#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/42/2104287.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104287_Fobs loop_ _publ_author_name 'Serezhkin, Viktor N.' 'Vologzhanina, Anna V.' 'Serezhkina, Larisa B.' 'Smirnova, Ekaterina S.' 'Grachova, Elena V.' 'Ostrova, Polina V.' 'Antipin, Mikhail Yu.' _publ_section_title ; Crystallochemical formula as a tool for describing metal--ligand complexes -- a pyridine-2,6-dicarboxylate example ; _journal_coeditor_code GP5026 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 45 _journal_page_last 53 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.761 _cell_angle_beta 77.597 _cell_angle_gamma 72.899 _cell_length_a 10.2800 _cell_length_b 10.9960 _cell_length_c 17.1772 _exptl_crystal_F_000 970.00 _reflns_d_resolution_high 0.6614 _[local]_cod_data_source_file gp5026Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 345.89 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ 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2426.49 108.23 o -8 6 0 1820.44 1878.17 101.22 o -7 6 0 710.67 674.36 47.47 o -6 6 0 1975.18 1851.59 52.03 o -5 6 0 6065.98 6183.56 109.08 o -4 6 0 3790.47 3679.12 73.97 o -3 6 0 4792.06 5229.01 92.26 o -2 6 0 7158.86 7353.13 137.14 o -1 6 0 4163.42 4292.51 77.56 o 0 6 0 25172.41 24978.28 320.66 o 1 6 0 5480.01 5655.49 91.89 o 2 6 0 11252.81 11073.37 154.82 o 3 6 0 2552.92 2431.72 67.33 o 4 6 0 4232.66 4369.82 103.18 o 5 6 0 25493.97 24725.63 408.69 o 6 6 0 1440.05 1542.65 58.27 o 7 6 0 71.28 96.59 33.67 o 8 6 0 850.71 833.87 109.17 o 9 6 0 538.29 553.90 42.84 o 10 6 0 1680.62 1608.28 71.35 o 11 6 0 958.80 922.67 57.07 o 12 6 0 11.28 35.84 20.81 o 13 6 0 371.90 375.14 59.50 o 14 6 0 116.28 99.15 43.15 o 15 6 0 64.99 48.40 65.47 o -11 7 0 732.38 802.37 98.06 o -10 7 0 1437.16 1513.15 77.86 o -9 7 0 2652.79 2994.67 108.58 o -8 7 0 495.03 528.90 47.72 o -7 7 0 1390.97 1327.38 65.15 o -6 7 0 194.44 311.26 41.18 o -5 7 0 3.19 8.04 8.52 o -4 7 0 742.11 647.05 29.87 o -3 7 0 904.50 815.42 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76.83 o 3 15 0 130.15 165.03 35.95 o 4 15 0 417.37 337.97 54.02 o 5 15 0 537.78 481.55 54.15 o 6 15 0 904.78 826.16 67.90 o 7 15 0 47.63 50.71 32.98 o 8 15 0 1255.82 1251.29 83.90 o -7 -15 1 531.64 420.30 60.88 o -6 -15 1 329.11 323.36 48.72 o -5 -15 1 221.86 229.54 40.99 o -4 -15 1 232.23 188.07 67.65 o -3 -15 1 583.81 581.03 79.89 o -2 -15 1 541.40 627.47 86.41 o -1 -15 1 846.26 855.00 97.57 o 0 -15 1 805.51 875.34 95.49 o 1 -15 1 741.94 704.50 89.47 o -9 -14 1 93.86 28.05 40.88 o -8 -14 1 1451.13 1443.55 83.27 o -7 -14 1 636.42 604.21 60.33 o -6 -14 1 1554.98 1566.57 83.79 o -5 -14 1 588.46 487.27 53.27 o -4 -14 1 276.36 279.21 42.03 o -3 -14 1 162.02 168.68 33.83 o -2 -14 1 659.56 617.67 54.98 o -1 -14 1 76.23 141.51 48.19 o 1 -14 1 2.81 13.04 32.69 o 2 -14 1 4.89 31.40 35.55 o 3 -14 1 123.86 158.60 51.06 o -11 -13 1 75.21 87.55 30.25 o -10 -13 1 6.55 32.81 29.38 o -9 -13 1 260.47 370.45 48.18 o -8 -13 1 446.75 380.28 49.50 o -7 -13 1 462.21 397.93 49.79 o -6 -13 1 1714.32 1707.09 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