#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104883.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104883_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9790 _cell_length_b 8.9790 _cell_length_c 9.5973 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7007 _[local]_cod_data_source_file bk51011dsup5.hkl _[local]_cod_data_source_block 1d #BEGIN Tags that were not found in dictionaries: _shelx_title ' m104k' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3746.01 3845.09 14.38 o -1 2 0 5447.42 5848.92 22.42 o 0 2 0 5695.23 5813.41 23.41 o -1 3 0 400.72 414.17 2.03 o 0 3 0 1135.14 1129.80 6.16 o -2 4 0 3557.29 3639.89 19.86 o -1 4 0 706.56 691.58 3.28 o 0 4 0 1267.23 1326.19 7.47 o -2 5 0 18.47 12.95 0.46 o -1 5 0 3566.63 3540.15 13.64 o 0 5 0 1854.49 1909.42 11.50 o -3 6 0 1242.14 1233.32 8.99 o -2 6 0 548.92 538.82 3.12 o -1 6 0 1235.05 1282.71 5.83 o 0 6 0 3557.75 3770.29 21.33 o -3 7 0 849.52 845.92 4.86 o -2 7 0 1142.99 1206.50 5.98 o -1 7 0 151.43 165.83 1.73 o 0 7 0 10.31 8.40 1.09 o -4 8 0 1712.76 1733.13 14.47 o -3 8 0 117.47 114.01 1.78 o -2 8 0 501.61 509.84 3.66 o -1 8 0 870.98 920.28 5.61 o 0 8 0 372.66 394.17 4.73 o -4 9 0 156.57 140.54 2.22 o -3 9 0 939.05 949.02 6.69 o -2 9 0 306.39 312.67 3.45 o -1 9 0 252.33 245.28 3.02 o 0 9 0 502.29 518.85 6.65 o -5 10 0 1324.34 1323.86 11.49 o -4 10 0 221.91 195.45 2.94 o -3 10 0 272.65 265.88 3.60 o -2 10 0 588.56 584.21 6.08 o -1 10 0 118.50 110.97 3.35 o 0 10 0 162.17 152.49 8.14 o -5 11 0 163.65 162.90 2.90 o -4 11 0 304.25 290.68 4.38 o -3 11 0 46.78 45.91 2.33 o -2 11 0 28.98 31.24 3.12 o -1 11 0 410.91 417.60 7.02 o 0 11 0 127.33 104.38 6.72 o -6 12 0 188.74 202.54 6.04 o -5 12 0 159.61 158.21 3.80 o -4 12 0 17.53 16.17 2.63 o -3 12 0 322.69 330.73 5.82 o 0 1 1 1015.24 910.03 2.96 o 0 2 1 1527.68 1621.19 5.88 o 1 2 1 6.39 5.96 0.27 o -1 3 1 3230.12 3299.46 12.05 o 0 3 1 192.85 197.77 1.11 o 1 3 1 521.09 481.40 2.51 o 2 3 1 433.54 423.16 2.54 o -1 4 1 1577.19 1601.85 6.52 o 0 4 1 632.45 615.81 3.04 o 1 4 1 0.43 0.27 0.31 o 2 4 1 589.04 566.46 3.24 o 3 4 1 386.23 384.26 2.63 o -2 5 1 476.91 489.84 3.14 o -1 5 1 167.66 185.61 1.48 o 0 5 1 2242.62 2235.98 9.29 o 1 5 1 478.77 475.19 2.89 o 2 5 1 255.54 268.81 2.29 o 3 5 1 50.77 50.76 1.20 o 4 5 1 81.11 89.77 1.87 o -2 6 1 15.57 21.26 0.71 o -1 6 1 550.86 540.91 3.19 o 0 6 1 8.75 9.59 0.52 o 1 6 1 6.59 5.21 0.65 o 2 6 1 3.67 3.16 0.67 o 3 6 1 72.44 67.23 1.85 o 4 6 1 55.15 56.96 1.94 o 5 6 1 157.41 167.55 3.21 o -3 7 1 43.57 41.69 1.01 o -2 7 1 117.07 118.05 1.50 o -1 7 1 51.29 45.60 1.06 o 0 7 1 92.90 71.15 1.36 o 1 7 1 54.37 50.56 1.33 o 2 7 1 102.21 99.93 1.93 o 3 7 1 38.94 41.98 2.03 o 4 7 1 2.66 3.58 1.50 o 5 7 1 1.83 0.53 1.61 o -3 8 1 65.50 60.77 1.51 o -2 8 1 41.53 35.86 1.21 o -1 8 1 95.54 83.26 1.74 o 0 8 1 2.51 3.09 0.92 o 1 8 1 55.32 51.72 1.59 o 2 8 1 11.16 10.83 1.49 o 3 8 1 38.18 40.65 2.23 o 4 8 1 46.03 52.25 3.02 o -4 9 1 102.63 99.27 1.93 o -3 9 1 2.88 2.79 1.05 o -2 9 1 329.22 344.71 3.94 o -1 9 1 144.78 136.92 2.62 o 0 9 1 37.80 37.44 1.96 o 1 9 1 100.33 106.18 3.07 o 2 9 1 24.47 25.37 2.57 o 3 9 1 4.43 6.38 2.58 o -4 10 1 133.11 148.76 2.54 o -3 10 1 20.25 22.51 1.59 o -2 10 1 3.03 -0.34 1.41 o -1 10 1 12.82 19.38 1.83 o 0 10 1 74.53 78.39 3.33 o 1 10 1 3.67 4.08 2.64 o -5 11 1 90.60 92.21 2.39 o -4 11 1 19.04 22.05 2.02 o -3 11 1 7.10 8.64 1.73 o -2 11 1 26.36 28.17 2.35 o -1 11 1 2.38 3.04 2.35 o 0 11 1 65.83 60.53 3.64 o -5 12 1 1.87 4.12 2.08 o -4 12 1 22.18 28.92 2.32 o -3 12 1 0.20 -0.21 2.45 o 0 0 2 18763.06 16714.30 211.92 o 0 1 2 1335.65 1356.19 4.44 o 1 1 2 1753.91 1793.30 9.93 o -1 2 2 10957.54 10450.58 128.65 o 0 2 2 2492.13 2536.57 10.28 o 1 2 2 347.27 328.10 1.80 o 2 2 2 1385.00 1310.33 7.77 o -1 3 2 2812.54 2778.39 11.85 o 0 3 2 2944.75 2823.22 11.89 o 1 3 2 226.88 197.78 1.38 o 2 3 2 545.01 499.72 2.79 o 3 3 2 3452.71 3391.89 20.90 o -2 4 2 10557.73 10736.06 61.72 o -1 4 2 1272.05 1231.66 5.80 o 0 4 2 890.98 880.80 4.56 o 1 4 2 2326.41 2293.82 9.47 o 2 4 2 453.46 443.77 2.67 o 3 4 2 947.61 943.94 4.61 o 4 4 2 1486.60 1490.54 11.37 o -2 5 2 58.27 46.33 0.73 o -1 5 2 1944.51 1858.55 9.63 o 0 5 2 811.86 816.28 4.71 o 1 5 2 824.98 855.66 4.81 o 2 5 2 1395.73 1408.36 6.85 o 3 5 2 336.28 324.82 2.99 o 4 5 2 30.85 31.49 1.40 o 5 5 2 727.94 723.70 9.11 o -3 6 2 1144.83 1141.78 9.03 o -2 6 2 995.96 1024.21 5.94 o -1 6 2 338.84 338.64 2.98 o 0 6 2 2089.20 2188.87 10.74 o 1 6 2 90.35 92.23 1.42 o 2 6 2 149.44 156.39 2.17 o 3 6 2 566.12 570.82 4.64 o 4 6 2 290.84 268.01 4.59 o 5 6 2 157.09 154.58 3.12 o 6 6 2 267.96 265.41 6.22 o -3 7 2 328.35 341.28 2.71 o -2 7 2 1401.61 1438.57 8.42 o -1 7 2 421.37 411.20 3.55 o 0 7 2 146.91 141.13 2.03 o 1 7 2 639.19 672.12 4.99 o 2 7 2 242.24 223.33 3.08 o 3 7 2 91.90 97.45 2.44 o 4 7 2 507.14 516.46 6.27 o 5 7 2 124.58 118.70 3.49 o -4 8 2 1527.08 1587.34 13.47 o -3 8 2 309.64 315.65 3.43 o -2 8 2 648.42 634.28 5.20 o -1 8 2 1625.41 1675.17 10.23 o 0 8 2 180.40 178.09 2.70 o 1 8 2 337.83 341.28 3.93 o 2 8 2 561.58 578.53 5.62 o 3 8 2 88.60 76.55 2.81 o 4 8 2 74.41 68.14 2.95 o -4 9 2 234.18 210.59 2.71 o -3 9 2 1097.67 1093.90 7.89 o -2 9 2 278.21 302.98 3.77 o -1 9 2 152.10 142.25 2.74 o 0 9 2 435.43 444.54 5.34 o 1 9 2 72.35 73.11 2.59 o 2 9 2 116.97 120.48 4.44 o 3 9 2 378.94 395.86 7.10 o -5 10 2 729.22 722.89 8.20 o -4 10 2 55.22 58.00 2.13 o -3 10 2 272.51 247.07 3.62 o -2 10 2 403.47 384.05 4.52 o -1 10 2 152.88 146.64 3.83 o 0 10 2 86.19 78.75 3.18 o 1 10 2 389.76 387.25 6.09 o -5 11 2 123.90 116.52 2.93 o -4 11 2 202.48 191.15 3.70 o -3 11 2 53.34 46.74 2.36 o -2 11 2 0.67 1.30 1.71 o -1 11 2 238.99 240.62 5.13 o -6 12 2 263.67 283.88 7.19 o -5 12 2 63.25 63.73 2.86 o -4 12 2 56.21 55.12 3.58 o -3 12 2 248.21 256.17 5.99 o 0 1 3 10.89 14.42 0.32 o 0 2 3 1263.60 1352.67 6.02 o 1 2 3 217.50 222.73 1.54 o -1 3 3 2754.16 3030.33 12.58 o 0 3 3 97.54 108.33 1.34 o 1 3 3 338.11 365.24 2.25 o 2 3 3 382.32 379.16 2.29 o -1 4 3 731.60 839.54 4.49 o 0 4 3 13.58 12.05 0.65 o 1 4 3 8.88 10.21 0.63 o 2 4 3 479.60 496.71 2.97 o 3 4 3 584.17 595.51 3.66 o -2 5 3 316.45 368.14 2.69 o -1 5 3 14.61 19.68 0.63 o 0 5 3 11.52 15.85 0.78 o 1 5 3 56.08 61.19 1.30 o 2 5 3 1.63 0.68 0.51 o 3 5 3 85.54 80.33 1.56 o 4 5 3 41.93 45.64 1.65 o -2 6 3 4.34 3.98 0.66 o -1 6 3 57.27 55.96 1.43 o 0 6 3 1.90 3.31 0.72 o 1 6 3 84.29 75.87 2.03 o 2 6 3 120.56 114.49 2.04 o 3 6 3 67.68 79.39 1.88 o 4 6 3 15.79 14.58 1.45 o 5 6 3 33.72 37.90 2.25 o -3 7 3 174.07 178.11 2.52 o -2 7 3 20.07 14.06 1.05 o -1 7 3 262.92 258.54 3.00 o 0 7 3 110.09 113.01 2.10 o 1 7 3 27.11 20.55 1.28 o 2 7 3 42.29 33.60 1.73 o 3 7 3 50.30 50.72 2.18 o 4 7 3 2.91 3.07 1.80 o 5 7 3 45.34 46.66 2.69 o -3 8 3 79.19 76.09 1.93 o -2 8 3 288.65 273.47 3.37 o -1 8 3 2.81 2.97 1.18 o 0 8 3 187.69 196.07 3.06 o 1 8 3 24.85 24.51 1.56 o 2 8 3 1.87 1.46 1.50 o 3 8 3 46.13 44.41 2.62 o 4 8 3 40.91 35.67 3.19 o -4 9 3 64.82 54.76 1.84 o -3 9 3 2.16 2.77 1.15 o -2 9 3 167.92 199.45 3.25 o -1 9 3 87.54 91.42 2.43 o 0 9 3 1.40 0.98 1.38 o 1 9 3 46.91 43.39 2.25 o 2 9 3 26.48 23.65 2.33 o 3 9 3 0.38 -0.98 2.41 o -4 10 3 38.05 40.73 1.86 o -3 10 3 31.20 32.77 2.02 o -2 10 3 18.51 12.58 1.70 o -1 10 3 1.75 -1.07 1.53 o 0 10 3 18.06 20.46 2.17 o 1 10 3 0.01 -1.96 2.23 o -5 11 3 15.37 16.66 2.00 o -4 11 3 7.06 9.92 1.97 o -3 11 3 18.79 23.46 2.15 o -2 11 3 36.24 40.08 2.35 o -1 11 3 4.32 0.47 2.08 o -5 12 3 51.38 59.63 3.32 o -4 12 3 18.68 18.30 2.40 o -3 12 3 4.31 3.54 2.28 o 0 0 4 901.82 1016.95 10.92 o 0 1 4 494.28 468.54 2.45 o 1 1 4 4084.52 3984.34 19.07 o -1 2 4 4257.53 4098.88 22.08 o 0 2 4 424.76 402.51 2.25 o 1 2 4 1525.40 1495.91 6.67 o 2 2 4 3888.65 3794.86 20.96 o -1 3 4 1206.74 1160.87 5.67 o 0 3 4 4372.24 4259.07 18.08 o 1 3 4 814.73 803.48 4.38 o 2 3 4 970.33 941.49 4.72 o 3 3 4 2549.41 2547.63 14.17 o -2 4 4 3247.36 3210.40 24.03 o -1 4 4 601.05 573.41 3.85 o 0 4 4 380.02 343.75 2.97 o 1 4 4 1613.06 1625.72 8.25 o 2 4 4 570.52 576.58 3.49 o 3 4 4 252.85 260.54 2.49 o 4 4 4 766.97 764.36 7.51 o -2 5 4 857.70 816.87 4.96 o -1 5 4 1324.83 1272.29 7.10 o 0 5 4 192.74 179.80 2.15 o 1 5 4 120.61 118.56 1.80 o 2 5 4 1498.84 1517.56 8.05 o 3 5 4 430.34 414.65 3.62 o 4 5 4 116.49 119.04 2.17 o 5 5 4 240.98 247.12 4.96 o -3 6 4 2820.54 2915.87 17.69 o -2 6 4 588.31 599.87 4.18 o -1 6 4 228.71 234.90 2.56 o 0 6 4 860.33 876.48 5.68 o 1 6 4 350.12 319.83 4.05 o 2 6 4 138.48 149.90 2.31 o 3 6 4 634.55 643.07 5.73 o 4 6 4 79.47 69.65 2.29 o 5 6 4 107.67 113.17 4.20 o 6 6 4 322.22 322.16 8.67 o -3 7 4 247.08 264.98 3.30 o -2 7 4 1665.45 1687.27 10.17 o -1 7 4 397.89 367.12 3.62 o 0 7 4 770.97 767.80 5.68 o 1 7 4 939.41 974.01 6.74 o 2 7 4 158.97 136.82 3.01 o 3 7 4 64.78 75.89 2.50 o 4 7 4 448.01 468.14 5.62 o 5 7 4 35.31 32.11 3.00 o -4 8 4 994.83 1047.35 11.41 o -3 8 4 470.23 489.56 4.97 o -2 8 4 204.78 188.14 2.82 o -1 8 4 1081.97 1093.71 7.57 o 0 8 4 65.54 61.88 2.01 o 1 8 4 153.79 163.37 3.09 o 2 8 4 365.04 373.24 5.20 o 3 8 4 115.50 105.51 3.73 o 4 8 4 127.11 123.43 3.74 o -4 9 4 147.62 131.00 3.11 o -3 9 4 578.03 584.64 5.75 o -2 9 4 113.04 119.49 2.62 o -1 9 4 99.29 83.77 2.37 o 0 9 4 382.14 378.22 4.68 o 1 9 4 110.15 114.78 3.34 o 2 9 4 68.20 73.70 3.14 o -5 10 4 245.08 250.46 9.38 o -4 10 4 75.23 83.29 2.82 o -3 10 4 83.80 64.01 2.26 o -2 10 4 339.50 329.09 4.29 o -1 10 4 76.20 73.26 2.59 o 0 10 4 34.27 35.57 2.54 o 1 10 4 202.31 214.12 4.90 o -5 11 4 66.68 63.83 2.90 o -4 11 4 361.32 372.80 5.18 o -3 11 4 110.36 117.35 3.30 o -2 11 4 73.88 68.65 2.69 o -1 11 4 185.72 190.36 4.41 o -6 12 4 381.36 410.73 8.13 o -5 12 4 31.50 34.53 2.63 o -4 12 4 135.13 134.28 4.73 o 0 1 5 338.18 296.94 1.98 o 0 2 5 2298.43 2385.88 9.63 o 1 2 5 683.57 692.02 3.76 o -1 3 5 30.56 40.48 0.79 o 0 3 5 32.95 26.52 0.75 o 1 3 5 190.03 201.12 2.05 o 2 3 5 107.48 98.16 1.34 o -1 4 5 42.32 52.40 0.93 o 0 4 5 115.50 123.19 1.87 o 1 4 5 1.27 1.82 0.63 o 2 4 5 57.60 58.46 1.25 o 3 4 5 43.17 42.71 1.38 o -2 5 5 198.78 227.07 2.25 o -1 5 5 94.04 84.58 1.65 o 0 5 5 47.99 37.95 1.25 o 1 5 5 43.75 43.06 1.31 o 2 5 5 103.25 105.03 1.88 o 3 5 5 178.88 175.65 2.69 o 4 5 5 51.20 56.15 1.81 o -2 6 5 578.56 587.26 4.62 o -1 6 5 23.14 23.94 1.13 o 0 6 5 5.45 5.14 0.89 o 1 6 5 250.27 246.61 2.91 o 2 6 5 329.36 337.78 3.83 o 3 6 5 36.54 24.72 1.70 o 4 6 5 57.63 53.91 2.18 o 5 6 5 1.70 1.53 2.24 o -3 7 5 224.93 223.20 2.76 o -2 7 5 59.71 49.78 1.70 o -1 7 5 196.65 196.34 3.06 o 0 7 5 106.38 113.65 2.37 o 1 7 5 40.63 30.99 1.65 o 2 7 5 45.73 43.53 2.09 o 3 7 5 36.83 38.35 2.27 o 4 7 5 0.05 -0.04 1.85 o -3 8 5 67.02 61.92 1.89 o -2 8 5 134.29 119.59 2.55 o -1 8 5 29.67 30.80 1.68 o 0 8 5 180.62 179.06 3.07 o 1 8 5 43.68 46.37 2.28 o 2 8 5 6.07 6.89 1.96 o 3 8 5 12.96 10.31 2.33 o -4 9 5 47.77 38.48 2.06 o -3 9 5 1.44 2.49 1.30 o -2 9 5 2.08 0.49 1.37 o -1 9 5 13.16 12.66 1.69 o 0 9 5 22.69 18.07 2.13 o 1 9 5 6.17 3.81 2.09 o 2 9 5 18.66 14.63 2.52 o -4 10 5 7.89 8.93 2.23 o -3 10 5 70.25 67.56 2.85 o -2 10 5 0.17 2.45 1.67 o -1 10 5 39.36 42.93 2.60 o 0 10 5 6.55 7.58 2.40 o -5 11 5 12.30 13.02 2.38 o -4 11 5 15.79 13.81 2.28 o -3 11 5 78.18 82.69 3.27 o -2 11 5 31.06 36.41 2.74 o 0 0 6 69.25 63.82 2.41 o 0 1 6 681.27 684.80 3.66 o 1 1 6 3945.50 4090.14 23.61 o -1 2 6 1377.96 1422.19 9.07 o 0 2 6 172.19 168.98 1.61 o 1 2 6 952.19 980.30 4.95 o 2 2 6 2689.21 2730.17 17.82 o -1 3 6 168.51 169.00 1.62 o 0 3 6 2906.12 2997.92 13.10 o 1 3 6 1048.95 1091.64 6.06 o 2 3 6 767.34 784.64 4.87 o 3 3 6 839.80 872.18 8.39 o -2 4 6 263.55 271.05 3.09 o -1 4 6 362.24 350.31 2.82 o 0 4 6 281.62 293.82 2.63 o 1 4 6 1878.97 1969.93 10.20 o 2 4 6 271.99 269.10 3.02 o 3 4 6 44.59 47.77 1.47 o 4 4 6 395.19 401.27 5.69 o -2 5 6 1161.28 1148.49 6.53 o -1 5 6 1821.48 1879.40 10.51 o 0 5 6 179.09 177.56 2.52 o 1 5 6 109.11 103.22 1.93 o 2 5 6 1079.52 1125.54 7.92 o 3 5 6 143.48 127.06 2.57 o 4 5 6 393.01 403.92 4.64 o 5 5 6 270.92 265.96 6.26 o -3 6 6 2012.34 2051.13 15.31 o -2 6 6 127.80 124.59 2.33 o -1 6 6 337.40 346.32 3.71 o 0 6 6 618.85 614.24 5.11 o 1 6 6 491.83 468.50 4.53 o 2 6 6 187.16 194.49 3.08 o 3 6 6 682.29 707.93 6.13 o 4 6 6 33.66 24.72 2.14 o 5 6 6 43.17 40.01 3.81 o -3 7 6 194.20 192.39 2.87 o -2 7 6 1070.73 1064.18 7.86 o -1 7 6 238.63 230.93 3.42 o 0 7 6 421.88 416.27 4.50 o 1 7 6 712.88 716.83 6.77 o 2 7 6 74.40 63.47 2.49 o 3 7 6 90.14 95.96 3.15 o 4 7 6 279.41 281.39 5.80 o -4 8 6 497.70 530.73 8.15 o -3 8 6 175.21 174.91 3.45 o -2 8 6 36.19 31.43 1.76 o -1 8 6 296.73 282.84 3.87 o 0 8 6 121.12 120.43 3.03 o 1 8 6 23.37 25.27 2.41 o 2 8 6 280.81 301.43 5.15 o 3 8 6 88.35 84.13 4.00 o -4 9 6 197.75 201.06 3.90 o -3 9 6 362.63 374.88 5.06 o -2 9 6 33.24 32.91 1.93 o -1 9 6 65.15 56.66 2.72 o 0 9 6 448.63 467.11 6.03 o 1 9 6 117.72 112.33 3.65 o -5 10 6 300.02 322.08 7.12 o -4 10 6 170.46 181.77 3.93 o -3 10 6 39.91 39.49 2.62 o -2 10 6 391.50 403.55 5.80 o -1 10 6 39.86 40.49 2.97 o -5 11 6 37.05 34.29 2.79 o -4 11 6 476.74 509.98 7.36 o -3 11 6 122.31 117.37 3.86 o 0 1 7 589.99 523.20 3.22 o 0 2 7 506.11 477.92 3.07 o 1 2 7 99.44 96.42 1.47 o -1 3 7 40.22 38.93 1.11 o 0 3 7 128.71 116.33 1.65 o 1 3 7 59.19 54.91 1.26 o 2 3 7 38.66 32.00 1.23 o -1 4 7 33.32 31.11 1.05 o 0 4 7 566.88 555.90 4.34 o 1 4 7 2.68 2.57 0.81 o 2 4 7 81.21 75.98 1.72 o 3 4 7 12.31 9.57 1.24 o -2 5 7 120.03 115.32 1.80 o -1 5 7 50.77 48.24 1.65 o 0 5 7 79.81 75.72 1.94 o 1 5 7 124.66 107.95 2.39 o 2 5 7 21.34 20.00 1.49 o 3 5 7 133.52 134.22 2.95 o 4 5 7 78.76 79.72 2.42 o -2 6 7 576.06 575.30 5.09 o -1 6 7 126.07 127.93 2.58 o 0 6 7 0.33 1.34 1.20 o 1 6 7 135.03 138.17 2.80 o 2 6 7 86.93 83.79 2.45 o 3 6 7 100.23 94.34 2.75 o 4 6 7 69.59 68.57 3.18 o 5 6 7 3.66 3.93 2.81 o -3 7 7 23.23 23.69 1.48 o -2 7 7 10.19 8.18 1.33 o -1 7 7 42.57 46.21 2.00 o 0 7 7 59.03 62.07 2.34 o 1 7 7 0.26 0.66 1.60 o 2 7 7 9.66 6.66 1.85 o 3 7 7 30.09 26.73 2.48 o 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