#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104246.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104246_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Hao, Xiang' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; Five more phases of the structural family [M(H~2~O)~2~(15-crown-5)](NO~3~)~2~ ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 738 _journal_page_last 749 _journal_volume 64 _journal_year 2008 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1096 _cell_length_b 8.1096 _cell_length_c 27.2473 _exptl_crystal_F_000 916.00 _reflns_d_resolution_high 0.8304 _[local]_cod_data_source_file bs5069CoZprime0.5sup8.hkl _[local]_cod_data_source_block CoZprime0.5 #BEGIN Tags that were not found in dictionaries: _shelx_title ' x05058 in P4(1)2(1)2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 153.97 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+1/4' 'y+1/2, -x+1/2, z+3/4' '-x+1/2, y+1/2, -z+1/4' 'x+1/2, -y+1/2, -z+3/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 14511.12 15713.25 301.42 o 0 2 0 453.69 372.82 7.06 o 1 2 0 37.56 35.27 1.38 o 2 2 0 10352.66 10833.26 355.91 o 1 3 0 2.31 3.92 1.82 o 2 3 0 1548.73 1521.21 26.18 o 3 3 0 242.79 204.75 7.88 o 0 4 0 1818.87 1778.95 60.97 o 1 4 0 684.70 619.13 12.50 o 2 4 0 297.89 269.96 6.89 o 3 4 0 196.72 195.39 3.83 o 4 4 0 735.24 673.52 11.74 o 1 5 0 464.52 407.46 4.69 o 2 5 0 363.87 307.32 4.13 o 3 5 0 45.96 50.20 3.20 o 4 5 0 111.86 95.78 4.68 o 5 5 0 1616.80 1693.38 26.97 o 0 6 0 1097.09 1118.94 18.32 o 1 6 0 37.72 46.21 3.31 o 2 6 0 400.17 444.01 10.24 o 3 6 0 62.61 48.69 4.06 o 4 6 0 312.82 301.84 6.99 o 5 6 0 229.80 249.24 8.39 o 6 6 0 510.65 480.95 26.95 o 1 7 0 447.21 438.20 8.17 o 2 7 0 103.90 101.36 4.93 o 3 7 0 82.68 78.40 5.81 o 4 7 0 413.82 423.20 14.39 o 5 7 0 248.07 257.79 20.35 o 6 7 0 0.51 2.13 8.89 o 0 8 0 234.90 233.07 12.49 o 1 8 0 114.35 320.74 97.64 o 2 8 0 49.76 143.46 39.25 o 3 8 0 477.27 448.33 13.13 o 4 8 0 3.70 71.92 25.92 o 5 8 0 23.64 36.07 15.42 o 1 9 0 4.60 -6.23 11.66 o 2 9 0 135.87 111.44 10.23 o 3 9 0 26.98 30.11 11.90 o 0 1 1 837.44 580.20 8.51 o 1 1 1 1419.99 1226.90 23.16 o -1 2 1 2975.91 2941.85 53.42 o 0 2 1 139.00 98.35 1.94 o 1 2 1 1720.89 1673.19 22.35 o 2 2 1 11162.47 11983.68 194.39 o -2 3 1 723.56 628.45 11.27 o -1 3 1 4830.50 4692.92 109.37 o 0 3 1 5899.29 5578.45 73.87 o 1 3 1 3583.74 3417.85 47.91 o 2 3 1 676.99 595.39 14.55 o 3 3 1 15.14 18.21 2.64 o -3 4 1 258.51 250.34 4.49 o -2 4 1 972.80 918.46 15.26 o -1 4 1 1688.84 1632.16 35.15 o 0 4 1 166.41 167.98 4.52 o 1 4 1 1179.18 1110.08 18.97 o 2 4 1 951.36 882.04 19.47 o 3 4 1 154.30 125.56 2.99 o 4 4 1 1656.26 1718.70 16.94 o -4 5 1 384.66 409.67 6.89 o -3 5 1 1064.03 1159.28 15.00 o -2 5 1 1118.85 1059.00 11.86 o -1 5 1 823.81 820.66 8.00 o 0 5 1 272.23 264.29 3.89 o 1 5 1 670.54 659.67 7.43 o 2 5 1 837.58 776.92 11.41 o 3 5 1 849.57 905.73 9.84 o 4 5 1 381.91 415.79 6.98 o 5 5 1 910.08 1006.00 64.48 o -5 6 1 69.72 68.23 6.24 o -4 6 1 275.60 324.44 7.68 o -3 6 1 170.37 182.43 5.53 o -2 6 1 613.97 570.28 10.09 o -1 6 1 371.82 378.50 6.43 o 0 6 1 47.01 39.27 3.27 o 1 6 1 276.55 226.47 11.31 o 2 6 1 214.43 166.48 5.64 o 3 6 1 346.21 331.53 6.03 o 4 6 1 211.93 232.93 7.65 o 5 6 1 51.21 38.91 7.41 o 6 6 1 39.92 42.98 6.10 o -6 7 1 29.45 22.42 5.93 o -5 7 1 92.26 122.48 25.66 o -4 7 1 118.55 123.61 14.40 o -3 7 1 201.07 212.49 7.89 o -2 7 1 96.50 113.60 4.99 o -1 7 1 178.39 228.61 29.33 o 0 7 1 373.14 377.51 10.46 o 1 7 1 103.77 151.87 21.75 o 2 7 1 68.26 87.79 6.09 o 3 7 1 64.08 80.15 7.32 o 4 7 1 79.48 148.17 35.36 o 5 7 1 97.03 181.97 43.00 o 6 7 1 0.37 -6.89 6.89 o -5 8 1 26.80 25.55 6.61 o -4 8 1 130.77 172.91 15.77 o -3 8 1 31.33 314.80 122.26 o -2 8 1 118.29 130.38 11.38 o -1 8 1 354.76 317.94 20.45 o 0 8 1 593.06 619.69 49.70 o 1 8 1 366.53 363.65 12.16 o 2 8 1 117.02 131.65 12.03 o 3 8 1 8.15 137.07 104.04 o 4 8 1 173.37 175.90 9.99 o 5 8 1 51.68 59.36 7.04 o -3 9 1 6.24 12.76 9.88 o -2 9 1 28.07 21.77 11.38 o -1 9 1 186.29 184.74 24.96 o 0 9 1 262.18 233.15 8.44 o 1 9 1 171.67 152.72 11.27 o 2 9 1 22.46 4.41 11.38 o 3 9 1 3.03 -4.87 9.50 o 0 1 2 14686.82 16722.08 348.95 o 1 1 2 1160.04 944.64 11.57 o -1 2 2 636.42 556.33 10.09 o 0 2 2 3642.45 3659.27 60.21 o 1 2 2 211.61 194.65 3.62 o 2 2 2 1362.51 1276.34 19.59 o -2 3 2 772.82 801.93 17.02 o -1 3 2 1927.36 1733.28 31.48 o 0 3 2 6.90 3.56 1.52 o 1 3 2 2417.12 2236.60 31.20 o 2 3 2 805.69 846.52 12.70 o 3 3 2 4609.92 4874.73 80.42 o -3 4 2 37.42 33.54 2.34 o -2 4 2 2784.03 2709.85 47.13 o -1 4 2 1399.08 1327.27 25.04 o 0 4 2 2.06 5.71 2.58 o 1 4 2 1490.92 1434.89 18.82 o 2 4 2 3179.05 3205.65 48.00 o 3 4 2 35.31 31.79 2.54 o 4 4 2 1879.89 2034.92 20.00 o -4 5 2 592.03 572.66 8.25 o -3 5 2 570.68 568.48 7.39 o -2 5 2 1060.66 941.52 8.84 o -1 5 2 202.29 203.08 3.62 o 0 5 2 361.88 333.34 4.49 o 1 5 2 185.65 190.01 3.25 o 2 5 2 1133.72 1025.02 10.96 o 3 5 2 493.78 488.59 6.61 o 4 5 2 589.07 564.05 8.35 o 5 5 2 28.87 28.39 5.16 o -5 6 2 443.19 470.96 20.42 o -4 6 2 79.27 84.60 5.26 o -3 6 2 12.35 17.17 4.53 o -2 6 2 39.50 44.13 3.65 o -1 6 2 725.39 712.11 10.73 o 0 6 2 5.39 7.91 3.46 o 1 6 2 695.98 681.65 8.97 o 2 6 2 53.24 70.06 3.89 o 3 6 2 10.07 6.87 4.05 o 4 6 2 49.57 60.90 7.33 o 5 6 2 444.01 450.19 14.54 o 6 6 2 14.58 19.25 5.87 o -6 7 2 40.54 32.60 5.83 o -5 7 2 62.97 109.07 21.65 o -4 7 2 196.96 242.63 13.30 o -3 7 2 71.53 107.89 16.57 o -2 7 2 14.49 10.83 4.51 o -1 7 2 0.45 34.33 13.21 o 0 7 2 669.82 676.92 19.33 o 1 7 2 27.16 34.71 5.29 o 2 7 2 52.94 60.59 4.29 o 3 7 2 54.17 61.66 8.39 o 4 7 2 212.90 246.47 12.35 o 5 7 2 43.36 89.16 20.25 o 6 7 2 29.96 35.30 7.59 o -5 8 2 57.10 60.25 6.25 o -4 8 2 225.70 224.95 19.60 o -3 8 2 0.54 13.08 7.42 o -2 8 2 78.41 107.54 10.11 o -1 8 2 51.70 71.90 8.63 o 0 8 2 0.16 8.63 7.28 o 1 8 2 32.03 31.35 6.97 o 2 8 2 214.21 234.55 10.44 o 3 8 2 2.98 18.65 6.84 o 4 8 2 199.07 257.38 27.88 o 5 8 2 47.87 58.40 10.48 o -3 9 2 249.47 207.06 24.47 o -2 9 2 1.79 -1.49 16.23 o -1 9 2 53.42 42.44 9.86 o 0 9 2 19.65 18.76 5.46 o 1 9 2 63.50 63.72 7.82 o 2 9 2 0.65 -8.00 8.96 o 3 9 2 255.10 178.83 14.00 o 0 1 3 5388.58 5109.18 68.87 o 1 1 3 11339.49 11570.68 163.43 o -1 2 3 6472.68 5698.26 92.00 o 0 2 3 98.56 73.79 1.70 o 1 2 3 5251.08 4312.95 102.15 o 2 2 3 409.30 311.66 6.82 o -2 3 3 1174.83 1232.51 22.89 o -1 3 3 411.85 377.77 9.81 o 0 3 3 2421.55 2032.03 43.89 o 1 3 3 683.27 629.90 9.22 o 2 3 3 805.92 852.62 12.37 o 3 3 3 157.51 132.94 4.22 o -3 4 3 313.70 305.05 4.96 o -2 4 3 520.94 469.94 7.73 o -1 4 3 1509.12 1540.48 27.74 o 0 4 3 1447.30 1390.02 22.47 o 1 4 3 1383.15 1372.12 18.30 o 2 4 3 498.90 420.69 6.19 o 3 4 3 581.62 601.15 7.14 o 4 4 3 479.47 540.95 7.11 o -4 5 3 715.81 784.29 9.99 o -3 5 3 290.37 298.95 5.62 o -2 5 3 415.42 392.89 5.23 o -1 5 3 603.89 602.74 6.62 o 0 5 3 255.55 264.29 4.45 o 1 5 3 659.81 665.50 6.86 o 2 5 3 286.78 277.56 4.36 o 3 5 3 296.31 281.15 5.20 o 4 5 3 600.73 640.30 9.66 o 5 5 3 249.05 247.69 6.50 o -5 6 3 152.15 160.24 7.22 o -4 6 3 221.13 234.34 6.30 o -3 6 3 792.68 841.04 13.50 o -2 6 3 457.79 453.34 8.65 o -1 6 3 123.32 107.90 3.51 o 0 6 3 67.69 84.46 3.76 o 1 6 3 21.40 18.47 3.16 o 2 6 3 436.56 487.58 7.66 o 3 6 3 442.87 431.82 7.58 o 4 6 3 328.23 338.01 7.62 o 5 6 3 146.55 156.55 6.96 o 6 6 3 8.08 7.23 5.78 o -6 7 3 99.34 114.86 13.31 o -5 7 3 67.62 76.41 5.36 o -4 7 3 354.87 438.68 19.50 o -3 7 3 13.48 13.51 5.86 o -2 7 3 76.09 94.07 4.61 o -1 7 3 717.05 707.19 27.69 o 0 7 3 18.42 16.70 5.75 o 1 7 3 801.97 871.21 15.35 o 2 7 3 0.81 4.40 4.10 o 3 7 3 116.64 132.05 6.40 o 4 7 3 329.40 374.68 17.04 o 5 7 3 49.51 49.81 7.48 o 6 7 3 114.73 111.26 8.91 o -5 8 3 55.19 39.79 5.59 o -4 8 3 57.83 66.76 6.70 o -3 8 3 57.13 49.52 6.62 o -2 8 3 58.19 77.54 6.47 o -1 8 3 116.96 135.65 10.07 o 0 8 3 545.18 521.06 13.04 o 1 8 3 182.74 199.08 7.24 o 2 8 3 20.44 19.25 10.54 o 3 8 3 83.18 90.31 6.70 o 4 8 3 56.51 58.23 6.51 o 5 8 3 47.97 47.05 5.98 o -3 9 3 16.21 19.11 21.48 o -2 9 3 69.06 96.40 24.26 o -1 9 3 94.56 95.04 9.60 o 0 9 3 313.88 312.66 13.21 o 1 9 3 93.63 108.77 12.67 o 2 9 3 81.02 80.01 7.22 o 3 9 3 14.69 17.17 8.08 o 0 0 4 23706.76 31013.06 1177.81 o 0 1 4 177.48 145.59 2.29 o 1 1 4 1829.16 1558.35 24.85 o -1 2 4 5314.05 4824.16 83.33 o 0 2 4 1036.07 828.61 10.49 o 1 2 4 7002.54 6356.92 102.17 o 2 2 4 819.58 635.11 9.38 o -2 3 4 2956.50 2906.27 43.82 o -1 3 4 2438.89 2140.45 60.86 o 0 3 4 8967.47 9144.74 192.43 o 1 3 4 2346.54 2207.29 28.19 o 2 3 4 3133.51 3144.90 40.33 o 3 3 4 99.51 89.84 3.87 o -3 4 4 3405.44 3387.20 33.71 o -2 4 4 139.09 120.12 3.41 o -1 4 4 1529.75 1470.88 29.89 o 0 4 4 5040.57 5021.29 116.64 o 1 4 4 1316.32 1249.92 17.86 o 2 4 4 160.33 135.91 3.07 o 3 4 4 2642.56 2652.57 26.66 o 4 4 4 27.77 29.95 3.52 o -4 5 4 321.59 357.94 6.46 o -3 5 4 320.81 288.32 5.60 o -2 5 4 1388.14 1366.86 18.54 o -1 5 4 1545.76 1518.08 20.72 o 0 5 4 8.39 14.12 2.57 o 1 5 4 1407.37 1433.74 13.48 o 2 5 4 987.90 947.18 10.98 o 3 5 4 308.71 273.35 5.21 o 4 5 4 309.14 334.90 6.37 o 5 5 4 328.70 336.91 6.80 o -5 6 4 79.14 82.59 5.94 o -4 6 4 280.25 301.35 9.68 o -3 6 4 5.49 16.07 4.66 o -2 6 4 149.65 155.10 4.81 o -1 6 4 174.46 168.04 4.44 o 0 6 4 1186.85 1273.41 22.13 o 1 6 4 172.84 169.85 4.09 o 2 6 4 214.28 234.54 5.08 o 3 6 4 14.61 27.58 4.64 o 4 6 4 120.16 111.69 5.67 o 5 6 4 72.36 65.51 6.45 o 6 6 4 236.89 243.96 7.53 o -6 7 4 59.43 56.22 4.35 o -5 7 4 125.81 139.62 6.27 o -4 7 4 140.60 158.24 5.73 o -3 7 4 63.22 62.50 5.61 o -2 7 4 53.93 63.62 4.14 o -1 7 4 327.51 329.57 13.01 o 0 7 4 134.87 158.11 5.10 o 1 7 4 189.33 204.71 7.04 o 2 7 4 109.09 111.45 4.97 o 3 7 4 81.94 85.15 5.51 o 4 7 4 92.53 93.38 5.75 o 5 7 4 175.66 177.92 8.84 o 6 7 4 51.02 54.08 5.66 o -5 8 4 66.94 58.11 6.31 o -4 8 4 54.37 65.65 4.81 o -3 8 4 308.41 285.95 9.54 o -2 8 4 40.78 50.71 7.38 o -1 8 4 126.67 144.36 6.33 o 0 8 4 70.92 69.09 7.09 o 1 8 4 113.09 120.46 5.64 o 2 8 4 29.84 41.60 6.56 o 3 8 4 275.75 272.53 11.54 o 4 8 4 78.77 83.73 4.82 o 5 8 4 14.50 16.01 5.73 o -3 9 4 3.31 13.91 4.54 o -2 9 4 145.09 132.53 10.75 o -1 9 4 19.96 23.44 4.34 o 0 9 4 52.47 52.16 7.70 o 1 9 4 13.63 20.96 5.39 o 2 9 4 142.93 150.91 15.95 o 3 9 4 3.25 15.88 4.34 o 0 1 5 10091.21 10168.31 139.16 o 1 1 5 19968.29 24018.68 328.18 o -1 2 5 963.69 856.65 17.59 o 0 2 5 76.31 68.78 1.92 o 1 2 5 885.38 790.24 11.15 o 2 2 5 1216.87 1091.35 14.59 o -2 3 5 1863.40 1768.79 27.37 o -1 3 5 1522.94 1449.04 23.87 o 0 3 5 4132.37 4182.98 70.79 o 1 3 5 1524.37 1442.05 19.70 o 2 3 5 1862.70 1758.41 22.78 o 3 3 5 13.32 16.45 3.58 o -3 4 5 1009.68 920.80 9.87 o -2 4 5 540.20 533.61 8.04 o -1 4 5 2966.21 3003.96 60.72 o 0 4 5 896.83 929.19 21.58 o 1 4 5 3325.56 3301.56 44.41 o 2 4 5 723.79 702.68 7.60 o 3 4 5 1310.43 1247.31 13.71 o 4 4 5 511.24 502.84 6.80 o -4 5 5 66.51 64.49 4.23 o -3 5 5 694.94 723.91 9.97 o -2 5 5 1518.34 1574.16 19.96 o -1 5 5 192.71 194.02 4.26 o 0 5 5 247.63 239.80 4.71 o 1 5 5 381.92 393.00 6.37 o 2 5 5 1829.22 1904.23 16.60 o 3 5 5 697.16 738.61 10.04 o 4 5 5 140.66 139.24 4.46 o 5 5 5 203.25 206.01 5.71 o -5 6 5 46.06 54.52 5.34 o -4 6 5 83.34 70.02 6.64 o -3 6 5 303.76 307.16 7.29 o -2 6 5 136.02 143.93 4.28 o -1 6 5 335.61 337.45 6.48 o 0 6 5 160.06 184.11 5.02 o 1 6 5 205.23 206.17 4.45 o 2 6 5 196.72 239.67 5.31 o 3 6 5 483.30 485.04 12.24 o 4 6 5 251.04 241.56 7.37 o 5 6 5 34.04 29.58 6.22 o 6 6 5 79.14 63.75 8.61 o -6 7 5 28.00 26.90 3.95 o -5 7 5 57.29 53.44 5.57 o -4 7 5 151.37 141.79 5.72 o -3 7 5 172.18 167.09 7.31 o -2 7 5 110.16 107.94 4.60 o -1 7 5 93.68 90.86 4.99 o 0 7 5 111.44 125.31 5.08 o 1 7 5 154.65 134.62 5.45 o 2 7 5 168.02 175.04 6.08 o 3 7 5 243.98 234.71 10.22 o 4 7 5 112.80 112.00 5.27 o 5 7 5 28.25 28.34 5.61 o 6 7 5 0.35 2.54 3.93 o -5 8 5 56.47 59.25 5.13 o -4 8 5 30.49 35.37 4.42 o -3 8 5 63.86 51.33 5.30 o -2 8 5 110.90 118.52 9.53 o -1 8 5 103.52 121.31 5.77 o 0 8 5 352.39 373.98 17.82 o 1 8 5 146.05 169.00 6.85 o 2 8 5 103.07 116.31 7.77 o 3 8 5 110.96 95.53 7.30 o 4 8 5 25.12 31.22 4.48 o 5 8 5 39.08 34.58 4.59 o -3 9 5 16.70 19.94 3.88 o -2 9 5 8.02 10.26 8.40 o -1 9 5 93.95 99.70 8.60 o 0 9 5 130.08 116.62 5.30 o 1 9 5 111.07 112.83 6.45 o 2 9 5 7.24 12.30 6.97 o 3 9 5 9.28 15.09 3.60 o 0 1 6 13589.27 15471.66 198.64 o 1 1 6 9444.77 9576.63 123.52 o -1 2 6 5504.77 4967.52 93.32 o 0 2 6 4813.32 4363.88 62.63 o 1 2 6 4723.90 4492.18 69.50 o 2 2 6 2444.91 2299.82 32.75 o -2 3 6 56.22 65.66 3.52 o -1 3 6 952.21 899.26 18.76 o 0 3 6 86.20 113.46 3.30 o 1 3 6 1273.17 1258.18 15.83 o 2 3 6 69.88 78.64 3.04 o 3 3 6 939.18 871.33 12.14 o -3 4 6 140.19 149.77 3.53 o -2 4 6 1493.44 1396.47 15.06 o -1 4 6 317.97 265.70 11.66 o 0 4 6 383.17 451.41 9.06 o 1 4 6 467.24 403.25 7.55 o 2 4 6 839.70 713.96 7.74 o 3 4 6 136.78 150.04 3.21 o 4 4 6 100.75 100.93 3.37 o -4 5 6 242.80 246.08 5.45 o -3 5 6 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69.00 9.00 o 0 1 26 483.78 507.59 9.62 o 1 1 26 231.17 249.95 6.83 o -1 2 26 107.03 121.14 5.35 o 0 2 26 121.92 105.82 5.44 o 1 2 26 63.45 73.17 4.87 o 2 2 26 201.77 233.81 6.61 o -2 3 26 6.29 8.53 4.23 o -1 3 26 150.46 173.66 5.88 o 0 3 26 55.92 59.05 4.35 o 1 3 26 79.96 86.25 4.90 o 2 3 26 8.34 9.08 4.14 o 3 3 26 57.31 53.14 4.08 o -3 4 26 2.30 1.57 3.81 o -2 4 26 72.33 62.51 5.12 o -1 4 26 35.83 47.30 4.17 o 0 4 26 0.82 1.13 4.50 o 1 4 26 25.06 27.28 4.35 o 2 4 26 226.17 184.21 7.64 o 3 4 26 2.91 2.31 2.77 o 4 4 26 25.95 15.05 2.97 o -3 5 26 13.93 10.03 6.01 o -2 5 26 33.96 32.30 3.35 o -1 5 26 49.14 49.23 3.90 o 0 5 26 299.61 280.31 7.76 o 1 5 26 67.64 71.83 3.72 o 2 5 26 28.35 30.18 3.47 o 3 5 26 21.05 14.16 5.48 o 0 1 27 169.23 154.84 5.37 o 1 1 27 34.65 46.52 4.53 o -1 2 27 159.15 158.38 5.24 o 0 2 27 86.79 86.02 4.95 o 1 2 27 95.69 91.99 4.70 o 2 2 27 23.66 21.26 3.88 o -2 3 27 33.45 34.95 3.87 o -1 3 27 93.10 84.24 4.41 o 0 3 27 98.61 90.14 4.74 o 1 3 27 69.07 63.73 4.43 o 2 3 27 72.54 83.08 4.19 o 3 3 27 1.04 0.91 3.77 o -3 4 27 30.48 29.65 3.17 o -2 4 27 14.20 17.52 3.67 o -1 4 27 190.19 169.55 5.42 o 0 4 27 246.71 241.63 6.02 o 1 4 27 197.05 180.33 6.67 o 2 4 27 2.32 -0.25 3.73 o 3 4 27 24.21 17.01 3.16 o -2 5 27 35.03 33.64 3.07 o -1 5 27 13.54 8.83 3.22 o 0 5 27 41.92 27.81 4.24 o 1 5 27 2.52 7.10 3.16 o 2 5 27 32.41 30.13 3.08 o 0 0 28 38.76 39.25 13.38 o 0 1 28 11.36 11.11 5.39 o 1 1 28 119.88 121.26 5.04 o -1 2 28 135.72 133.54 5.32 o 0 2 28 102.27 112.49 4.54 o 1 2 28 66.01 62.95 4.69 o 2 2 28 62.21 78.87 4.45 o -2 3 28 107.92 114.57 4.57 o -1 3 28 2.89 3.14 4.46 o 0 3 28 8.35 6.59 4.11 o 1 3 28 1.56 4.03 4.36 o 2 3 28 91.69 80.18 3.64 o 3 3 28 22.52 15.11 3.21 o -3 4 28 153.00 106.42 5.43 o -2 4 28 6.24 4.84 3.25 o -1 4 28 32.15 27.14 3.80 o 0 4 28 218.31 215.47 5.89 o 1 4 28 48.06 47.41 3.52 o 2 4 28 7.52 9.79 3.09 o 3 4 28 210.38 131.86 9.81 o 0 5 28 12.56 5.95 3.79 o 0 1 29 170.66 187.83 6.47 o 1 1 29 40.21 43.72 4.33 o -1 2 29 183.21 185.20 5.66 o 0 2 29 125.32 124.79 4.69 o 1 2 29 265.05 257.24 10.07 o 2 2 29 17.22 13.17 3.60 o -2 3 29 3.21 4.63 3.60 o -1 3 29 87.98 74.18 4.19 o 0 3 29 65.34 47.63 3.94 o 1 3 29 72.32 66.61 3.93 o 2 3 29 13.20 9.04 2.99 o 3 3 29 0.26 -3.53 3.53 o -2 4 29 23.37 21.94 3.60 o -1 4 29 7.83 3.70 3.56 o 0 4 29 119.50 98.80 5.86 o 1 4 29 39.75 41.20 3.44 o 2 4 29 8.25 9.93 6.70 o 0 1 30 188.20 176.91 6.39 o 1 1 30 41.60 50.69 4.50 o -1 2 30 9.66 6.40 3.13 o 0 2 30 34.48 27.45 4.17 o 1 2 30 1.17 3.68 4.05 o 2 2 30 115.50 110.27 6.79 o -2 3 30 7.70 8.49 3.94 o -1 3 30 42.61 35.61 3.10 o 0 3 30 3.70 2.70 3.54 o 1 3 30 46.32 49.79 4.00 o 2 3 30 7.30 -1.30 3.91 o 0 1 31 14.04 11.74 4.52 o 1 1 31 81.17 82.14 4.83 o -1 2 31 24.49 14.69 3.94 o 0 2 31 50.51 41.23 4.62 o 1 2 31 46.34 40.74 5.08 o 2 2 31 69.34 56.04 5.17 o -1 3 31 43.53 6.01 9.16 o 0 3 31 55.81 66.04 14.61 o 1 3 31 71.64 67.61 11.43 o 0 0 32 587.93 471.14 21.03 o 0 1 32 2.14 -4.13 4.13 o 1 1 32 101.12 88.14 4.86 o 0 2 32 58.57 58.22 8.04 o