#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104885.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104885_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9929 _cell_length_b 8.9929 _cell_length_c 9.6101 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7004 _[local]_cod_data_source_file bk51011fsup7.hkl _[local]_cod_data_source_block 1f #BEGIN Tags that were not found in dictionaries: _shelx_title ' m104i' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3763.38 3751.28 15.01 o -1 2 0 5398.38 5608.97 34.98 o 0 2 0 5681.24 5636.08 26.50 o -1 3 0 389.28 414.68 2.07 o 0 3 0 1130.03 1128.95 5.99 o -2 4 0 3503.67 3569.94 22.23 o -1 4 0 676.12 660.21 3.42 o 0 4 0 1236.65 1286.12 7.84 o -2 5 0 20.67 15.21 0.57 o -1 5 0 3381.88 3341.86 14.07 o 0 5 0 1732.09 1783.50 11.79 o -3 6 0 1166.72 1159.73 9.34 o -2 6 0 520.38 514.70 3.17 o -1 6 0 1124.65 1163.86 5.84 o 0 6 0 3236.08 3422.17 23.31 o -3 7 0 764.97 768.17 4.79 o -2 7 0 1039.17 1100.48 6.49 o -1 7 0 139.22 151.32 1.68 o 0 7 0 7.82 5.78 1.03 o -4 8 0 1494.20 1540.54 11.85 o -3 8 0 99.96 102.15 1.64 o -2 8 0 423.70 438.08 3.15 o -1 8 0 730.78 786.19 4.81 o 0 8 0 316.16 333.19 4.80 o -4 9 0 132.77 123.13 1.93 o -3 9 0 791.11 820.40 5.81 o -2 9 0 255.33 264.09 3.37 o -1 9 0 207.56 199.61 3.17 o 0 9 0 403.25 407.01 6.80 o -5 10 0 1056.39 1055.46 10.14 o -4 10 0 181.57 171.93 2.64 o -3 10 0 219.93 211.05 3.54 o -2 10 0 475.18 459.43 5.26 o -1 10 0 87.45 81.54 2.94 o 0 10 0 124.36 113.68 4.91 o -5 11 0 132.09 133.70 3.05 o -4 11 0 244.32 236.44 4.37 o -3 11 0 36.07 33.33 2.31 o -2 11 0 23.56 23.21 2.29 o -1 11 0 306.60 304.43 5.77 o 0 11 0 89.21 78.73 5.19 o -6 12 0 146.28 153.04 7.50 o -5 12 0 115.28 112.83 4.37 o -4 12 0 13.52 12.23 2.57 o -3 12 0 233.32 236.27 6.95 o 0 1 1 1019.02 914.50 3.05 o 0 2 1 1535.93 1622.31 6.02 o 1 2 1 6.28 5.93 0.26 o -1 3 1 3167.28 3190.42 12.12 o 0 3 1 174.34 176.91 1.08 o 1 3 1 493.37 453.80 2.34 o 2 3 1 396.92 390.28 2.54 o -1 4 1 1517.49 1547.61 6.52 o 0 4 1 591.67 588.09 2.90 o 1 4 1 0.58 0.45 0.31 o 2 4 1 537.45 511.01 3.19 o 3 4 1 343.62 332.53 2.50 o -2 5 1 460.90 487.05 3.06 o -1 5 1 157.15 179.01 1.41 o 0 5 1 2072.13 2057.14 9.24 o 1 5 1 444.99 439.72 2.80 o 2 5 1 228.07 233.72 2.09 o 3 5 1 48.04 45.47 1.13 o 4 5 1 69.06 72.94 1.53 o -2 6 1 12.71 16.73 0.75 o -1 6 1 511.09 497.86 2.97 o 0 6 1 6.42 6.44 0.51 o 1 6 1 7.29 6.17 0.63 o 2 6 1 3.02 2.24 0.62 o 3 6 1 59.43 57.40 1.56 o 4 6 1 47.31 54.50 1.96 o 5 6 1 125.06 131.21 4.07 o -3 7 1 40.32 39.09 1.02 o -2 7 1 103.88 105.73 1.42 o -1 7 1 47.94 43.21 0.97 o 0 7 1 81.15 60.23 1.16 o 1 7 1 46.79 43.34 1.24 o 2 7 1 85.54 81.68 1.90 o 3 7 1 36.42 37.94 1.95 o 4 7 1 2.14 1.86 1.72 o 5 7 1 1.12 0.86 2.58 o -3 8 1 61.24 57.73 1.30 o -2 8 1 35.41 29.87 1.26 o -1 8 1 78.03 68.47 1.53 o 0 8 1 2.32 1.63 0.87 o 1 8 1 47.67 46.03 1.86 o 2 8 1 8.59 7.31 1.48 o 3 8 1 29.28 27.53 2.04 o 4 8 1 32.44 33.90 3.16 o -4 9 1 87.08 85.30 1.75 o -3 9 1 2.01 3.05 0.97 o -2 9 1 270.97 289.49 3.37 o -1 9 1 120.81 116.96 2.54 o 0 9 1 28.40 32.82 2.14 o 1 9 1 77.81 82.71 2.79 o 2 9 1 19.88 15.06 2.29 o 3 9 1 2.64 0.17 2.50 o -4 10 1 108.93 118.86 2.49 o -3 10 1 19.06 22.84 1.42 o -2 10 1 2.07 -1.41 1.43 o -1 10 1 10.61 10.22 1.80 o 0 10 1 55.28 54.88 2.69 o 1 10 1 2.12 3.14 2.20 o -5 11 1 68.02 71.08 2.21 o -4 11 1 14.45 14.68 2.03 o -3 11 1 5.27 8.97 2.37 o -2 11 1 20.03 20.14 2.85 o -1 11 1 2.06 2.14 2.11 o 0 11 1 47.26 47.58 3.00 o -5 12 1 1.30 -0.85 2.12 o -4 12 1 15.56 14.71 2.40 o -3 12 1 0.23 -0.16 2.48 o 0 0 2 18672.67 15697.56 165.74 o 0 1 2 1316.10 1357.22 4.64 o 1 1 2 1729.15 1753.55 9.71 o -1 2 2 10761.37 9983.65 109.93 o 0 2 2 2459.52 2473.05 10.99 o 1 2 2 343.44 331.07 1.82 o 2 2 2 1365.78 1289.24 7.98 o -1 3 2 2734.09 2707.51 11.73 o 0 3 2 2854.56 2754.03 12.39 o 1 3 2 209.64 181.11 1.28 o 2 3 2 522.10 483.32 2.93 o 3 3 2 3228.69 3155.54 19.02 o -2 4 2 10065.66 9986.18 54.40 o -1 4 2 1212.04 1173.85 5.91 o 0 4 2 855.88 847.08 4.55 o 1 4 2 2202.71 2200.23 9.07 o 2 4 2 426.14 419.23 2.70 o 3 4 2 861.14 865.64 4.45 o 4 4 2 1305.45 1308.55 10.02 o -2 5 2 56.74 48.34 0.73 o -1 5 2 1824.55 1753.59 9.46 o 0 5 2 758.51 750.12 4.54 o 1 5 2 759.88 795.43 4.07 o 2 5 2 1273.28 1311.14 6.49 o 3 5 2 291.63 286.61 2.51 o 4 5 2 26.56 29.68 1.18 o 5 5 2 576.01 602.51 8.34 o -3 6 2 1037.96 1030.01 8.54 o -2 6 2 908.37 937.31 5.91 o -1 6 2 303.97 300.76 2.81 o 0 6 2 1887.77 2001.15 10.10 o 1 6 2 87.01 90.01 1.60 o 2 6 2 128.63 134.30 1.94 o 3 6 2 472.01 488.07 4.11 o 4 6 2 231.72 216.17 3.30 o 5 6 2 121.64 111.32 3.49 o 6 6 2 203.15 203.88 7.90 o -3 7 2 293.42 304.46 2.67 o -2 7 2 1243.19 1284.41 7.93 o -1 7 2 367.50 369.05 3.40 o 0 7 2 127.65 121.41 1.93 o 1 7 2 548.18 575.27 4.48 o 2 7 2 199.44 186.16 2.74 o 3 7 2 73.63 83.32 2.15 o 4 7 2 385.95 403.79 6.72 o 5 7 2 90.51 83.59 4.02 o -4 8 2 1334.54 1397.84 11.52 o -3 8 2 269.97 274.03 3.15 o -2 8 2 551.99 534.24 4.57 o -1 8 2 1380.17 1416.72 8.58 o 0 8 2 154.16 150.70 2.41 o 1 8 2 270.36 278.24 3.69 o 2 8 2 440.46 450.19 5.12 o 3 8 2 65.60 60.14 2.40 o 4 8 2 55.39 55.70 3.66 o -4 9 2 199.97 180.60 2.97 o -3 9 2 934.16 939.98 6.76 o -2 9 2 233.11 246.63 3.38 o -1 9 2 131.18 118.71 2.35 o 0 9 2 352.16 358.11 4.60 o 1 9 2 54.74 49.14 2.22 o 2 9 2 88.15 89.33 3.25 o 3 9 2 272.40 275.89 6.01 o -5 10 2 600.26 589.64 7.81 o -4 10 2 47.41 45.37 1.98 o -3 10 2 219.57 200.60 3.35 o -2 10 2 326.81 305.95 4.31 o -1 10 2 118.15 112.99 2.97 o 0 10 2 65.42 61.97 2.76 o 1 10 2 289.23 283.59 4.73 o -5 11 2 97.14 95.12 2.55 o -4 11 2 163.33 161.94 3.63 o -3 11 2 42.42 40.17 2.59 o -2 11 2 0.60 -0.34 1.99 o -1 11 2 176.42 175.32 4.77 o 0 11 2 57.14 55.40 3.19 o -6 12 2 192.93 203.36 6.51 o -5 12 2 47.86 46.79 2.72 o -4 12 2 40.02 41.12 3.13 o -3 12 2 181.47 180.15 4.71 o 0 1 3 11.33 12.70 0.31 o 0 2 3 1219.79 1323.15 5.94 o 1 2 3 218.84 228.13 1.50 o -1 3 3 2672.85 2985.60 12.89 o 0 3 3 94.36 103.05 1.36 o 1 3 3 321.99 358.54 2.18 o 2 3 3 348.34 351.51 2.35 o -1 4 3 706.30 827.75 4.73 o 0 4 3 15.72 15.07 0.70 o 1 4 3 8.08 8.34 0.62 o 2 4 3 428.33 437.96 3.01 o 3 4 3 508.91 513.98 3.34 o -2 5 3 305.48 358.51 2.93 o -1 5 3 15.86 19.43 0.75 o 0 5 3 12.25 15.23 0.78 o 1 5 3 50.22 55.74 1.25 o 2 5 3 1.18 0.59 0.48 o 3 5 3 71.04 70.76 1.51 o 4 5 3 36.47 39.25 1.60 o -2 6 3 3.43 5.07 0.74 o -1 6 3 52.83 54.30 1.45 o 0 6 3 1.50 2.53 0.69 o 1 6 3 71.68 65.67 1.36 o 2 6 3 101.68 100.95 1.85 o 3 6 3 53.77 61.20 1.71 o 4 6 3 13.65 14.64 1.54 o 5 6 3 28.67 32.97 2.13 o -3 7 3 157.38 162.18 2.26 o -2 7 3 15.75 12.48 1.00 o -1 7 3 222.75 216.37 2.76 o 0 7 3 93.65 92.62 1.90 o 1 7 3 21.15 18.36 1.19 o 2 7 3 36.50 34.72 1.59 o 3 7 3 40.09 41.95 1.83 o 4 7 3 2.06 -0.26 1.91 o 5 7 3 33.74 34.32 3.44 o -3 8 3 69.63 67.01 1.73 o -2 8 3 245.13 232.47 3.00 o -1 8 3 2.68 5.07 1.12 o 0 8 3 155.17 161.18 2.65 o 1 8 3 20.14 21.89 1.56 o 2 8 3 1.45 -0.05 1.45 o 3 8 3 36.26 34.97 2.12 o 4 8 3 30.75 30.71 3.13 o -4 9 3 54.95 46.64 1.96 o -3 9 3 1.56 2.53 1.27 o -2 9 3 136.91 160.55 2.70 o -1 9 3 69.85 73.14 2.10 o 0 9 3 1.15 4.28 1.35 o 1 9 3 35.98 34.74 2.13 o 2 9 3 20.91 15.83 2.14 o 3 9 3 0.29 -2.77 2.77 o -4 10 3 30.68 35.82 1.96 o -3 10 3 22.35 22.45 1.84 o -2 10 3 13.83 7.37 1.65 o -1 10 3 1.31 -0.10 1.66 o 0 10 3 14.86 17.39 2.06 o 1 10 3 0.00 -1.94 2.07 o -5 11 3 10.95 10.66 1.78 o -4 11 3 4.91 7.65 1.80 o -3 11 3 13.63 15.33 2.14 o -2 11 3 26.16 29.14 2.53 o -1 11 3 3.05 4.25 2.34 o -5 12 3 35.61 38.39 2.74 o -4 12 3 15.10 13.11 2.76 o -3 12 3 2.48 2.19 2.35 o 0 0 4 795.32 894.46 10.20 o 0 1 4 476.82 454.09 2.53 o 1 1 4 3939.56 3814.69 20.58 o -1 2 4 4115.80 3969.32 23.43 o 0 2 4 411.15 386.79 2.29 o 1 2 4 1452.61 1403.95 6.91 o 2 2 4 3593.68 3490.49 21.17 o -1 3 4 1170.40 1122.38 5.51 o 0 3 4 4104.32 3957.18 17.10 o 1 3 4 745.83 735.76 3.98 o 2 3 4 881.76 855.58 4.64 o 3 3 4 2336.21 2333.15 14.76 o -2 4 4 3061.41 3002.72 19.27 o -1 4 4 572.25 535.74 3.92 o 0 4 4 351.64 317.27 2.90 o 1 4 4 1477.60 1489.36 7.97 o 2 4 4 510.60 512.19 3.35 o 3 4 4 230.02 237.30 2.30 o 4 4 4 675.67 658.76 6.45 o -2 5 4 763.87 735.99 4.92 o -1 5 4 1219.48 1181.70 7.14 o 0 5 4 179.62 166.20 2.10 o 1 5 4 115.64 113.04 1.77 o 2 5 4 1316.69 1337.58 7.37 o 3 5 4 375.62 356.58 3.45 o 4 5 4 96.38 96.64 2.18 o 5 5 4 201.81 200.01 4.79 o -3 6 4 2509.37 2626.79 17.73 o -2 6 4 521.12 534.86 3.97 o -1 6 4 205.39 211.39 2.45 o 0 6 4 762.15 774.48 5.87 o 1 6 4 303.29 279.61 3.03 o 2 6 4 122.24 133.07 2.12 o 3 6 4 525.47 531.19 4.83 o 4 6 4 63.95 54.39 2.39 o 5 6 4 78.73 78.96 2.82 o 6 6 4 230.24 238.69 8.80 o -3 7 4 223.21 240.09 2.91 o -2 7 4 1449.66 1472.86 9.05 o -1 7 4 341.78 328.51 3.44 o 0 7 4 642.33 640.91 5.19 o 1 7 4 805.43 817.43 6.14 o 2 7 4 129.43 113.35 2.54 o 3 7 4 52.69 65.11 2.18 o 4 7 4 330.50 343.87 4.93 o 5 7 4 26.84 25.91 3.12 o -4 8 4 853.67 885.30 10.51 o -3 8 4 405.44 416.37 4.98 o -2 8 4 178.13 163.57 2.51 o -1 8 4 927.14 931.79 6.70 o 0 8 4 54.54 50.23 1.77 o 1 8 4 124.36 130.98 2.59 o 2 8 4 282.14 292.00 4.03 o 3 8 4 86.56 81.30 3.24 o 4 8 4 90.34 88.19 3.68 o -4 9 4 123.15 113.42 3.30 o -3 9 4 484.56 476.94 5.63 o -2 9 4 94.73 99.89 2.50 o -1 9 4 82.70 77.03 2.17 o 0 9 4 303.21 297.31 3.81 o 1 9 4 85.99 77.38 3.34 o 2 9 4 49.45 52.93 2.60 o -5 10 4 207.63 204.71 5.38 o -4 10 4 58.55 66.02 2.50 o -3 10 4 66.74 50.82 2.26 o -2 10 4 259.52 255.66 3.91 o -1 10 4 63.28 59.50 2.35 o 0 10 4 25.56 23.43 2.64 o 1 10 4 147.23 144.35 4.16 o -5 11 4 50.50 52.59 2.46 o -4 11 4 272.17 280.73 4.48 o -3 11 4 83.07 85.37 2.94 o -2 11 4 53.66 49.69 2.97 o -1 11 4 134.97 139.47 4.44 o -6 12 4 269.79 288.37 6.53 o -5 12 4 25.40 27.04 2.41 o -4 12 4 95.10 93.61 3.68 o 0 1 5 299.75 259.83 1.90 o 0 2 5 2138.91 2220.96 9.45 o 1 2 5 655.92 678.73 4.03 o -1 3 5 31.58 40.52 0.85 o 0 3 5 23.92 19.19 0.66 o 1 3 5 184.21 197.58 2.06 o 2 3 5 107.75 102.03 1.27 o -1 4 5 41.89 50.25 0.87 o 0 4 5 109.61 114.70 2.02 o 1 4 5 1.24 1.84 0.67 o 2 4 5 52.84 54.29 1.35 o 3 4 5 39.98 40.80 1.22 o -2 5 5 178.77 203.13 2.29 o -1 5 5 77.52 69.31 1.53 o 0 5 5 36.26 28.39 1.14 o 1 5 5 36.46 37.50 1.24 o 2 5 5 86.10 87.43 1.72 o 3 5 5 136.04 137.93 2.35 o 4 5 5 41.77 41.32 1.96 o -2 6 5 505.73 517.84 4.17 o -1 6 5 20.74 21.90 1.10 o 0 6 5 4.07 4.37 0.89 o 1 6 5 204.06 201.59 2.67 o 2 6 5 269.18 284.43 3.44 o 3 6 5 27.53 19.42 1.56 o 4 6 5 44.08 42.70 2.21 o 5 6 5 1.14 -0.15 2.03 o -3 7 5 200.76 196.68 3.76 o -2 7 5 46.70 40.31 1.49 o -1 7 5 163.59 163.79 2.71 o 0 7 5 89.33 98.65 2.20 o 1 7 5 32.04 28.08 1.56 o 2 7 5 38.41 35.98 1.85 o 3 7 5 25.85 27.73 2.21 o 4 7 5 0.04 1.60 1.98 o -3 8 5 55.04 49.55 2.02 o -2 8 5 116.76 102.02 2.62 o -1 8 5 23.37 25.99 1.56 o 0 8 5 142.44 143.07 2.67 o 1 8 5 32.73 35.54 1.88 o 2 8 5 4.61 5.85 1.75 o 3 8 5 10.82 13.60 2.35 o -4 9 5 38.24 32.16 2.03 o -3 9 5 1.19 2.66 1.56 o -2 9 5 1.56 1.81 1.51 o -1 9 5 9.96 11.04 1.79 o 0 9 5 16.00 10.07 1.85 o 1 9 5 4.68 1.65 1.82 o 2 9 5 13.84 15.05 2.59 o -4 10 5 6.78 6.23 1.85 o -3 10 5 47.80 46.39 2.45 o -2 10 5 0.02 -0.83 1.70 o -1 10 5 28.02 29.41 2.95 o 0 10 5 5.92 5.71 2.47 o -5 11 5 9.99 4.83 2.02 o -4 11 5 10.89 10.11 2.15 o -3 11 5 56.75 62.02 2.96 o -2 11 5 22.94 23.72 2.92 o 0 0 6 85.40 82.86 3.50 o 0 1 6 643.34 652.01 3.65 o 1 1 6 3699.56 3804.82 23.08 o -1 2 6 1318.66 1374.88 9.14 o 0 2 6 167.48 166.40 1.69 o 1 2 6 878.69 898.63 5.00 o 2 2 6 2424.29 2486.19 18.04 o -1 3 6 166.33 166.17 1.63 o 0 3 6 2636.52 2681.41 12.68 o 1 3 6 947.69 982.53 5.96 o 2 3 6 652.51 666.37 4.75 o 3 3 6 742.74 780.88 7.36 o -2 4 6 262.09 263.43 3.33 o -1 4 6 330.73 327.35 2.75 o 0 4 6 248.03 261.43 2.46 o 1 4 6 1625.86 1715.68 9.07 o 2 4 6 237.61 237.17 2.70 o 3 4 6 39.40 42.02 1.53 o 4 4 6 334.95 337.74 6.03 o -2 5 6 996.11 1018.18 5.90 o -1 5 6 1601.50 1673.47 9.89 o 0 5 6 159.95 157.62 2.34 o 1 5 6 97.38 96.69 1.89 o 2 5 6 902.15 929.11 6.84 o 3 5 6 123.74 117.98 2.61 o 4 5 6 306.44 308.85 4.43 o 5 5 6 221.99 229.00 6.76 o -3 6 6 1769.48 1837.50 15.78 o -2 6 6 116.07 108.87 2.08 o -1 6 6 293.95 308.88 3.40 o 0 6 6 533.98 543.83 4.68 o 1 6 6 399.09 385.93 3.91 o 2 6 6 159.43 163.00 2.77 o 3 6 6 543.80 558.31 5.63 o 4 6 6 26.38 25.21 2.27 o 5 6 6 31.82 32.78 2.94 o -3 7 6 170.84 171.69 3.10 o -2 7 6 907.90 897.22 7.19 o -1 7 6 199.17 196.26 3.35 o 0 7 6 344.43 349.83 4.00 o 1 7 6 589.75 593.68 5.53 o 2 7 6 59.77 51.76 2.12 o 3 7 6 71.02 71.74 2.94 o 4 7 6 204.32 203.87 5.46 o -4 8 6 408.96 441.11 7.47 o -3 8 6 148.38 145.49 3.22 o -2 8 6 32.30 31.26 1.99 o -1 8 6 250.84 236.48 3.80 o 0 8 6 90.92 84.72 2.47 o 1 8 6 19.41 26.26 1.91 o 2 8 6 211.57 229.56 4.94 o 3 8 6 66.57 61.81 3.12 o -4 9 6 151.27 154.51 3.48 o -3 9 6 286.24 298.21 4.75 o -2 9 6 27.45 29.69 2.06 o -1 9 6 50.22 44.39 2.41 o 0 9 6 332.38 338.20 5.63 o 1 9 6 89.02 84.11 3.08 o -5 10 6 237.04 254.77 6.45 o -4 10 6 124.86 132.20 3.64 o -3 10 6 31.28 33.55 2.41 o -2 10 6 286.23 304.49 5.01 o -1 10 6 31.96 33.08 2.68 o 0 10 6 45.13 41.21 2.90 o -5 11 6 28.79 29.23 2.57 o -4 11 6 343.98 364.46 5.42 o -3 11 6 86.82 85.09 3.31 o 0 1 7 515.06 452.20 3.01 o 0 2 7 443.73 409.18 2.91 o 1 2 7 97.90 93.08 1.49 o -1 3 7 36.93 36.78 1.02 o 0 3 7 102.86 97.78 1.52 o 1 3 7 56.85 51.36 1.20 o 2 3 7 39.02 36.19 1.34 o -1 4 7 29.68 27.81 0.98 o 0 4 7 476.97 476.14 3.80 o 1 4 7 1.90 1.70 0.95 o 2 4 7 67.84 62.79 1.76 o 3 4 7 8.25 7.25 1.23 o -2 5 7 101.62 96.85 1.63 o -1 5 7 45.26 44.58 1.50 o 0 5 7 73.51 69.17 2.02 o 1 5 7 104.18 94.23 2.16 o 2 5 7 17.08 16.24 1.40 o 3 5 7 101.87 103.81 2.73 o 4 5 7 60.01 61.96 2.49 o -2 6 7 480.98 472.35 4.37 o -1 6 7 105.48 108.05 2.30 o 0 6 7 0.31 1.92 1.16 o 1 6 7 110.20 110.36 2.39 o 2 6 7 71.37 71.13 2.13 o 3 6 7 73.55 75.85 2.73 o 4 6 7 51.11 49.89 2.75 o 5 6 7 2.64 -1.71 2.42 o -3 7 7 21.59 20.78 1.75 o -2 7 7 7.50 7.70 1.48 o -1 7 7 35.35 35.82 1.84 o 0 7 7 48.98 49.86 1.95 o 1 7 7 0.26 0.86 1.47 o 2 7 7 8.22 6.30 1.96 o 3 7 7 20.99 20.27 2.48 o -3 8 7 57.94 57.58 2.47 o -2 8 7 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