#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/46/2104638.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104638_Fobs loop_ _publ_author_name 'Dittrich, Birger' 'Weber, Manuela' 'Kalinowski, Roman' 'Grabowsky, Simon' 'H\"ubschle, Christian B.' 'Luger, Peter' _publ_section_title ; How to easily replace the independent atom model -- the example of bergenin, a potential anti-HIV agent of traditional Asian medicine ; _journal_coeditor_code SN5088 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 749 _journal_page_last 756 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.4880 _cell_length_b 13.9340 _cell_length_c 14.2750 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.8506 _[local]_cod_data_source_file sn5088Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bergenin aus vietnam 2008' _shelx_refln_list_code 4 _shelx_f_calc_maximum 132.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1365.11 1271.67 5.72 o 4 0 0 25.06 23.13 0.55 o 6 0 0 302.86 288.29 5.22 o 8 0 0 11.93 10.43 0.64 o 1 1 0 324.51 319.08 9.53 o 2 1 0 688.34 656.40 12.28 o 3 1 0 1419.68 1296.04 12.92 o 4 1 0 72.27 78.11 19.16 o 5 1 0 10.42 6.20 0.47 o 6 1 0 986.81 969.06 6.67 o 7 1 0 920.97 912.34 6.97 o 8 1 0 0.17 0.28 1.01 o 0 2 0 712.79 676.94 3.14 o 1 2 0 0.84 5.35 0.84 o 2 2 0 47.09 46.04 0.68 o 3 2 0 360.96 364.33 5.07 o 4 2 0 95.01 103.30 1.51 o 5 2 0 117.70 119.02 1.70 o 6 2 0 285.53 285.33 3.71 o 7 2 0 705.97 705.69 5.94 o 8 2 0 141.54 146.35 2.36 o 1 3 0 21.00 27.94 0.62 o 2 3 0 2881.75 2887.79 55.11 o 3 3 0 1.60 1.65 0.82 o 4 3 0 39.34 39.66 2.02 o 5 3 0 235.92 228.01 3.00 o 6 3 0 187.98 181.96 4.27 o 7 3 0 28.62 29.54 0.55 o 8 3 0 98.03 103.43 1.47 o 0 4 0 759.99 745.64 4.53 o 1 4 0 502.90 482.97 2.67 o 2 4 0 1441.66 1416.46 24.91 o 3 4 0 2221.38 2364.38 61.20 o 4 4 0 44.82 49.71 2.23 o 5 4 0 539.17 537.64 4.66 o 6 4 0 367.70 364.43 8.64 o 7 4 0 0.07 1.17 1.10 o 8 4 0 2.61 3.36 0.33 o 1 5 0 4034.86 3987.07 60.14 o 2 5 0 1456.67 1372.89 18.76 o 3 5 0 1059.75 1169.67 17.42 o 4 5 0 3.58 4.52 1.45 o 5 5 0 2.60 4.72 2.05 o 6 5 0 4.05 5.83 0.97 o 7 5 0 10.63 11.68 0.43 o 8 5 0 3.38 3.37 0.42 o 0 6 0 2374.09 2187.03 9.98 o 1 6 0 4.08 6.42 0.22 o 2 6 0 1930.98 1960.34 35.83 o 3 6 0 219.95 216.20 6.09 o 4 6 0 0.31 1.38 0.46 o 5 6 0 419.15 388.89 6.05 o 6 6 0 0.84 2.22 0.59 o 7 6 0 33.18 35.02 0.71 o 8 6 0 109.67 111.48 1.70 o 1 7 0 260.29 269.49 2.14 o 2 7 0 507.13 518.13 6.92 o 3 7 0 161.44 168.97 4.77 o 4 7 0 691.37 667.35 5.21 o 5 7 0 12.75 13.65 0.43 o 6 7 0 11.65 9.17 0.48 o 7 7 0 0.47 1.31 1.00 o 0 8 0 445.78 537.64 5.60 o 1 8 0 388.27 410.48 4.27 o 2 8 0 1757.90 1823.34 25.32 o 3 8 0 544.26 556.81 4.61 o 4 8 0 589.54 597.15 11.85 o 5 8 0 148.36 151.17 2.16 o 6 8 0 30.74 23.84 0.54 o 7 8 0 17.01 18.06 0.48 o 1 9 0 1952.29 1977.15 7.26 o 2 9 0 63.63 66.13 1.99 o 3 9 0 11.39 9.48 0.39 o 4 9 0 352.17 337.98 9.28 o 5 9 0 64.40 56.00 0.82 o 6 9 0 65.73 52.04 0.75 o 7 9 0 4.10 5.64 1.83 o 0 10 0 846.28 819.97 8.09 o 1 10 0 769.37 783.07 5.92 o 2 10 0 92.92 98.47 4.31 o 3 10 0 0.21 1.35 0.80 o 4 10 0 90.04 82.14 4.08 o 5 10 0 249.63 224.80 2.96 o 6 10 0 420.97 402.70 4.08 o 1 11 0 1152.09 1151.71 5.93 o 2 11 0 15.28 17.22 0.56 o 3 11 0 4.71 1.89 1.42 o 4 11 0 31.42 23.49 0.57 o 5 11 0 474.53 464.81 4.55 o 6 11 0 3.11 3.10 0.31 o 0 12 0 14.86 15.24 0.77 o 1 12 0 1233.00 1179.37 10.32 o 2 12 0 29.48 30.98 0.54 o 3 12 0 60.82 58.61 0.87 o 4 12 0 1.22 2.64 0.57 o 5 12 0 2.20 1.35 1.03 o 1 13 0 636.13 618.57 6.60 o 2 13 0 15.27 14.86 0.37 o 3 13 0 3.13 3.74 0.84 o 4 13 0 6.11 4.86 1.29 o 5 13 0 13.96 13.34 0.33 o 0 14 0 341.53 330.46 5.64 o 1 14 0 23.19 24.99 0.42 o 2 14 0 216.20 234.12 2.55 o 3 14 0 3.92 3.89 0.41 o 4 14 0 8.62 9.06 0.35 o 1 15 0 52.97 57.84 0.80 o 2 15 0 0.95 0.89 0.42 o 3 15 0 6.19 10.65 0.35 o 0 16 0 31.92 39.09 0.72 o 1 16 0 37.65 47.65 0.67 o 1 0 1 813.90 816.63 28.12 o 2 0 1 145.24 140.95 1.37 o 3 0 1 227.02 222.82 2.08 o 4 0 1 14.82 15.18 1.37 o 5 0 1 195.69 199.86 2.74 o 6 0 1 473.38 454.07 4.77 o 7 0 1 0.30 0.67 1.22 o 8 0 1 57.09 58.97 1.40 o -8 1 1 61.79 63.83 0.90 o -7 1 1 821.99 835.26 15.65 o -6 1 1 122.86 128.95 1.86 o -5 1 1 456.65 443.82 4.02 o -4 1 1 1068.03 1102.80 10.42 o -3 1 1 98.70 95.64 3.03 o -2 1 1 833.98 780.37 23.75 o -1 1 1 2534.89 2501.29 135.48 o 0 1 1 55.79 53.17 0.67 o 1 1 1 2532.77 2454.46 37.95 o 2 1 1 829.22 764.56 8.29 o 3 1 1 99.91 94.31 1.25 o 4 1 1 1071.72 1103.47 6.03 o 5 1 1 455.29 449.69 10.40 o 6 1 1 122.51 128.58 1.86 o 7 1 1 825.42 830.05 15.28 o 8 1 1 62.06 64.21 0.90 o -8 2 1 2.80 0.54 1.06 o -7 2 1 215.41 214.92 2.90 o -6 2 1 306.74 307.09 3.80 o -5 2 1 63.94 68.20 1.94 o -4 2 1 328.12 310.44 2.97 o -3 2 1 2050.05 2148.80 65.58 o -2 2 1 7.26 11.96 1.62 o -1 2 1 93.61 92.17 1.82 o 0 2 1 348.36 333.69 1.63 o 1 2 1 96.01 93.50 2.53 o 2 2 1 6.90 12.66 2.14 o 3 2 1 2062.04 2148.28 25.16 o 4 2 1 324.36 303.92 7.47 o 5 2 1 63.23 65.98 1.01 o 6 2 1 301.01 297.42 10.88 o 7 2 1 215.04 214.12 2.90 o 8 2 1 2.76 2.61 1.04 o -8 3 1 12.95 13.33 0.64 o -7 3 1 413.03 410.22 12.46 o -6 3 1 341.72 331.35 4.06 o -5 3 1 350.24 359.94 3.70 o -4 3 1 649.51 698.08 10.82 o -3 3 1 4116.65 4322.82 139.54 o -2 3 1 847.55 849.41 20.77 o -1 3 1 269.92 271.80 4.37 o 0 3 1 2929.92 2833.64 17.11 o 1 3 1 274.75 275.78 2.27 o 2 3 1 843.17 844.95 8.39 o 3 3 1 4103.12 4242.90 100.26 o 4 3 1 655.32 694.22 5.44 o 5 3 1 349.22 350.59 10.14 o 6 3 1 340.48 333.78 4.01 o 7 3 1 416.28 407.21 4.56 o 8 3 1 13.48 13.46 0.43 o -8 4 1 0.97 1.78 0.44 o -7 4 1 143.91 141.85 2.04 o -6 4 1 122.46 127.87 2.91 o -5 4 1 27.25 26.23 0.76 o -4 4 1 54.98 56.17 0.78 o -3 4 1 52.84 56.32 0.78 o -2 4 1 4883.89 5062.25 148.98 o -1 4 1 1323.48 1321.37 6.42 o 0 4 1 2512.76 2424.96 14.11 o 1 4 1 1335.49 1327.98 10.61 o 2 4 1 4872.08 5064.18 48.05 o 3 4 1 52.97 57.31 0.80 o 4 4 1 54.97 54.97 0.75 o 5 4 1 27.46 23.12 0.46 o 6 4 1 122.36 123.76 1.72 o 7 4 1 143.27 143.24 2.45 o 8 4 1 0.85 1.93 0.47 o -8 5 1 33.15 36.32 0.54 o -7 5 1 205.16 203.10 2.76 o -6 5 1 76.22 74.37 1.65 o -5 5 1 403.59 403.57 4.11 o -4 5 1 177.95 167.10 2.15 o -3 5 1 258.72 281.23 8.71 o -2 5 1 626.80 641.74 6.10 o -1 5 1 95.89 85.03 0.94 o 0 5 1 3013.58 3071.23 22.22 o 1 5 1 96.87 89.31 1.39 o 2 5 1 627.51 642.40 7.85 o 3 5 1 256.92 274.72 3.24 o 4 5 1 175.96 167.49 10.40 o 5 5 1 400.66 391.56 4.11 o 6 5 1 74.87 71.06 1.27 o 7 5 1 206.18 202.42 2.76 o 8 5 1 32.94 36.41 1.49 o -8 6 1 100.56 103.78 1.83 o -7 6 1 61.53 66.48 0.94 o -6 6 1 6.88 5.96 0.53 o -5 6 1 42.01 41.30 0.68 o -4 6 1 339.87 347.76 3.78 o -3 6 1 488.81 482.25 9.02 o -2 6 1 90.57 95.12 1.33 o -1 6 1 671.93 701.36 6.92 o 0 6 1 1767.17 1747.42 5.11 o 1 6 1 677.63 707.53 3.90 o 2 6 1 86.16 94.41 9.49 o 3 6 1 489.15 478.08 9.46 o 4 6 1 338.85 335.49 4.78 o 5 6 1 41.93 38.45 0.91 o 6 6 1 6.77 5.57 0.41 o 7 6 1 60.21 62.74 0.90 o 8 6 1 101.13 103.72 1.02 o -7 7 1 205.16 211.27 2.65 o -6 7 1 50.64 43.19 0.63 o -5 7 1 136.30 146.43 2.10 o -4 7 1 169.43 163.68 2.32 o -3 7 1 53.99 56.23 1.59 o -2 7 1 289.46 317.35 4.10 o -1 7 1 1512.81 1574.42 13.03 o 0 7 1 0.93 1.38 0.64 o 1 7 1 1520.32 1596.60 22.83 o 2 7 1 289.33 320.52 7.64 o 3 7 1 52.77 59.26 4.08 o 4 7 1 170.70 164.21 5.24 o 5 7 1 135.48 144.16 3.95 o 6 7 1 50.79 42.09 0.63 o 7 7 1 206.33 209.25 2.69 o -7 8 1 40.09 39.07 0.79 o -6 8 1 26.59 24.44 0.53 o -5 8 1 619.06 596.13 15.12 o -4 8 1 284.09 288.39 3.59 o -3 8 1 34.70 34.88 1.45 o -2 8 1 519.63 547.52 14.59 o -1 8 1 1691.77 1749.91 21.46 o 0 8 1 2.04 1.83 0.73 o 1 8 1 1687.76 1750.58 10.49 o 2 8 1 520.74 554.72 4.33 o 3 8 1 34.75 36.81 0.80 o 4 8 1 287.23 282.67 5.16 o 5 8 1 625.11 592.18 8.09 o 6 8 1 25.84 23.15 0.53 o 7 8 1 40.21 38.00 0.77 o -7 9 1 75.01 85.70 1.67 o -6 9 1 179.69 188.96 2.55 o -5 9 1 830.22 758.08 6.14 o -4 9 1 81.80 76.22 1.10 o -3 9 1 111.58 105.43 1.63 o -2 9 1 1231.77 1226.12 5.67 o -1 9 1 411.05 417.90 3.15 o 0 9 1 153.34 150.47 2.04 o 1 9 1 413.64 420.05 3.86 o 2 9 1 1231.20 1217.75 14.68 o 3 9 1 111.03 108.55 5.84 o 4 9 1 79.91 73.12 1.06 o 5 9 1 831.41 760.31 6.09 o 6 9 1 181.19 185.93 2.59 o 7 9 1 74.62 85.04 1.25 o -6 10 1 30.17 33.23 2.28 o -5 10 1 13.36 15.35 0.58 o -4 10 1 28.95 30.58 1.31 o -3 10 1 15.83 15.77 1.49 o -2 10 1 73.81 73.28 1.75 o -1 10 1 98.64 103.91 2.64 o 0 10 1 184.98 187.32 2.63 o 1 10 1 99.97 97.66 1.40 o 2 10 1 73.19 71.87 3.17 o 3 10 1 15.86 15.75 0.43 o 4 10 1 28.90 28.93 0.55 o 5 10 1 13.12 15.31 0.47 o 6 10 1 30.06 33.35 0.51 o -6 11 1 55.08 58.51 0.80 o -5 11 1 30.89 30.14 0.57 o -4 11 1 12.82 13.32 1.16 o -3 11 1 117.54 108.02 1.52 o -2 11 1 642.32 656.93 6.49 o -1 11 1 1137.07 1131.27 5.91 o 0 11 1 3.15 2.31 0.45 o 1 11 1 1137.60 1120.84 7.16 o 2 11 1 646.61 657.18 11.56 o 3 11 1 117.28 105.61 2.41 o 4 11 1 13.54 13.65 0.77 o 5 11 1 31.59 31.23 0.57 o 6 11 1 55.48 58.74 1.07 o -5 12 1 78.72 79.13 1.87 o -4 12 1 9.60 10.81 0.42 o -3 12 1 40.11 37.00 0.55 o -2 12 1 699.99 680.60 9.62 o -1 12 1 114.13 110.41 1.28 o 0 12 1 43.81 51.89 0.83 o 1 12 1 115.26 111.55 1.54 o 2 12 1 701.30 683.77 5.84 o 3 12 1 40.01 36.94 0.55 o 4 12 1 9.35 10.21 0.42 o 5 12 1 78.56 78.25 1.13 o -5 13 1 34.99 34.59 0.51 o -4 13 1 36.36 35.83 0.52 o -3 13 1 169.86 172.70 2.52 o -2 13 1 31.24 31.78 0.90 o -1 13 1 320.32 328.91 6.70 o 0 13 1 18.57 17.99 1.48 o 1 13 1 315.97 317.30 6.05 o 2 13 1 32.39 32.59 0.44 o 3 13 1 172.35 168.60 2.98 o 4 13 1 35.56 34.74 1.48 o 5 13 1 36.43 36.22 0.65 o -4 14 1 8.79 10.18 0.35 o -3 14 1 32.42 36.02 0.85 o -2 14 1 11.12 9.80 0.34 o -1 14 1 87.75 85.17 0.99 o 0 14 1 36.17 39.59 0.61 o 1 14 1 86.93 84.53 1.19 o 2 14 1 11.24 10.02 0.36 o 3 14 1 32.64 35.32 1.00 o 4 14 1 8.79 10.08 0.86 o -3 15 1 63.06 57.92 0.53 o -2 15 1 9.32 10.71 0.51 o -1 15 1 72.91 73.01 1.74 o 0 15 1 25.44 24.81 0.51 o 1 15 1 72.67 72.80 1.41 o 2 15 1 9.38 12.28 0.52 o 3 15 1 61.41 55.92 0.56 o -1 16 1 1.24 2.10 0.27 o 0 16 1 0.01 1.16 0.54 o 1 16 1 1.21 1.98 0.88 o 0 0 2 8628.05 8169.78 76.55 o 1 0 2 1543.35 1421.89 61.14 o 2 0 2 2054.15 2014.83 75.22 o 3 0 2 116.14 103.72 2.22 o 4 0 2 421.71 433.03 3.43 o 5 0 2 588.80 565.95 6.69 o 6 0 2 233.63 246.58 3.39 o 7 0 2 210.43 215.33 5.80 o 8 0 2 98.56 96.92 2.76 o -8 1 2 81.36 83.12 1.17 o -7 1 2 33.01 37.85 1.98 o -6 1 2 424.95 421.88 4.45 o -5 1 2 19.32 20.57 0.41 o -4 1 2 810.58 844.47 8.20 o -3 1 2 84.95 88.15 1.24 o -2 1 2 1161.49 1141.04 44.73 o -1 1 2 9264.96 9490.18 410.16 o 0 1 2 28.99 35.59 1.73 o 1 1 2 9271.59 9725.06 571.83 o 2 1 2 1148.58 1095.52 10.93 o 3 1 2 85.51 87.20 1.23 o 4 1 2 810.87 843.74 11.83 o 5 1 2 20.41 22.13 1.60 o 6 1 2 426.59 432.00 4.49 o 7 1 2 33.65 37.69 0.63 o 8 1 2 80.54 82.90 1.80 o -8 2 2 10.37 11.97 0.62 o -7 2 2 350.20 365.40 4.26 o -6 2 2 273.28 270.18 5.01 o -5 2 2 227.85 215.65 2.90 o -4 2 2 530.15 593.63 8.70 o -3 2 2 3050.18 3128.14 82.91 o -2 2 2 1114.69 1066.95 38.11 o -1 2 2 7311.40 7424.67 157.42 o 0 2 2 574.00 564.29 4.19 o 1 2 2 7286.31 7446.52 149.20 o 2 2 2 1114.03 1047.74 4.09 o 3 2 2 3041.68 3036.36 8.80 o 4 2 2 531.92 578.76 6.96 o 5 2 2 224.62 201.80 4.05 o 6 2 2 270.32 262.31 3.58 o 7 2 2 348.28 349.83 4.16 o 8 2 2 9.90 11.62 0.43 o -8 3 2 11.05 14.44 0.41 o -7 3 2 142.21 143.73 2.91 o -6 3 2 674.95 684.51 5.69 o -5 3 2 97.48 97.18 1.37 o -4 3 2 821.68 872.96 14.39 o -3 3 2 1700.18 1690.02 45.47 o -2 3 2 504.20 492.79 4.04 o -1 3 2 1721.00 1706.89 24.27 o 0 3 2 4921.66 4874.10 54.45 o 1 3 2 1711.28 1702.22 6.52 o 2 3 2 508.99 494.12 2.90 o 3 3 2 1715.48 1681.30 25.95 o 4 3 2 821.62 861.64 5.12 o 5 3 2 96.17 98.05 2.77 o 6 3 2 681.51 670.47 11.31 o 7 3 2 142.12 141.14 4.02 o 8 3 2 10.80 12.77 0.62 o -8 4 2 51.30 51.64 0.72 o -7 4 2 18.40 16.61 0.71 o -6 4 2 11.44 12.47 1.55 o -5 4 2 63.17 68.90 1.77 o -4 4 2 616.84 639.57 10.54 o -3 4 2 130.74 149.00 2.92 o -2 4 2 297.02 275.57 8.95 o -1 4 2 2440.78 2414.86 22.76 o 0 4 2 344.56 353.38 2.31 o 1 4 2 2440.29 2407.55 9.51 o 2 4 2 299.75 277.09 2.34 o 3 4 2 130.11 155.55 12.49 o 4 4 2 615.00 611.93 7.51 o 5 4 2 63.51 69.67 0.98 o 6 4 2 10.88 12.53 0.45 o 7 4 2 18.09 17.44 1.01 o 8 4 2 51.75 51.17 0.72 o -8 5 2 103.24 110.59 1.58 o -7 5 2 133.34 135.11 1.92 o -6 5 2 96.81 98.03 1.45 o -5 5 2 448.89 455.32 5.38 o -4 5 2 492.44 467.41 7.38 o -3 5 2 623.91 635.46 15.17 o -2 5 2 803.44 792.24 25.98 o -1 5 2 1144.72 1144.72 5.42 o 0 5 2 363.45 395.81 3.88 o 1 5 2 1143.69 1148.15 6.69 o 2 5 2 797.66 784.47 5.25 o 3 5 2 624.80 629.39 6.78 o 4 5 2 492.80 466.88 11.44 o 5 5 2 452.50 452.19 9.98 o 6 5 2 95.01 94.63 1.35 o 7 5 2 133.34 134.03 1.88 o 8 5 2 103.64 111.23 1.58 o -8 6 2 33.87 35.00 0.76 o -7 6 2 72.71 77.41 1.09 o -6 6 2 47.34 40.06 0.64 o -5 6 2 133.09 126.48 1.76 o -4 6 2 6.01 6.83 0.41 o -3 6 2 261.05 280.66 2.98 o -2 6 2 571.58 548.81 6.05 o -1 6 2 2683.72 2721.37 9.57 o 0 6 2 4878.24 5171.98 20.26 o 1 6 2 2686.63 2738.63 11.86 o 2 6 2 574.28 554.37 3.77 o 3 6 2 261.64 275.51 3.72 o 4 6 2 5.99 5.30 0.35 o 5 6 2 132.64 126.83 1.76 o 6 6 2 47.64 40.76 0.64 o 7 6 2 73.15 77.07 1.09 o 8 6 2 33.42 33.63 0.49 o -7 7 2 45.13 48.04 0.68 o -6 7 2 183.38 172.73 3.06 o -5 7 2 0.39 2.05 0.93 o -4 7 2 47.44 47.41 4.52 o -3 7 2 32.71 36.72 0.66 o -2 7 2 137.34 138.92 3.09 o -1 7 2 4336.10 4737.28 48.63 o 0 7 2 97.38 94.56 1.49 o 1 7 2 4325.55 4680.40 17.78 o 2 7 2 140.68 137.46 1.82 o 3 7 2 32.32 37.51 2.09 o 4 7 2 46.58 43.95 2.77 o 5 7 2 0.23 7.16 2.97 o 6 7 2 181.12 163.06 2.30 o 7 7 2 45.53 48.67 0.76 o -7 8 2 24.34 28.16 0.47 o -6 8 2 250.14 241.43 3.21 o -5 8 2 4.77 7.00 0.45 o -4 8 2 51.28 52.87 0.75 o -3 8 2 204.34 216.87 2.98 o -2 8 2 234.78 239.01 5.09 o -1 8 2 28.31 29.86 0.42 o 0 8 2 15.63 15.73 0.27 o 1 8 2 26.82 27.72 0.58 o 2 8 2 230.09 230.85 2.84 o 3 8 2 203.85 209.05 3.90 o 4 8 2 49.77 49.50 0.94 o 5 8 2 4.23 5.02 2.31 o 6 8 2 250.62 240.24 3.00 o 7 8 2 24.49 28.92 0.47 o -7 9 2 103.07 96.70 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