#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:05 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180907 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104882.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104882_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9696 _cell_length_b 8.9696 _cell_length_c 9.5842 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7003 _cod_data_source_file bk51011csup4.hkl _cod_data_source_block 1c #BEGIN Tags that were not found in dictionaries: _shelx_title ' m104l' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3747.92 3862.25 15.05 o -1 2 0 5482.79 5917.53 23.61 o 0 2 0 5708.54 5875.85 24.63 o -1 3 0 403.21 417.71 2.10 o 0 3 0 1138.08 1113.17 6.14 o -2 4 0 3552.77 3663.55 21.20 o -1 4 0 710.37 694.84 3.39 o 0 4 0 1297.69 1352.76 7.85 o -2 5 0 17.43 11.77 0.46 o -1 5 0 3656.74 3601.50 14.37 o 0 5 0 1920.96 1993.59 12.33 o -3 6 0 1282.83 1263.04 9.39 o -2 6 0 567.14 549.51 3.24 o -1 6 0 1303.06 1352.95 6.27 o 0 6 0 3792.35 3953.55 24.93 o -3 7 0 900.81 903.33 5.38 o -2 7 0 1208.22 1262.44 6.38 o -1 7 0 161.08 174.85 1.82 o 0 7 0 12.26 9.04 1.08 o -4 8 0 1860.98 1889.32 13.89 o -3 8 0 127.63 122.61 1.87 o -2 8 0 551.51 568.11 3.97 o -1 8 0 961.91 1005.13 6.68 o 0 8 0 415.80 442.83 5.17 o -4 9 0 172.61 160.11 2.45 o -3 9 0 1033.32 1042.54 7.05 o -2 9 0 343.50 346.67 3.70 o -1 9 0 279.12 266.43 3.19 o 0 9 0 568.03 586.53 7.31 o -5 10 0 1506.12 1491.03 12.89 o -4 10 0 249.23 226.40 3.20 o -3 10 0 308.26 301.98 3.87 o -2 10 0 667.14 646.93 6.51 o -1 10 0 139.67 134.21 3.67 o 0 10 0 189.36 181.02 6.43 o -5 11 0 185.70 183.99 3.44 o -4 11 0 342.90 338.92 5.19 o -3 11 0 52.90 48.13 2.38 o -2 11 0 31.75 30.15 2.68 o -1 11 0 481.73 507.08 7.79 o 0 11 0 154.56 143.36 6.51 o -6 12 0 215.73 216.43 6.93 o -5 12 0 189.61 188.63 4.81 o -4 12 0 19.94 19.41 2.49 o -3 12 0 382.37 396.41 6.82 o 0 1 1 1009.73 906.14 3.02 o 0 2 1 1526.75 1644.51 6.20 o 1 2 1 6.37 6.15 0.27 o -1 3 1 3277.81 3334.03 12.62 o 0 3 1 193.85 201.45 1.16 o 1 3 1 531.76 497.68 2.59 o 2 3 1 454.71 452.78 3.00 o -1 4 1 1624.48 1635.48 6.86 o 0 4 1 663.35 649.89 3.26 o 1 4 1 0.39 1.00 0.33 o 2 4 1 620.72 601.71 3.47 o 3 4 1 414.79 412.57 2.80 o -2 5 1 495.37 503.06 3.39 o -1 5 1 176.63 200.72 1.58 o 0 5 1 2353.29 2378.50 12.62 o 1 5 1 503.58 504.99 3.08 o 2 5 1 275.45 286.86 2.42 o 3 5 1 52.10 55.16 1.28 o 4 5 1 87.00 95.94 1.96 o -2 6 1 17.60 24.49 0.71 o -1 6 1 583.11 586.29 3.46 o 0 6 1 9.98 10.48 0.53 o 1 6 1 6.52 6.72 0.69 o 2 6 1 4.79 6.35 0.72 o 3 6 1 79.94 78.29 1.74 o 4 6 1 58.64 64.05 2.02 o 5 6 1 182.08 186.81 4.41 o -3 7 1 44.56 46.08 1.04 o -2 7 1 125.02 126.68 1.48 o -1 7 1 53.63 47.19 1.09 o 0 7 1 97.88 77.68 1.43 o 1 7 1 58.70 55.00 1.40 o 2 7 1 110.44 107.28 2.02 o 3 7 1 40.33 43.79 1.86 o 4 7 1 3.14 1.10 1.41 o 5 7 1 2.30 0.35 1.80 o -3 8 1 66.64 63.32 1.43 o -2 8 1 43.15 39.50 1.28 o -1 8 1 104.95 94.06 1.86 o 0 8 1 2.60 2.91 0.95 o 1 8 1 58.83 55.78 1.64 o 2 8 1 12.86 10.87 1.49 o 3 8 1 45.54 47.27 2.36 o 4 8 1 56.62 60.33 3.17 o -4 9 1 112.46 108.19 2.02 o -3 9 1 3.46 3.93 0.96 o -2 9 1 368.00 389.95 4.30 o -1 9 1 161.20 155.53 3.16 o 0 9 1 44.77 43.79 2.09 o 1 9 1 115.90 121.77 3.10 o 2 9 1 28.02 31.45 2.65 o 3 9 1 5.96 2.58 2.55 o -4 10 1 151.67 166.70 2.68 o -3 10 1 21.60 23.32 1.71 o -2 10 1 3.79 1.71 1.42 o -1 10 1 14.58 17.49 1.86 o 0 10 1 88.84 93.38 3.56 o 1 10 1 5.06 3.55 2.67 o -5 11 1 108.51 112.96 2.70 o -4 11 1 22.99 26.34 1.96 o -3 11 1 8.52 9.87 1.86 o -2 11 1 31.46 31.35 2.44 o -1 11 1 2.91 7.17 2.48 o 0 11 1 81.86 79.58 3.98 o -5 12 1 2.22 1.08 2.04 o -4 12 1 27.38 32.19 2.57 o -3 12 1 0.26 2.16 2.47 o 0 0 2 18640.28 16721.73 161.77 o 0 1 2 1342.58 1356.46 4.62 o 1 1 2 1786.26 1817.18 9.97 o -1 2 2 11075.97 10648.28 95.76 o 0 2 2 2518.92 2571.06 10.81 o 1 2 2 352.18 333.07 1.87 o 2 2 2 1400.92 1316.12 8.05 o -1 3 2 2869.00 2859.95 12.63 o 0 3 2 3011.22 2890.65 12.61 o 1 3 2 232.10 203.33 1.44 o 2 3 2 563.81 515.06 2.91 o 3 3 2 3594.73 3528.30 20.03 o -2 4 2 10867.17 11096.77 67.00 o -1 4 2 1299.77 1263.17 6.12 o 0 4 2 918.43 910.72 4.82 o 1 4 2 2375.11 2333.02 9.75 o 2 4 2 467.87 457.92 2.79 o 3 4 2 1003.69 998.11 4.94 o 4 4 2 1620.90 1614.02 12.61 o -2 5 2 59.57 46.63 0.76 o -1 5 2 2012.99 1949.92 10.35 o 0 5 2 839.13 843.46 4.96 o 1 5 2 855.99 886.02 5.30 o 2 5 2 1471.28 1478.43 7.34 o 3 5 2 366.06 355.10 2.85 o 4 5 2 33.69 33.69 1.34 o 5 5 2 828.42 837.01 10.28 o -3 6 2 1196.05 1200.61 9.63 o -2 6 2 1046.71 1067.76 6.30 o -1 6 2 353.13 360.62 3.14 o 0 6 2 2200.38 2313.82 11.39 o 1 6 2 93.93 97.05 1.47 o 2 6 2 163.34 171.88 2.05 o 3 6 2 628.52 642.99 5.11 o 4 6 2 334.01 300.61 4.00 o 5 6 2 179.89 179.96 3.40 o 6 6 2 314.11 319.03 6.47 o -3 7 2 345.40 365.78 3.00 o -2 7 2 1487.73 1525.92 9.04 o -1 7 2 454.12 459.07 3.87 o 0 7 2 158.35 151.91 2.14 o 1 7 2 698.36 750.54 5.53 o 2 7 2 271.47 253.70 3.30 o 3 7 2 103.24 110.17 2.58 o 4 7 2 590.10 593.63 6.85 o 5 7 2 149.37 145.53 3.78 o -4 8 2 1642.96 1700.64 14.53 o -3 8 2 337.64 351.08 3.68 o -2 8 2 703.88 688.90 5.59 o -1 8 2 1787.07 1840.03 10.87 o 0 8 2 197.69 195.33 2.85 o 1 8 2 382.16 396.41 4.33 o 2 8 2 645.73 657.31 6.19 o 3 8 2 105.79 93.31 3.09 o 4 8 2 87.57 89.26 3.21 o -4 9 2 255.53 227.15 2.84 o -3 9 2 1206.06 1204.26 8.61 o -2 9 2 309.27 330.95 4.06 o -1 9 2 170.55 153.19 2.88 o 0 9 2 493.77 483.81 5.36 o 1 9 2 83.49 79.31 2.67 o 2 9 2 136.20 131.06 3.77 o 3 9 2 454.64 470.88 8.88 o -5 10 2 812.58 792.37 8.83 o -4 10 2 59.69 60.19 2.40 o -3 10 2 308.51 279.72 3.89 o -2 10 2 455.40 439.88 4.97 o -1 10 2 175.37 167.31 3.63 o 0 10 2 101.16 95.15 3.11 o 1 10 2 459.65 470.53 8.14 o -5 11 2 142.20 131.41 3.26 o -4 11 2 225.78 214.34 3.90 o -3 11 2 58.54 53.95 2.47 o -2 11 2 0.77 0.66 1.73 o -1 11 2 280.76 269.33 5.00 o -6 12 2 309.69 321.98 7.66 o -5 12 2 72.56 72.07 3.02 o -4 12 2 67.61 63.75 3.21 o -3 12 2 293.45 292.34 6.52 o 0 1 3 11.20 15.68 0.36 o 0 2 3 1280.07 1363.02 6.28 o 1 2 3 218.17 220.10 1.56 o -1 3 3 2764.20 3031.37 13.04 o 0 3 3 98.43 109.26 1.36 o 1 3 3 346.90 367.80 2.32 o 2 3 3 404.78 399.54 2.43 o -1 4 3 739.49 840.10 4.63 o 0 4 3 12.43 10.38 0.63 o 1 4 3 9.74 11.85 0.67 o 2 4 3 510.98 535.17 3.31 o 3 4 3 632.44 642.14 3.88 o -2 5 3 320.18 369.25 3.70 o -1 5 3 13.56 18.63 0.63 o 0 5 3 11.48 16.78 0.81 o 1 5 3 59.78 65.01 1.35 o 2 5 3 2.20 1.95 0.53 o 3 5 3 94.81 91.83 1.63 o 4 5 3 45.45 47.13 1.65 o -2 6 3 4.53 4.55 0.67 o -1 6 3 59.94 61.20 1.51 o 0 6 3 2.17 2.62 0.72 o 1 6 3 91.37 81.48 1.63 o 2 6 3 133.38 131.96 2.15 o 3 6 3 76.60 91.42 2.18 o 4 6 3 16.53 18.07 1.74 o 5 6 3 36.27 42.26 2.31 o -3 7 3 185.20 190.79 2.66 o -2 7 3 21.40 15.88 1.04 o -1 7 3 290.10 282.97 3.19 o 0 7 3 120.76 117.93 2.12 o 1 7 3 30.43 24.43 1.36 o 2 7 3 46.08 41.20 1.74 o 3 7 3 57.38 61.61 2.48 o 4 7 3 3.51 4.01 1.79 o 5 7 3 53.87 52.65 2.79 o -3 8 3 87.86 79.49 1.98 o -2 8 3 321.01 306.54 3.63 o -1 8 3 3.14 5.61 1.28 o 0 8 3 210.76 210.61 3.20 o 1 8 3 27.72 25.24 1.67 o 2 8 3 2.19 0.60 1.48 o 3 8 3 53.28 51.69 2.58 o 4 8 3 47.54 48.45 3.40 o -4 9 3 72.94 63.54 1.92 o -3 9 3 2.24 5.04 1.24 o -2 9 3 188.44 218.57 3.40 o -1 9 3 100.40 100.13 2.55 o 0 9 3 1.46 -0.28 1.41 o 1 9 3 53.86 52.75 2.45 o 2 9 3 30.20 25.10 2.37 o 3 9 3 0.52 -0.32 2.40 o -4 10 3 43.07 44.20 1.95 o -3 10 3 37.51 39.64 2.04 o -2 10 3 22.21 13.89 1.75 o -1 10 3 2.08 0.15 1.58 o 0 10 3 20.26 21.56 2.21 o 1 10 3 0.01 2.23 2.29 o -5 11 3 18.28 17.28 2.08 o -4 11 3 8.01 8.75 2.01 o -3 11 3 21.51 25.00 2.10 o -2 11 3 43.57 47.96 2.48 o -1 11 3 5.62 5.37 2.65 o -5 12 3 62.44 60.14 3.10 o -4 12 3 21.61 24.03 2.63 o -3 12 3 5.94 7.60 2.37 o 0 0 4 967.79 1104.93 12.12 o 0 1 4 503.62 475.49 2.55 o 1 1 4 4182.05 4070.07 20.28 o -1 2 4 4333.81 4193.19 23.44 o 0 2 4 434.15 410.68 2.36 o 1 2 4 1572.06 1540.49 7.07 o 2 2 4 4072.69 3949.89 22.57 o -1 3 4 1229.04 1195.66 5.99 o 0 3 4 4536.93 4438.98 19.49 o 1 3 4 855.24 842.73 4.66 o 2 3 4 1025.89 989.35 5.04 o 3 3 4 2678.50 2664.15 15.23 o -2 4 4 3377.34 3367.01 22.62 o -1 4 4 633.91 596.00 4.04 o 0 4 4 393.39 351.89 3.08 o 1 4 4 1700.91 1711.72 8.87 o 2 4 4 605.06 609.33 3.70 o 3 4 4 265.08 264.79 2.55 o 4 4 4 814.38 813.52 8.03 o -2 5 4 911.73 867.75 5.54 o -1 5 4 1399.93 1360.02 7.70 o 0 5 4 203.35 187.27 2.23 o 1 5 4 122.85 116.33 1.81 o 2 5 4 1603.67 1626.43 9.11 o 3 5 4 461.74 442.72 3.81 o 4 5 4 129.59 131.24 2.28 o 5 5 4 265.25 273.04 5.21 o -3 6 4 2995.30 3087.17 19.23 o -2 6 4 623.03 644.09 4.49 o -1 6 4 242.26 250.88 2.70 o 0 6 4 909.18 909.21 5.95 o 1 6 4 379.68 346.96 3.39 o 2 6 4 148.59 152.89 2.39 o 3 6 4 706.79 711.76 6.18 o 4 6 4 89.34 69.67 2.31 o 5 6 4 127.80 126.08 3.31 o 6 6 4 390.32 409.74 9.79 o -3 7 4 262.14 274.66 3.42 o -2 7 4 1797.35 1821.14 11.08 o -1 7 4 432.99 410.75 4.08 o 0 7 4 849.86 847.74 6.18 o 1 7 4 1021.89 1045.04 7.23 o 2 7 4 175.17 155.52 3.22 o 3 7 4 74.14 90.36 2.65 o 4 7 4 532.89 553.22 6.27 o 5 7 4 41.55 39.07 3.13 o -4 8 4 1073.71 1143.94 17.24 o -3 8 4 509.61 530.60 5.25 o -2 8 4 220.73 203.89 3.32 o -1 8 4 1181.42 1184.54 8.17 o 0 8 4 71.91 63.72 2.07 o 1 8 4 174.79 188.67 3.80 o 2 8 4 422.05 440.53 5.72 o 3 8 4 137.18 124.77 4.39 o 4 8 4 153.87 154.06 3.93 o -4 9 4 163.63 149.11 3.17 o -3 9 4 637.97 634.99 6.08 o -2 9 4 123.32 135.34 2.78 o -1 9 4 111.18 98.51 2.67 o 0 9 4 435.71 419.10 5.02 o 1 9 4 126.05 126.92 3.45 o 2 9 4 82.37 83.85 3.60 o -5 10 4 267.90 267.33 6.07 o -4 10 4 85.18 97.55 3.11 o -3 10 4 95.08 74.62 2.44 o -2 10 4 390.94 384.96 4.72 o -1 10 4 84.29 83.22 2.65 o 0 10 4 40.19 41.70 2.56 o 1 10 4 242.54 246.26 5.14 o -5 11 4 77.31 71.60 2.95 o -4 11 4 423.50 429.84 5.62 o -3 11 4 129.32 121.86 3.41 o -2 11 4 90.54 81.27 3.67 o -1 11 4 222.26 225.50 4.77 o -6 12 4 463.55 498.48 11.29 o -5 12 4 36.39 40.07 3.20 o -4 12 4 164.91 154.69 4.33 o 0 1 5 371.07 325.77 2.15 o 0 2 5 2389.06 2490.11 10.39 o 1 2 5 687.77 696.83 3.89 o -1 3 5 29.21 35.94 0.76 o 0 3 5 37.53 28.45 0.75 o 1 3 5 189.04 200.61 2.08 o 2 3 5 105.02 93.96 1.23 o -1 4 5 39.58 52.37 0.94 o 0 4 5 117.43 122.35 1.90 o 1 4 5 1.13 0.69 0.62 o 2 4 5 62.46 62.15 1.30 o 3 4 5 45.61 44.06 1.40 o -2 5 5 207.71 229.46 2.31 o -1 5 5 101.63 91.16 1.84 o 0 5 5 55.63 42.37 1.31 o 1 5 5 48.05 49.37 1.37 o 2 5 5 114.28 118.30 2.18 o 3 5 5 207.96 209.30 2.94 o 4 5 5 58.00 60.63 1.85 o -2 6 5 625.12 629.32 4.93 o -1 6 5 24.22 26.89 1.18 o 0 6 5 6.65 8.16 1.09 o 1 6 5 280.82 270.64 3.08 o 2 6 5 375.55 391.17 4.21 o 3 6 5 41.96 29.23 1.80 o 4 6 5 68.25 66.42 2.35 o 5 6 5 2.21 4.51 2.55 o -3 7 5 239.79 244.10 2.92 o -2 7 5 67.40 59.23 1.83 o -1 7 5 220.99 220.28 3.26 o 0 7 5 119.60 125.99 2.50 o 1 7 5 45.88 35.07 1.85 o 2 7 5 51.12 43.95 2.35 o 3 7 5 45.58 41.97 2.35 o 4 7 5 0.03 -1.87 1.87 o -3 8 5 76.58 74.14 2.03 o -2 8 5 149.55 133.33 2.82 o -1 8 5 33.28 34.31 1.73 o 0 8 5 207.59 208.08 3.31 o 1 8 5 51.54 58.13 2.70 o 2 8 5 7.13 6.92 2.01 o 3 8 5 14.16 6.84 2.22 o -4 9 5 53.81 43.33 2.25 o -3 9 5 1.38 -0.56 1.29 o -2 9 5 2.52 1.90 1.43 o -1 9 5 15.27 21.56 1.87 o 0 9 5 28.88 27.02 2.27 o 1 9 5 7.17 2.81 2.08 o 2 9 5 22.04 16.98 2.58 o -4 10 5 8.60 7.52 1.90 o -3 10 5 84.66 79.02 3.16 o -2 10 5 0.29 1.12 1.68 o -1 10 5 46.13 52.46 2.84 o 0 10 5 7.04 6.35 2.32 o -5 11 5 13.34 11.97 2.42 o -4 11 5 20.03 15.06 2.48 o -3 11 5 93.40 98.72 3.53 o -2 11 5 37.16 39.08 2.82 o 0 0 6 55.99 47.72 2.20 o 0 1 6 692.97 695.91 4.11 o 1 1 6 4055.15 4192.93 25.10 o -1 2 6 1408.69 1433.56 9.44 o 0 2 6 170.90 170.36 1.65 o 1 2 6 1004.39 1018.86 5.25 o 2 2 6 2853.61 2913.54 19.44 o -1 3 6 175.97 175.18 1.69 o 0 3 6 3086.20 3153.73 14.20 o 1 3 6 1109.33 1157.83 6.50 o 2 3 6 837.84 843.94 5.23 o 3 3 6 905.73 933.43 9.00 o -2 4 6 276.04 279.68 3.21 o -1 4 6 388.95 371.91 3.00 o 0 4 6 303.11 315.58 2.81 o 1 4 6 2044.88 2130.00 11.20 o 2 4 6 294.08 296.36 3.05 o 3 4 6 48.58 51.13 1.63 o 4 4 6 427.38 439.06 6.06 o -2 5 6 1263.86 1254.67 7.18 o -1 5 6 1958.50 2007.52 11.39 o 0 5 6 189.38 191.45 2.65 o 1 5 6 118.21 113.10 2.03 o 2 5 6 1197.84 1227.65 8.60 o 3 5 6 156.37 144.23 2.71 o 4 5 6 449.67 460.96 5.06 o 5 5 6 300.67 303.33 7.79 o -3 6 6 2173.03 2187.40 16.63 o -2 6 6 136.66 130.46 2.38 o -1 6 6 364.31 364.51 3.88 o 0 6 6 667.77 669.47 5.66 o 1 6 6 548.66 531.89 4.95 o 2 6 6 204.66 211.11 3.24 o 3 6 6 773.02 790.66 6.66 o 4 6 6 37.32 36.23 2.31 o 5 6 6 51.56 56.24 3.47 o -3 7 6 206.80 205.69 2.89 o -2 7 6 1175.08 1186.38 8.64 o -1 7 6 265.71 255.95 3.64 o 0 7 6 474.63 467.35 4.85 o 1 7 6 792.16 800.95 7.33 o 2 7 6 82.68 76.32 2.67 o 3 7 6 102.56 105.87 3.32 o 4 7 6 332.87 356.98 6.61 o -4 8 6 549.94 571.76 8.63 o -3 8 6 193.18 191.28 3.17 o -2 8 6 38.11 32.26 1.78 o -1 8 6 327.68 314.76 4.12 o 0 8 6 140.19 140.48 3.37 o 1 8 6 26.45 29.24 2.26 o 2 8 6 325.10 335.37 5.50 o 3 8 6 103.59 104.79 3.70 o -4 9 6 229.66 233.96 4.18 o -3 9 6 412.81 436.49 5.76 o -2 9 6 36.74 42.35 2.07 o -1 9 6 73.27 64.83 2.74 o 0 9 6 527.49 536.32 6.54 o 1 9 6 138.25 139.41 4.00 o -5 10 6 345.11 362.89 7.55 o -4 10 6 202.17 209.98 4.20 o -3 10 6 46.29 49.29 2.78 o -2 10 6 465.11 485.33 6.65 o -1 10 6 45.66 48.12 2.75 o -5 11 6 42.85 37.60 2.87 o -4 11 6 577.70 612.63 7.72 o -3 11 6 150.95 155.88 4.12 o 0 1 7 636.69 576.78 3.53 o 0 2 7 546.43 520.40 3.33 o 1 2 7 103.18 103.77 1.54 o -1 3 7 42.66 40.85 1.11 o 0 3 7 142.26 130.76 1.75 o 1 3 7 61.27 56.03 1.33 o 2 3 7 37.97 34.11 1.27 o -1 4 7 33.65 32.95 1.09 o 0 4 7 618.05 616.14 4.72 o 1 4 7 2.64 2.09 0.82 o 2 4 7 86.86 80.22 1.80 o 3 4 7 15.92 13.07 1.22 o -2 5 7 130.37 125.77 1.92 o -1 5 7 54.06 52.77 1.74 o 0 5 7 80.88 80.20 2.29 o 1 5 7 135.83 117.80 2.47 o 2 5 7 24.65 19.76 1.49 o 3 5 7 153.82 151.65 2.94 o 4 5 7 91.49 92.26 2.61 o -2 6 7 635.34 626.27 5.46 o -1 6 7 137.12 139.84 2.69 o 0 6 7 0.31 1.03 1.19 o 1 6 7 149.64 152.02 2.92 o 2 6 7 99.40 99.54 2.64 o 3 6 7 117.41 108.54 2.97 o 4 6 7 85.31 82.25 3.37 o -3 7 7 25.42 27.32 1.51 o -2 7 7 12.60 9.73 1.40 o -1 7 7 47.79 48.62 2.03 o 0 7 7 65.49 65.76 2.40 o 1 7 7 0.21 1.08 1.64 o 2 7 7 10.85 9.41 1.90 o 3 7 7 37.14 32.29 2.57 o -3 8 7 88.63 85.15 2.83 o -2 8 7 16.20 18.74 1.82 o -1 8 7 0.48 1.71 1.61 o 0 8 7 18.07 15.22 2.06 o 1 8 7 44.29 47.11 2.65 o 2 8 7 0.25 2.43 2.30 o -4 9 7 64.53 65.44 2.77 o -3 9 7 8.17 11.19 2.15 o -2 9 7 11.11 10.30 2.13 o -1 9 7 10.51 10.32 2.15 o 0 9 7 32.82 31.80 2.60 o -4 10 7 39.44 37.73 2.83 o -3 10 7 66.75 57.52 2.89 o -2 10 7 14.75 13.46 2.82 o 0 0 8 2574.66 2724.87 29.28 o 0 1 8 701.38 709.03 4.26 o 1 1 8 1764.30 1814.93 12.07 o -1 2 8 1404.18 1430.58 10.01 o 0 2 8 233.03 241.46 2.33 o 1 2 8 191.97 189.36 2.14 o 2 2 8 673.40 710.60 7.29 o -1 3 8 164.74 160.72 1.80 o 0 3 8 1427.00 1464.12 8.14 o 1 3 8 422.12 437.14 3.97 o 2 3 8 497.21 497.22 4.97 o 3 3 8 633.98 677.00 7.94 o -2 4 8 422.11 448.44 5.06 o -1 4 8 376.07 374.00 3.44 o 0 4 8 307.01 309.40 3.34 o 1 4 8 1582.67 1623.88 9.80 o 2 4 8 89.86 91.57 2.06 o 3 4 8 91.08 82.57 2.29 o 4 4 8 433.31 443.32 7.40 o -2 5 8 457.23 459.36 4.29 o -1 5 8 1576.20 1635.04 10.07 o 0 5 8 230.66 238.93 3.54 o 1 5 8 306.58 303.16 3.97 o 2 5 8 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