#------------------------------------------------------------------------------
#$Date: 2016-02-20 02:53:41 +0200 (Sat, 20 Feb 2016) $
#$Revision: 176768 $
#$URL: svn://www.crystallography.net/cod/cif/2/10/43/2104304.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2104304
loop_
_publ_author_name
'Daszkiewicz, Marek'
'Gulay, Lubomir D.'
'Lychmanyuk, Olga S.'
_publ_section_title
;
 Ln₃M~1{-~δ}TX₇ -- quasi-isostructural compounds:
 stereochemistry and silver-ion motion in the Ln₃Ag~1{-~δ}GeS₇ (Ln
 = La--Nd, Sm, Gd--Er and Y; δ = 0.11--0.50) compounds
;
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section B'
_journal_page_first              126
_journal_page_last               133
_journal_paper_doi               10.1107/S010876810900144X
_journal_volume                  65
_journal_year                    2009
_chemical_formula_moiety         'Ag0.88 Ce3 Ge S7'
_chemical_formula_sum            'Ag0.88 Ce3 Ge S7'
_chemical_formula_weight         812.30
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           173
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  'P 6c'
_symmetry_space_group_name_H-M   'P 63'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            2
_cell_length_a                   10.3902(15)
_cell_length_b                   10.3902(15)
_cell_length_c                   5.8425(12)
_cell_measurement_reflns_used    704
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      26.37
_cell_measurement_theta_min      4.16
_cell_volume                     546.23(16)
_computing_cell_refinement       'CrysAlis RED'
_computing_data_collection       'CrysAlis CCD (Oxford Diffraction, 2007)'
_computing_data_reduction        'CrysAlis RED'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      295(2)
_diffrn_detector_area_resol_mean '1024x1024 with blocks 2x2, 33.133pixel/mm'
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'KUMA KM-4 with area CCD detector'
_diffrn_measurement_method       ω-scan
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0431
_diffrn_reflns_av_sigmaI/netI    0.0236
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       6
_diffrn_reflns_limit_l_min       -7
_diffrn_reflns_number            6515
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         4.16
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    17.792
_exptl_absorpt_correction_T_max  0.599
_exptl_absorpt_correction_T_min  0.097
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'CrysAlis (Oxford Diffraction, 2007)'
_exptl_crystal_colour            'dark red'
_exptl_crystal_density_diffrn    4.939
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             719
_exptl_crystal_size_max          0.09
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.06
_refine_diff_density_max         1.013
_refine_diff_density_min         -0.701
_refine_ls_abs_structure_details
'Flack H D (1983), Acta Cryst. A39, 876-881, 319 Friedel pairs'
_refine_ls_abs_structure_Flack   -0.04(2)
_refine_ls_extinction_coef       0.0122(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.057
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     43
_refine_ls_number_reflns         726
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.056
_refine_ls_R_factor_all          0.0224
_refine_ls_R_factor_gt           0.0214
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         <0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0294P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0461
_refine_ls_wR_factor_ref         0.0464
_reflns_number_gt                704
_reflns_number_total             726
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            bp5017.cif
_cod_data_source_block           ce
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_database_code               2104304
_cod_database_fobs_code          2104304
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-x, -y, z+1/2'
'y, -x+y, z+1/2'
'x-y, x, z+1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ce Ce 0.87483(3) 0.64142(3) 0.23920(14) 0.01007(13) Uani d . 1 . .
Ag Ag1 0.0000 0.0000 0.1694(6) 0.0391(16) Uani d SP 0.783(9) . .
Ag Ag2 0.0000 0.0000 0.965(4) 0.026(7) Uani d SP 0.098(9) . .
Ge Ge1 0.3333 0.6667 0.3228(2) 0.0100(3) Uani d S 1 . .
S S1 0.3333 0.6667 0.9480(5) 0.0116(6) Uani d S 1 . .
S S2 0.90743(17) 0.73512(17) 0.7237(4) 0.0135(3) Uani d . 1 . .
S S3 0.5867(2) 0.47870(19) 0.9745(3) 0.0108(3) Uani d . 1 . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
S3 Ce S2 3_664 6_654 106.58(5) ?
S3 Ce S2 3_664 5_564 140.39(6) ?
S2 Ce S2 6_654 5_564 90.76(6) ?
S3 Ce S2 3_664 . 137.17(5) ?
S2 Ce S2 6_654 . 80.01(5) ?
S2 Ce S2 5_564 . 79.98(5) ?
S3 Ce S3 3_664 1_554 73.73(7) ?
S2 Ce S3 6_654 1_554 142.23(6) ?
S2 Ce S3 5_564 1_554 71.11(5) ?
S2 Ce S3 . 1_554 126.28(5) ?
S3 Ce S3 3_664 6_654 73.27(3) ?
S2 Ce S3 6_654 6_654 68.46(5) ?
S2 Ce S3 5_564 6_654 145.89(5) ?
S2 Ce S3 . 6_654 70.23(5) ?
S3 Ce S3 1_554 6_654 140.90(5) ?
S3 Ce S1 3_664 4_664 70.19(5) ?
S2 Ce S1 6_654 4_664 148.24(5) ?
S2 Ce S1 5_564 4_664 111.99(4) ?
S2 Ce S1 . 4_664 82.44(6) ?
S3 Ce S1 1_554 4_664 68.73(5) ?
S3 Ce S1 6_654 4_664 80.76(4) ?
S3 Ce S2 3_664 1_554 72.60(5) ?
S2 Ce S2 6_654 1_554 77.22(5) ?
S2 Ce S2 5_564 1_554 77.19(5) ?
S2 Ce S2 . 1_554 147.31(6) ?
S3 Ce S2 1_554 1_554 66.74(4) ?
S3 Ce S2 6_654 1_554 120.98(5) ?
S1 Ce S2 4_664 1_554 127.92(6) ?
S3 Ce Ag1 3_664 1_665 134.75(7) ?
S2 Ce Ag1 6_654 1_665 45.56(3) ?
S2 Ce Ag1 5_564 1_665 45.55(3) ?
S2 Ce Ag1 . 1_665 80.27(7) ?
S3 Ce Ag1 1_554 1_665 106.80(5) ?
S3 Ce Ag1 6_654 1_665 111.20(5) ?
S1 Ce Ag1 4_664 1_665 153.84(5) ?
S2 Ce Ag1 1_554 1_665 67.04(7) ?
S3 Ce Ag2 3_664 4_664 156.6(2) ?
S2 Ce Ag2 6_654 4_664 50.24(14) ?
S2 Ce Ag2 5_564 4_664 50.23(14) ?
S2 Ce Ag2 . 4_664 51.3(4) ?
S3 Ce Ag2 1_554 4_664 121.33(15) ?
S3 Ce Ag2 6_654 4_664 96.9(2) ?
S1 Ce Ag2 4_664 4_664 130.2(3) ?
S2 Ce Ag2 1_554 4_664 96.0(4) ?
Ag1 Ce Ag2 1_665 4_664 29.0(3) ?
S3 Ce Ag2 3_664 1_664 117.6(3) ?
S2 Ce Ag2 6_654 1_664 49.93(13) ?
S2 Ce Ag2 5_564 1_664 49.92(13) ?
S2 Ce Ag2 . 1_664 99.3(3) ?
S3 Ce Ag2 1_554 1_664 95.4(2) ?
S3 Ce Ag2 6_654 1_664 118.29(11) ?
S1 Ce Ag2 4_664 1_664 160.43(3) ?
S2 Ce Ag2 1_554 1_664 48.0(3) ?
Ag1 Ce Ag2 1_665 1_664 19.0(3) ?
Ag2 Ce Ag2 4_664 1_664 48.00(3) ?
Ag2 Ag1 Ag2 1_554 4_554 180.000(3) ?
Ag2 Ag1 S2 1_554 4_664 97.47(9) ?
Ag2 Ag1 S2 4_554 4_664 82.53(9) ?
Ag2 Ag1 S2 1_554 5_454 97.47(9) ?
Ag2 Ag1 S2 4_554 5_454 82.53(9) ?
S2 Ag1 S2 4_664 5_454 118.34(4) ?
Ag2 Ag1 S2 1_554 6_544 97.47(9) ?
Ag2 Ag1 S2 4_554 6_544 82.53(9) ?
S2 Ag1 S2 4_664 6_544 118.34(4) ?
S2 Ag1 S2 5_454 6_544 118.34(4) ?
Ag2 Ag1 Ag1 1_554 4_554 0.0 ?
Ag2 Ag1 Ag1 4_554 4_554 180.000(3) ?
S2 Ag1 Ag1 4_664 4_554 97.47(9) ?
S2 Ag1 Ag1 5_454 4_554 97.47(9) ?
S2 Ag1 Ag1 6_544 4_554 97.47(9) ?
Ag2 Ag1 Ag1 1_554 4 180.0 ?
Ag2 Ag1 Ag1 4_554 4 0.000(3) ?
S2 Ag1 Ag1 4_664 4 82.53(9) ?
S2 Ag1 Ag1 5_454 4 82.53(9) ?
S2 Ag1 Ag1 6_544 4 82.53(9) ?
Ag1 Ag1 Ag1 4_554 4 180.0 ?
Ag2 Ag1 Ce 1_554 2_655 97.09(6) ?
Ag2 Ag1 Ce 4_554 2_655 82.91(6) ?
S2 Ag1 Ce 4_664 2_655 59.44(4) ?
S2 Ag1 Ce 5_454 2_655 165.44(14) ?
S2 Ag1 Ce 6_544 2_655 59.49(4) ?
Ag1 Ag1 Ce 4_554 2_655 97.09(6) ?
Ag1 Ag1 Ce 4 2_655 82.91(6) ?
Ag2 Ag1 Ce 1_554 1_445 97.09(6) ?
Ag2 Ag1 Ce 4_554 1_445 82.91(6) ?
S2 Ag1 Ce 4_664 1_445 165.44(14) ?
S2 Ag1 Ce 5_454 1_445 59.49(4) ?
S2 Ag1 Ce 6_544 1_445 59.44(4) ?
Ag1 Ag1 Ce 4_554 1_445 97.09(6) ?
Ag1 Ag1 Ce 4 1_445 82.91(6) ?
Ce Ag1 Ce 2_655 1_445 118.50(3) ?
Ag2 Ag1 Ce 1_554 3_565 97.09(6) ?
Ag2 Ag1 Ce 4_554 3_565 82.91(6) ?
S2 Ag1 Ce 4_664 3_565 59.49(4) ?
S2 Ag1 Ce 5_454 3_565 59.44(4) ?
S2 Ag1 Ce 6_544 3_565 165.44(14) ?
Ag1 Ag1 Ce 4_554 3_565 97.09(6) ?
Ag1 Ag1 Ce 4 3_565 82.91(6) ?
Ce Ag1 Ce 2_655 3_565 118.50(3) ?
Ce Ag1 Ce 1_445 3_565 118.50(3) ?
Ag1 Ag2 Ag1 1_556 4 180.000(3) ?
Ag1 Ag2 S2 1_556 1_445 120.2(4) ?
Ag1 Ag2 S2 4 1_445 59.8(4) ?
Ag1 Ag2 S2 1_556 2_655 120.2(4) ?
Ag1 Ag2 S2 4 2_655 59.8(4) ?
S2 Ag2 S2 1_445 2_655 96.9(6) ?
Ag1 Ag2 S2 1_556 3_565 120.2(4) ?
Ag1 Ag2 S2 4 3_565 59.8(4) ?
S2 Ag2 S2 1_445 3_565 96.9(6) ?
S2 Ag2 S2 2_655 3_565 96.9(6) ?
Ag1 Ag2 S2 1_556 4_665 58.0(4) ?
Ag1 Ag2 S2 4 4_665 122.0(4) ?
S2 Ag2 S2 1_445 4_665 178.2(8) ?
S2 Ag2 S2 2_655 4_665 84.28(3) ?
S2 Ag2 S2 3_565 4_665 84.28(3) ?
Ag1 Ag2 S2 1_556 6_545 58.0(4) ?
Ag1 Ag2 S2 4 6_545 122.0(4) ?
S2 Ag2 S2 1_445 6_545 84.28(3) ?
S2 Ag2 S2 2_655 6_545 84.28(3) ?
S2 Ag2 S2 3_565 6_545 178.2(8) ?
S2 Ag2 S2 4_665 6_545 94.5(6) ?
Ag1 Ag2 S2 1_556 5_455 58.0(4) ?
Ag1 Ag2 S2 4 5_455 122.0(4) ?
S2 Ag2 S2 1_445 5_455 84.28(3) ?
S2 Ag2 S2 2_655 5_455 178.2(8) ?
S2 Ag2 S2 3_565 5_455 84.28(3) ?
S2 Ag2 S2 4_665 5_455 94.5(6) ?
S2 Ag2 S2 6_545 5_455 94.5(6) ?
Ag1 Ag2 Ag2 1_556 4 0.000(4) ?
Ag1 Ag2 Ag2 4 4 180.000(9) ?
S2 Ag2 Ag2 1_445 4 120.2(4) ?
S2 Ag2 Ag2 2_655 4 120.2(4) ?
S2 Ag2 Ag2 3_565 4 120.2(4) ?
S2 Ag2 Ag2 4_665 4 58.0(4) ?
S2 Ag2 Ag2 6_545 4 58.0(4) ?
S2 Ag2 Ag2 5_455 4 58.0(4) ?
Ag1 Ag2 Ag2 1_556 4_554 180.000(12) ?
Ag1 Ag2 Ag2 4 4_554 0.000(2) ?
S2 Ag2 Ag2 1_445 4_554 59.8(4) ?
S2 Ag2 Ag2 2_655 4_554 59.8(4) ?
S2 Ag2 Ag2 3_565 4_554 59.8(4) ?
S2 Ag2 Ag2 4_665 4_554 122.0(4) ?
S2 Ag2 Ag2 6_545 4_554 122.0(4) ?
S2 Ag2 Ag2 5_455 4_554 122.0(4) ?
Ag2 Ag2 Ag2 4 4_554 180.000(11) ?
Ag1 Ag2 Ce 1_556 5_455 111.9(4) ?
Ag1 Ag2 Ce 4 5_455 68.1(4) ?
S2 Ag2 Ce 1_445 5_455 53.92(19) ?
S2 Ag2 Ce 2_655 5_455 127.9(8) ?
S2 Ag2 Ce 3_565 5_455 53.96(19) ?
S2 Ag2 Ce 4_665 5_455 126.26(12) ?
S2 Ag2 Ce 6_545 5_455 126.22(12) ?
S2 Ag2 Ce 5_455 5_455 53.94(6) ?
Ag2 Ag2 Ce 4 5_455 111.9(4) ?
Ag2 Ag2 Ce 4_554 5_455 68.1(4) ?
Ag1 Ag2 Ce 1_556 4_665 111.9(4) ?
Ag1 Ag2 Ce 4 4_665 68.1(4) ?
S2 Ag2 Ce 1_445 4_665 127.9(8) ?
S2 Ag2 Ce 2_655 4_665 53.96(19) ?
S2 Ag2 Ce 3_565 4_665 53.92(19) ?
S2 Ag2 Ce 4_665 4_665 53.94(6) ?
S2 Ag2 Ce 6_545 4_665 126.26(12) ?
S2 Ag2 Ce 5_455 4_665 126.22(12) ?
Ag2 Ag2 Ce 4 4_665 111.9(4) ?
Ag2 Ag2 Ce 4_554 4_665 68.1(4) ?
Ce Ag2 Ce 5_455 4_665 106.9(4) ?
S1 Ge1 S3 1_554 5_564 113.33(5) ?
S1 Ge1 S3 1_554 6_554 113.33(5) ?
S3 Ge1 S3 5_564 6_554 105.35(6) ?
S1 Ge1 S3 1_554 4_664 113.33(5) ?
S3 Ge1 S3 5_564 4_664 105.35(6) ?
S3 Ge1 S3 6_554 4_664 105.35(6) ?
Ge1 S1 Ce 1_556 6 113.33(5) ?
Ge1 S1 Ce 1_556 4_665 113.33(5) ?
Ce S1 Ce 6 4_665 105.35(6) ?
Ge1 S1 Ce 1_556 5_565 113.33(5) ?
Ce S1 Ce 6 5_565 105.35(6) ?
Ce S1 Ce 4_665 5_565 105.35(6) ?
Ag2 S2 Ag2 1_665 4_664 62.23(4) ?
Ag1 S2 Ce 4_665 5_565 74.99(4) ?
Ag2 S2 Ce 1_665 5_565 75.84(7) ?
Ag2 S2 Ce 4_664 5_565 77.96(9) ?
Ag1 S2 Ce 4_665 6_655 74.95(4) ?
Ag2 S2 Ce 1_665 6_655 75.80(7) ?
Ag2 S2 Ce 4_664 6_655 77.93(9) ?
Ce S2 Ce 5_565 6_655 148.99(6) ?
Ag1 S2 Ce 4_665 . 99.36(10) ?
Ag2 S2 Ce 1_665 . 137.0(4) ?
Ag2 S2 Ce 4_664 . 74.8(4) ?
Ce S2 Ce 5_565 . 96.12(6) ?
Ce S2 Ce 6_655 . 96.08(5) ?
Ag1 S2 Ce 4_665 1_556 113.33(10) ?
Ag2 S2 Ce 1_665 1_556 75.7(4) ?
Ag2 S2 Ce 4_664 1_556 137.9(4) ?
Ce S2 Ce 5_565 1_556 92.49(5) ?
Ce S2 Ce 6_655 1_556 92.45(5) ?
Ce S2 Ce . 1_556 147.31(6) ?
Ge1 S3 Ce 4_665 2_656 91.96(6) ?
Ge1 S3 Ce 4_665 1_556 88.97(6) ?
Ce S3 Ce 2_656 1_556 111.29(6) ?
Ge1 S3 Ce 4_665 5_565 121.90(7) ?
Ce S3 Ce 2_656 5_565 139.74(7) ?
Ce S3 Ce 1_556 5_565 92.00(5) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Ce S3 3_664 2.9091(18) ?
Ce S2 6_654 2.9425(16) ?
Ce S2 5_564 2.9446(16) ?
Ce S2 . 2.957(2) ?
Ce S3 1_554 3.0251(18) ?
Ce S3 6_654 3.0758(18) ?
Ce S1 4_664 3.0805(13) ?
Ce S2 1_554 3.131(2) ?
Ce Ag1 1_665 3.3005(7) ?
Ce Ag2 4_664 3.530(9) ?
Ce Ag2 1_664 3.647(11) ?
Ag1 Ag2 1_554 1.20(2) ?
Ag1 Ag2 4_554 1.73(2) ?
Ag1 S2 4_664 2.4399(16) ?
Ag1 S2 5_454 2.4399(16) ?
Ag1 S2 6_544 2.4399(16) ?
Ag1 Ag1 4_554 2.9212(6) ?
Ag1 Ag1 4 2.9213(6) ?
Ag1 Ce 2_655 3.3005(7) ?
Ag1 Ce 1_445 3.3005(7) ?
Ag1 Ce 3_565 3.3005(7) ?
Ag2 Ag1 1_556 1.20(2) ?
Ag2 Ag1 4 1.73(2) ?
Ag2 S2 1_445 2.799(12) ?
Ag2 S2 2_655 2.799(12) ?
Ag2 S2 3_565 2.799(12) ?
Ag2 S2 4_665 2.854(13) ?
Ag2 S2 6_545 2.854(13) ?
Ag2 S2 5_455 2.854(13) ?
Ag2 Ag2 4 2.9212(6) ?
Ag2 Ag2 4_554 2.9212(6) ?
Ag2 Ce 5_455 3.530(9) ?
Ag2 Ce 4_665 3.530(9) ?
Ge1 S1 1_554 2.190(3) ?
Ge1 S3 5_564 2.2391(19) ?
Ge1 S3 6_554 2.2391(19) ?
Ge1 S3 4_664 2.2391(19) ?
S1 Ge1 1_556 2.190(3) ?
S1 Ce 6 3.0805(13) ?
S1 Ce 4_665 3.0805(13) ?
S1 Ce 5_565 3.0805(13) ?
S2 Ag1 4_665 2.4399(16) ?
S2 Ag2 1_665 2.799(12) ?
S2 Ag2 4_664 2.854(13) ?
S2 Ce 5_565 2.9425(16) ?
S2 Ce 6_655 2.9446(16) ?
S2 Ce 1_556 3.131(2) ?
S3 Ge1 4_665 2.2391(19) ?
S3 Ce 2_656 2.9091(18) ?
S3 Ce 1_556 3.0251(18) ?
S3 Ce 5_565 3.0758(18) ?
