#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/44/2104469.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104469_Fobs loop_ _publ_author_name 'Wahl, B.' 'Ruck, M.' _publ_section_title ; Superspace description of the modulated structure of the metal-salt-hybrid Bi~7{-~\d}Ni~2~Br~5{-~2\d} (\d = 1/9) ; _journal_coeditor_code SN5087 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 593 _journal_page_last 599 _journal_volume 65 _journal_year 2009 _space_group_IT_number 59 _symmetry_space_group_name_Hall '-P 2c 2a' _symmetry_space_group_name_H-M 'P m n m :2' _[local]_cod_data_source_file sn5087Bi7Ni2Br5averagesup2.hkl _[local]_cod_data_source_block Bi7Ni2Br5average loop_ _refln_index_h _refln_index_k _refln_index_l _refln_intensity_meas _refln_intensity_calc _refln_intensity_sigma _refln_observed_status 4 0 0 130790.3 120382.8 689.4 o 1 1 0 407.6 167.7 72.6 o 2 1 0 296.6 46.4 49.5 o 3 1 0 850.9 660.5 47.5 o 4 1 0 480.8 17.4 61.8 o 0 2 0 17462.7 24216.0 1260.5 o 1 2 0 8.8 40.8 52.5 < 2 2 0 23802.4 21383.3 139.4 o 3 2 0 69.5 86.7 46.9 < 4 2 0 14394.6 13423.1 107.8 o 0 3 0 965.8 1.9 670.6 < 1 3 0 22177.5 19367.2 158.5 o 2 3 0 115.5 110.6 52.9 < 3 3 0 16412.8 15260.6 106.4 o 4 3 0 87.4 325.1 74.8 < 0 4 0 424.5 83.3 476.7 < 1 4 0 430.6 469.7 103.6 o 2 4 0 229.9 73.4 64.0 o 3 4 0 443.1 435.2 58.6 o 4 4 0 105.9 36.5 75.2 < 0 5 0 1767.2 5.2 363.6 o 1 5 0 496238.0 388449.2 2576.0 o 2 5 0 98.4 37.7 61.0 < 3 5 0 128235.9 116484.7 658.4 o 4 5 0 13.9 93.9 73.4 < 0 6 0 23207.0 35727.0 377.7 o 1 6 0 333.0 72.1 95.6 o 2 6 0 22681.9 20831.3 146.1 o 3 6 0 30.0 35.8 60.8 < 4 6 0 7555.6 7469.9 93.3 o 0 7 0 498.5 392.2 239.5 < 1 7 0 2264.2 1796.4 116.8 o 2 7 0 322.4 264.1 67.3 o 3 7 0 208.7 74.7 62.3 o 4 7 0 104.1 73.6 73.9 < 0 8 0 2734.5 4409.3 208.4 o 1 8 0 510.6 455.9 132.8 o 2 8 0 7847.1 7800.2 102.8 o 3 8 0 246.6 278.3 67.2 o 4 8 0 8605.8 8490.8 103.9 o 0 9 0 1022.5 1038.3 169.4 o 1 9 0 96328.8 99553.5 564.6 o 2 9 0 804.7 546.9 77.8 o 3 9 0 35979.1 34606.6 233.8 o 4 9 0 107.0 119.9 107.0 < 0 10 0 161683.2 243705.4 913.3 o 1 10 0 166.2 173.5 153.8 < 2 10 0 135243.6 127686.2 711.2 o 3 10 0 209.7 146.6 83.8 < 4 10 0 29080.1 28680.3 194.9 o 0 11 0 505.6 391.0 129.7 o 1 11 0 47859.6 49109.2 343.8 o 2 11 0 212.9 102.5 94.2 < 3 11 0 25607.5 24052.0 173.0 o 4 11 0 -33.9 5.0 111.0 < 0 12 0 4058.8 5115.3 133.0 o 1 12 0 191.6 1.3 164.1 < 2 12 0 2376.4 2005.8 99.3 o 3 12 0 138.0 90.1 93.1 < 4 12 0 241.9 124.8 128.5 < 0 13 0 112.1 300.5 110.9 < 1 13 0 7564.9 8833.9 150.7 o 2 13 0 311.3 497.7 93.6 o 3 13 0 7064.1 7236.0 101.7 o 4 13 0 204.7 562.7 141.8 < 0 14 0 36939.2 48586.4 255.6 o 1 14 0 387.1 277.8 133.1 < 2 14 0 30778.6 29279.8 215.8 o 3 14 0 200.8 89.3 76.4 < 4 14 0 8180.9 8050.4 162.7 o 0 15 0 552.9 572.9 95.3 o 1 15 0 32752.2 37271.7 216.9 o 2 15 0 739.2 590.1 111.3 o 3 15 0 12865.1 12195.0 131.8 o 0 16 0 6877.1 8505.0 109.3 o 1 16 0 85.4 26.0 79.9 < 2 16 0 6984.0 6008.9 135.5 o 3 16 0 54.7 1.8 104.8 < 0 17 0 109.3 108.7 85.8 < 1 17 0 3500.2 3469.2 85.3 o 2 17 0 0.8 41.6 87.4 < 3 17 0 2037.7 1857.0 89.9 o 0 18 0 3368.1 3309.9 73.7 o 1 18 0 360.0 538.7 64.3 o 2 18 0 1381.4 1322.8 99.8 o 3 18 0 157.9 335.9 82.5 < 0 19 0 418.6 316.4 62.2 o 1 19 0 38846.0 43053.9 217.0 o 2 19 0 196.8 190.6 81.0 < 3 19 0 16672.6 17440.6 139.2 o 0 20 0 2682.4 2738.9 67.9 o 1 20 0 193.6 119.7 50.0 o 2 20 0 1114.4 1229.8 89.7 o 3 20 0 171.8 141.2 76.7 < 0 21 0 31.9 22.8 59.1 < 1 21 0 2314.2 2389.8 53.2 o 2 21 0 56.5 32.9 113.3 < 3 21 0 1361.2 1522.5 79.7 o 0 22 0 159.8 120.6 52.1 o 1 22 0 -28.1 17.0 40.8 < 2 22 0 364.8 246.7 101.6 o 0 23 0 1003.1 1038.0 58.5 o 1 23 0 1784.8 1660.4 48.7 o 2 23 0 549.5 695.4 238.1 < 0 24 0 13580.9 13721.4 101.8 o 1 24 0 313.9 245.1 41.1 o 2 24 0 8360.8 8028.1 272.4 o 0 25 0 49.6 27.4 53.8 < 1 25 0 1025.6 1310.6 43.5 o 0 26 0 841.7 1086.1 53.9 o 1 26 0 71.6 13.9 37.9 < 0 27 0 102.9 21.5 48.2 < 1 0 1 137.3 38.3 70.7 < 3 0 1 -14.3 0.4 48.7 < 0 1 1 122.2 123.7 76.5 < 1 1 1 1266.5 931.6 50.2 o 2 1 1 15.2 48.7 36.6 < 3 1 1 127.8 56.5 34.6 o 4 1 1 57.1 11.2 50.3 < 0 2 1 292.6 47.7 100.8 < 1 2 1 351.7 356.6 51.1 o 2 2 1 97.5 23.8 34.2 < 3 2 1 132.8 143.8 36.5 o 4 2 1 17.0 2.8 46.9 < 0 3 1 5.8 8.4 124.6 < 1 3 1 4599.8 3775.6 70.5 o 2 3 1 29.2 7.7 34.1 < 3 3 1 1285.8 1179.6 38.9 o 4 3 1 63.6 13.9 59.7 < 0 4 1 1303.9 1062.2 192.2 o 1 4 1 226.3 219.2 61.6 o 2 4 1 610.0 477.5 40.7 o 3 4 1 70.9 20.7 42.6 < 4 4 1 177.8 115.5 61.7 < 0 5 1 276.3 6.5 205.7 < 1 5 1 780.6 713.9 77.1 o 2 5 1 5.3 2.4 35.8 < 3 5 1 85.3 22.8 43.4 < 4 5 1 29.8 26.7 64.1 < 0 6 1 144.9 84.1 218.0 < 1 6 1 474.9 214.8 94.0 o 2 6 1 354.8 328.5 44.8 o 3 6 1 177.4 54.0 46.0 o 4 6 1 635.8 506.3 72.4 o 0 7 1 391.2 292.9 225.6 < 1 7 1 252.5 101.0 99.2 < 2 7 1 75.7 100.2 44.4 < 3 7 1 38.0 8.6 49.0 < 4 7 1 58.6 3.7 70.8 < 0 8 1 52049.0 44954.7 429.4 o 1 8 1 60.4 138.2 94.8 < 2 8 1 22796.6 21733.2 152.0 o 3 8 1 8.1 58.4 50.1 < 4 8 1 4332.7 4433.5 72.1 o 0 9 1 1329.8 1479.6 214.3 o 1 9 1 7832.5 5604.2 133.7 o 2 9 1 540.3 607.7 83.8 o 3 9 1 2639.9 1987.6 57.4 o 4 9 1 44.4 61.2 58.5 < 0 10 1 5778.9 879.5 156.9 o 1 10 1 110.6 270.1 88.1 < 2 10 1 1697.0 82.6 63.0 o 3 10 1 139.2 42.1 56.1 < 4 10 1 472.7 110.7 60.3 o 0 11 1 -10.7 7.1 93.9 < 1 11 1 6739.7 6934.2 101.5 o 2 11 1 45.7 0.5 67.0 < 3 11 1 4187.8 3695.4 68.4 o 4 11 1 40.9 0.1 72.5 < 0 12 1 2596.6 3229.5 95.5 o 1 12 1 90.6 175.1 78.1 < 2 12 1 1540.4 1118.3 77.5 o 3 12 1 32.6 44.4 64.5 < 4 12 1 172.7 42.3 80.1 < 0 13 1 161.7 137.6 75.5 < 1 13 1 22943.7 24034.8 161.2 o 2 13 1 87.2 59.7 84.6 < 3 13 1 9318.8 8774.1 100.4 o 4 13 1 42.7 5.1 83.6 < 0 14 1 18298.9 22437.5 133.9 o 1 14 1 38.4 24.6 76.5 < 2 14 1 12885.7 12247.5 113.2 o 3 14 1 70.1 2.0 73.3 < 4 14 1 3041.4 2954.4 80.5 o 0 15 1 653.8 679.9 61.4 o 1 15 1 312.5 155.1 77.4 o 2 15 1 433.7 322.9 74.5 o 3 15 1 302.8 159.2 63.7 o 0 16 1 714.0 766.1 58.8 o 1 16 1 444.9 496.0 66.5 o 2 16 1 1396.4 1344.0 86.7 o 3 16 1 299.9 161.2 62.9 o 0 17 1 864.8 775.9 54.9 o 1 17 1 146.0 95.8 58.7 < 2 17 1 391.0 352.5 77.5 o 3 17 1 203.4 210.0 57.7 o 0 18 1 13480.6 15308.4 94.7 o 1 18 1 -17.5 17.9 57.2 < 2 18 1 8092.9 8548.1 102.1 o 3 18 1 53.2 24.3 65.3 < 0 19 1 498.3 418.0 51.0 o 1 19 1 11222.0 11985.8 81.1 o 2 19 1 311.8 175.4 73.8 o 3 19 1 5366.1 5382.1 76.2 o 0 20 1 2972.7 3295.1 54.2 o 1 20 1 51.8 74.0 39.0 < 2 20 1 1462.0 1540.1 81.2 o 3 20 1 58.5 27.5 60.5 < 0 21 1 -81.1 16.2 47.1 < 1 21 1 1573.7 1867.5 38.2 o 2 21 1 43.9 31.7 95.4 < 3 21 1 1218.0 1528.8 62.5 o 0 22 1 268.4 327.1 42.7 o 1 22 1 47.9 55.1 31.8 < 2 22 1 403.5 544.5 103.2 o 0 23 1 1523.2 1222.9 43.3 o 1 23 1 770.6 881.8 31.4 o 2 23 1 694.2 716.4 123.0 o 0 24 1 13312.1 13975.4 86.4 o 1 24 1 60.1 17.3 30.3 < 2 24 1 8254.8 8669.3 176.1 o 0 25 1 401.6 345.9 38.7 o 1 25 1 1613.1 1603.6 32.0 o 0 26 1 3.3 26.9 37.9 < 1 26 1 189.3 319.3 29.1 o 0 27 1 159.4 6.8 37.4 o 0 0 2 56724.7 49742.1 325.3 o 2 0 2 32352.9 29346.6 208.0 o 4 0 2 10384.0 9662.2 149.3 o 0 1 2 187.4 56.3 46.0 o 1 1 2 1262.3 869.2 235.3 o 2 1 2 76.9 6.1 44.4 < 3 1 2 132.1 40.8 46.5 < 4 1 2 92.6 1.3 78.7 < 0 2 2 36053.6 32841.4 226.5 o 1 2 2 28.3 2.4 121.4 < 2 2 2 17228.4 15312.9 107.4 o 3 2 2 43.7 23.4 45.7 < 4 2 2 4096.6 3761.1 95.9 o 0 3 2 610.6 27.2 90.7 o 1 3 2 1442.9 988.5 91.1 o 2 3 2 231.8 140.5 46.7 o 3 3 2 977.0 838.8 54.4 o 4 3 2 154.6 231.7 103.8 < 0 4 2 35935.8 33284.2 250.5 o 1 4 2 383.4 0.3 76.8 o 2 4 2 13421.8 12102.9 94.1 o 3 4 2 9.0 72.3 57.6 < 4 4 2 955.6 917.6 67.1 o 0 5 2 69.4 52.8 101.7 < 1 5 2 28485.7 28516.4 190.5 o 2 5 2 84.7 70.9 53.5 < 3 5 2 8700.8 8372.4 85.1 o 4 5 2 84.0 82.5 65.1 < 0 6 2 1548.4 1469.4 104.8 o 1 6 2 -36.9 0.5 107.9 < 2 6 2 241.7 168.4 55.1 o 3 6 2 65.7 135.5 62.2 < 4 6 2 288.1 164.4 64.5 o 0 7 2 532.0 498.8 127.9 o 1 7 2 2251.9 2326.1 91.2 o 2 7 2 151.2 81.7 60.2 < 3 7 2 930.7 880.3 72.2 o 4 7 2 100.3 2.9 65.7 < 0 8 2 12966.6 12448.7 171.3 o 1 8 2 191.3 37.2 80.6 < 2 8 2 6980.0 6728.8 90.3 o 3 8 2 36.3 4.0 84.1 < 4 8 2 2074.1 1969.7 81.0 o 0 9 2 199.1 33.9 137.4 < 1 9 2 48003.4 53358.2 278.7 o 2 9 2 9.0 50.9 92.8 < 3 9 2 16950.0 16808.2 123.7 o 4 9 2 -11.0 37.8 77.3 < 0 10 2 33491.9 31507.5 264.4 o 1 10 2 36.1 5.3 73.0 < 2 10 2 16984.9 17580.7 125.8 o 3 10 2 -18.1 7.2 82.0 < 4 10 2 4428.6 4231.0 74.9 o 0 11 2 323.6 53.1 150.8 < 1 11 2 3926.4 4090.9 87.8 o 2 11 2 180.5 54.0 62.0 < 3 11 2 3056.1 2808.9 69.7 o 4 11 2 80.3 20.8 63.2 < 0 12 2 7885.5 6549.9 164.8 o 1 12 2 71.1 9.5 75.9 < 2 12 2 2984.5 2788.0 68.3 o 3 12 2 93.0 79.4 59.5 < 4 12 2 379.6 307.8 67.0 o 0 13 2 68.6 39.3 128.5 < 1 13 2 426.8 309.8 84.9 o 2 13 2 86.6 107.5 67.7 < 3 13 2 37.7 9.3 55.1 < 4 13 2 111.3 173.7 68.1 < 0 14 2 22941.0 25542.1 175.5 o 1 14 2 155.7 203.7 70.0 < 2 14 2 12590.3 13088.7 104.1 o 3 14 2 25.2 40.2 50.7 < 4 14 2 2313.4 2339.6 75.8 o 0 15 2 159.0 191.5 70.7 < 1 15 2 8810.2 9096.9 90.4 o 2 15 2 6.3 21.9 64.7 < 3 15 2 2667.4 2564.3 59.0 o 0 16 2 3889.1 4771.2 77.1 o 1 16 2 -2.4 9.6 68.2 < 2 16 2 2021.5 2195.8 71.3 o 3 16 2 167.2 20.4 56.5 < 0 17 2 81.4 66.0 59.9 < 1 17 2 722.0 699.9 69.8 o 2 17 2 38.5 71.8 72.4 < 3 17 2 677.6 559.8 60.6 o 0 18 2 11954.5 13686.6 93.5 o 1 18 2 215.0 216.3 62.3 o 2 18 2 7229.8 7612.2 98.6 o 3 18 2 196.3 174.9 64.8 o 0 19 2 123.9 194.2 52.6 < 1 19 2 22493.2 23708.9 136.8 o 2 19 2 43.7 131.9 83.0 < 3 19 2 8256.0 8432.8 86.6 o 0 20 2 482.4 375.1 49.4 o 1 20 2 54.3 3.4 48.0 < 2 20 2 227.0 84.0 93.2 < 3 20 2 9.1 3.8 70.6 < 0 21 2 3.7 0.3 48.1 < 1 21 2 170.5 116.7 42.3 o 2 21 2 89.5 15.7 95.4 < 0 22 2 353.8 362.1 47.6 o 1 22 2 28.4 27.0 36.3 < 2 22 2 339.8 319.1 112.6 o 0 23 2 135.8 3.2 46.1 < 1 23 2 2740.4 2625.4 41.2 o 2 23 2 128.2 12.3 148.0 < 0 24 2 6430.2 6364.1 61.8 o 1 24 2 26.8 16.3 31.8 < 2 24 2 3516.8 3729.6 180.9 o 0 25 2 50.0 105.3 35.4 < 1 25 2 2370.7 2521.9 35.3 o 0 26 2 364.6 341.5 38.9 o 1 26 2 95.0 24.2 30.0 o 0 27 2 276.0 105.0 38.2 o 1 0 3 553.9 0.3 257.1 < 3 0 3 121.6 105.4 268.8 < 0 1 3 40.1 5.6 37.4 < 1 1 3 3253.1 3024.3 245.3 o 2 1 3 65.0 14.9 246.4 < 3 1 3 985.9 826.0 187.2 o 4 1 3 183.0 9.0 213.7 < 0 2 3 4308.4 4159.7 63.1 o 1 2 3 271.9 453.0 100.0 < 2 2 3 1506.2 1399.0 160.1 o 3 2 3 209.5 93.5 126.1 < 4 2 3 97.7 66.4 117.7 < 0 3 3 293.5 16.1 59.9 o 1 3 3 29265.5 28966.7 175.6 o 2 3 3 13.1 1.0 99.8 < 3 3 3 8120.5 7902.2 122.0 o 4 3 3 117.3 11.3 84.2 < 0 4 3 3286.7 2946.2 73.3 o 1 4 3 82.0 8.2 72.8 < 2 4 3 1528.3 1312.9 69.4 o 3 4 3 80.2 5.4 82.5 < 4 4 3 342.4 189.4 72.2 o 0 5 3 204.8 0.8 69.6 < 1 5 3 21903.2 21680.3 137.8 o 2 5 3 53.8 31.9 63.1 < 3 5 3 7979.8 7335.6 129.7 o 4 5 3 34.0 121.7 67.1 < 0 6 3 417.9 321.3 75.0 o 1 6 3 83.3 93.9 83.1 < 2 6 3 69.0 38.2 46.3 < 3 6 3 71.9 22.4 86.1 < 4 6 3 75.0 50.6 57.1 < 0 7 3 203.8 66.8 70.4 < 1 7 3 554.5 468.1 68.3 o 2 7 3 103.2 37.1 50.8 < 3 7 3 437.4 372.5 62.4 o 4 7 3 52.5 14.0 54.3 < 0 8 3 44802.7 40484.3 268.9 o 1 8 3 332.2 521.6 82.7 o 2 8 3 23987.1 24486.2 141.6 o 3 8 3 202.1 145.2 50.7 o 4 8 3 7638.7 7653.4 73.1 o 0 9 3 214.7 4.1 83.4 < 1 9 3 1541.0 1679.7 86.4 o 2 9 3 208.8 21.2 60.8 o 3 9 3 721.5 798.0 50.3 o 4 9 3 24.3 39.6 49.8 < 0 10 3 40262.5 38443.2 265.0 o 1 10 3 297.1 292.1 74.1 o 2 10 3 20051.1 21043.7 133.4 o 3 10 3 229.8 187.7 47.6 o 4 10 3 5104.1 5358.9 75.0 o 0 11 3 506.0 317.0 113.8 o 1 11 3 275.2 193.0 64.7 o 2 11 3 251.2 165.5 58.0 o 3 11 3 931.3 907.4 52.3 o 4 11 3 229.9 20.9 76.9 < 0 12 3 10067.3 9218.0 144.1 o 1 12 3 -111.7 26.2 61.3 < 2 12 3 3766.0 3877.3 73.2 o 3 12 3 116.1 9.2 52.0 < 4 12 3 433.6 387.1 59.4 o 0 13 3 92.5 152.9 122.6 < 1 13 3 42836.4 43723.0 243.2 o 2 13 3 131.7 147.6 66.6 < 3 13 3 18089.6 18299.7 117.4 o 4 13 3 135.4 65.6 61.4 < 0 14 3 11829.3 10016.3 160.0 o 1 14 3 549.3 683.4 67.3 o 2 14 3 7281.4 7803.0 93.8 o 3 14 3 165.7 72.7 58.9 < 4 14 3 3135.8 3534.2 62.4 o 0 15 3 559.4 433.1 112.3 o 1 15 3 4978.6 5223.3 76.3 o 2 15 3 277.0 161.0 71.3 o 3 15 3 2304.9 2262.3 69.1 o 0 16 3 13190.1 13388.8 132.5 o 1 16 3 73.1 4.3 64.3 < 2 16 3 8789.5 9581.6 100.7 o 3 16 3 9.6 1.4 66.2 < 0 17 3 365.1 88.2 80.9 o 1 17 3 15573.6 15680.8 110.6 o 2 17 3 140.8 33.3 74.2 < 3 17 3 5620.4 6003.7 70.2 o 0 18 3 19521.3 20445.6 135.0 o 1 18 3 541.6 573.8 66.4 o 2 18 3 13820.6 14530.8 124.4 o 3 18 3 295.6 280.5 57.0 o 0 19 3 82.2 246.8 62.5 < 1 19 3 26174.8 24968.1 160.1 o 2 19 3 98.1 128.9 92.7 < 3 19 3 10985.5 12314.2 88.7 o 0 20 3 2659.2 3045.2 58.7 o 1 20 3 -28.8 12.2 59.8 < 2 20 3 1054.0 1326.3 110.4 o 3 20 3 48.4 10.3 62.7 < 0 21 3 760.5 675.8 55.2 o 1 21 3 4061.0 4596.5 59.3 o 2 21 3 265.8 407.1 124.6 < 0 22 3 25505.0 26984.1 149.6 o 1 22 3 253.2 323.0 44.5 o 2 22 3 14593.4 16768.1 161.4 o 0 23 3 168.1 17.9 48.6 o 1 23 3 5815.8 5687.7 54.0 o 2 23 3 66.3 2.1 160.0 < 0 24 3 9941.6 10199.7 75.3 o 1 24 3 765.1 919.1 37.3 o 2 24 3 6952.1 8100.2 193.0 o 0 25 3 416.2 183.6 45.2 o 1 25 3 629.6 453.7 36.3 o 0 26 3 1029.0 1254.8 43.5 o 1 26 3 74.4 133.4 30.9 < 0 27 3 44.7 0.7 94.9 < 0 0 4 4178.7 3499.8 57.6 o 2 0 4 208.3 77.9 60.9 o 4 0 4 1983.1 2023.5 81.3 o 0 1 4 107.5 188.2 34.4 o 1 1 4 123596.9 123791.6 633.8 o 2 1 4 89.5 83.9 42.7 < 3 1 4 38418.8 35262.9 224.8 o 4 1 4 146.8 4.4 72.2 < 0 2 4 50010.7 47609.5 268.4 o 1 2 4 255.4 277.2 61.7 o 2 2 4 26386.2 25106.0 150.2 o 3 2 4 573.1 224.6 100.7 o 4 2 4 6487.4 6653.6 78.8 o 0 3 4 4.6 1.0 47.6 < 1 3 4 107235.0 111814.6 554.8 o 2 3 4 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0 11 4 25.4 17.2 78.9 < 1 11 4 45337.6 48423.9 251.4 o 2 11 4 139.5 60.9 51.5 < 3 11 4 18821.7 18474.2 129.8 o 4 11 4 81.3 74.9 58.7 < 0 12 4 601.3 546.1 89.6 o 1 12 4 285.8 612.7 58.5 o 2 12 4 245.2 181.7 50.8 o 3 12 4 205.9 641.2 70.3 < 4 12 4 77.5 7.7 55.3 < 0 13 4 99.1 31.3 99.4 < 1 13 4 28242.6 27977.0 165.6 o 2 13 4 71.5 1.3 52.7 < 3 13 4 11192.2 11820.6 97.8 o 4 13 4 27.2 6.6 50.1 < 0 14 4 468.5 386.8 105.2 o 1 14 4 18.9 19.7 53.7 < 2 14 4 546.5 608.6 56.5 o 3 14 4 -6.6 1.8 63.8 < 0 15 4 422.8 125.9 113.4 o 1 15 4 709.5 610.9 59.4 o 2 15 4 159.0 55.5 66.6 < 3 15 4 69.4 7.3 62.9 < 0 16 4 38639.5 32899.4 256.9 o 1 16 4 114.0 135.5 59.7 < 2 16 4 20902.2 21891.2 144.3 o 3 16 4 94.8 139.9 60.8 < 0 17 4 584.7 408.8 110.2 o 1 17 4 1355.9 1033.8 66.7 o 2 17 4 310.3 300.7 82.5 o 3 17 4 578.3 399.4 65.9 o 0 18 4 27691.1 23943.7 192.5 o 1 18 4 42.3 39.0 65.5 < 2 18 4 14225.4 15153.0 139.1 o 3 18 4 146.2 41.9 62.1 < 0 19 4 62.7 0.5 73.9 < 1 19 4 1105.1 981.2 66.5 o 2 19 4 82.6 4.9 117.1 < 3 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