#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:05 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180907 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104880.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104880_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9594 _cell_length_b 8.9594 _cell_length_c 9.5583 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7004 _cod_data_source_file bk51011asup2.hkl _cod_data_source_block 1a #BEGIN Tags that were not found in dictionaries: _shelx_title ' m104n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3751.53 3835.09 16.05 o -1 2 0 5588.28 5938.03 25.50 o 0 2 0 5715.02 5812.90 26.21 o -1 3 0 439.13 435.69 2.26 o 0 3 0 1135.01 1075.10 6.31 o -2 4 0 3635.03 3648.08 22.14 o -1 4 0 687.05 663.43 3.43 o 0 4 0 1437.26 1469.18 8.93 o -2 5 0 15.77 9.23 0.43 o -1 5 0 3847.88 3683.05 15.67 o 0 5 0 1999.52 2007.01 13.15 o -3 6 0 1392.16 1356.10 10.50 o -2 6 0 590.99 565.85 3.43 o -1 6 0 1467.34 1508.92 7.23 o 0 6 0 4237.59 4311.50 26.69 o -3 7 0 1027.30 1029.50 6.19 o -2 7 0 1336.51 1373.80 7.17 o -1 7 0 180.13 178.39 1.87 o 0 7 0 19.87 16.63 1.26 o -4 8 0 2237.46 2267.63 17.04 o -3 8 0 161.68 152.35 2.09 o -2 8 0 666.13 685.32 4.64 o -1 8 0 1201.14 1237.80 7.43 o 0 8 0 536.83 542.96 6.00 o -4 9 0 204.37 191.81 2.60 o -3 9 0 1263.44 1280.74 8.49 o -2 9 0 450.96 451.75 4.38 o -1 9 0 338.43 332.74 3.65 o 0 9 0 732.47 737.06 8.76 o -5 10 0 1965.11 1989.21 16.76 o -4 10 0 312.50 309.21 3.79 o -3 10 0 399.90 375.48 4.45 o -2 10 0 870.39 867.04 8.02 o -1 10 0 200.02 189.81 4.64 o 0 10 0 268.43 274.21 9.05 o -5 11 0 238.32 233.46 3.43 o -4 11 0 431.89 405.85 5.35 o -3 11 0 67.77 64.74 2.63 o -2 11 0 36.05 31.75 2.76 o -1 11 0 658.25 667.09 9.19 o 0 11 0 220.43 203.21 7.65 o -6 12 0 278.47 280.43 8.00 o -5 12 0 272.38 279.98 4.92 o -4 12 0 29.50 27.52 2.67 o -3 12 0 562.97 580.06 8.01 o 0 1 1 1011.23 913.83 3.30 o 0 2 1 1586.39 1678.40 6.74 o 1 2 1 6.73 7.65 0.30 o -1 3 1 3382.09 3468.98 14.07 o 0 3 1 181.26 186.23 1.13 o 1 3 1 539.33 531.16 2.89 o 2 3 1 522.18 536.62 3.19 o -1 4 1 1665.93 1694.37 7.53 o 0 4 1 765.23 767.82 3.89 o 1 4 1 0.25 0.34 0.35 o 2 4 1 685.38 681.95 3.95 o 3 4 1 478.00 479.90 3.21 o -2 5 1 547.21 566.31 3.72 o -1 5 1 221.46 253.40 1.87 o 0 5 1 2607.40 2674.98 12.00 o 1 5 1 558.75 579.08 3.62 o 2 5 1 331.27 344.39 2.69 o 3 5 1 55.71 56.44 1.28 o 4 5 1 99.90 101.45 2.01 o -2 6 1 21.75 29.59 0.77 o -1 6 1 668.71 695.67 4.08 o 0 6 1 13.02 16.31 0.60 o 1 6 1 6.96 5.88 0.67 o 2 6 1 8.03 7.10 0.79 o 3 6 1 93.11 86.78 1.83 o 4 6 1 70.53 79.74 2.23 o 5 6 1 246.32 255.03 4.00 o -3 7 1 56.90 59.61 1.19 o -2 7 1 141.92 139.39 1.58 o -1 7 1 59.99 56.20 1.16 o 0 7 1 107.75 94.93 1.58 o 1 7 1 59.92 60.57 1.44 o 2 7 1 145.04 144.45 2.52 o 3 7 1 41.88 45.34 1.89 o 4 7 1 5.70 5.50 1.55 o 5 7 1 3.87 4.37 1.93 o -3 8 1 69.72 63.05 1.45 o -2 8 1 46.45 45.90 1.35 o -1 8 1 124.46 113.45 2.52 o 0 8 1 3.17 3.14 0.95 o 1 8 1 70.57 71.14 1.81 o 2 8 1 16.30 14.19 1.63 o 3 8 1 69.15 71.89 2.66 o 4 8 1 94.60 95.91 4.82 o -4 9 1 142.01 136.13 2.23 o -3 9 1 4.44 4.13 1.09 o -2 9 1 465.06 493.04 4.99 o -1 9 1 195.40 195.92 3.16 o 0 9 1 66.55 63.16 2.32 o 1 9 1 157.28 161.53 3.65 o 2 9 1 39.00 42.42 2.92 o 3 9 1 10.56 8.44 2.74 o -4 10 1 192.08 204.20 3.01 o -3 10 1 22.16 26.25 1.80 o -2 10 1 6.91 5.74 1.50 o -1 10 1 17.96 26.00 2.02 o 0 10 1 132.67 131.60 4.12 o 1 10 1 8.36 5.45 2.69 o -5 11 1 164.96 167.41 3.03 o -4 11 1 34.51 43.42 2.24 o -3 11 1 13.92 17.16 2.00 o -2 11 1 48.90 51.04 2.74 o -1 11 1 4.13 3.82 2.46 o 0 11 1 133.45 120.35 4.57 o -5 12 1 3.23 -1.59 1.99 o -4 12 1 47.08 50.93 2.66 o -3 12 1 0.70 1.73 2.59 o 0 0 2 18566.78 16849.33 128.86 o 0 1 2 1363.93 1388.39 5.05 o 1 1 2 1861.42 1893.47 11.10 o -1 2 2 11406.97 11007.91 98.99 o 0 2 2 2555.81 2602.13 11.71 o 1 2 2 383.33 364.19 2.07 o 2 2 2 1451.18 1363.19 8.78 o -1 3 2 3022.83 3079.77 14.49 o 0 3 2 3144.19 3042.37 14.12 o 1 3 2 231.77 204.27 1.48 o 2 3 2 597.96 538.94 3.12 o 3 3 2 3918.11 3773.55 22.67 o -2 4 2 11459.87 11848.95 75.86 o -1 4 2 1322.46 1292.45 6.59 o 0 4 2 1011.85 1018.14 5.51 o 1 4 2 2507.96 2438.64 10.99 o 2 4 2 502.51 488.42 3.01 o 3 4 2 1126.07 1105.52 5.58 o 4 4 2 1902.44 1889.99 14.76 o -2 5 2 60.89 52.15 0.90 o -1 5 2 2139.69 2092.72 11.65 o 0 5 2 889.10 875.90 5.30 o 1 5 2 933.14 957.48 5.82 o 2 5 2 1640.34 1626.43 8.32 o 3 5 2 444.03 434.02 3.37 o 4 5 2 38.97 38.85 1.43 o 5 5 2 1089.10 1084.60 12.47 o -3 6 2 1282.79 1325.16 11.00 o -2 6 2 1136.47 1155.05 6.83 o -1 6 2 400.68 405.64 3.45 o 0 6 2 2483.43 2567.10 14.29 o 1 6 2 103.58 107.69 1.55 o 2 6 2 190.63 194.67 2.20 o 3 6 2 789.50 805.11 6.08 o 4 6 2 444.69 420.69 4.92 o 5 6 2 240.23 236.22 3.86 o 6 6 2 429.72 411.51 7.56 o -3 7 2 385.52 408.62 3.33 o -2 7 2 1675.75 1708.34 10.37 o -1 7 2 536.29 515.06 4.25 o 0 7 2 179.22 173.89 2.29 o 1 7 2 856.64 897.81 6.68 o 2 7 2 368.61 345.37 3.90 o 3 7 2 126.18 130.30 2.78 o 4 7 2 808.21 820.03 8.43 o 5 7 2 220.75 220.55 4.50 o -4 8 2 1950.47 2017.33 17.59 o -3 8 2 400.98 401.08 4.06 o -2 8 2 851.58 850.69 6.64 o -1 8 2 2181.10 2207.66 13.66 o 0 8 2 246.85 244.14 3.18 o 1 8 2 487.69 495.16 5.02 o 2 8 2 862.55 872.55 7.48 o 3 8 2 150.43 135.28 3.57 o 4 8 2 122.27 127.22 3.70 o -4 9 2 306.27 272.73 3.19 o -3 9 2 1453.58 1456.97 10.38 o -2 9 2 372.25 386.47 4.48 o -1 9 2 214.22 206.58 3.30 o 0 9 2 643.52 638.32 6.41 o 1 9 2 121.17 112.19 3.76 o 2 9 2 181.33 182.30 6.03 o 3 9 2 660.33 684.60 9.61 o -5 10 2 1048.60 1063.21 11.13 o -4 10 2 69.60 73.10 2.27 o -3 10 2 416.25 377.05 4.59 o -2 10 2 591.03 555.82 5.76 o -1 10 2 228.12 232.28 4.69 o 0 10 2 145.94 139.78 4.03 o 1 10 2 639.73 665.77 9.17 o -5 11 2 192.33 188.42 3.61 o -4 11 2 279.83 272.38 4.40 o -3 11 2 69.07 64.91 2.68 o -2 11 2 1.24 -1.39 1.89 o -1 11 2 401.50 394.37 7.72 o -6 12 2 441.69 476.28 9.75 o -5 12 2 96.80 96.00 3.82 o -4 12 2 103.39 97.12 3.69 o -3 12 2 423.92 426.71 6.54 o 0 1 3 13.01 20.36 0.40 o 0 2 3 1312.75 1359.38 6.67 o 1 2 3 207.19 204.44 1.54 o -1 3 3 2816.57 2959.87 13.69 o 0 3 3 98.15 108.14 1.43 o 1 3 3 353.78 364.00 2.38 o 2 3 3 443.95 432.98 2.65 o -1 4 3 764.19 811.24 4.73 o 0 4 3 11.08 6.61 0.58 o 1 4 3 10.38 12.91 0.69 o 2 4 3 594.65 618.26 3.79 o 3 4 3 744.39 750.08 4.47 o -2 5 3 340.07 364.80 2.93 o -1 5 3 11.61 19.06 0.65 o 0 5 3 13.59 16.89 0.82 o 1 5 3 71.29 68.75 1.40 o 2 5 3 1.80 2.48 0.55 o 3 5 3 124.36 117.83 2.37 o 4 5 3 52.40 53.14 1.74 o -2 6 3 5.31 6.56 0.72 o -1 6 3 77.00 75.82 1.67 o 0 6 3 2.81 3.77 0.72 o 1 6 3 114.55 103.37 1.79 o 2 6 3 158.55 155.90 2.32 o 3 6 3 94.56 104.36 2.05 o 4 6 3 20.68 18.94 1.54 o 5 6 3 42.80 49.10 2.43 o -3 7 3 214.57 221.27 2.91 o -2 7 3 29.10 22.60 1.19 o -1 7 3 362.53 345.91 3.61 o 0 7 3 146.60 143.69 2.38 o 1 7 3 44.93 37.06 1.53 o 2 7 3 55.68 47.89 1.84 o 3 7 3 74.20 77.24 2.53 o 4 7 3 5.15 -1.84 1.84 o 5 7 3 77.62 80.08 3.44 o -3 8 3 101.62 95.02 2.15 o -2 8 3 398.07 378.45 4.14 o -1 8 3 2.61 4.97 1.22 o 0 8 3 261.27 254.03 3.52 o 1 8 3 34.32 32.80 1.81 o 2 8 3 3.11 2.53 1.59 o 3 8 3 70.37 65.18 2.74 o 4 8 3 68.75 67.41 3.11 o -4 9 3 97.62 82.71 2.17 o -3 9 3 1.85 0.26 1.20 o -2 9 3 235.10 273.84 3.86 o -1 9 3 128.49 123.49 2.73 o 0 9 3 1.69 -0.34 1.54 o 1 9 3 73.92 64.46 2.52 o 2 9 3 39.66 40.88 2.63 o -4 10 3 55.02 51.12 2.07 o -3 10 3 55.80 54.24 2.16 o -2 10 3 33.50 20.00 1.86 o -1 10 3 3.16 0.65 1.57 o 0 10 3 28.27 32.16 2.39 o 1 10 3 0.15 0.22 2.18 o -5 11 3 32.20 32.06 2.45 o -4 11 3 10.54 17.14 2.12 o -3 11 3 28.70 42.70 2.37 o -2 11 3 66.83 67.79 2.73 o -1 11 3 9.58 7.36 2.12 o -5 12 3 97.57 94.62 3.60 o -4 12 3 26.74 31.74 2.71 o 0 0 4 1203.18 1368.68 17.96 o 0 1 4 501.90 475.74 2.67 o 1 1 4 4336.31 4245.38 23.52 o -1 2 4 4493.05 4406.35 26.41 o 0 2 4 450.75 435.57 2.57 o 1 2 4 1688.71 1684.37 8.14 o 2 2 4 4475.32 4398.01 26.75 o -1 3 4 1305.28 1313.53 6.88 o 0 3 4 5000.39 5001.90 23.41 o 1 3 4 954.74 968.32 5.45 o 2 3 4 1146.29 1119.82 5.83 o 3 3 4 2951.16 2935.11 17.59 o -2 4 4 3777.60 3894.65 27.67 o -1 4 4 705.02 689.03 4.66 o 0 4 4 434.79 407.49 3.46 o 1 4 4 1880.46 1944.57 10.36 o 2 4 4 694.41 712.74 4.30 o 3 4 4 292.29 292.45 2.74 o 4 4 4 932.74 940.71 8.62 o -2 5 4 1064.99 1033.09 6.61 o -1 5 4 1564.38 1581.05 9.14 o 0 5 4 225.73 229.03 2.52 o 1 5 4 114.81 109.45 1.78 o 2 5 4 1856.02 1888.94 10.29 o 3 5 4 545.00 539.37 4.41 o 4 5 4 165.72 163.81 2.56 o 5 5 4 332.92 325.44 5.84 o -3 6 4 3385.60 3535.54 23.22 o -2 6 4 706.05 737.52 5.11 o -1 6 4 271.69 279.61 2.92 o 0 6 4 1024.54 1053.18 6.85 o 1 6 4 453.79 436.32 3.95 o 2 6 4 166.92 176.43 2.59 o 3 6 4 900.30 904.15 7.39 o 4 6 4 119.21 103.04 2.67 o 5 6 4 186.15 186.78 4.52 o 6 6 4 576.01 570.66 11.71 o -3 7 4 285.99 305.34 3.71 o -2 7 4 2099.58 2087.62 12.95 o -1 7 4 528.61 497.70 4.63 o 0 7 4 1039.56 1012.13 7.19 o 1 7 4 1215.62 1251.05 8.50 o 2 7 4 218.56 204.62 3.65 o 3 7 4 94.21 111.99 3.03 o 4 7 4 776.80 806.87 9.96 o 5 7 4 59.67 49.55 3.19 o -4 8 4 1255.70 1310.15 14.18 o -3 8 4 599.05 621.34 5.95 o -2 8 4 262.06 239.67 3.36 o -1 8 4 1437.36 1430.82 9.67 o 0 8 4 84.81 79.72 2.27 o 1 8 4 241.14 252.45 3.83 o 2 8 4 570.28 586.36 7.03 o 3 8 4 196.25 181.88 4.77 o 4 8 4 220.49 231.13 7.34 o -4 9 4 201.84 177.67 3.43 o -3 9 4 789.19 785.16 7.21 o -2 9 4 146.74 170.71 3.10 o -1 9 4 151.18 128.26 2.90 o 0 9 4 586.13 569.43 6.04 o 1 9 4 167.37 163.40 3.85 o 2 9 4 123.63 123.88 3.75 o -5 10 4 324.30 350.91 6.98 o -4 10 4 115.78 134.52 3.77 o -3 10 4 128.45 106.07 2.76 o -2 10 4 542.12 537.91 5.73 o -1 10 4 96.72 98.87 2.79 o 0 10 4 58.09 52.81 2.74 o 1 10 4 356.72 367.42 6.31 o -5 11 4 106.12 97.49 4.10 o -4 11 4 585.48 605.75 6.86 o -3 11 4 177.21 185.03 5.51 o -2 11 4 140.40 127.67 3.20 o -1 11 4 332.23 339.54 5.80 o -6 12 4 717.48 767.02 12.55 o -5 12 4 46.83 27.96 6.30 o -4 12 4 246.99 236.58 5.10 o 0 1 5 467.88 441.66 2.73 o 0 2 5 2599.25 2718.99 12.01 o 1 2 5 709.85 711.80 4.15 o -1 3 5 21.53 25.04 0.66 o 0 3 5 50.76 38.10 0.85 o 1 3 5 197.37 198.70 2.12 o 2 3 5 105.63 94.96 1.25 o -1 4 5 30.87 36.59 0.83 o 0 4 5 112.38 108.74 1.84 o 1 4 5 0.52 0.69 0.72 o 2 4 5 78.51 77.53 1.44 o 3 4 5 53.25 54.44 1.50 o -2 5 5 214.42 224.25 2.34 o -1 5 5 136.70 128.07 2.05 o 0 5 5 76.26 63.84 1.55 o 1 5 5 59.61 55.56 1.45 o 2 5 5 144.35 138.96 2.15 o 3 5 5 289.72 296.93 3.55 o 4 5 5 74.58 79.41 2.04 o -2 6 5 740.36 730.71 5.66 o -1 6 5 25.64 23.68 1.16 o 0 6 5 10.55 13.49 1.09 o 1 6 5 349.87 335.51 3.51 o 2 6 5 492.87 501.46 4.94 o 3 6 5 53.97 38.06 2.00 o 4 6 5 98.85 89.07 2.64 o 5 6 5 4.23 -1.39 2.30 o -3 7 5 274.13 274.25 3.11 o -2 7 5 82.07 71.23 2.00 o -1 7 5 292.46 282.34 3.71 o 0 7 5 152.55 156.36 2.76 o 1 7 5 57.00 48.88 2.06 o 2 7 5 59.98 54.70 2.64 o 3 7 5 74.02 74.03 2.93 o 4 7 5 0.01 -1.87 1.87 o -3 8 5 107.40 104.72 2.35 o -2 8 5 191.10 172.12 3.10 o -1 8 5 39.91 41.19 1.84 o 0 8 5 275.83 270.22 3.79 o 1 8 5 72.87 68.13 3.25 o 2 8 5 9.39 12.69 3.06 o 3 8 5 16.75 10.31 2.33 o -4 9 5 71.32 63.72 2.53 o -3 9 5 1.35 -1.27 1.27 o -2 9 5 3.63 2.70 1.48 o -1 9 5 22.38 23.47 1.91 o 0 9 5 48.83 39.89 2.38 o 1 9 5 10.52 6.22 2.13 o 2 9 5 32.33 26.31 2.75 o -4 10 5 9.85 5.22 1.89 o -3 10 5 137.72 137.60 3.56 o -2 10 5 0.75 2.96 1.77 o -1 10 5 66.15 74.54 2.98 o 0 10 5 7.70 6.66 2.34 o -5 11 5 15.88 13.18 2.43 o -4 11 5 35.68 40.45 2.64 o -3 11 5 133.29 137.29 5.67 o -2 11 5 54.26 56.08 3.05 o 0 0 6 25.37 15.83 1.56 o 0 1 6 710.87 689.34 3.95 o 1 1 6 4278.47 4324.46 27.65 o -1 2 6 1472.97 1474.40 10.22 o 0 2 6 174.66 168.65 1.68 o 1 2 6 1107.31 1123.42 5.96 o 2 2 6 3255.11 3291.47 23.13 o -1 3 6 188.04 188.39 2.05 o 0 3 6 3549.01 3615.66 17.18 o 1 3 6 1284.08 1328.69 7.61 o 2 3 6 1017.15 1018.87 6.25 o 3 3 6 1049.97 1083.98 10.41 o -2 4 6 326.04 335.47 3.70 o -1 4 6 471.22 459.01 3.55 o 0 4 6 346.97 349.72 3.08 o 1 4 6 2461.64 2542.37 13.71 o 2 4 6 350.35 343.56 3.38 o 3 4 6 57.87 56.93 1.60 o 4 4 6 502.03 490.62 6.56 o -2 5 6 1539.54 1518.21 8.77 o -1 5 6 2324.66 2405.55 13.96 o 0 5 6 223.98 225.48 2.91 o 1 5 6 133.03 124.39 2.16 o 2 5 6 1496.82 1519.62 10.43 o 3 5 6 180.18 163.02 2.93 o 4 5 6 610.88 625.80 6.11 o 5 5 6 373.45 374.55 9.05 o -3 6 6 2594.42 2607.64 20.34 o -2 6 6 162.01 154.78 2.61 o -1 6 6 428.94 430.97 4.35 o 0 6 6 786.24 783.09 6.42 o 1 6 6 698.61 677.19 5.85 o 2 6 6 249.17 259.73 3.85 o 3 6 6 1015.34 1020.77 8.09 o 4 6 6 45.45 43.68 2.40 o 5 6 6 77.58 76.82 3.73 o -3 7 6 238.91 230.70 3.12 o -2 7 6 1444.23 1412.15 10.19 o -1 7 6 336.20 338.87 4.27 o 0 7 6 608.64 587.76 5.65 o 1 7 6 978.43 976.92 8.57 o 2 7 6 94.77 85.04 2.93 o 3 7 6 143.58 146.53 4.17 o 4 7 6 495.83 516.11 7.89 o -4 8 6 667.65 690.67 9.84 o -3 8 6 229.20 224.73 3.48 o -2 8 6 41.54 37.64 1.91 o -1 8 6 400.24 383.20 4.60 o 0 8 6 192.09 193.75 4.69 o 1 8 6 37.57 40.82 2.47 o 2 8 6 447.86 475.00 6.61 o 3 8 6 145.12 147.53 4.19 o -4 9 6 315.41 306.04 4.72 o -3 9 6 546.99 571.81 6.51 o -2 9 6 47.46 48.13 2.15 o -1 9 6 93.77 87.23 3.08 o 0 9 6 742.43 756.62 8.05 o 1 9 6 185.82 184.33 4.43 o -5 10 6 438.92 469.34 8.65 o -4 10 6 293.64 298.56 4.91 o -3 10 6 60.88 58.17 3.06 o -2 10 6 677.64 714.43 7.99 o -1 10 6 57.52 57.93 3.03 o -5 11 6 56.17 56.70 3.23 o -4 11 6 874.80 932.42 9.26 o -3 11 6 239.79 235.13 4.98 o 0 1 7 790.49 747.12 4.39 o 0 2 7 647.57 642.20 3.97 o 1 2 7 107.28 114.04 1.64 o -1 3 7 53.02 43.68 1.03 o 0 3 7 181.58 164.68 2.24 o 1 3 7 63.14 62.94 1.39 o 2 3 7 34.83 33.33 1.39 o -1 4 7 28.52 29.70 1.07 o 0 4 7 720.97 721.30 5.44 o 1 4 7 4.29 3.69 0.85 o 2 4 7 107.17 101.08 2.01 o 3 4 7 26.73 22.06 1.35 o -2 5 7 144.30 139.09 2.04 o -1 5 7 62.45 63.29 1.88 o 0 5 7 79.93 79.48 2.07 o 1 5 7 163.75 154.85 2.94 o 2 5 7 34.60 30.05 1.63 o 3 5 7 206.30 210.33 3.43 o 4 5 7 123.44 125.00 3.01 o -2 6 7 785.27 785.99 6.52 o -1 6 7 158.59 156.52 2.89 o 0 6 7 0.09 0.40 1.20 o 1 6 7 189.31 191.14 3.26 o 2 6 7 137.89 137.80 3.54 o 3 6 7 156.90 147.70 3.37 o 4 6 7 127.16 115.11 4.01 o -3 7 7 29.56 31.73 1.67 o -2 7 7 16.51 13.03 1.50 o -1 7 7 63.49 64.93 2.27 o 0 7 7 85.15 86.33 2.73 o 1 7 7 0.65 3.14 1.75 o 2 7 7 12.40 7.73 1.90 o 3 7 7 63.76 53.71 2.93 o -3 8 7 133.07 132.96 3.75 o -2 8 7 19.48 22.45 1.90 o -1 8 7 1.03 -0.44 1.53 o 0 8 7 27.80 25.38 2.22 o 1 8 7 68.05 66.42 3.61 o 2 8 7 0.17 1.25 2.23 o -4 9 7 86.23 80.86 2.97 o -3 9 7 18.20 18.77 2.26 o -2 9 7 17.65 10.26 2.16 o -1 9 7 15.05 16.14 2.49 o 0 9 7 57.01 58.31 2.92 o -4 10 7 55.96 55.85 2.99 o -3 10 7 97.26 97.14 3.51 o -2 10 7 26.64 13.95 2.91 o 0 0 8 2867.94 2959.05 33.38 o 0 1 8 795.92 794.80 4.78 o 1 1 8 2006.68 2015.37 13.89 o -1 2 8 1632.03 1648.53 11.79 o 0 2 8 260.18 262.59 2.41 o 1 2 8 225.67 221.57 2.36 o 2 2 8 778.48 812.19 8.28 o -1 3 8 202.36 190.93 2.00 o 0 3 8 1713.35 1726.62 9.73 o 1 3 8 495.46 497.56 4.41 o 2 3 8 634.54 632.17 5.30 o 3 3 8 819.61 863.23 9.39 o -2 4 8 506.45 519.51 5.75 o -1 4 8 463.93 458.30 3.98 o 0 4 8 375.39 381.90 3.84 o 1 4 8 1997.95 2021.78 12.15 o 2 4 8 109.30 108.42 2.25 o 3 4 8 127.06 118.72 2.43 o 4 4 8 596.33 604.53 8.93 o -2 5 8 565.93 564.30 5.00 o -1 5 8 1962.94 1995.71 12.33 o 0 5 8 285.35 290.99 3.97 o 1 5 8 415.06 405.92 4.69 o 2 5 8 895.42 901.59 8.15 o 3 5 8 73.14 70.57 2.47 o 4 5 8 433.53 426.32 5.49 o 5 5 8 611.97 620.68 10.39 o -3 6 8 605.05 602.42 7.88 o -2 6 8 82.40 80.06 3.02 o -1 6 8 275.81 258.03 3.74 o 0 6 8 856.37 854.45 7.30 o 1 6 8 314.93 311.49 4.29 o 2 6 8 146.80 139.10 3.19 o 3 6 8 610.18 609.68 8.35 o 4 6 8 169.43 180.13 4.68 o -3 7 8 137.72 131.63 3.23 o -2 7 8 761.02 754.89 7.14 o -1 7 8 250.32 239.70 3.91 o 0 7 8 133.05 121.01 3.37 o 1 7 8 431.06 436.53 5.77 o 2 7 8 56.77 56.65 2.62 o 3 7 8 107.33 94.95 4.54 o -4 8 8 520.81 516.50 8.92 o -3 8 8 60.17 54.36 2.68 o -2 8 8 110.67 113.54 3.01 o -1 8 8 331.67 339.20 5.49 o 0 8 8 289.47 286.54 4.86 o 1 8 8 36.69 31.47 2.74 o -4 9 8 437.73 445.16 6.09 o -3 9 8 738.79 776.24 8.28 o -2 9 8 80.89 73.83 3.36 o -1 9 8 76.89 83.34 3.48 o -5 10 8 675.57 699.59 11.44 o -4 10 8 187.73 173.12 4.45 o -3 10 8 102.92 110.93 3.96 o 0 1 9 223.73 234.50 2.41 o 0 2 9 55.82 49.21 1.26 o 1 2 9 5.89 3.14 0.88 o -1 3 9 131.69 129.60 1.93 o 0 3 9 27.16 24.07 1.17 o 1 3 9 29.87 29.17 1.46 o 2 3 9 80.55 79.01 2.12 o -1 4 9 167.95 167.19 2.47 o 0 4 9 369.51 359.90 3.94 o 1 4 9 21.08 23.30 1.53 o 2 4 9 246.48 243.88 3.47 o 3 4 9 39.75 37.93 2.03 o -2 5 9 97.70 89.79 2.21 o -1 5 9 18.08 15.55 1.35 o 0 5 9 210.32 208.58 3.60 o 1 5 9 121.64 111.63 2.88 o 2 5 9 1.69 3.03 1.66 o 3 5 9 29.50 37.07 2.32 o 4 5 9 68.04 68.46 3.07 o -2 6 9 39.71 41.89 2.06 o -1 6 9 190.37 188.41 3.49 o 0 6 9 3.14 2.05 1.57 o 1 6 9 38.27 46.37 2.35 o 2 6 9 2.38 0.64 1.95 o 3 6 9 0.04 2.81 2.28 o -3 7 9 2.67 4.47 1.94 o -2 7 9 1.55 0.99 1.66 o -1 7 9 28.98 31.31 2.29 o 0 7 9 36.70 39.78 2.65 o 1 7 9 5.83 2.95 1.97 o 2 7 9 2.16 -1.27 2.25 o -3 8 9 110.23 111.73 3.47 o -2 8 9 33.98 45.65 2.90 o -1 8 9 0.63 -0.62 2.12 o 0 8 9 7.79 10.36 2.49 o -4 9 9 49.43 53.59 3.07 o -3 9 9 32.80 21.84 2.78 o -2 9 9 34.59 33.72 3.03 o 0 0 10 2033.96 2111.99 26.68 o 0 1 10 334.09 321.66 3.03 o 1 1 10 808.89 789.96 7.28 o -1 2 10 1693.41 1682.16 13.17 o 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12.39 1.43 o 1 2 11 81.36 85.26 2.61 o -1 3 11 322.26 326.27 3.97 o 0 3 11 34.29 30.21 1.73 o 1 3 11 88.97 85.02 2.43 o 2 3 11 142.05 139.54 2.96 o -1 4 11 144.92 148.67 3.35 o 0 4 11 2.78 3.68 1.61 o 1 4 11 0.46 1.91 1.71 o 2 4 11 55.64 47.91 2.41 o 3 4 11 229.45 223.80 5.07 o -2 5 11 46.31 40.08 2.04 o -1 5 11 33.15 28.58 2.31 o 0 5 11 38.83 45.17 2.64 o 1 5 11 28.25 24.71 2.41 o 2 5 11 1.57 -0.19 2.15 o -2 6 11 13.71 10.08 2.10 o -1 6 11 37.50 38.53 2.53 o 0 6 11 0.09 -2.07 2.07 o 1 6 11 16.47 15.42 2.48 o -3 7 11 60.48 60.23 3.15 o -2 7 11 0.99 0.88 2.69 o -1 7 11 41.33 45.15 3.08 o 0 0 12 736.47 749.62 14.85 o 0 1 12 83.85 72.84 2.41 o 1 1 12 614.27 598.20 9.65 o -1 2 12 709.90 692.47 9.97 o 0 2 12 296.16 292.18 4.00 o 1 2 12 249.17 245.39 4.04 o 2 2 12 1003.17 1049.31 12.25 o -1 3 12 305.97 288.73 4.23 o 0 3 12 528.22 524.07 5.74 o 1 3 12 75.22 74.11 2.62 o 2 3 12 23.50 20.86 2.09 o 3 3 12 529.34 544.22 9.12 o -2 4 12 1294.61 1315.86 15.21 o -1 4 12 88.09 85.12 2.97 o 0 4 12 149.79 142.32 3.58 o 1 4 12 189.32 196.07 5.23 o -2 5 12 45.10 39.11 2.68 o -1 5 12 265.28 270.03 4.90 o 0 5 12 104.82 98.00 3.46 o -3 6 12 653.07 695.58 12.31 o 0 1 13 15.38 15.13 2.40 o 0 2 13 5.52 3.54 2.19 o 1 2 13 264.06 258.82 4.39 o -1 3 13 43.84 48.23 2.83 o 0 3 13 33.24 31.93 2.47 o