.00 127.63 o -6 4 0 779.07 765.74 28.20 o -5 4 0 11785.11 11964.72 235.96 o -4 4 0 2075.44 2444.30 51.87 o -3 4 0 9582.55 9645.07 146.29 o -2 4 0 13574.38 12851.90 456.26 o -1 4 0 2817.08 2707.07 53.32 o 0 4 0 47015.49 44850.16 1109.22 o 1 4 0 2225.77 2178.06 60.21 o 2 4 0 15606.40 14786.79 276.73 o 3 4 0 8275.96 8439.70 239.94 o 4 4 0 1605.05 1913.36 56.67 o 5 4 0 11123.28 11635.15 207.19 o 6 4 0 714.16 723.96 34.79 o 7 4 0 4700.12 4789.84 99.42 o 8 4 0 3966.68 4097.11 113.33 o 9 4 0 340.07 320.14 28.95 o 10 4 0 3736.85 3958.71 120.15 o 11 4 0 199.22 181.05 34.63 o 12 4 0 225.46 122.21 50.84 o 13 4 0 108.71 36.59 53.88 o 14 4 0 62.04 71.74 66.90 o -14 5 0 1415.34 1265.76 133.80 o -13 5 0 84.18 51.55 49.90 o -12 5 0 73.90 70.79 54.86 o -11 5 0 2169.54 2389.26 94.82 o -10 5 0 981.08 892.66 89.65 o -9 5 0 2314.90 2224.43 124.44 o -8 5 0 104.54 100.14 26.23 o -7 5 0 30.82 26.97 23.74 o -6 5 0 5795.69 5761.67 126.46 o -5 5 0 49.76 36.49 10.70 o -4 5 0 7758.65 7845.63 139.15 o -3 5 0 8986.22 9175.38 162.44 o -2 5 0 10647.67 11199.04 196.55 o -1 5 0 12637.21 12350.61 180.92 o 0 5 0 850.72 860.30 23.74 o 1 5 0 12851.34 12696.34 224.19 o 2 5 0 9465.43 9900.65 255.37 o 3 5 0 9686.39 9619.47 201.81 o 4 5 0 6425.73 6725.55 233.96 o 5 5 0 44.10 41.48 11.35 o 6 5 0 5071.71 5240.77 172.03 o 7 5 0 35.11 23.42 18.73 o 8 5 0 136.56 154.37 31.61 o 9 5 0 1983.08 1978.27 97.42 o 10 5 0 745.53 703.41 63.63 o 11 5 0 1813.92 1945.22 103.46 o 12 5 0 82.14 76.36 39.09 o 13 5 0 73.49 19.53 59.89 o 14 5 0 1219.44 1112.57 140.20 o -14 6 0 35.44 50.84 128.45 o -13 6 0 640.28 735.71 94.05 o -12 6 0 551.17 531.13 152.53 o -11 6 0 379.33 389.45 52.08 o -10 6 0 2030.80 2046.55 85.34 o -9 6 0 322.04 289.19 48.17 o -8 6 0 148.74 191.11 33.62 o -7 6 0 3451.89 3751.81 104.81 o -6 6 0 116.00 150.52 17.46 o -5 6 0 5809.86 6088.90 179.29 o -4 6 0 449.44 435.46 14.79 o -3 6 0 341.93 303.69 34.79 o -2 6 0 9404.78 9803.39 181.93 o -1 6 0 320.02 332.02 11.35 o 0 6 0 16001.73 17089.91 312.46 o 1 6 0 328.41 353.04 20.07 o 2 6 0 9090.60 9784.41 170.78 o 3 6 0 264.71 264.45 19.37 o 4 6 0 402.75 356.35 23.60 o 5 6 0 5333.85 5700.60 203.25 o 6 6 0 146.05 172.60 40.14 o 7 6 0 3429.65 3748.30 105.97 o 8 6 0 112.62 127.91 28.38 o 9 6 0 316.40 278.38 36.86 o 10 6 0 2033.03 1994.59 116.66 o 11 6 0 294.08 294.85 92.32 o 12 6 0 458.05 468.37 65.56 o 13 6 0 514.99 424.32 58.51 o 14 6 0 34.54 106.79 77.22 o -13 7 0 104.39 131.29 108.38 o -12 7 0 299.98 413.80 77.80 o -11 7 0 1135.45 1183.95 71.83 o -10 7 0 256.19 160.20 41.50 o -9 7 0 324.73 296.84 46.83 o -8 7 0 139.02 101.18 49.51 o -7 7 0 519.45 581.17 37.46 o -6 7 0 3063.35 3208.25 87.85 o -5 7 0 140.31 183.51 15.35 o -4 7 0 1073.02 962.85 30.10 o -3 7 0 627.52 613.48 40.14 o -2 7 0 1581.28 1626.21 57.53 o -1 7 0 1306.17 1329.15 41.30 o 0 7 0 604.79 544.95 19.27 o 1 7 0 1067.48 1069.73 39.20 o 2 7 0 1193.25 1221.17 53.71 o 3 7 0 638.79 581.44 25.47 o 4 7 0 999.30 959.51 53.33 o 5 7 0 136.15 145.95 36.86 o 6 7 0 2941.51 2943.77 174.73 o 7 7 0 498.70 519.71 27.00 o 8 7 0 108.06 85.63 28.38 o 9 7 0 305.12 222.40 44.06 o 10 7 0 337.52 278.56 48.17 o 11 7 0 1135.69 1118.58 67.81 o 12 7 0 242.35 390.59 57.21 o 13 7 0 101.14 119.04 62.28 o -13 8 0 119.48 24.08 90.83 o -12 8 0 44.25 79.70 69.25 o -11 8 0 30.71 96.09 81.62 o -10 8 0 841.51 1024.13 92.08 o -9 8 0 36.49 53.06 28.47 o -8 8 0 503.36 440.84 34.42 o -7 8 0 3.81 19.30 17.31 o -6 8 0 1459.91 1480.50 64.00 o -5 8 0 4389.71 4918.10 158.64 o -4 8 0 527.65 519.76 28.10 o -3 8 0 840.89 812.26 28.19 o -2 8 0 768.49 803.94 40.44 o -1 8 0 1146.75 1143.50 88.31 o 0 8 0 2270.79 2456.07 64.77 o 1 8 0 866.25 805.34 107.04 o 2 8 0 585.27 639.20 53.52 o 3 8 0 857.76 802.05 36.83 o 4 8 0 424.60 373.87 36.00 o 5 8 0 4305.17 4543.20 189.60 o 6 8 0 1128.03 1179.84 93.20 o 7 8 0 3.42 -32.69 32.69 o 8 8 0 459.07 469.95 47.19 o 9 8 0 27.50 -13.24 34.66 o 10 8 0 868.75 873.88 53.90 o 11 8 0 24.89 56.20 50.60 o 12 8 0 41.05 64.06 45.30 o 13 8 0 89.87 104.82 140.49 o -12 9 0 206.24 206.23 82.90 o -11 9 0 247.47 470.57 95.54 o -10 9 0 56.49 59.16 59.75 o -9 9 0 442.05 473.04 90.99 o -8 9 0 633.38 499.97 108.38 o -7 9 0 1959.73 1962.78 79.41 o -6 9 0 401.62 333.71 25.47 o -5 9 0 882.06 857.66 58.17 o -4 9 0 2.60 5.35 36.13 o -3 9 0 515.78 473.03 82.96 o -2 9 0 1410.83 1507.34 109.72 o -1 9 0 776.80 825.42 52.18 o 0 9 0 73.99 62.11 16.18 o 1 9 0 721.76 664.03 54.86 o 2 9 0 1291.78 1425.89 128.45 o 3 9 0 445.03 427.54 41.05 o 4 9 0 2.54 20.18 77.60 o 5 9 0 1122.42 1170.30 83.59 o 6 9 0 436.09 305.80 65.56 o 7 9 0 1720.81 1697.21 127.11 o 8 9 0 616.54 606.30 53.90 o 9 9 0 341.39 296.32 61.55 o 10 9 0 70.76 61.18 47.36 o 11 9 0 187.62 176.10 52.08 o 12 9 0 161.75 153.89 57.50 o -11 10 0 97.46 78.99 76.48 o -10 10 0 67.04 103.16 66.20 o -9 10 0 2.92 64.26 60.87 o -8 10 0 324.62 309.37 119.08 o -7 10 0 11.99 44.64 47.19 o -6 10 0 221.58 157.89 40.18 o -5 10 0 282.87 165.91 61.55 o -4 10 0 238.39 262.19 108.38 o -3 10 0 1430.43 1437.45 68.24 o -2 10 0 311.01 280.68 26.08 o -1 10 0 598.46 548.41 58.87 o 0 10 0 6644.37 7325.24 297.04 o 1 10 0 794.15 777.23 88.31 o 2 10 0 303.30 248.32 43.03 o 3 10 0 1286.53 1348.37 135.14 o 4 10 0 233.58 213.73 44.53 o 5 10 0 231.46 159.49 82.96 o 6 10 0 217.57 154.14 42.82 o 7 10 0 10.36 5.48 54.95 o 8 10 0 281.27 299.85 52.18 o 9 10 0 2.19 -41.05 41.05 o 10 10 0 50.30 2.63 55.22 o 11 10 0 82.90 105.33 67.81 o -10 11 0 13.98 -46.65 76.20 o -9 11 0 61.19 31.19 71.21 o -8 11 0 35.29 16.32 74.56 o -7 11 0 57.62 69.03 55.22 o -6 11 0 280.02 141.32 90.99 o -5 11 0 81.00 17.66 36.89 o -4 11 0 11.79 26.76 34.63 o -3 11 0 230.40 207.56 46.90 o -2 11 0 205.80 188.44 40.14 o -1 11 0 515.03 480.42 46.33 o 0 11 0 9.86 7.87 61.55 o 1 11 0 388.85 256.47 44.96 o 2 11 0 243.55 201.82 44.06 o 3 11 0 240.13 169.10 48.22 o 4 11 0 14.99 -51.37 81.62 o 5 11 0 94.84 74.26 44.36 o 6 11 0 236.18 150.69 42.53 o 7 11 0 48.28 74.83 69.25 o 8 11 0 46.17 18.20 57.89 o 9 11 0 69.10 -24.60 56.40 o 10 11 0 12.89 60.82 74.35 o -9 12 0 28.76 42.82 112.39 o -8 12 0 64.72 81.78 104.37 o -7 12 0 143.58 112.79 89.15 o -6 12 0 34.50 54.17 65.23 o -5 12 0 444.00 407.33 56.94 o -4 12 0 341.28 292.01 57.12 o -3 12 0 283.12 365.52 92.32 o -2 12 0 76.12 115.33 37.93 o -1 12 0 500.58 492.52 57.84 o 0 12 0 63.07 64.33 46.33 o 1 12 0 377.74 339.86 117.75 o 2 12 0 64.96 73.13 95.00 o 3 12 0 332.87 355.83 179.29 o 4 12 0 271.43 172.21 46.04 o 5 12 0 393.26 314.79 61.69 o 6 12 0 28.77 66.68 69.94 o 7 12 0 190.50 316.59 94.87 o 8 12 0 70.10 152.05 61.67 o 9 12 0 36.09 7.24 66.68 o -8 13 0 41.92 -29.73 80.28 o -7 13 0 108.41 0.25 151.20 o -6 13 0 340.48 142.84 78.94 o -5 13 0 48.46 114.08 61.73 o -4 13 0 15.73 74.08 52.72 o -3 13 0 90.67 103.26 48.22 o -2 13 0 80.78 108.61 74.93 o -1 13 0 191.85 116.57 88.31 o 0 13 0 292.01 440.34 64.22 o 1 13 0 240.10 133.99 53.33 o 2 13 0 61.17 40.24 78.94 o 3 13 0 83.16 142.12 50.78 o 4 13 0 18.42 95.00 56.77 o 5 13 0 63.86 30.37 59.54 o 6 13 0 399.68 465.63 111.21 o 7 13 0 82.45 144.60 76.20 o 8 13 0 54.92 78.77 71.24 o -6 14 0 86.04 -65.61 80.40 o -5 14 0 96.95 129.14 76.48 o -4 14 0 216.03 168.04 59.58 o -3 14 0 133.21 281.51 68.91 o -2 14 0 100.86 142.86 53.31 o -1 14 0 72.71 66.69 48.22 o 0 14 0 164.75 53.82 73.72 o 1 14 0 55.07 8.94 73.59 o 2 14 0 130.66 91.43 69.05 o 3 14 0 129.50 165.36 59.16 o 4 14 0 286.67 110.23 101.69 o 5 14 0 118.91 190.61 99.01 o 6 14 0 64.66 3.75 123.10 o -4 15 0 132.11 96.34 155.21 o -3 15 0 41.61 125.84 101.69 o -2 15 0 31.41 126.75 82.61 o -1 15 0 127.13 64.22 66.80 o 0 15 0 73.21 74.74 75.35 o 1 15 0 147.65 98.59 70.72 o 2 15 0 30.32 214.59 73.44 o 3 15 0 50.86 181.15 72.00 o 4 15 0 127.49 229.76 109.18 o -4 -15 1 269.88 154.15 99.01 o -3 -15 1 202.85 113.61 72.69 o -2 -15 1 671.90 473.65 95.23 o -1 -15 1 345.89 262.91 90.99 o 0 -15 1 123.04 82.93 77.70 o 1 -15 1 79.35 118.48 71.95 o 2 -15 1 46.35 74.97 64.77 o 3 -15 1 154.15 64.05 72.83 o 4 -15 1 78.20 84.81 85.34 o -7 -14 1 363.79 489.43 118.69 o -6 -14 1 240.39 379.46 190.00 o -5 -14 1 487.80 457.79 113.07 o -4 -14 1 427.70 386.26 76.99 o -3 -14 1 490.39 650.60 90.10 o -2 -14 1 88.42 133.94 77.60 o -1 -14 1 434.24 459.02 65.50 o 0 -14 1 114.47 126.46 117.75 o 1 -14 1 112.62 105.70 56.77 o 2 -14 1 306.88 340.36 72.25 o 3 -14 1 216.09 184.65 58.66 o 4 -14 1 245.36 294.89 70.72 o 5 -14 1 185.88 219.70 94.10 o 6 -14 1 138.35 125.92 111.88 o -8 -13 1 203.06 196.49 125.77 o -7 -13 1 861.40 714.55 104.37 o -6 -13 1 266.92 224.73 93.53 o -5 -13 1 289.63 304.36 58.76 o -4 -13 1 1014.62 1053.17 89.15 o -3 -13 1 547.16 639.68 108.38 o -2 -13 1 1279.70 1259.70 107.99 o -1 -13 1 595.36 648.12 76.22 o 0 -13 1 877.80 1019.07 212.74 o 1 -13 1 1298.42 1441.45 91.64 o 2 -13 1 433.88 357.21 55.22 o 3 -13 1 443.39 483.89 59.58 o 4 -13 1 483.82 454.25 81.62 o 5 -13 1 341.83 292.13 83.59 o 6 -13 1 659.37 761.85 165.91 o 7 -13 1 139.55 7.46 69.25 o 8 -13 1 202.22 228.86 113.53 o -10 -12 1 443.14 271.04 115.60 o -9 -12 1 214.13 188.41 92.32 o -8 -12 1 592.15 679.74 88.68 o -7 -12 1 381.55 431.08 75.70 o -6 -12 1 1232.90 1145.39 77.95 o -5 -12 1 2220.70 2549.62 141.39 o -4 -12 1 272.29 202.53 50.98 o -3 -12 1 1579.91 1710.17 208.73 o -2 -12 1 697.85 632.70 72.25 o -1 -12 1 810.26 689.66 93.65 o 0 -12 1 3420.91 3801.72 212.74 o 1 -12 1 866.94 831.34 87.24 o 2 -12 1 4136.48 4464.82 236.83 o 3 -12 1 1053.74 924.24 88.74 o 4 -12 1 949.40 831.60 180.63 o 5 -12 1 881.22 879.56 117.75 o 6 -12 1 370.34 346.22 94.39 o 7 -12 1 845.04 924.10 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