#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:05 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180907 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104884.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104884_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9855 _cell_length_b 8.9855 _cell_length_c 9.6043 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7012 _cod_data_source_file bk51011esup6.hkl _cod_data_source_block 1e #BEGIN Tags that were not found in dictionaries: _shelx_title ' m104j' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3759.42 3835.73 14.63 o -1 2 0 5427.86 5736.06 30.84 o 0 2 0 5716.72 5758.52 25.99 o -1 3 0 390.85 411.58 2.06 o 0 3 0 1130.76 1132.39 6.78 o -2 4 0 3525.10 3603.67 22.47 o -1 4 0 690.51 674.16 3.48 o 0 4 0 1246.31 1285.22 7.82 o -2 5 0 19.06 13.59 0.53 o -1 5 0 3460.35 3425.79 14.37 o 0 5 0 1790.54 1857.93 12.23 o -3 6 0 1201.81 1193.78 9.61 o -2 6 0 534.69 528.15 3.24 o -1 6 0 1176.77 1221.42 6.08 o 0 6 0 3395.58 3587.05 22.94 o -3 7 0 807.56 805.54 4.98 o -2 7 0 1092.37 1151.06 5.95 o -1 7 0 145.76 155.07 1.70 o 0 7 0 8.58 5.63 0.92 o -4 8 0 1600.95 1622.65 12.39 o -3 8 0 107.19 106.82 1.67 o -2 8 0 460.61 473.92 3.32 o -1 8 0 797.33 851.58 5.09 o 0 8 0 345.97 369.31 5.05 o -4 9 0 144.13 132.53 1.96 o -3 9 0 861.23 881.41 6.11 o -2 9 0 279.53 283.46 4.11 o -1 9 0 228.51 222.12 3.34 o 0 9 0 448.46 455.33 7.21 o -5 10 0 1177.21 1189.70 11.05 o -4 10 0 200.98 184.72 2.74 o -3 10 0 244.09 238.38 3.66 o -2 10 0 528.97 517.99 5.87 o -1 10 0 101.29 97.80 3.10 o 0 10 0 140.31 143.72 5.92 o -5 11 0 147.63 140.42 3.17 o -4 11 0 272.57 258.80 5.09 o -3 11 0 40.62 32.57 2.31 o -2 11 0 26.02 23.82 2.30 o -1 11 0 354.29 358.67 6.52 o 0 11 0 106.50 104.65 5.21 o -6 12 0 167.02 161.37 7.74 o -5 12 0 135.22 123.45 4.53 o -4 12 0 15.37 11.78 2.57 o -3 12 0 273.11 283.58 5.60 o 0 1 1 1016.65 908.80 3.08 o 0 2 1 1532.00 1620.84 6.00 o 1 2 1 6.51 5.54 0.29 o -1 3 1 3200.74 3237.41 12.31 o 0 3 1 183.97 186.33 1.20 o 1 3 1 505.26 468.46 2.41 o 2 3 1 409.49 401.41 2.59 o -1 4 1 1550.33 1571.14 6.62 o 0 4 1 608.13 600.55 2.96 o 1 4 1 0.57 0.83 0.32 o 2 4 1 559.78 531.33 3.27 o 3 4 1 362.04 357.17 2.62 o -2 5 1 468.47 482.68 3.07 o -1 5 1 162.98 181.31 1.43 o 0 5 1 2146.47 2148.70 9.07 o 1 5 1 458.18 457.74 2.88 o 2 5 1 241.15 249.97 2.24 o 3 5 1 48.99 48.99 1.20 o 4 5 1 73.37 80.98 1.62 o -2 6 1 14.34 19.77 0.66 o -1 6 1 533.10 520.01 3.08 o 0 6 1 7.47 8.13 0.52 o 1 6 1 7.00 6.10 0.62 o 2 6 1 3.46 2.77 0.62 o 3 6 1 65.49 62.36 1.47 o 4 6 1 49.45 54.62 1.97 o 5 6 1 138.61 142.25 3.98 o -3 7 1 41.37 43.33 1.08 o -2 7 1 109.29 114.19 1.49 o -1 7 1 48.52 42.22 0.97 o 0 7 1 85.98 66.97 1.22 o 1 7 1 50.14 46.31 1.26 o 2 7 1 91.58 88.78 2.35 o 3 7 1 36.64 38.48 1.96 o 4 7 1 2.31 0.58 1.66 o 5 7 1 1.43 0.80 2.58 o -3 8 1 63.12 60.57 1.32 o -2 8 1 36.79 30.32 1.30 o -1 8 1 85.89 76.11 1.66 o 0 8 1 2.35 4.22 0.89 o 1 8 1 50.18 46.97 1.82 o 2 8 1 10.05 6.98 1.52 o 3 8 1 32.27 30.40 2.13 o 4 8 1 37.69 38.28 3.13 o -4 9 1 92.12 92.62 1.81 o -3 9 1 2.39 3.95 0.99 o -2 9 1 295.29 312.94 3.51 o -1 9 1 130.11 122.13 2.58 o 0 9 1 32.67 35.05 2.03 o 1 9 1 86.17 83.67 2.91 o 2 9 1 21.44 23.02 2.30 o 3 9 1 3.39 4.49 2.57 o -4 10 1 118.64 132.35 3.20 o -3 10 1 19.45 22.26 1.59 o -2 10 1 2.40 2.45 1.59 o -1 10 1 11.22 17.76 1.94 o 0 10 1 62.54 65.52 3.55 o 1 10 1 2.69 2.41 2.23 o -5 11 1 77.47 82.35 2.31 o -4 11 1 16.85 19.59 2.12 o -3 11 1 5.74 5.62 1.91 o -2 11 1 22.43 24.65 2.71 o -1 11 1 2.40 0.21 2.17 o 0 11 1 55.04 53.06 3.07 o -5 12 1 1.55 -1.50 2.27 o -4 12 1 17.93 17.86 2.45 o -3 12 1 0.22 -1.06 2.86 o 0 0 2 18606.04 16312.96 219.45 o 0 1 2 1318.04 1353.11 4.61 o 1 1 2 1736.99 1762.35 9.78 o -1 2 2 10841.39 10173.08 106.44 o 0 2 2 2475.41 2500.87 11.08 o 1 2 2 346.31 326.04 1.81 o 2 2 2 1380.86 1281.66 7.94 o -1 3 2 2775.86 2734.72 11.83 o 0 3 2 2908.46 2780.49 12.48 o 1 3 2 216.71 187.58 1.32 o 2 3 2 534.43 489.87 2.97 o 3 3 2 3340.50 3278.51 19.62 o -2 4 2 10307.40 10317.20 56.26 o -1 4 2 1240.46 1200.26 6.02 o 0 4 2 876.85 869.54 4.64 o 1 4 2 2256.39 2255.74 9.26 o 2 4 2 437.36 426.31 2.74 o 3 4 2 902.50 905.81 4.61 o 4 4 2 1396.26 1410.31 10.62 o -2 5 2 58.90 49.04 0.74 o -1 5 2 1892.55 1795.27 9.69 o 0 5 2 784.03 782.10 4.68 o 1 5 2 790.52 822.92 4.81 o 2 5 2 1331.51 1361.91 6.69 o 3 5 2 314.46 307.09 2.49 o 4 5 2 29.16 29.01 1.20 o 5 5 2 647.55 645.36 8.72 o -3 6 2 1083.53 1086.73 9.68 o -2 6 2 953.21 975.32 6.08 o -1 6 2 318.56 317.99 2.91 o 0 6 2 1980.76 2087.53 10.50 o 1 6 2 88.06 91.08 1.43 o 2 6 2 138.46 147.10 2.00 o 3 6 2 517.08 527.35 4.32 o 4 6 2 260.09 239.05 3.37 o 5 6 2 137.17 129.50 3.77 o 6 6 2 232.45 228.38 7.34 o -3 7 2 308.85 325.74 2.80 o -2 7 2 1316.54 1349.76 8.46 o -1 7 2 393.01 391.04 3.53 o 0 7 2 137.64 131.53 2.01 o 1 7 2 593.08 630.96 4.75 o 2 7 2 218.14 205.14 3.11 o 3 7 2 81.88 86.40 2.15 o 4 7 2 440.12 448.75 6.66 o 5 7 2 105.96 97.50 4.19 o -4 8 2 1424.63 1473.73 12.03 o -3 8 2 287.83 294.82 3.30 o -2 8 2 593.32 585.21 5.30 o -1 8 2 1489.12 1540.37 9.17 o 0 8 2 166.82 169.16 2.55 o 1 8 2 302.15 309.43 3.64 o 2 8 2 495.36 505.93 5.34 o 3 8 2 76.05 67.50 2.47 o 4 8 2 63.54 63.10 3.80 o -4 9 2 214.75 194.04 3.07 o -3 9 2 1010.68 1010.44 7.13 o -2 9 2 255.91 272.71 3.38 o -1 9 2 141.79 133.61 2.48 o 0 9 2 392.08 391.97 5.04 o 1 9 2 62.75 55.67 2.31 o 2 9 2 100.97 96.72 3.21 o 3 9 2 320.62 338.85 6.39 o -5 10 2 657.48 661.97 8.33 o -4 10 2 51.47 56.02 2.18 o -3 10 2 242.99 221.32 3.51 o -2 10 2 363.99 352.42 4.39 o -1 10 2 134.12 128.21 3.34 o 0 10 2 74.74 70.33 2.85 o 1 10 2 334.70 336.20 5.17 o -5 11 2 110.60 102.99 3.33 o -4 11 2 182.53 175.70 3.78 o -3 11 2 47.29 45.74 2.62 o -2 11 2 0.63 1.16 2.00 o -1 11 2 205.72 200.94 5.05 o -6 12 2 225.78 230.53 6.69 o -5 12 2 54.42 55.24 2.87 o -4 12 2 47.70 48.22 3.11 o -3 12 2 210.72 209.36 5.30 o 0 1 3 11.02 13.80 0.32 o 0 2 3 1249.90 1340.86 6.04 o 1 2 3 219.63 223.75 1.49 o -1 3 3 2695.93 3005.54 13.00 o 0 3 3 97.13 106.41 1.39 o 1 3 3 331.14 356.55 2.18 o 2 3 3 365.29 364.44 2.41 o -1 4 3 716.57 827.24 4.72 o 0 4 3 14.25 13.08 0.66 o 1 4 3 8.37 9.56 0.63 o 2 4 3 449.38 461.29 3.01 o 3 4 3 542.22 550.95 3.50 o -2 5 3 306.24 361.77 2.84 o -1 5 3 14.57 18.01 0.65 o 0 5 3 11.41 16.28 0.79 o 1 5 3 51.87 57.56 1.28 o 2 5 3 1.77 1.59 0.55 o 3 5 3 75.88 77.14 1.52 o 4 5 3 39.22 42.57 1.66 o -2 6 3 3.82 3.12 0.77 o -1 6 3 55.36 55.53 1.47 o 0 6 3 1.62 2.09 0.72 o 1 6 3 76.05 69.06 1.41 o 2 6 3 110.41 107.35 1.91 o 3 6 3 60.25 68.23 1.78 o 4 6 3 14.59 15.50 1.56 o 5 6 3 30.13 29.95 2.19 o -3 7 3 163.87 169.36 2.35 o -2 7 3 17.51 14.31 1.05 o -1 7 3 241.19 242.35 2.96 o 0 7 3 100.69 101.48 2.03 o 1 7 3 23.96 19.28 1.22 o 2 7 3 38.56 36.13 1.57 o 3 7 3 43.78 44.56 1.81 o 4 7 3 2.40 0.49 1.95 o 5 7 3 38.05 35.39 3.24 o -3 8 3 74.76 72.42 1.80 o -2 8 3 265.05 253.34 3.15 o -1 8 3 2.79 4.42 1.13 o 0 8 3 170.43 178.29 3.19 o 1 8 3 21.98 25.83 1.82 o 2 8 3 1.70 -1.38 1.38 o 3 8 3 40.19 36.22 2.37 o 4 8 3 34.76 33.98 3.13 o -4 9 3 59.18 53.41 2.09 o -3 9 3 1.78 4.20 1.30 o -2 9 3 150.40 174.69 2.81 o -1 9 3 77.13 80.61 2.16 o 0 9 3 1.29 2.01 1.43 o 1 9 3 40.06 38.66 2.64 o 2 9 3 22.86 22.93 2.29 o 3 9 3 0.31 1.99 2.76 o -4 10 3 33.50 38.68 1.98 o -3 10 3 26.29 28.19 1.95 o -2 10 3 15.91 9.04 1.68 o -1 10 3 1.50 -0.82 1.64 o 0 10 3 15.82 12.94 2.20 o 1 10 3 0.00 -1.89 2.19 o -5 11 3 12.45 14.39 1.90 o -4 11 3 5.92 6.48 1.96 o -3 11 3 15.31 17.60 2.23 o -2 11 3 29.92 25.40 2.51 o -1 11 3 3.59 5.67 2.37 o -5 12 3 42.13 48.03 2.75 o -4 12 3 16.15 10.12 2.38 o -3 12 3 3.30 4.20 2.38 o 0 0 4 844.67 951.52 10.74 o 0 1 4 487.56 463.47 2.57 o 1 1 4 4026.00 3913.97 20.99 o -1 2 4 4187.61 4026.92 23.70 o 0 2 4 417.87 394.90 2.32 o 1 2 4 1485.66 1450.07 7.11 o 2 2 4 3725.59 3655.94 22.10 o -1 3 4 1181.91 1140.33 5.61 o 0 3 4 4227.34 4091.42 17.67 o 1 3 4 781.63 767.02 4.13 o 2 3 4 927.17 894.59 4.80 o 3 3 4 2447.82 2439.30 15.31 o -2 4 4 3147.41 3095.11 20.50 o -1 4 4 590.87 553.86 4.02 o 0 4 4 360.49 327.23 2.96 o 1 4 4 1544.40 1557.18 8.45 o 2 4 4 539.94 551.96 3.76 o 3 4 4 240.80 247.14 2.36 o 4 4 4 715.00 715.84 6.85 o -2 5 4 814.01 772.10 5.10 o -1 5 4 1275.39 1225.53 7.36 o 0 5 4 185.07 172.20 2.14 o 1 5 4 118.14 112.00 1.77 o 2 5 4 1402.33 1413.63 7.69 o 3 5 4 401.71 382.53 3.61 o 4 5 4 106.45 104.80 2.42 o 5 5 4 220.80 227.78 5.09 o -3 6 4 2660.99 2751.93 18.49 o -2 6 4 551.01 570.61 4.13 o -1 6 4 220.04 222.96 2.53 o 0 6 4 806.98 815.42 5.55 o 1 6 4 322.50 299.41 3.68 o 2 6 4 129.91 142.55 2.17 o 3 6 4 576.31 586.63 5.15 o 4 6 4 70.32 65.12 2.29 o 5 6 4 91.42 91.38 4.58 o 6 6 4 269.15 263.76 9.34 o -3 7 4 234.63 252.15 3.01 o -2 7 4 1552.54 1572.42 9.69 o -1 7 4 366.63 348.50 3.58 o 0 7 4 703.07 701.52 5.50 o 1 7 4 866.60 886.34 6.51 o 2 7 4 142.45 123.94 2.64 o 3 7 4 58.80 68.82 2.26 o 4 7 4 384.58 395.04 5.33 o 5 7 4 30.63 26.73 2.83 o -4 8 4 917.11 961.22 11.08 o -3 8 4 434.49 451.20 5.23 o -2 8 4 190.51 171.27 2.59 o -1 8 4 996.73 1001.03 7.03 o 0 8 4 59.35 52.12 1.79 o 1 8 4 136.95 142.71 2.68 o 2 8 4 319.69 331.20 4.33 o 3 8 4 100.59 91.97 3.40 o 4 8 4 106.77 114.85 4.32 o -4 9 4 134.21 122.72 2.92 o -3 9 4 526.81 522.61 5.92 o -2 9 4 103.54 110.15 2.63 o -1 9 4 89.53 78.69 2.18 o 0 9 4 340.27 333.47 4.03 o 1 9 4 98.32 94.58 2.90 o 2 9 4 58.02 56.83 3.24 o -5 10 4 224.02 228.55 5.69 o -4 10 4 66.30 75.06 2.63 o -3 10 4 74.08 58.57 2.35 o -2 10 4 296.45 280.58 4.09 o -1 10 4 69.57 64.58 2.48 o 0 10 4 29.71 23.84 2.58 o 1 10 4 171.85 174.81 4.71 o -5 11 4 57.72 58.87 2.54 o -4 11 4 313.47 324.17 4.77 o -3 11 4 96.32 94.12 2.99 o -2 11 4 63.41 55.31 2.83 o -1 11 4 158.87 162.83 4.69 o -6 12 4 320.37 343.99 7.00 o -5 12 4 28.13 31.31 2.40 o -4 12 4 113.33 116.17 5.07 o 0 1 5 316.48 274.78 1.98 o 0 2 5 2227.13 2306.21 9.75 o 1 2 5 671.96 683.62 4.08 o -1 3 5 30.47 40.71 0.85 o 0 3 5 28.64 22.64 0.74 o 1 3 5 187.65 195.13 2.05 o 2 3 5 107.89 99.58 1.36 o -1 4 5 40.96 51.12 0.96 o 0 4 5 113.11 117.18 1.86 o 1 4 5 1.37 2.13 0.62 o 2 4 5 55.63 54.67 1.14 o 3 4 5 41.29 42.96 1.28 o -2 5 5 189.27 213.62 2.34 o -1 5 5 85.19 75.24 1.60 o 0 5 5 42.67 29.22 1.16 o 1 5 5 39.84 40.49 1.37 o 2 5 5 94.56 97.77 1.83 o 3 5 5 155.15 159.39 2.49 o 4 5 5 45.26 42.39 2.07 o -2 6 5 538.89 551.04 4.78 o -1 6 5 21.35 21.08 1.14 o 0 6 5 4.51 5.03 0.91 o 1 6 5 224.13 214.87 2.76 o 2 6 5 298.99 313.45 3.63 o 3 6 5 31.98 23.33 1.59 o 4 6 5 50.61 46.44 2.29 o 5 6 5 1.45 -0.04 2.00 o -3 7 5 210.84 210.33 2.99 o -2 7 5 53.41 45.85 1.55 o -1 7 5 178.86 176.24 2.81 o 0 7 5 97.41 106.79 2.25 o 1 7 5 36.05 30.77 1.58 o 2 7 5 41.59 39.22 1.86 o 3 7 5 30.26 31.32 2.28 o 4 7 5 0.05 -1.92 1.92 o -3 8 5 59.71 58.16 2.10 o -2 8 5 125.52 111.31 2.71 o -1 8 5 25.86 25.35 1.53 o 0 8 5 159.21 156.05 2.81 o 1 8 5 37.50 42.90 2.00 o 2 8 5 5.41 4.51 1.71 o 3 8 5 11.72 10.48 2.32 o -4 9 5 42.80 42.36 2.17 o -3 9 5 1.19 -0.55 1.48 o -2 9 5 1.79 1.45 1.50 o -1 9 5 11.04 11.21 1.73 o 0 9 5 19.02 14.91 1.97 o 1 9 5 5.21 0.24 1.83 o 2 9 5 15.61 6.78 2.55 o -4 10 5 7.16 11.44 1.94 o -3 10 5 57.16 54.03 2.55 o -2 10 5 0.09 -0.23 1.72 o -1 10 5 32.87 36.68 2.49 o 0 10 5 5.96 4.34 2.45 o -5 11 5 10.67 8.62 2.11 o -4 11 5 13.20 9.15 2.12 o -3 11 5 66.20 67.17 3.57 o -2 11 5 25.97 22.96 2.67 o 0 0 6 80.06 74.61 3.91 o 0 1 6 665.67 664.91 3.91 o 1 1 6 3822.42 3962.32 23.90 o -1 2 6 1345.78 1398.90 9.28 o 0 2 6 167.65 163.17 1.63 o 1 2 6 914.99 939.20 5.19 o 2 2 6 2535.19 2622.13 18.94 o -1 3 6 165.53 167.82 1.65 o 0 3 6 2761.36 2837.15 13.35 o 1 3 6 995.50 1028.40 6.20 o 2 3 6 704.35 713.94 4.78 o 3 3 6 781.84 827.17 7.69 o -2 4 6 262.56 268.05 3.38 o -1 4 6 347.55 333.68 2.82 o 0 4 6 263.75 272.27 2.54 o 1 4 6 1747.10 1836.68 9.60 o 2 4 6 251.33 254.55 3.04 o 3 4 6 42.20 44.09 1.54 o 4 4 6 359.06 365.33 6.24 o -2 5 6 1077.94 1073.96 6.15 o -1 5 6 1706.93 1738.19 10.21 o 0 5 6 167.34 169.71 2.57 o 1 5 6 103.36 101.36 1.95 o 2 5 6 986.38 1027.06 7.37 o 3 5 6 132.17 118.83 2.61 o 4 5 6 345.97 354.35 4.75 o 5 5 6 244.92 248.46 6.10 o -3 6 6 1900.91 1935.99 16.39 o -2 6 6 121.55 118.39 2.17 o -1 6 6 318.18 325.29 3.50 o 0 6 6 572.56 587.55 5.05 o 1 6 6 440.95 423.03 4.13 o 2 6 6 173.31 176.41 2.87 o 3 6 6 608.98 621.78 6.25 o 4 6 6 29.28 25.94 2.32 o 5 6 6 37.13 33.34 2.80 o -3 7 6 181.56 180.37 3.05 o -2 7 6 984.51 987.98 7.69 o -1 7 6 217.79 215.05 3.21 o 0 7 6 379.78 384.10 4.23 o 1 7 6 646.35 651.02 5.87 o 2 7 6 67.24 57.29 2.24 o 3 7 6 79.70 88.50 3.32 o 4 7 6 239.54 258.73 4.92 o -4 8 6 451.17 486.03 7.97 o -3 8 6 161.53 166.75 3.38 o -2 8 6 34.33 31.56 1.93 o -1 8 6 272.36 265.80 4.02 o 0 8 6 104.23 100.25 2.65 o 1 8 6 21.06 19.42 1.87 o 2 8 6 243.08 242.95 4.96 o 3 8 6 76.88 79.15 3.50 o -4 9 6 173.42 172.06 3.68 o -3 9 6 320.22 343.01 5.13 o -2 9 6 29.62 30.54 2.12 o -1 9 6 55.82 49.27 2.59 o 0 9 6 384.57 400.34 5.51 o 1 9 6 103.36 105.56 3.36 o -5 10 6 267.08 310.09 7.02 o -4 10 6 145.73 156.36 3.75 o -3 10 6 35.35 31.78 2.40 o -2 10 6 333.45 358.62 5.34 o -1 10 6 35.54 35.79 2.61 o -5 11 6 31.80 29.56 2.61 o -4 11 6 402.94 433.25 5.87 o -3 11 6 103.86 98.23 3.37 o 0 1 7 551.49 487.40 3.16 o 0 2 7 475.21 439.27 3.05 o 1 2 7 100.46 95.49 1.53 o -1 3 7 38.57 37.59 0.98 o 0 3 7 114.92 109.28 1.63 o 1 3 7 60.69 56.52 1.27 o 2 3 7 39.70 34.18 1.21 o -1 4 7 31.03 29.37 0.98 o 0 4 7 525.20 519.47 4.06 o 1 4 7 2.16 1.17 0.94 o 2 4 7 74.99 65.91 1.77 o 3 4 7 10.28 9.18 1.26 o -2 5 7 110.10 100.83 1.65 o -1 5 7 48.29 49.77 1.55 o 0 5 7 77.30 73.72 1.96 o 1 5 7 114.83 104.58 2.29 o 2 5 7 18.58 18.88 1.44 o 3 5 7 116.85 117.44 2.84 o 4 5 7 67.41 64.82 2.51 o -2 6 7 522.10 513.59 4.62 o -1 6 7 113.25 109.84 2.32 o 0 6 7 0.39 0.51 1.13 o 1 6 7 120.53 122.59 2.51 o 2 6 7 79.00 79.28 2.26 o 3 6 7 85.58 80.26 2.73 o 4 6 7 59.23 55.60 2.84 o 5 6 7 3.02 7.08 2.53 o -3 7 7 21.91 24.19 1.83 o -2 7 7 8.96 6.94 1.48 o -1 7 7 38.49 36.78 1.87 o 0 7 7 53.70 57.54 2.04 o 1 7 7 0.25 0.09 1.50 o 2 7 7 8.82 9.59 2.14 o 3 7 7 24.62 21.19 2.51 o -3 8 7 65.29 67.68 2.65 o -2 8 7 13.76 10.93 1.95 o -1 8 7 0.21 -1.61 1.67 o 0 8 7 12.63 9.27 1.91 o 1 8 7 32.17 37.03 2.34 o 2 8 7 0.32 0.76 2.28 o -4 9 7 48.85 45.92 2.51 o -3 9 7 5.30 5.26 1.98 o -2 9 7 6.86 4.19 1.93 o -1 9 7 8.11 9.88 2.20 o 0 9 7 21.82 25.56 2.37 o 1 9 7 21.29 20.69 3.19 o -4 10 7 29.61 27.46 2.55 o -3 10 7 48.37 47.43 2.68 o -2 10 7 9.02 6.21 2.48 o -1 10 7 85.62 83.96 3.53 o -5 11 7 12.39 5.84 2.41 o 0 0 8 2337.66 2472.38 31.87 o 0 1 8 626.80 642.41 4.00 o 1 1 8 1555.62 1626.18 11.10 o -1 2 8 1241.53 1271.75 9.18 o 0 2 8 212.61 225.27 2.17 o 1 2 8 162.35 164.37 1.98 o 2 2 8 581.90 619.93 6.27 o -1 3 8 139.07 138.32 1.87 o 0 3 8 1218.94 1266.25 7.10 o 1 3 8 366.84 379.03 3.65 o 2 3 8 401.39 403.50 4.41 o 3 3 8 510.23 549.96 7.61 o -2 4 8 375.32 407.99 4.52 o -1 4 8 326.07 330.51 2.97 o 0 4 8 254.57 266.14 3.09 o 1 4 8 1305.92 1339.75 8.87 o 2 4 8 74.73 74.97 2.01 o 3 4 8 72.28 67.49 2.38 o 4 4 8 332.07 346.38 6.59 o -2 5 8 380.92 384.56 4.02 o -1 5 8 1319.45 1370.79 8.73 o 0 5 8 197.49 200.16 3.01 o 1 5 8 245.01 243.81 3.27 o 2 5 8 512.39 526.83 4.88 o 3 5 8 40.65 42.47 2.29 o 4 5 8 219.17 207.65 3.96 o 5 5 8 309.09 316.35 7.46 o -3 6 8 416.40 410.14 7.23 o -2 6 8 57.37 53.99 2.18 o -1 6 8 181.88 176.04 2.91 o 0 6 8 542.54 561.20 5.16 o 1 6 8 182.81 185.98 3.13 o 2 6 8 83.56 79.18 2.60 o 3 6 8 319.25 316.41 4.95 o 4 6 8 83.74 83.92 3.35 o -3 7 8 88.93 82.05 2.71 o -2 7 8 466.19 470.25 5.51 o -1 7 8 147.02 146.20 3.24 o 0 7 8 72.07 70.52 3.16 o 1 7 8 231.70 229.71 3.93 o 2 7 8 32.85 36.08 2.55 o 3 7 8 52.87 46.32 2.99 o -4 8 8 305.61 305.43 6.86 o -3 8 8 34.71 35.52 2.42 o -2 8 8 70.12 76.15 2.90 o -1 8 8 182.63 189.85 4.09 o 0 8 8 138.88 132.51 3.59 o 1 8 8 19.21 16.04 2.63 o -4 9 8 213.99 226.55 4.49 o -3 9 8 376.31 409.42 6.26 o -2 9 8 40.05 37.11 2.71 o -1 9 8 43.32 50.32 2.91 o 0 9 8 331.84 361.21 6.44 o -5 10 8 320.96 343.14 11.41 o -4 10 8 89.68 80.31 3.58 o -3 10 8 52.23 59.30 3.21 o 0 1 9 188.85 188.80 2.13 o 0 2 9 43.36 37.35 1.34 o 1 2 9 4.52 2.78 0.81 o -1 3 9 92.58 84.15 1.50 o 0 3 9 20.61 18.46 1.05 o 1 3 9 19.51 23.09 1.21 o 2 3 9 48.26 53.69 1.87 o -1 4 9 114.56 114.24 2.04 o 0 4 9 226.21 211.75 3.01 o 1 4 9 15.60 15.67 1.48 o 2 4 9 154.96 158.08 2.95 o 3 4 9 27.63 32.37 2.18 o -2 5 9 65.31 59.59 2.15 o -1 5 9 6.45 4.77 1.26 o 0 5 9 130.49 136.47 2.78 o 1 5 9 77.43 68.48 2.21 o 2 5 9 1.42 5.76 1.75 o 3 5 9 25.81 26.30 2.20 o 4 5 9 36.40 36.97 2.55 o -2 6 9 24.83 23.22 1.91 o -1 6 9 109.24 106.12 2.85 o 0 6 9 1.45 -0.43 1.39 o 1 6 9 25.65 25.98 1.78 o 2 6 9 1.43 2.93 2.01 o 3 6 9 0.13 0.14 2.13 o -3 7 9 1.58 3.07 1.75 o -2 7 9 0.76 2.32 1.91 o -1 7 9 18.55 18.28 2.15 o 0 7 9 21.71 17.42 2.25 o 1 7 9 3.03 -2.04 2.36 o 2 7 9 1.03 -0.55 2.42 o -3 8 9 59.09 59.95 2.74 o -2 8 9 17.59 21.77 2.47 o -1 8 9 0.85 0.76 2.20 o 0 8 9 3.26 5.05 2.41 o -4 9 9 26.79 29.45 2.70 o -3 9 9 13.80 10.11 2.33 o -2 9 9 18.67 15.05 2.63 o 0 0 10 1142.64 1196.66 16.16 o 0 1 10 202.16 192.81 2.30 o 1 1 10 485.54 473.82 5.16 o -1 2 10 1031.06 1027.18 8.43 o 0 2 10 205.82 208.69 2.53 o 1 2 10 83.31 71.78 1.75 o 2 2 10 307.65 300.45 4.89 o -1 3 10 294.91 286.82 2.99 o 0 3 10 600.00 580.90 4.59 o 1 3 10 51.23 47.53 1.82 o 2 3 10 143.26 125.51 2.85 o 3 3 10 552.61 572.20 8.43 o -2 4 10 1056.36 1109.73 12.41 o -1 4 10 200.79 204.79 3.16 o 0 4 10 169.79 151.21 2.75 o 1 4 10 409.08 397.17 4.40 o 2 4 10 78.78 80.36 2.65 o 3 4 10 117.08 107.15 3.04 o 4 4 10 345.78 358.86 7.34 o -2 5 10 66.33 61.07 2.43 o -1 5 10 424.51 417.23 5.10 o 0 5 10 93.43 99.52 2.75 o 1 5 10 150.85 143.77 3.08 o 2 5 10 273.35 277.31 4.56 o 3 5 10 70.51 75.67 2.91 o -3 6 10 157.74 156.30 5.11 o -2 6 10 115.77 119.33 3.33 o -1 6 10 41.35 36.85 2.30 o 0 6 10 345.19 349.55 5.09 o 1 6 10 34.80 40.15 2.97 o 2 6 10 31.60 29.68 2.70 o -3 7 10 56.00 54.01 2.76 o -2 7 10 285.78 285.78 4.91 o -1 7 10 83.50 81.20 3.18 o 0 7 10 48.72 49.87 2.92 o 1 7 10 143.92 136.83 4.58 o -4 8 10 288.72 291.76 7.34 o -3 8 10 54.23 52.72 2.84 o -2 8 10 105.13 113.95 3.58 o -1 8 10 287.67 290.19 5.17 o 0 1 11 10.64 12.97 1.19 o 0 2 11 16.84 17.82 1.31 o 1 2 11 36.57 44.00 1.73 o -1 3 11 195.49 202.55 2.90 o 0 3 11 10.90 13.35 1.50 o 1 3 11 41.14 50.05 1.99 o 2 3 11 59.31 65.39 2.40 o -1 4 11 77.96 85.64 2.79 o 0 4 11 1.96 -0.38 1.52 o 1 4 11 0.00 1.69 1.63 o 2 4 11 32.34 27.96 2.16 o 3 4 11 102.43 101.14 3.21 o -2 5 11 29.80 29.06 2.36 o -1 5 11 15.67 15.55 2.16 o 0 5 11 12.40 14.76 2.02 o 1 5 11 14.83 13.80 2.34 o 2 5 11 0.37 -2.12 2.12 o -2 6 11 4.57 5.90 2.21 o -1 6 11 18.88 18.84 2.32 o 0 6 11 0.31 4.05 2.34 o 1 6 11 10.38 9.71 2.68 o -3 7 11 28.33 30.48 2.71 o -2 7 11 0.01 0.59 2.41 o -1 7 11 24.30 26.34 2.80 o 0 0 12 277.32 296.93 8.86 o 0 1 12 40.69 33.03 1.67 o 1 1 12 312.63 307.10 5.62 o -1 2 12 359.71 349.72 5.94 o 0 2 12 132.51 132.23 3.03 o 1 2 12 137.79 126.25 2.81 o 2 2 12 518.79 535.38 8.82 o -1 3 12 156.32 140.37 3.15 o 0 3 12 303.36 292.21 4.11 o 1 3 12 40.14 39.81 2.37 o 2 3 12 25.03 19.61 2.17 o 3 3 12 253.33 253.10 5.95 o -2 4 12 599.89 627.82 9.72 o -1 4 12 45.19 45.91 2.71 o 0 4 12 78.38 68.21 2.81 o 1 4 12 113.68 111.58 3.39 o 2 4 12 97.51 93.84 3.10 o -2 5 12 28.57 27.29 2.60 o -1 5 12 126.85 124.65 3.64 o 0 5 12 41.86 46.74 3.18 o -3 6 12 278.42 288.43 7.22 o -2 6 12 101.88 103.11 3.70 o 0 1 13 11.20 8.13 1.83 o 0 2 13 7.60 6.36 1.99 o 1 2 13 112.44 107.70 3.27 o -1 3 13 22.54 23.12 2.49 o 0 3 13 9.30 7.47 2.17 o