#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:05 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180907 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104881.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104881_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9649 _cell_length_b 8.9649 _cell_length_c 9.5685 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7003 _cod_data_source_file bk51011bsup3.hkl _cod_data_source_block 1b #BEGIN Tags that were not found in dictionaries: _shelx_title ' m104m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3764.73 3845.53 14.76 o -1 2 0 5573.04 5920.68 23.26 o 0 2 0 5697.35 5798.55 23.95 o -1 3 0 429.93 428.41 2.10 o 0 3 0 1126.67 1071.99 5.85 o -2 4 0 3601.11 3629.16 20.14 o -1 4 0 684.27 663.74 3.22 o 0 4 0 1382.22 1408.70 7.99 o -2 5 0 16.08 8.59 0.42 o -1 5 0 3739.85 3598.33 14.12 o 0 5 0 1951.09 1968.54 14.05 o -3 6 0 1328.97 1306.50 9.48 o -2 6 0 578.85 559.62 3.22 o -1 6 0 1388.05 1428.48 6.44 o 0 6 0 4021.06 4144.08 23.70 o -3 7 0 962.71 964.25 5.55 o -2 7 0 1269.54 1312.87 6.48 o -1 7 0 169.75 169.67 1.75 o 0 7 0 17.05 13.45 1.13 o -4 8 0 2059.22 2099.99 14.90 o -3 8 0 146.49 140.46 2.01 o -2 8 0 612.61 621.81 4.15 o -1 8 0 1090.05 1124.56 6.54 o 0 8 0 485.10 496.95 6.07 o -4 9 0 186.46 174.94 2.47 o -3 9 0 1151.75 1150.85 7.45 o -2 9 0 402.61 403.26 3.94 o -1 9 0 308.16 305.20 3.38 o 0 9 0 647.00 655.58 7.73 o -5 10 0 1740.04 1738.44 14.26 o -4 10 0 280.77 268.58 3.42 o -3 10 0 356.43 339.66 4.18 o -2 10 0 771.58 750.36 7.00 o -1 10 0 169.00 164.61 3.88 o 0 10 0 230.05 221.87 6.91 o -5 11 0 213.86 201.49 3.12 o -4 11 0 385.29 367.66 4.90 o -3 11 0 59.09 52.08 2.41 o -2 11 0 32.95 29.51 2.62 o -1 11 0 567.11 565.54 8.08 o 0 11 0 185.97 169.97 6.89 o -6 12 0 246.75 242.28 6.56 o -5 12 0 231.17 223.97 4.33 o -4 12 0 24.38 24.50 2.55 o -3 12 0 470.66 479.34 6.91 o 0 1 1 1012.19 909.89 2.99 o 0 2 1 1569.42 1664.67 6.18 o 1 2 1 6.35 7.74 0.29 o -1 3 1 3332.55 3407.22 12.66 o 0 3 1 183.16 185.87 1.08 o 1 3 1 526.70 517.98 2.63 o 2 3 1 495.70 505.99 2.90 o -1 4 1 1645.77 1670.99 6.88 o 0 4 1 724.60 716.73 3.45 o 1 4 1 0.11 0.68 0.31 o 2 4 1 649.45 648.58 3.61 o 3 4 1 447.50 445.84 2.91 o -2 5 1 529.02 546.95 3.86 o -1 5 1 203.55 231.31 1.69 o 0 5 1 2493.72 2533.85 11.15 o 1 5 1 534.86 550.82 3.22 o 2 5 1 307.49 313.60 2.45 o 3 5 1 53.63 53.98 1.22 o 4 5 1 92.04 92.67 1.90 o -2 6 1 19.71 25.79 0.72 o -1 6 1 631.96 644.93 3.65 o 0 6 1 10.74 14.28 0.60 o 1 6 1 7.06 7.37 0.68 o 2 6 1 6.55 7.16 0.75 o 3 6 1 87.12 82.66 1.74 o 4 6 1 63.04 68.50 2.04 o 5 6 1 215.36 228.62 3.71 o -3 7 1 53.12 55.10 1.10 o -2 7 1 135.09 136.15 1.51 o -1 7 1 57.73 52.35 1.38 o 0 7 1 101.16 88.09 1.54 o 1 7 1 59.07 60.93 1.44 o 2 7 1 127.91 127.75 2.14 o 3 7 1 39.18 44.54 1.84 o 4 7 1 4.62 3.88 1.46 o 5 7 1 3.12 2.14 1.81 o -3 8 1 67.81 63.69 1.44 o -2 8 1 43.20 41.14 1.27 o -1 8 1 113.82 101.47 1.87 o 0 8 1 2.88 1.70 0.92 o 1 8 1 64.00 64.34 1.69 o 2 8 1 14.42 13.55 1.51 o 3 8 1 56.45 58.30 2.43 o 4 8 1 75.78 78.54 3.39 o -4 9 1 124.41 117.58 2.03 o -3 9 1 4.18 6.37 1.08 o -2 9 1 419.43 445.62 4.54 o -1 9 1 175.32 172.97 2.94 o 0 9 1 56.20 51.64 2.56 o 1 9 1 134.49 136.07 3.20 o 2 9 1 33.35 34.38 2.69 o 3 9 1 8.35 11.13 2.68 o -4 10 1 170.18 180.89 2.72 o -3 10 1 21.07 20.12 1.67 o -2 10 1 5.40 2.92 1.43 o -1 10 1 15.35 20.21 1.93 o 0 10 1 110.33 109.68 3.76 o 1 10 1 6.65 3.99 2.63 o -5 11 1 137.93 141.50 2.94 o -4 11 1 29.67 38.28 2.12 o -3 11 1 11.01 10.33 1.89 o -2 11 1 40.57 41.23 2.54 o -1 11 1 3.85 1.37 2.43 o 0 11 1 109.05 110.43 4.59 o -5 12 1 2.76 2.65 2.14 o -4 12 1 37.19 41.42 2.77 o -3 12 1 0.56 -2.31 2.31 o 0 0 2 18531.66 16690.63 135.43 o 0 1 2 1351.06 1375.55 4.63 o 1 1 2 1839.22 1858.09 10.05 o -1 2 2 11239.81 10925.18 79.29 o 0 2 2 2534.96 2592.15 10.73 o 1 2 2 372.55 353.69 1.99 o 2 2 2 1425.46 1332.91 8.02 o -1 3 2 2966.20 2976.85 12.91 o 0 3 2 3085.64 2979.04 12.75 o 1 3 2 230.24 201.22 1.90 o 2 3 2 580.24 531.71 2.94 o 3 3 2 3764.87 3655.19 20.39 o -2 4 2 11222.62 11555.42 67.55 o -1 4 2 1299.03 1275.39 6.08 o 0 4 2 977.15 973.72 5.01 o 1 4 2 2444.58 2380.27 9.78 o 2 4 2 484.02 471.14 3.05 o 3 4 2 1070.37 1061.85 5.11 o 4 4 2 1767.75 1774.20 13.17 o -2 5 2 60.84 51.13 0.76 o -1 5 2 2071.38 2018.51 10.48 o 0 5 2 861.32 859.39 4.95 o 1 5 2 900.35 928.78 5.41 o 2 5 2 1556.56 1544.91 7.50 o 3 5 2 404.45 399.38 3.01 o 4 5 2 36.44 35.99 1.36 o 5 5 2 963.68 968.09 11.01 o -3 6 2 1234.35 1254.24 9.78 o -2 6 2 1092.05 1127.17 6.72 o -1 6 2 374.54 379.24 3.18 o 0 6 2 2345.45 2435.58 11.74 o 1 6 2 96.88 101.28 1.48 o 2 6 2 179.72 190.81 2.12 o 3 6 2 709.94 714.67 6.18 o 4 6 2 389.10 368.30 4.81 o 5 6 2 209.40 206.05 3.53 o 6 6 2 369.33 359.51 7.31 o -3 7 2 362.76 382.02 3.04 o -2 7 2 1575.32 1618.48 9.32 o -1 7 2 501.25 474.77 3.87 o 0 7 2 166.23 161.37 2.29 o 1 7 2 783.65 814.99 5.98 o 2 7 2 322.70 300.42 3.54 o 3 7 2 113.55 124.61 2.76 o 4 7 2 693.56 699.54 7.37 o 5 7 2 186.10 185.45 4.08 o -4 8 2 1798.67 1865.35 17.92 o -3 8 2 373.25 383.23 3.80 o -2 8 2 772.54 763.73 5.88 o -1 8 2 1985.89 2033.85 11.55 o 0 8 2 224.22 220.85 2.96 o 1 8 2 435.69 446.47 4.55 o 2 8 2 751.57 781.27 6.76 o 3 8 2 127.07 113.62 3.25 o 4 8 2 103.35 110.50 3.52 o -4 9 2 277.19 250.12 3.10 o -3 9 2 1330.36 1336.02 9.14 o -2 9 2 343.12 367.63 4.21 o -1 9 2 192.86 178.97 3.03 o 0 9 2 568.09 567.74 5.75 o 1 9 2 102.07 93.37 2.85 o 2 9 2 157.67 166.10 6.39 o 3 9 2 556.72 583.57 8.57 o -5 10 2 930.46 940.74 9.70 o -4 10 2 64.70 67.09 2.16 o -3 10 2 365.93 328.50 4.16 o -2 10 2 526.08 496.71 5.22 o -1 10 2 201.00 205.89 3.82 o 0 10 2 124.25 118.29 3.21 o 1 10 2 546.87 551.67 7.32 o -5 11 2 168.57 161.09 3.32 o -4 11 2 252.33 242.08 4.62 o -3 11 2 62.64 60.29 2.53 o -2 11 2 1.00 0.05 1.77 o -1 11 2 339.07 340.53 6.53 o -6 12 2 373.13 400.19 8.40 o -5 12 2 83.08 81.49 3.14 o -4 12 2 86.12 71.99 3.24 o -3 12 2 354.81 346.89 5.73 o 0 1 3 12.56 17.66 0.37 o 0 2 3 1294.43 1347.26 6.12 o 1 2 3 212.94 208.30 1.49 o -1 3 3 2784.80 2963.12 12.56 o 0 3 3 95.95 106.52 1.32 o 1 3 3 343.98 362.57 2.26 o 2 3 3 424.67 417.35 2.46 o -1 4 3 749.71 813.10 4.45 o 0 4 3 11.47 7.12 0.58 o 1 4 3 9.27 10.90 0.65 o 2 4 3 553.55 573.39 3.42 o 3 4 3 686.86 694.33 4.04 o -2 5 3 326.05 361.50 2.86 o -1 5 3 11.60 18.35 0.62 o 0 5 3 12.65 18.06 0.81 o 1 5 3 65.74 68.14 1.36 o 2 5 3 1.92 0.37 0.51 o 3 5 3 108.69 104.08 1.76 o 4 5 3 49.93 52.61 1.71 o -2 6 3 4.86 5.56 0.67 o -1 6 3 69.24 68.71 1.56 o 0 6 3 2.31 3.40 0.70 o 1 6 3 103.09 94.61 1.70 o 2 6 3 146.65 145.72 2.22 o 3 6 3 87.17 99.29 1.99 o 4 6 3 18.56 18.87 1.50 o 5 6 3 39.08 43.30 2.32 o -3 7 3 201.91 209.85 2.74 o -2 7 3 24.97 18.80 1.14 o -1 7 3 326.10 318.63 3.39 o 0 7 3 133.33 128.92 2.20 o 1 7 3 38.00 29.83 1.41 o 2 7 3 49.91 43.28 1.78 o 3 7 3 64.58 66.38 2.36 o 4 7 3 4.21 -0.33 1.70 o 5 7 3 64.74 58.36 2.78 o -3 8 3 95.11 86.62 2.02 o -2 8 3 357.70 344.08 3.79 o -1 8 3 3.18 5.87 1.21 o 0 8 3 237.41 238.21 3.34 o 1 8 3 31.03 31.48 1.73 o 2 8 3 2.52 1.44 1.49 o 3 8 3 61.25 57.09 2.54 o 4 8 3 58.10 60.22 2.94 o -4 9 3 85.88 70.42 1.96 o -3 9 3 2.13 1.39 1.15 o -2 9 3 213.51 240.26 3.50 o -1 9 3 112.59 114.22 2.62 o 0 9 3 1.66 2.64 1.46 o 1 9 3 63.26 58.55 2.55 o 2 9 3 34.30 37.78 2.51 o 3 9 3 1.05 3.76 2.57 o -4 10 3 49.57 48.43 1.94 o -3 10 3 47.15 47.30 2.01 o -2 10 3 28.06 15.67 1.73 o -1 10 3 2.66 2.73 1.57 o 0 10 3 24.40 25.72 2.22 o 1 10 3 0.05 4.43 2.26 o -5 11 3 25.07 23.20 2.14 o -4 11 3 9.44 11.37 2.01 o -3 11 3 24.60 35.23 2.29 o -2 11 3 55.08 58.47 2.64 o -1 11 3 8.05 2.59 1.99 o -5 12 3 78.86 79.21 3.31 o -4 12 3 23.66 19.94 2.50 o -3 12 3 9.56 6.24 2.34 o 0 0 4 1116.28 1263.67 13.44 o 0 1 4 497.24 469.20 2.50 o 1 1 4 4256.29 4137.68 21.10 o -1 2 4 4404.87 4274.87 23.56 o 0 2 4 443.54 423.98 2.38 o 1 2 4 1632.35 1623.05 7.29 o 2 2 4 4280.00 4169.89 23.39 o -1 3 4 1273.80 1264.35 6.19 o 0 3 4 4805.12 4769.94 20.52 o 1 3 4 909.40 914.76 4.88 o 2 3 4 1093.88 1061.87 5.25 o 3 3 4 2835.45 2805.83 15.69 o -2 4 4 3612.93 3708.82 24.31 o -1 4 4 674.64 659.68 4.27 o 0 4 4 419.93 384.50 3.20 o 1 4 4 1799.47 1843.01 9.29 o 2 4 4 648.01 670.55 3.90 o 3 4 4 280.64 281.97 2.61 o 4 4 4 872.59 884.87 7.90 o -2 5 4 1000.80 974.91 5.96 o -1 5 4 1497.09 1492.39 8.15 o 0 5 4 215.25 215.93 2.36 o 1 5 4 119.21 115.93 1.79 o 2 5 4 1732.75 1766.93 9.17 o 3 5 4 503.53 491.60 3.99 o 4 5 4 149.24 146.83 2.35 o 5 5 4 300.19 302.20 5.42 o -3 6 4 3205.65 3338.29 20.29 o -2 6 4 665.45 705.27 5.64 o -1 6 4 255.84 262.90 2.94 o 0 6 4 966.07 995.23 6.25 o 1 6 4 417.40 397.09 3.60 o 2 6 4 157.19 167.29 2.45 o 3 6 4 802.40 821.01 6.65 o 4 6 4 103.71 84.42 2.70 o 5 6 4 154.16 151.12 4.14 o 6 6 4 475.95 473.88 10.33 o -3 7 4 273.50 284.27 3.42 o -2 7 4 1948.20 1946.96 11.49 o -1 7 4 487.02 465.16 4.30 o 0 7 4 946.83 936.33 6.50 o 1 7 4 1120.14 1143.10 7.58 o 2 7 4 195.20 173.07 3.32 o 3 7 4 83.40 99.32 2.73 o 4 7 4 651.02 666.45 6.83 o 5 7 4 50.30 44.49 3.31 o -4 8 4 1159.74 1228.90 12.80 o -3 8 4 555.88 575.48 5.43 o -2 8 4 237.10 217.38 3.01 o -1 8 4 1306.65 1303.66 8.62 o 0 8 4 76.47 70.24 2.14 o 1 8 4 208.47 221.85 3.54 o 2 8 4 492.23 524.98 7.83 o 3 8 4 167.36 148.94 3.87 o 4 8 4 185.82 195.85 4.44 o -4 9 4 181.33 160.51 3.16 o -3 9 4 712.26 708.96 6.45 o -2 9 4 135.07 150.25 2.87 o -1 9 4 132.73 114.29 2.67 o 0 9 4 513.55 502.23 5.47 o 1 9 4 147.32 144.41 3.54 o 2 9 4 102.61 97.85 3.74 o -5 10 4 293.44 304.46 6.25 o -4 10 4 100.88 111.32 3.14 o -3 10 4 110.61 87.69 2.54 o -2 10 4 465.53 468.04 5.16 o -1 10 4 89.75 94.43 2.73 o 0 10 4 49.12 47.77 3.66 o 1 10 4 296.28 303.73 7.31 o -5 11 4 90.88 86.93 3.58 o -4 11 4 502.66 511.08 6.08 o -3 11 4 152.60 157.93 4.23 o -2 11 4 115.81 101.41 2.86 o -1 11 4 275.99 280.04 5.18 o -6 12 4 585.91 629.78 10.57 o -5 12 4 40.64 42.61 2.88 o -4 12 4 206.50 196.60 4.60 o 0 1 5 431.62 395.47 2.41 o 0 2 5 2512.60 2601.28 10.68 o 1 2 5 701.70 702.69 3.86 o -1 3 5 23.76 28.72 0.68 o 0 3 5 45.61 33.62 0.79 o 1 3 5 189.70 199.79 2.04 o 2 3 5 103.06 92.68 1.20 o -1 4 5 32.63 41.76 0.84 o 0 4 5 112.28 108.39 1.79 o 1 4 5 0.67 -0.33 0.67 o 2 4 5 70.78 71.71 1.36 o 3 4 5 49.36 51.78 1.43 o -2 5 5 204.46 220.90 2.23 o -1 5 5 121.10 110.48 1.86 o 0 5 5 68.92 52.78 1.40 o 1 5 5 53.00 52.59 1.40 o 2 5 5 132.92 129.87 2.04 o 3 5 5 247.55 259.34 3.22 o 4 5 5 67.49 65.70 1.89 o -2 6 5 684.89 686.41 5.17 o -1 6 5 24.23 25.06 1.15 o 0 6 5 7.95 9.50 0.99 o 1 6 5 313.38 303.12 3.24 o 2 6 5 437.22 455.18 4.52 o 3 6 5 48.83 37.04 2.27 o 4 6 5 84.78 77.58 2.43 o 5 6 5 3.41 2.06 2.30 o -3 7 5 253.66 252.98 2.94 o -2 7 5 74.20 64.55 1.87 o -1 7 5 255.95 258.07 3.44 o 0 7 5 136.63 136.46 2.56 o 1 7 5 51.79 42.79 1.97 o 2 7 5 54.83 47.33 2.23 o 3 7 5 59.70 59.37 2.69 o 4 7 5 0.00 -0.80 1.84 o -3 8 5 94.03 91.32 2.15 o -2 8 5 172.39 155.62 2.86 o -1 8 5 37.27 37.83 1.76 o 0 8 5 245.72 231.54 3.44 o 1 8 5 62.17 61.89 2.49 o 2 8 5 8.23 6.93 1.96 o 3 8 5 15.75 14.07 2.30 o -4 9 5 64.29 52.20 2.36 o -3 9 5 1.40 2.29 1.30 o -2 9 5 3.12 0.86 1.36 o -1 9 5 18.65 16.66 1.97 o 0 9 5 38.91 31.39 2.19 o 1 9 5 8.70 7.24 2.17 o 2 9 5 26.71 21.84 2.59 o -4 10 5 9.27 5.89 1.87 o -3 10 5 111.88 109.74 3.29 o -2 10 5 0.51 -0.21 1.66 o -1 10 5 56.99 65.25 2.82 o 0 10 5 7.23 8.11 2.31 o -5 11 5 13.90 9.03 2.30 o -4 11 5 28.65 22.98 2.87 o -3 11 5 111.15 117.20 3.68 o -2 11 5 44.43 48.49 2.92 o 0 0 6 32.23 23.85 1.68 o 0 1 6 694.91 675.72 3.69 o 1 1 6 4161.54 4200.34 24.84 o -1 2 6 1430.63 1446.71 9.40 o 0 2 6 171.32 164.37 1.60 o 1 2 6 1060.92 1078.00 5.42 o 2 2 6 3074.18 3084.09 20.12 o -1 3 6 182.46 181.40 1.70 o 0 3 6 3351.55 3396.90 15.18 o 1 3 6 1204.94 1249.92 6.78 o 2 3 6 940.62 946.52 5.59 o 3 3 6 986.40 1014.82 9.43 o -2 4 6 305.65 311.56 3.37 o -1 4 6 438.89 418.58 3.17 o 0 4 6 329.34 338.31 2.89 o 1 4 6 2272.41 2354.77 11.98 o 2 4 6 321.85 328.25 3.18 o 3 4 6 52.35 53.70 1.53 o 4 4 6 460.32 465.99 6.16 o -2 5 6 1420.47 1391.98 7.68 o -1 5 6 2174.12 2229.66 12.22 o 0 5 6 207.33 212.07 2.74 o 1 5 6 126.34 118.93 2.06 o 2 5 6 1350.02 1383.18 9.23 o 3 5 6 168.17 146.77 2.72 o 4 5 6 534.60 535.45 5.39 o 5 5 6 337.22 345.49 7.56 o -3 6 6 2401.22 2410.45 17.80 o -2 6 6 148.49 143.10 2.45 o -1 6 6 400.81 393.90 3.98 o 0 6 6 725.70 725.40 5.86 o 1 6 6 628.32 605.43 5.26 o 2 6 6 224.86 233.64 3.37 o 3 6 6 894.46 909.68 7.18 o 4 6 6 41.26 38.82 2.30 o 5 6 6 63.21 64.22 3.95 o -3 7 6 225.32 223.49 2.98 o -2 7 6 1318.79 1298.98 9.08 o -1 7 6 301.63 300.18 3.89 o 0 7 6 544.65 531.74 5.14 o 1 7 6 882.86 891.17 7.75 o 2 7 6 86.93 76.55 2.73 o 3 7 6 124.42 134.60 3.50 o 4 7 6 416.09 433.77 7.10 o -4 8 6 605.46 614.08 8.82 o -3 8 6 208.58 211.46 3.27 o -2 8 6 39.81 33.50 1.82 o -1 8 6 361.62 351.19 4.28 o 0 8 6 165.38 167.04 3.46 o 1 8 6 31.04 30.62 2.31 o 2 8 6 386.45 394.74 5.89 o 3 8 6 125.73 123.89 3.89 o -4 9 6 275.13 277.03 4.93 o -3 9 6 479.78 506.58 5.91 o -2 9 6 41.60 44.43 2.13 o -1 9 6 82.96 70.01 3.00 o 0 9 6 635.54 656.80 7.17 o 1 9 6 162.29 162.73 4.20 o -5 10 6 388.09 411.00 7.81 o -4 10 6 246.98 258.33 4.49 o -3 10 6 51.90 51.11 2.78 o -2 10 6 567.00 609.51 7.10 o -1 10 6 51.47 53.13 2.78 o -5 11 6 48.63 50.84 3.02 o -4 11 6 724.87 769.63 8.01 o -3 11 6 195.87 193.66 4.31 o 0 1 7 729.99 673.87 3.87 o 0 2 7 601.83 585.66 3.56 o 1 2 7 102.86 109.84 1.47 o -1 3 7 50.04 43.41 1.00 o 0 3 7 165.33 148.18 1.83 o 1 3 7 60.21 58.14 1.30 o 2 3 7 35.44 32.58 1.23 o -1 4 7 28.56 30.86 1.05 o 0 4 7 670.23 669.75 4.92 o 1 4 7 3.87 2.92 0.80 o 2 4 7 98.71 93.12 1.90 o 3 4 7 21.50 17.80 1.25 o -2 5 7 134.12 131.42 1.94 o -1 5 7 56.85 57.19 1.76 o 0 5 7 77.39 74.28 1.97 o 1 5 7 148.77 136.38 2.60 o 2 5 7 30.54 29.38 1.64 o 3 5 7 179.24 186.27 3.68 o 4 5 7 105.72 105.78 2.69 o -2 6 7 708.98 706.78 5.83 o -1 6 7 146.91 151.19 2.78 o 0 6 7 0.18 1.52 1.18 o 1 6 7 170.17 171.14 3.05 o 2 6 7 118.30 120.71 2.81 o 3 6 7 139.94 124.80 3.16 o 4 6 7 104.91 96.25 3.50 o -3 7 7 26.12 26.19 1.50 o -2 7 7 14.83 12.22 1.43 o -1 7 7 55.55 54.94 2.07 o 0 7 7 75.73 77.93 2.54 o 1 7 7 0.45 -1.64 1.64 o 2 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557.44 7.37 o 0 1 11 5.78 6.62 1.12 o 0 2 11 12.21 14.64 1.42 o 1 2 11 66.91 76.61 2.43 o -1 3 11 280.46 287.21 3.59 o 0 3 11 26.50 27.13 1.66 o 1 3 11 74.28 80.37 2.33 o 2 3 11 115.03 114.81 2.69 o -1 4 11 122.20 121.26 3.24 o 0 4 11 2.39 4.33 1.58 o 1 4 11 0.26 -0.31 1.67 o 2 4 11 48.11 45.75 2.37 o 3 4 11 187.45 178.69 4.22 o -2 5 11 41.17 40.26 1.97 o -1 5 11 26.77 21.42 2.11 o 0 5 11 30.15 33.80 2.26 o 1 5 11 24.49 25.51 2.35 o 2 5 11 1.35 2.49 2.19 o -2 6 11 10.75 7.05 1.97 o -1 6 11 30.90 27.17 2.33 o 0 6 11 0.23 0.17 2.09 o 1 6 11 14.54 16.03 2.42 o -3 7 11 50.41 54.96 2.99 o -2 7 11 0.62 3.89 2.42 o -1 7 11 36.03 26.63 3.17 o 0 0 12 596.01 619.75 18.65 o 0 1 12 70.81 61.78 2.13 o 1 1 12 523.47 518.08 8.88 o -1 2 12 604.34 579.35 8.66 o 0 2 12 247.58 239.86 3.59 o 1 2 12 216.70 210.03 3.53 o 2 2 12 861.10 879.54 10.58 o -1 3 12 259.34 248.48 3.86 o 0 3 12 462.95 467.17 5.37 o 1 3 12 65.11 64.19 2.46 o 2 3 12 23.65 19.48 2.01 o 3 3 12 436.45 446.25 10.72 o -2 4 12 1083.49 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