#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:05 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180907 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104886.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104886_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9387 _cell_length_b 8.9387 _cell_length_c 9.5766 _exptl_crystal_F_000 358.00 _reflns_d_resolution_high 0.7006 _cod_data_source_file bk51012asup8.hkl _cod_data_source_block 2a #BEGIN Tags that were not found in dictionaries: _shelx_title ' m107e' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3789.66 3824.06 28.36 o -1 2 0 5409.21 5506.38 37.95 o 0 2 0 5635.57 5682.72 36.53 o -1 3 0 373.81 383.56 2.63 o 0 3 0 1053.80 1024.84 7.71 o -2 4 0 3302.45 3426.52 18.88 o -1 4 0 622.69 610.06 3.43 o 0 4 0 1161.08 1220.56 9.37 o -2 5 0 11.18 5.58 0.38 o -1 5 0 3230.36 3151.08 14.20 o 0 5 0 1789.82 1832.20 13.69 o -3 6 0 1097.19 1053.58 7.50 o -2 6 0 565.29 541.50 3.34 o -1 6 0 1149.52 1177.54 6.38 o 0 6 0 3693.86 3892.16 25.76 o -3 7 0 793.60 789.57 4.55 o -2 7 0 1129.40 1172.93 6.51 o -1 7 0 140.54 147.77 1.86 o 0 7 0 1.39 0.49 0.94 o -4 8 0 1671.65 1707.84 11.88 o -3 8 0 107.81 100.25 1.46 o -2 8 0 508.11 526.77 3.81 o -1 8 0 847.17 902.31 5.61 o 0 8 0 363.10 387.15 4.66 o -4 9 0 128.17 121.78 1.77 o -3 9 0 801.93 818.33 5.45 o -2 9 0 271.27 275.99 2.87 o -1 9 0 224.79 214.11 2.52 o 0 9 0 436.78 456.09 5.82 o -5 10 0 1158.72 1162.68 10.26 o -4 10 0 201.65 188.45 2.76 o -3 10 0 237.60 233.02 2.93 o -2 10 0 525.88 532.74 4.40 o -1 10 0 115.12 111.05 2.28 o 0 10 0 121.78 110.44 3.31 o -5 11 0 171.21 172.15 3.13 o -4 11 0 288.31 282.44 3.75 o -3 11 0 34.91 32.34 1.87 o -2 11 0 19.81 17.78 1.58 o -1 11 0 389.62 393.81 4.64 o 0 11 0 139.53 120.69 4.28 o -6 12 0 234.90 241.29 5.53 o -5 12 0 151.40 142.51 3.28 o -4 12 0 24.54 24.92 2.05 o -3 12 0 308.57 319.00 4.50 o 0 1 1 1013.16 870.44 2.77 o 0 2 1 1501.34 1653.14 5.90 o 1 2 1 3.74 3.73 0.19 o -1 3 1 2983.68 3014.84 11.72 o 0 3 1 203.68 219.39 1.29 o 1 3 1 454.57 445.12 2.31 o 2 3 1 347.79 343.68 2.16 o -1 4 1 1502.49 1529.37 6.87 o 0 4 1 506.51 480.89 2.57 o 1 4 1 0.20 0.05 0.31 o 2 4 1 429.52 414.46 2.69 o 3 4 1 350.00 352.54 2.61 o -2 5 1 415.75 433.13 2.82 o -1 5 1 147.89 166.84 1.42 o 0 5 1 2049.19 2034.41 10.02 o 1 5 1 455.98 449.00 3.27 o 2 5 1 227.50 232.90 2.28 o 3 5 1 53.42 50.63 1.13 o 4 5 1 69.80 74.94 1.56 o -2 6 1 21.01 27.65 0.92 o -1 6 1 563.75 553.51 3.42 o 0 6 1 7.03 7.56 0.70 o 1 6 1 8.52 5.64 0.73 o 2 6 1 6.93 6.74 0.82 o 3 6 1 58.71 56.84 1.47 o 4 6 1 39.41 44.97 2.02 o 5 6 1 146.22 148.14 2.98 o -3 7 1 34.34 37.94 0.82 o -2 7 1 99.79 101.95 1.45 o -1 7 1 58.38 51.96 1.22 o 0 7 1 89.42 69.68 1.43 o 1 7 1 40.12 33.65 1.26 o 2 7 1 83.98 81.20 1.77 o 3 7 1 24.15 27.32 1.40 o 4 7 1 5.21 3.71 1.47 o 5 7 1 1.10 2.90 1.70 o -3 8 1 37.61 36.79 1.03 o -2 8 1 23.61 21.91 0.89 o -1 8 1 93.73 79.65 1.56 o 0 8 1 2.06 2.39 0.85 o 1 8 1 39.28 37.84 1.44 o 2 8 1 9.43 9.57 1.21 o 3 8 1 24.28 25.72 2.07 o 4 8 1 40.35 45.22 2.45 o -4 9 1 64.15 67.30 1.54 o -3 9 1 0.50 1.36 0.86 o -2 9 1 265.28 277.39 2.86 o -1 9 1 129.18 121.24 2.08 o 0 9 1 30.40 31.45 1.48 o 1 9 1 63.38 64.40 1.96 o 2 9 1 16.17 18.23 1.65 o 3 9 1 2.87 3.96 1.84 o -4 10 1 101.93 109.09 2.04 o -3 10 1 16.76 22.19 1.30 o -2 10 1 2.01 -0.19 1.06 o -1 10 1 8.99 15.41 1.46 o 0 10 1 59.92 61.41 2.04 o 1 10 1 1.18 2.07 1.45 o -5 11 1 109.66 121.47 2.75 o -4 11 1 25.75 28.84 1.77 o -3 11 1 9.63 11.83 1.54 o -2 11 1 23.10 23.72 1.71 o -1 11 1 3.54 4.21 1.60 o 0 11 1 71.62 79.15 2.65 o -5 12 1 1.47 4.39 1.83 o -4 12 1 15.73 16.73 1.96 o -3 12 1 0.00 1.08 1.85 o 0 0 2 18580.51 16241.15 194.84 o 0 1 2 1337.72 1359.18 4.79 o 1 1 2 1722.97 1744.22 9.54 o -1 2 2 10703.14 10074.55 66.13 o 0 2 2 2503.99 2516.79 9.70 o 1 2 2 290.47 279.67 1.60 o 2 2 2 1198.77 1191.99 7.81 o -1 3 2 2636.92 2607.45 10.65 o 0 3 2 2726.78 2563.42 10.05 o 1 3 2 220.23 194.61 1.30 o 2 3 2 446.32 416.28 2.44 o 3 3 2 3130.27 3096.79 20.39 o -2 4 2 10474.02 10412.94 60.97 o -1 4 2 1227.96 1160.49 5.28 o 0 4 2 802.62 794.27 3.85 o 1 4 2 2076.50 2048.65 9.05 o 2 4 2 458.56 459.03 3.46 o 3 4 2 902.30 889.43 5.14 o 4 4 2 1538.22 1549.50 11.61 o -2 5 2 76.98 61.45 0.87 o -1 5 2 1948.03 1837.70 8.57 o 0 5 2 789.95 787.53 4.25 o 1 5 2 742.71 754.67 4.75 o 2 5 2 1357.20 1361.00 7.32 o 3 5 2 307.75 307.78 2.71 o 4 5 2 37.90 36.65 1.57 o 5 5 2 657.67 663.88 8.93 o -3 6 2 1144.18 1123.26 8.87 o -2 6 2 980.21 992.51 5.27 o -1 6 2 369.32 374.59 3.11 o 0 6 2 2122.23 2219.05 11.43 o 1 6 2 81.30 86.32 1.53 o 2 6 2 175.89 184.87 2.36 o 3 6 2 549.98 573.94 5.00 o 4 6 2 261.26 240.65 3.64 o 5 6 2 145.80 141.81 3.26 o 6 6 2 257.86 258.16 6.78 o -3 7 2 302.01 312.25 2.72 o -2 7 2 1325.83 1383.62 7.37 o -1 7 2 396.19 383.68 3.01 o 0 7 2 146.28 135.97 1.95 o 1 7 2 585.20 620.18 4.82 o 2 7 2 217.59 202.96 2.82 o 3 7 2 78.26 86.46 2.14 o 4 7 2 447.55 462.95 5.43 o 5 7 2 118.69 117.33 3.04 o -4 8 2 1293.46 1347.22 10.08 o -3 8 2 259.83 254.53 2.49 o -2 8 2 573.38 570.89 4.04 o -1 8 2 1488.73 1535.62 8.88 o 0 8 2 181.13 182.80 2.58 o 1 8 2 289.93 288.52 3.35 o 2 8 2 487.17 502.02 4.98 o 3 8 2 84.87 77.24 2.57 o 4 8 2 64.86 66.18 2.56 o -4 9 2 186.00 163.95 2.25 o -3 9 2 952.91 952.36 6.00 o -2 9 2 270.01 290.74 3.06 o -1 9 2 140.32 132.14 2.26 o 0 9 2 395.71 399.34 4.11 o 1 9 2 67.51 63.02 1.99 o 2 9 2 85.20 85.46 2.50 o 3 9 2 362.25 386.29 5.32 o -5 10 2 679.54 699.84 7.38 o -4 10 2 57.24 57.06 1.79 o -3 10 2 276.83 257.24 3.20 o -2 10 2 441.36 436.70 4.34 o -1 10 2 141.35 136.13 2.71 o 0 10 2 83.39 79.20 2.35 o 1 10 2 360.51 381.94 4.71 o -5 11 2 138.33 129.77 2.78 o -4 11 2 225.62 219.17 3.24 o -3 11 2 45.53 42.88 1.93 o -2 11 2 1.85 -0.24 1.59 o -1 11 2 247.52 255.62 4.02 o -6 12 2 280.12 285.35 6.48 o -5 12 2 57.57 55.23 2.59 o -4 12 2 60.30 59.33 3.01 o -3 12 2 228.31 221.41 5.95 o 0 1 3 11.35 11.37 0.22 o 0 2 3 1158.11 1225.57 5.73 o 1 2 3 182.38 189.57 1.41 o -1 3 3 2581.16 2728.43 11.45 o 0 3 3 82.80 91.09 0.82 o 1 3 3 263.56 280.86 1.69 o 2 3 3 304.31 317.54 2.09 o -1 4 3 718.87 780.64 4.13 o 0 4 3 6.82 5.36 0.35 o 1 4 3 9.32 8.87 0.39 o 2 4 3 416.77 423.97 2.62 o 3 4 3 520.34 520.61 3.38 o -2 5 3 345.66 384.71 2.51 o -1 5 3 6.28 10.64 0.54 o 0 5 3 11.45 14.78 0.54 o 1 5 3 42.63 48.55 0.89 o 2 5 3 0.01 0.00 0.45 o 3 5 3 103.89 95.35 1.71 o 4 5 3 40.96 41.66 1.44 o -2 6 3 3.08 4.19 0.53 o -1 6 3 49.25 47.51 0.98 o 0 6 3 2.51 3.30 0.54 o 1 6 3 69.75 63.35 1.33 o 2 6 3 95.63 95.74 1.94 o 3 6 3 48.60 59.75 1.71 o 4 6 3 13.76 15.53 1.50 o 5 6 3 23.04 26.16 1.81 o -3 7 3 121.09 130.01 1.66 o -2 7 3 21.75 17.82 0.89 o -1 7 3 203.29 201.59 2.24 o 0 7 3 84.13 79.09 1.72 o 1 7 3 23.11 18.30 1.15 o 2 7 3 32.76 31.80 1.46 o 3 7 3 42.41 44.97 2.07 o 4 7 3 1.53 -0.21 1.50 o 5 7 3 30.50 25.16 2.11 o -3 8 3 39.56 39.57 1.19 o -2 8 3 236.52 228.84 2.89 o -1 8 3 0.15 -0.75 0.87 o 0 8 3 137.27 134.57 2.47 o 1 8 3 16.62 19.97 1.34 o 2 8 3 0.93 -0.45 1.23 o 3 8 3 29.83 32.16 2.03 o 4 8 3 38.47 37.79 2.26 o -4 9 3 46.35 45.07 1.53 o -3 9 3 0.74 1.96 1.08 o -2 9 3 158.36 185.25 2.97 o -1 9 3 90.61 91.19 2.19 o 0 9 3 1.79 2.98 1.26 o 1 9 3 38.79 36.94 1.83 o 2 9 3 20.53 20.65 1.81 o -4 10 3 42.27 47.15 1.88 o -3 10 3 44.76 45.42 1.83 o -2 10 3 13.21 6.95 1.36 o -1 10 3 1.90 4.29 1.53 o 0 10 3 12.99 18.32 2.07 o 1 10 3 0.15 -0.27 1.60 o -5 11 3 16.03 16.96 1.78 o -4 11 3 8.49 11.00 1.69 o -3 11 3 26.16 30.86 2.01 o -2 11 3 37.14 34.10 2.17 o -1 11 3 2.44 5.95 1.86 o -5 12 3 38.68 33.19 2.46 o -4 12 3 10.19 7.81 2.09 o 0 0 4 945.71 1072.62 9.85 o 0 1 4 460.06 456.41 2.22 o 1 1 4 3865.75 3854.17 25.96 o -1 2 4 4063.02 3986.21 20.77 o 0 2 4 418.35 405.01 2.40 o 1 2 4 1406.00 1386.71 7.56 o 2 2 4 3584.13 3504.11 24.18 o -1 3 4 1156.85 1121.53 5.19 o 0 3 4 4275.50 4125.04 18.04 o 1 3 4 799.90 796.76 4.55 o 2 3 4 921.58 911.09 4.97 o 3 3 4 2446.15 2432.38 14.80 o -2 4 4 3511.18 3391.80 20.77 o -1 4 4 674.54 618.45 3.52 o 0 4 4 376.29 340.07 2.07 o 1 4 4 1580.94 1627.54 7.41 o 2 4 4 514.63 535.66 2.98 o 3 4 4 275.41 282.70 2.51 o 4 4 4 781.01 775.91 6.92 o -2 5 4 927.73 884.55 4.81 o -1 5 4 1396.26 1332.96 6.71 o 0 5 4 181.87 167.94 1.65 o 1 5 4 126.95 130.00 1.47 o 2 5 4 1474.93 1516.66 8.28 o 3 5 4 399.37 379.54 3.50 o 4 5 4 125.30 124.60 2.18 o 5 5 4 236.51 239.02 5.07 o -3 6 4 2797.90 2856.07 19.33 o -2 6 4 555.88 561.92 3.73 o -1 6 4 209.03 216.69 2.48 o 0 6 4 734.74 770.86 4.82 o 1 6 4 329.88 310.64 3.08 o 2 6 4 131.23 142.41 2.30 o 3 6 4 637.03 642.28 5.40 o 4 6 4 83.29 71.64 2.18 o 5 6 4 91.45 94.19 3.37 o 6 6 4 280.98 289.52 7.80 o -3 7 4 211.59 223.95 2.26 o -2 7 4 1451.13 1442.63 10.32 o -1 7 4 368.79 358.30 3.08 o 0 7 4 637.73 628.22 5.01 o 1 7 4 834.41 850.38 6.46 o 2 7 4 162.48 143.52 2.53 o 3 7 4 53.96 61.78 2.28 o 4 7 4 420.35 433.27 5.71 o 5 7 4 39.57 34.21 2.92 o -4 8 4 887.19 935.55 8.18 o -3 8 4 435.16 455.62 3.91 o -2 8 4 173.56 158.18 2.26 o -1 8 4 991.50 1030.36 7.42 o 0 8 4 64.77 61.84 1.78 o 1 8 4 143.18 154.16 2.71 o 2 8 4 354.44 378.27 4.29 o 3 8 4 120.22 110.04 3.24 o -4 9 4 155.34 141.79 2.50 o -3 9 4 616.36 629.62 5.46 o -2 9 4 117.54 130.39 2.49 o -1 9 4 114.14 110.14 2.38 o 0 9 4 398.66 401.88 4.33 o 1 9 4 97.18 92.10 2.66 o 2 9 4 79.49 75.94 2.77 o -5 10 4 267.61 275.36 5.09 o -4 10 4 81.31 88.76 2.34 o -3 10 4 105.11 90.54 2.49 o -2 10 4 393.76 404.22 4.99 o -1 10 4 68.76 66.83 2.25 o 0 10 4 48.65 49.14 2.42 o 1 10 4 203.55 216.37 5.10 o -5 11 4 58.34 50.85 2.33 o -4 11 4 348.47 339.57 4.67 o -3 11 4 115.80 114.18 2.98 o -2 11 4 76.07 65.67 2.54 o -1 11 4 174.40 169.55 4.28 o -6 12 4 301.19 313.64 7.32 o -5 12 4 24.27 22.90 2.18 o 0 1 5 279.21 252.64 1.46 o 0 2 5 2159.04 2272.58 10.36 o 1 2 5 611.59 612.53 4.06 o -1 3 5 29.18 35.21 0.59 o 0 3 5 33.86 29.88 0.70 o 1 3 5 187.92 188.06 1.78 o 2 3 5 87.28 77.05 1.39 o -1 4 5 46.91 51.72 0.83 o 0 4 5 130.37 132.88 1.43 o 1 4 5 0.05 -0.10 0.44 o 2 4 5 71.81 69.26 1.31 o 3 4 5 35.92 37.80 1.06 o -2 5 5 203.58 210.72 1.86 o -1 5 5 89.64 84.13 1.10 o 0 5 5 54.99 45.18 1.13 o 1 5 5 26.56 28.67 1.02 o 2 5 5 83.59 85.40 1.55 o 3 5 5 167.22 165.43 2.68 o 4 5 5 47.58 49.37 1.60 o -2 6 5 505.15 507.91 3.70 o -1 6 5 7.54 7.33 0.67 o 0 6 5 2.92 3.04 0.68 o 1 6 5 185.09 182.42 2.42 o 2 6 5 311.55 334.36 3.47 o 3 6 5 26.50 17.12 1.37 o 4 6 5 47.10 42.07 2.50 o 5 6 5 2.32 2.63 2.17 o -3 7 5 181.61 186.25 2.43 o -2 7 5 65.52 55.66 1.30 o -1 7 5 127.14 130.09 1.88 o 0 7 5 78.54 86.69 1.85 o 1 7 5 32.01 26.19 1.28 o 2 7 5 35.83 33.84 1.74 o 3 7 5 37.37 39.16 1.91 o 4 7 5 0.81 -0.51 2.15 o -3 8 5 65.07 64.78 1.65 o -2 8 5 133.49 128.45 2.17 o -1 8 5 28.19 29.24 1.36 o 0 8 5 183.22 187.15 2.82 o 1 8 5 42.27 46.11 1.99 o 2 8 5 4.42 3.38 1.54 o 3 8 5 12.30 5.18 2.33 o -4 9 5 63.75 57.79 1.83 o -3 9 5 0.43 -1.19 1.19 o -2 9 5 2.05 4.40 1.25 o -1 9 5 14.24 12.71 1.35 o 0 9 5 14.69 10.47 1.65 o 1 9 5 12.62 10.03 1.93 o 2 9 5 17.75 14.17 2.30 o -4 10 5 8.67 5.37 1.45 o -3 10 5 69.32 64.79 2.29 o -2 10 5 0.42 1.89 1.55 o -1 10 5 40.96 39.35 2.45 o 0 10 5 5.67 1.26 1.87 o -5 11 5 2.88 2.38 1.77 o -4 11 5 20.30 9.88 1.93 o -3 11 5 59.95 58.58 2.47 o -2 11 5 25.48 23.27 2.19 o 0 0 6 51.46 46.36 1.46 o 0 1 6 657.10 679.05 3.22 o 1 1 6 3782.23 3903.35 25.37 o -1 2 6 1402.02 1425.65 8.26 o 0 2 6 153.89 156.28 1.46 o 1 2 6 975.98 987.47 5.69 o 2 2 6 2659.92 2662.01 19.30 o -1 3 6 197.05 192.79 1.44 o 0 3 6 3044.57 3099.33 14.49 o 1 3 6 1012.03 1039.85 6.25 o 2 3 6 831.38 826.56 5.41 o 3 3 6 898.09 921.64 8.51 o -2 4 6 278.75 274.10 2.84 o -1 4 6 386.15 371.26 2.80 o 0 4 6 312.68 316.71 2.53 o 1 4 6 1946.60 1994.29 10.82 o 2 4 6 240.19 232.99 2.66 o 3 4 6 49.89 53.12 1.44 o 4 4 6 374.63 379.74 5.12 o -2 5 6 1111.35 1091.86 6.07 o -1 5 6 1743.39 1799.40 12.13 o 0 5 6 161.97 160.96 2.35 o 1 5 6 106.94 106.91 1.65 o 2 5 6 1033.80 1091.52 7.03 o 3 5 6 161.48 144.98 2.54 o 4 5 6 364.99 362.72 4.60 o 5 5 6 278.84 272.68 9.17 o -3 6 6 1888.86 1944.14 15.03 o -2 6 6 107.13 107.08 1.60 o -1 6 6 284.30 286.75 3.00 o 0 6 6 485.19 496.74 4.23 o 1 6 6 479.83 470.89 4.18 o 2 6 6 148.28 154.38 2.40 o 3 6 6 678.10 677.72 6.61 o 4 6 6 42.46 40.32 2.67 o 5 6 6 39.09 38.08 2.88 o -3 7 6 190.31 197.89 2.42 o -2 7 6 1023.40 1027.06 6.65 o -1 7 6 233.25 237.68 2.89 o 0 7 6 395.52 393.00 4.31 o 1 7 6 711.82 732.26 6.40 o 2 7 6 80.17 71.19 3.00 o 3 7 6 86.69 87.88 3.08 o 4 7 6 290.21 294.87 5.54 o -4 8 6 586.91 613.00 7.27 o -3 8 6 201.87 209.12 2.87 o -2 8 6 44.18 39.14 1.47 o -1 8 6 329.16 333.13 4.25 o 0 8 6 108.50 107.29 2.67 o 1 8 6 40.46 43.30 2.00 o 2 8 6 303.65 325.58 4.86 o 3 8 6 87.12 82.79 3.56 o -4 9 6 234.75 233.03 3.49 o -3 9 6 421.36 436.05 4.90 o -2 9 6 32.43 29.96 1.74 o -1 9 6 76.75 73.64 2.81 o 0 9 6 487.07 498.09 5.78 o 1 9 6 115.28 106.55 3.79 o -5 10 6 304.02 303.71 6.02 o -4 10 6 165.57 169.72 3.42 o -3 10 6 33.67 26.35 1.96 o -2 10 6 349.00 344.89 5.07 o -1 10 6 42.23 36.40 2.44 o -5 11 6 22.87 21.43 2.38 o -4 11 6 413.99 418.38 6.03 o -3 11 6 131.15 128.05 3.85 o 0 1 7 478.76 445.67 2.43 o 0 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10.56 2.06 o -2 9 7 11.70 9.29 1.80 o -1 9 7 5.42 4.03 1.67 o 0 9 7 25.10 24.62 2.31 o -4 10 7 20.54 12.22 1.84 o -3 10 7 30.85 24.97 2.21 o -2 10 7 7.23 4.13 1.92 o 0 0 8 2412.51 2546.17 25.93 o 0 1 8 688.96 703.98 3.82 o 1 1 8 1785.62 1804.88 12.33 o -1 2 8 1443.56 1516.57 10.22 o 0 2 8 219.13 230.39 2.14 o 1 2 8 220.96 217.70 2.29 o 2 2 8 720.60 754.51 7.05 o -1 3 8 175.75 177.90 2.18 o 0 3 8 1380.68 1417.48 7.97 o 1 3 8 403.67 411.03 3.49 o 2 3 8 482.44 476.61 4.02 o 3 3 8 638.44 664.77 7.26 o -2 4 8 322.39 350.63 4.54 o -1 4 8 316.92 325.13 3.23 o 0 4 8 270.22 279.09 3.03 o 1 4 8 1453.49 1469.18 8.55 o 2 4 8 94.86 87.32 1.80 o 3 4 8 66.68 61.72 1.70 o 4 4 8 333.69 347.99 5.33 o -2 5 8 373.02 376.03 3.77 o -1 5 8 1343.69 1388.91 8.92 o 0 5 8 205.81 218.11 3.05 o 1 5 8 252.18 246.09 3.07 o 2 5 8 559.69 567.18 4.85 o 3 5 8 61.40 55.71 1.96 o 4 5 8 245.76 234.48 3.85 o 5 5 8 386.44 379.14 9.35 o -3 6 8 455.81 475.25 5.91 o -2 6 8 57.50 59.10 1.71 o -1 6 8 219.37 211.50 2.84 o 0 6 8 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218.58 2.76 o 0 4 10 178.28 162.76 2.73 o 1 4 10 478.79 454.18 4.54 o 2 4 10 108.65 111.05 2.44 o 3 4 10 135.53 128.32 2.60 o 4 4 10 402.89 422.78 8.20 o -2 5 10 82.22 84.42 2.20 o -1 5 10 539.67 555.93 5.38 o 0 5 10 126.57 131.03 3.66 o 1 5 10 198.31 189.93 3.73 o 2 5 10 363.65 367.26 4.65 o 3 5 10 79.87 82.39 2.66 o -3 6 10 248.67 263.07 5.32 o -2 6 10 150.90 161.46 3.02 o -1 6 10 79.63 79.86 2.80 o 0 6 10 519.94 537.24 5.63 o 1 6 10 51.51 51.49 2.36 o 2 6 10 57.10 55.38 2.63 o -3 7 10 79.67 72.76 2.34 o -2 7 10 392.11 393.61 5.31 o -1 7 10 110.24 102.37 3.11 o 0 7 10 70.30 66.82 2.71 o -4 8 10 299.68 290.61 7.97 o -3 8 10 62.83 53.58 2.76 o -2 8 10 120.54 121.36 3.83 o 0 1 11 22.85 26.92 1.14 o 0 2 11 14.57 15.50 1.32 o 1 2 11 50.15 57.36 1.90 o -1 3 11 207.60 210.37 3.59 o 0 3 11 10.73 12.77 1.45 o 1 3 11 36.63 42.36 1.83 o 2 3 11 61.05 61.74 2.12 o -1 4 11 92.44 103.77 2.81 o 0 4 11 2.19 1.47 1.36 o 1 4 11 0.24 0.27 1.36 o 2 4 11 37.97 36.63 1.95 o 3 4 11 124.45 119.01 2.89 o -2 5 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