#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/42/2104240.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104240_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Parkin, Sean' 'Selegue, John P.' 'Brock, Carolyn Pratt' _publ_section_title ; The elusive [Ni(H~2~O)~2~(15-crown-5)]^2+^ cation and related co-crystals of nickel(II) hydrates and 15-crown-5 ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 725 _journal_page_last 737 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.560 _cell_angle_gamma 90.000 _cell_length_a 14.6760 _cell_length_b 13.9610 _cell_length_c 25.5520 _exptl_crystal_F_000 2760.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file bs50686sup8.hkl _[local]_cod_data_source_block 6 #BEGIN Tags that were not found in dictionaries: _shelx_title ' k05256 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 570.78 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11.46 26.83 6.71 o 2 0 0 171905.83 163282.61 7645.38 o 3 0 0 16.71 20.12 6.71 o 4 0 0 26893.74 25444.38 415.80 o 5 0 0 37.60 33.53 13.41 o 6 0 0 64729.05 62705.57 999.27 o 7 0 0 2640.90 2856.96 80.48 o 8 0 0 516.31 409.10 33.53 o 9 0 0 4357.32 4687.83 120.72 o 10 0 0 13804.18 14392.10 348.74 o 11 0 0 8.51 0.00 53.65 o 12 0 0 7246.85 7739.28 281.67 o 13 0 0 54.88 87.18 100.60 o 14 0 0 4273.12 4332.38 221.31 o 15 0 0 283.02 201.19 93.89 o 16 0 0 221.94 -6.71 147.54 o 17 0 0 129.76 174.37 127.42 o 18 0 0 25.24 -60.36 207.90 o 1 1 0 11.78 33.53 4.74 o 2 1 0 35460.68 37129.60 333.69 o 3 1 0 100.54 99.33 6.00 o 4 1 0 88.62 118.23 10.06 o 5 1 0 23.54 -3.35 9.48 o 6 1 0 51977.08 54527.80 654.63 o 7 1 0 873.16 933.84 25.76 o 8 1 0 1356.48 1209.08 32.19 o 9 1 0 316.34 281.67 25.76 o 10 1 0 567.69 567.05 37.06 o 11 1 0 161.64 207.33 40.10 o 12 1 0 2890.54 3170.57 97.97 o 13 1 0 156.09 179.25 77.28 o 14 1 0 200.45 153.09 67.66 o 15 1 0 3.59 59.93 72.48 o 16 1 0 83.43 21.67 91.65 o 17 1 0 11.80 20.12 94.84 o 18 1 0 1289.55 1149.59 132.12 o 1 2 0 42.31 41.36 6.71 o 3 2 0 366.79 315.35 9.48 o 4 2 0 44010.38 41792.84 421.74 o 5 2 0 128.05 115.64 23.47 o 6 2 0 104044.67 106135.38 1478.78 o 7 2 0 2803.46 2976.17 51.52 o 8 2 0 50721.54 52152.95 652.21 o 9 2 0 374.11 349.25 18.00 o 10 2 0 62.39 124.51 43.59 o 11 2 0 191.08 225.11 40.10 o 12 2 0 2892.13 2928.86 94.49 o 13 2 0 77.96 86.44 60.79 o 14 2 0 609.79 506.34 88.09 o 15 2 0 66.69 51.07 81.92 o 16 2 0 1756.31 1472.62 318.56 o 17 2 0 28.82 26.83 160.96 o 18 2 0 101.60 42.65 117.42 o 1 3 0 318.51 281.83 9.48 o 2 3 0 168851.67 167665.58 3231.43 o 3 3 0 240.00 214.61 11.16 o 4 3 0 13898.15 12595.49 141.32 o 5 3 0 747.97 748.35 22.32 o 6 3 0 19635.39 20862.03 273.95 o 7 3 0 1556.09 1531.22 41.90 o 8 3 0 19114.28 20278.69 295.00 o 9 3 0 175.02 133.21 40.24 o 10 3 0 1323.36 1506.01 150.90 o 11 3 0 991.53 1054.28 87.18 o 12 3 0 9015.44 9619.87 227.70 o 13 3 0 294.20 133.74 76.92 o 14 3 0 4673.24 4771.79 198.03 o 15 3 0 62.56 114.57 174.37 o 16 3 0 1993.15 2149.15 191.13 o 17 3 0 52.37 104.77 106.62 o 18 3 0 86.94 29.02 127.27 o 0 4 0 1052.15 954.02 40.24 o 1 4 0 33.46 30.48 6.71 o 2 4 0 56996.46 56443.70 842.16 o 3 4 0 0.70 0.00 13.41 o 4 4 0 63874.86 61689.00 711.14 o 5 4 0 2218.60 2211.81 44.86 o 6 4 0 17941.89 16733.31 229.08 o 7 4 0 1436.73 1577.65 46.71 o 8 4 0 61318.20 60705.02 870.67 o 9 4 0 1648.03 1606.25 103.95 o 10 4 0 9275.54 9181.29 328.62 o 11 4 0 777.40 825.24 134.13 o 12 4 0 740.03 559.57 68.04 o 13 4 0 1.62 -65.44 73.10 o 14 4 0 3494.42 3379.86 147.97 o 15 4 0 53.48 -1.18 78.96 o 16 4 0 143.48 332.28 101.45 o 17 4 0 0.26 -63.71 113.81 o 18 4 0 361.67 303.69 125.60 o 1 5 0 10.70 13.41 14.23 o 2 5 0 1140.21 938.87 25.76 o 3 5 0 370.77 383.93 43.59 o 4 5 0 1123.50 1233.99 33.20 o 5 5 0 1413.73 1382.06 37.94 o 6 5 0 200.62 240.30 25.76 o 7 5 0 49.95 64.27 36.89 o 8 5 0 19903.73 21555.57 371.40 o 9 5 0 430.21 430.32 43.59 o 10 5 0 4945.87 4852.16 118.55 o 11 5 0 16.29 -12.97 43.59 o 12 5 0 84.12 7.45 80.48 o 13 5 0 24.74 -77.12 77.12 o 14 5 0 1129.71 1008.08 211.25 o 15 5 0 1.52 -50.21 93.89 o 16 5 0 1157.81 1372.14 170.72 o 17 5 0 40.21 60.11 130.35 o 18 5 0 946.61 806.50 182.05 o 0 6 0 207.33 150.97 18.97 o 1 6 0 72.79 57.48 16.10 o 2 6 0 19873.31 19212.39 342.03 o 3 6 0 355.47 354.09 20.95 o 4 6 0 31139.88 30380.17 419.15 o 5 6 0 1220.17 1301.56 40.10 o 6 6 0 42876.83 41996.65 532.72 o 7 6 0 43.42 20.12 25.76 o 8 6 0 27102.36 26535.77 529.81 o 9 6 0 1375.00 1279.25 59.49 o 10 6 0 326.66 246.90 49.63 o 11 6 0 753.66 650.86 73.77 o 12 6 0 21.11 -62.95 62.95 o 13 6 0 450.22 282.42 83.79 o 14 6 0 1919.49 1852.75 157.54 o 15 6 0 56.07 -1.14 111.37 o 16 6 0 235.10 454.22 132.12 o 17 6 0 1.74 55.58 139.35 o 1 7 0 136.28 143.53 20.95 o 2 7 0 7522.17 8393.16 132.78 o 3 7 0 244.70 277.69 23.47 o 4 7 0 8555.42 8779.57 184.43 o 5 7 0 92.69 134.81 67.06 o 6 7 0 24.13 66.46 43.59 o 7 7 0 222.10 162.68 36.54 o 8 7 0 981.04 858.14 80.48 o 9 7 0 536.93 505.98 46.71 o 10 7 0 14653.06 15508.96 268.95 o 11 7 0 354.36 406.48 59.49 o 12 7 0 730.75 667.50 82.89 o 13 7 0 287.60 331.97 109.07 o 14 7 0 105.90 53.23 111.17 o 15 7 0 412.09 217.20 132.12 o 16 7 0 2470.42 3255.81 419.15 o 17 7 0 36.59 98.68 160.96 o 0 8 0 110889.70 112241.10 2413.76 o 1 8 0 339.46 337.77 32.19 o 2 8 0 56496.72 55168.95 833.60 o 3 8 0 27.01 -2.06 63.71 o 4 8 0 10079.02 9262.98 144.11 o 5 8 0 290.35 233.24 60.36 o 6 8 0 1337.13 1163.04 157.60 o 7 8 0 33.54 69.75 36.89 o 8 8 0 399.20 377.99 47.99 o 9 8 0 0.13 -35.33 35.33 o 10 8 0 10878.14 11690.15 368.86 o 11 8 0 194.88 200.30 107.30 o 12 8 0 4347.48 4298.64 172.41 o 13 8 0 72.43 236.85 97.13 o 14 8 0 8.69 -113.81 113.81 o 15 8 0 50.82 16.51 118.98 o 16 8 0 92.45 123.51 184.43 o 1 9 0 264.20 233.64 46.95 o 2 9 0 2208.38 2116.12 69.26 o 3 9 0 164.09 144.49 35.33 o 4 9 0 6184.76 6614.47 125.69 o 5 9 0 43.03 39.28 53.65 o 6 9 0 196.44 241.62 38.46 o 7 9 0 327.35 272.23 43.39 o 8 9 0 3357.28 3123.94 98.36 o 9 9 0 179.62 118.87 65.75 o 10 9 0 4241.84 5035.13 338.68 o 11 9 0 33.79 2.84 59.49 o 12 9 0 397.47 494.28 106.62 o 13 9 0 23.62 -41.69 86.87 o 14 9 0 1914.05 1994.57 181.07 o 15 9 0 3.02 -46.95 132.78 o 16 9 0 1135.17 1162.60 183.70 o 0 10 0 122367.74 124843.62 2979.13 o 1 10 0 54.06 71.16 39.61 o 2 10 0 12209.42 12180.38 205.92 o 3 10 0 1.35 12.16 37.06 o 4 10 0 17887.58 17969.37 283.36 o 5 10 0 14.47 1.34 33.48 o 6 10 0 20060.07 21036.10 375.56 o 7 10 0 224.88 170.10 60.36 o 8 10 0 54.04 75.56 63.84 o 9 10 0 383.47 434.24 80.48 o 10 10 0 5569.19 6362.78 295.09 o 11 10 0 2.19 48.53 84.26 o 12 10 0 9843.96 11012.47 472.81 o 13 10 0 226.72 397.12 146.56 o 14 10 0 1124.40 1002.32 197.84 o 15 10 0 171.16 66.01 202.18 o 1 11 0 2452.46 2549.00 80.20 o 2 11 0 173.08 299.47 63.71 o 3 11 0 2.18 27.72 35.33 o 4 11 0 3418.96 3355.06 94.28 o 5 11 0 1.90 0.00 41.33 o 6 11 0 3263.37 3225.36 110.66 o 7 11 0 73.18 44.51 46.58 o 8 11 0 600.72 482.31 73.10 o 9 11 0 149.87 56.25 68.04 o 10 11 0 449.57 574.22 93.43 o 11 11 0 46.48 38.00 90.21 o 12 11 0 8407.54 8856.24 276.44 o 13 11 0 45.11 186.75 140.84 o 14 11 0 1552.08 1407.20 274.97 o 15 11 0 80.68 -74.63 405.74 o 0 12 0 6169.40 6062.47 301.79 o 1 12 0 50.49 45.67 45.69 o 2 12 0 24830.29 26538.04 433.43 o 3 12 0 104.32 97.72 110.66 o 4 12 0 10313.30 11019.14 232.22 o 5 12 0 116.65 127.98 54.57 o 6 12 0 16761.31 18044.79 435.92 o 7 12 0 16.31 91.21 69.26 o 8 12 0 19072.03 19352.20 468.84 o 9 12 0 189.42 274.58 97.24 o 10 12 0 1522.50 1467.45 110.42 o 11 12 0 2.76 -19.51 140.84 o 12 12 0 2353.70 2407.02 188.53 o 13 12 0 103.10 212.27 174.37 o 14 12 0 972.01 925.49 243.16 o 1 13 0 1002.09 957.58 73.10 o 2 13 0 282.49 294.68 60.79 o 3 13 0 77.25 87.85 69.26 o 4 13 0 2149.87 2242.70 106.62 o 5 13 0 101.88 137.14 68.64 o 6 13 0 2409.98 2370.30 110.76 o 7 13 0 8.61 20.34 110.66 o 8 13 0 820.20 743.89 112.71 o 9 13 0 51.84 -43.33 91.65 o 10 13 0 1165.64 994.45 124.07 o 11 13 0 216.99 332.03 141.80 o 12 13 0 1347.94 1326.77 163.14 o 13 13 0 89.89 -197.84 197.84 o 0 14 0 131.83 134.13 140.84 o 1 14 0 396.62 438.87 88.61 o 2 14 0 15398.12 16645.82 549.93 o 3 14 0 52.73 147.33 75.43 o 4 14 0 28735.45 31047.98 660.52 o 5 14 0 48.94 -13.88 110.66 o 6 14 0 6982.04 7082.94 238.08 o 7 14 0 11.80 99.48 100.60 o 8 14 0 6511.54 6468.65 224.53 o 9 14 0 354.96 296.73 114.71 o 10 14 0 406.83 204.22 112.71 o 11 14 0 0.89 -112.39 147.54 o 12 14 0 43.76 28.21 131.50 o 1 15 0 108.29 2.55 157.60 o 2 15 0 3553.33 3655.70 193.74 o 3 15 0 7.31 -32.57 83.83 o 4 15 0 49.43 -61.58 97.24 o 5 15 0 0.88 -13.97 81.86 o 6 15 0 48.73 106.47 86.26 o 7 15 0 9.25 23.47 99.59 o 8 15 0 3284.87 3188.33 174.90 o 9 15 0 40.75 37.01 111.99 o 10 15 0 1222.01 879.48 127.76 o 0 16 0 12605.87 13939.51 723.17 o 1 16 0 14.71 -9.39 111.60 o 2 16 0 5577.81 6388.74 277.39 o 3 16 0 26.98 87.78 132.53 o 4 16 0 8224.66 8468.78 307.25 o 5 16 0 0.27 94.53 99.25 o 6 16 0 8284.68 9313.98 321.53 o 7 16 0 196.16 -30.12 124.00 o 8 16 0 127.95 209.06 116.60 o 1 17 0 230.05 293.70 142.67 o 2 17 0 180.48 180.96 138.39 o 3 17 0 2.74 58.12 142.03 o 4 17 0 85.45 -34.87 167.40 o 5 17 0 16.65 -75.01 127.78 o 6 17 0 478.06 556.24 161.03 o 0 18 0 8615.75 7980.19 563.94 o 1 18 0 28.81 -170.72 170.72 o 2 18 0 3961.68 4183.63 269.81 o -18 1 1 149.63 62.27 100.60 o -17 1 1 516.26 755.59 171.02 o -16 1 1 100.86 254.19 95.06 o -15 1 1 84.91 23.47 85.36 o -14 1 1 55.39 62.73 76.92 o -13 1 1 4061.86 4153.78 143.37 o -12 1 1 51.77 79.77 46.95 o -11 1 1 2392.23 2300.03 140.84 o -10 1 1 41.66 34.28 20.95 o -9 1 1 3909.35 4217.34 130.78 o -8 1 1 8.19 19.16 16.10 o -7 1 1 386.98 410.67 20.95 o -6 1 1 7.04 10.06 10.06 o -5 1 1 8.03 20.12 13.41 o -4 1 1 7.20 3.35 9.48 o -3 1 1 1274.13 1173.63 16.10 o -2 1 1 21.25 30.55 4.74 o -1 1 1 124.55 117.46 4.74 o 0 1 1 7.82 10.06 4.74 o 1 1 1 1371.65 1274.27 14.23 o 2 1 1 43.75 33.53 4.74 o 3 1 1 271.42 244.83 9.48 o 4 1 1 56.48 52.45 6.00 o 5 1 1 24203.53 24015.18 292.98 o 6 1 1 117.59 116.51 16.10 o 7 1 1 5676.66 5669.99 94.49 o 8 1 1 214.28 197.90 23.71 o 9 1 1 10712.61 11681.60 248.14 o 10 1 1 199.98 173.60 30.55 o 11 1 1 6942.71 7263.66 143.19 o 12 1 1 568.61 592.92 53.16 o 13 1 1 1430.53 1409.62 77.28 o 14 1 1 568.34 570.56 73.39 o 15 1 1 111.20 68.10 92.38 o 16 1 1 135.52 124.07 90.10 o 17 1 1 949.52 895.05 113.52 o 18 1 1 12.71 -124.00 124.00 o -18 2 1 109.64 -7.12 144.19 o -17 2 1 16.23 185.45 110.66 o -16 2 1 77.74 83.38 85.35 o -15 2 1 225.06 182.01 92.31 o -14 2 1 84.03 73.00 82.89 o -13 2 1 676.74 767.95 124.07 o -12 2 1 7.13 85.69 57.81 o -11 2 1 195.18 224.57 33.20 o -10 2 1 109.89 57.38 20.95 o -9 2 1 1925.62 1958.29 44.86 o -8 2 1 42.98 44.07 16.10 o -7 2 1 2409.82 2385.56 44.86 o -6 2 1 199.83 201.19 18.97 o -5 2 1 144.69 144.27 14.23 o -4 2 1 2.19 3.35 9.48 o -3 2 1 443.95 422.93 13.41 o -2 2 1 32.09 34.87 6.71 o -1 2 1 524.13 526.48 9.48 o 0 2 1 57.35 53.65 4.74 o 1 2 1 395.75 389.09 9.48 o 2 2 1 190.66 178.76 10.06 o 3 2 1 425.55 470.99 26.83 o 4 2 1 7.34 -6.71 9.48 o 5 2 1 3295.95 3222.94 53.65 o 6 2 1 709.83 758.46 22.32 o 7 2 1 303.41 269.47 23.47 o 8 2 1 1310.10 1272.87 50.30 o 9 2 1 0.45 -13.41 23.71 o 10 2 1 290.00 327.03 50.30 o 11 2 1 2018.24 1898.81 75.43 o 12 2 1 1032.26 1138.25 67.66 o 13 2 1 14.59 45.03 64.38 o 14 2 1 49.11 213.20 93.89 o 15 2 1 1484.58 1823.60 120.86 o 16 2 1 4.28 -1.76 97.24 o 17 2 1 1.51 -80.65 94.49 o 18 2 1 49.64 86.02 120.85 o -18 3 1 195.01 56.94 125.07 o -17 3 1 680.42 633.68 197.84 o -16 3 1 377.02 349.56 116.11 o -15 3 1 112.39 -30.44 90.21 o -14 3 1 16.60 -86.74 107.30 o -13 3 1 263.52 418.61 85.35 o -12 3 1 147.36 253.13 69.01 o -11 3 1 5875.42 6111.90 139.35 o -10 3 1 385.39 400.61 32.19 o -9 3 1 15217.85 15274.52 223.43 o -8 3 1 3.21 33.53 22.32 o -7 3 1 655.46 833.26 32.19 o -6 3 1 81.85 95.76 17.25 o -5 3 1 1337.61 1307.94 30.55 o -4 3 1 43.62 67.71 16.77 o -3 3 1 5530.86 5170.17 59.14 o -2 3 1 145.12 160.96 9.48 o -1 3 1 788.34 798.72 16.10 o 0 3 1 0.30 -6.71 6.71 o 1 3 1 2844.30 3026.04 40.10 o 2 3 1 323.44 310.54 13.41 o 3 3 1 662.52 600.25 18.97 o 4 3 1 609.18 605.45 33.53 o 5 3 1 1203.68 1272.39 32.19 o 6 3 1 229.12 223.98 20.95 o 7 3 1 157.13 102.93 22.32 o 8 3 1 745.28 717.57 30.55 o 9 3 1 6005.34 5869.52 115.53 o 10 3 1 1.94 -18.44 27.29 o 11 3 1 1354.57 1355.82 61.10 o 12 3 1 33.55 88.19 46.71 o 13 3 1 1487.89 1502.92 99.91 o 14 3 1 275.28 312.14 82.08 o 15 3 1 2775.44 2804.01 217.96 o 16 3 1 449.33 359.21 96.44 o 17 3 1 4.74 -100.60 104.33 o 18 3 1 208.39 4.73 160.40 o -18 4 1 13.95 60.60 125.25 o -17 4 1 313.25 275.11 113.52 o -16 4 1 3.60 55.33 103.51 o -15 4 1 1052.46 1060.05 109.56 o -14 4 1 26.94 47.59 72.48 o -13 4 1 0.41 -75.43 75.43 o -12 4 1 36.66 38.08 61.94 o -11 4 1 457.77 508.82 51.52 o -10 4 1 0.18 6.71 33.20 o -9 4 1 204.65 181.32 33.20 o -8 4 1 90.82 89.66 46.95 o -7 4 1 87.29 111.77 22.32 o -6 4 1 232.64 229.68 20.95 o -5 4 1 6586.33 6609.39 94.49 o -4 4 1 163.18 164.92 16.10 o -3 4 1 1371.75 1238.81 43.59 o -2 4 1 29.23 41.58 23.47 o -1 4 1 4657.18 4571.37 61.10 o 0 4 1 15.93 13.41 6.00 o 1 4 1 64.87 70.58 9.48 o 2 4 1 4.16 16.77 16.77 o 3 4 1 3.79 17.44 13.41 o 4 4 1 337.81 349.54 16.10 o 5 4 1 5001.38 5264.23 78.96 o 6 4 1 68.45 46.20 20.95 o 7 4 1 306.77 346.27 33.48 o 8 4 1 67.73 29.87 23.29 o 9 4 1 2101.59 2115.05 137.48 o 10 4 1 481.61 507.39 43.39 o 11 4 1 2288.59 2340.56 87.18 o 12 4 1 40.69 90.14 70.42 o 13 4 1 2184.42 2166.37 117.55 o 14 4 1 543.94 510.75 90.21 o 15 4 1 77.85 -82.89 82.89 o 16 4 1 0.34 90.67 123.02 o 17 4 1 174.25 281.67 138.51 o 18 4 1 17.73 65.89 130.01 o -18 5 1 6.51 259.00 157.36 o -17 5 1 72.71 190.31 141.80 o -16 5 1 43.69 94.17 106.58 o -15 5 1 2066.42 2134.84 148.88 o -14 5 1 84.01 32.15 130.78 o -13 5 1 581.34 431.99 77.28 o -12 5 1 14.35 31.94 49.62 o -11 5 1 4902.46 5104.95 154.25 o -10 5 1 892.81 977.56 56.32 o -9 5 1 22018.03 22475.46 336.70 o -8 5 1 127.69 121.39 70.42 o -7 5 1 53.71 119.79 23.29 o -6 5 1 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