#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104887.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104887_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9445 _cell_length_b 8.9445 _cell_length_c 9.5826 _exptl_crystal_F_000 358.00 _reflns_d_resolution_high 0.7003 _[local]_cod_data_source_file bk51012bsup9.hkl _[local]_cod_data_source_block 2b #BEGIN Tags that were not found in dictionaries: _shelx_title ' m107d' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3800.08 3799.48 28.49 o -1 2 0 5392.77 5506.40 27.94 o 0 2 0 5611.54 5615.82 33.04 o -1 3 0 375.96 379.30 2.03 o 0 3 0 1050.75 1032.71 8.10 o -2 4 0 3320.90 3401.44 19.69 o -1 4 0 612.14 592.04 3.45 o 0 4 0 1170.51 1220.05 9.75 o -2 5 0 12.06 7.47 0.38 o -1 5 0 3185.90 3113.03 14.70 o 0 5 0 1756.24 1805.38 14.10 o -3 6 0 1075.37 1036.24 8.25 o -2 6 0 555.60 539.39 3.42 o -1 6 0 1104.45 1136.32 6.41 o 0 6 0 3579.46 3751.86 26.11 o -3 7 0 755.31 764.52 4.59 o -2 7 0 1084.62 1142.49 6.58 o -1 7 0 139.62 146.24 1.86 o 0 7 0 1.25 1.38 0.97 o -4 8 0 1595.10 1627.80 14.72 o -3 8 0 104.29 101.63 1.59 o -2 8 0 480.34 497.75 3.74 o -1 8 0 794.28 858.84 5.56 o 0 8 0 335.46 367.53 4.58 o -4 9 0 121.61 111.93 1.71 o -3 9 0 755.83 792.87 5.64 o -2 9 0 252.83 258.65 2.80 o -1 9 0 209.84 201.08 2.45 o 0 9 0 404.65 413.94 5.92 o -5 10 0 1081.70 1083.30 10.02 o -4 10 0 189.48 180.55 2.73 o -3 10 0 221.94 214.35 2.74 o -2 10 0 493.29 486.43 4.24 o -1 10 0 102.83 97.02 2.19 o 0 10 0 116.04 108.17 3.27 o -5 11 0 158.75 153.77 3.01 o -4 11 0 269.44 270.04 3.67 o -3 11 0 32.18 27.91 1.76 o -2 11 0 18.69 18.65 1.61 o -1 11 0 349.89 353.64 4.26 o 0 11 0 123.99 121.23 4.33 o -6 12 0 218.74 219.61 5.30 o -5 12 0 134.93 129.93 3.15 o -4 12 0 23.96 24.10 1.93 o -3 12 0 276.48 282.87 4.26 o 0 1 1 1014.40 868.90 2.91 o 0 2 1 1521.76 1654.39 6.21 o 1 2 1 3.65 3.34 0.18 o -1 3 1 2970.88 3012.86 12.58 o 0 3 1 194.73 209.33 1.35 o 1 3 1 442.48 431.89 2.33 o 2 3 1 341.78 335.37 2.18 o -1 4 1 1475.09 1514.36 7.12 o 0 4 1 492.79 466.69 2.58 o 1 4 1 0.10 -0.03 0.36 o 2 4 1 420.35 398.77 2.69 o 3 4 1 340.00 337.65 2.58 o -2 5 1 418.29 435.81 2.89 o -1 5 1 143.43 166.04 1.54 o 0 5 1 2002.67 1979.19 11.62 o 1 5 1 444.18 434.65 3.05 o 2 5 1 217.19 221.59 2.25 o 3 5 1 52.59 50.60 1.13 o 4 5 1 67.92 71.82 1.52 o -2 6 1 19.10 24.41 0.75 o -1 6 1 544.48 538.95 3.43 o 0 6 1 6.12 5.68 0.65 o 1 6 1 9.40 6.24 0.70 o 2 6 1 6.14 4.04 0.77 o 3 6 1 54.93 54.07 1.44 o 4 6 1 37.39 43.08 1.94 o 5 6 1 135.89 140.09 3.02 o -3 7 1 35.27 37.48 0.82 o -2 7 1 96.93 102.18 1.46 o -1 7 1 59.28 50.02 1.19 o 0 7 1 85.93 64.22 1.39 o 1 7 1 37.12 32.92 1.21 o 2 7 1 79.79 76.45 1.72 o 3 7 1 25.23 26.76 1.41 o 4 7 1 4.72 3.46 1.47 o 5 7 1 1.08 0.44 1.63 o -3 8 1 38.16 39.07 1.01 o -2 8 1 22.85 20.44 0.87 o -1 8 1 85.31 74.58 1.51 o 0 8 1 1.88 1.81 0.82 o 1 8 1 39.50 35.01 1.41 o 2 8 1 7.38 4.97 1.18 o 3 8 1 23.45 25.53 1.71 o 4 8 1 35.83 37.89 2.21 o -4 9 1 63.80 65.15 1.54 o -3 9 1 0.40 1.55 0.84 o -2 9 1 250.17 259.71 2.77 o -1 9 1 124.01 119.23 2.40 o 0 9 1 27.07 25.72 1.40 o 1 9 1 60.51 59.95 1.90 o 2 9 1 16.03 21.15 1.69 o 3 9 1 2.38 1.50 1.75 o -4 10 1 92.81 103.95 2.00 o -3 10 1 16.54 21.18 1.29 o -2 10 1 2.12 0.99 1.07 o -1 10 1 9.16 15.39 1.42 o 0 10 1 55.56 59.26 2.00 o 1 10 1 0.90 -0.41 1.41 o -5 11 1 99.07 106.94 2.72 o -4 11 1 22.75 27.04 1.65 o -3 11 1 9.30 10.55 1.48 o -2 11 1 21.53 26.02 1.71 o -1 11 1 2.97 0.18 1.55 o 0 11 1 64.63 69.38 2.62 o -5 12 1 1.35 0.96 1.74 o -4 12 1 13.95 10.20 1.85 o -3 12 1 0.00 0.82 1.73 o 0 0 2 18562.00 15851.76 257.69 o 0 1 2 1334.13 1360.09 5.13 o 1 1 2 1722.37 1733.26 10.04 o -1 2 2 10650.53 10039.50 63.89 o 0 2 2 2475.77 2490.12 10.14 o 1 2 2 297.45 284.94 1.67 o 2 2 2 1203.61 1189.41 8.18 o -1 3 2 2622.89 2583.01 11.12 o 0 3 2 2699.13 2546.06 10.52 o 1 3 2 212.14 187.14 1.29 o 2 3 2 438.52 410.75 2.39 o 3 3 2 3069.38 3052.34 21.19 o -2 4 2 10273.89 10154.00 62.70 o -1 4 2 1200.54 1134.87 5.39 o 0 4 2 798.86 792.14 3.87 o 1 4 2 2048.39 2025.50 9.38 o 2 4 2 455.88 456.68 2.95 o 3 4 2 867.53 870.17 5.24 o 4 4 2 1468.24 1486.59 12.56 o -2 5 2 75.43 59.72 0.99 o -1 5 2 1895.14 1802.00 8.78 o 0 5 2 772.97 769.60 4.31 o 1 5 2 719.01 742.21 4.62 o 2 5 2 1319.90 1339.61 7.24 o 3 5 2 295.27 295.04 2.75 o 4 5 2 36.55 34.75 1.49 o 5 5 2 606.13 626.55 8.75 o -3 6 2 1098.63 1087.66 7.89 o -2 6 2 944.37 960.36 5.31 o -1 6 2 354.75 358.30 2.84 o 0 6 2 2060.64 2150.29 11.61 o 1 6 2 82.71 81.94 1.49 o 2 6 2 167.71 173.64 2.31 o 3 6 2 515.64 547.80 4.93 o 4 6 2 239.17 225.64 3.67 o 5 6 2 134.22 132.12 3.03 o 6 6 2 235.98 242.44 5.96 o -3 7 2 287.01 298.25 2.59 o -2 7 2 1266.98 1320.51 7.35 o -1 7 2 380.76 374.16 3.00 o 0 7 2 140.98 131.90 1.93 o 1 7 2 555.07 585.22 4.73 o 2 7 2 201.89 186.74 2.71 o 3 7 2 72.99 79.37 2.07 o 4 7 2 408.89 429.05 5.26 o 5 7 2 105.44 104.28 3.06 o -4 8 2 1241.83 1285.53 10.06 o -3 8 2 251.58 250.00 2.47 o -2 8 2 545.16 535.32 3.94 o -1 8 2 1416.54 1450.61 8.77 o 0 8 2 169.74 176.72 2.54 o 1 8 2 268.08 267.84 3.25 o 2 8 2 449.02 463.86 4.80 o 3 8 2 75.88 70.08 2.47 o 4 8 2 60.25 55.76 3.37 o -4 9 2 175.89 156.87 2.23 o -3 9 2 901.72 908.72 5.94 o -2 9 2 254.39 274.21 2.98 o -1 9 2 133.36 125.01 2.28 o 0 9 2 368.81 376.78 4.15 o 1 9 2 62.22 59.56 1.94 o 2 9 2 77.20 77.07 2.51 o 3 9 2 322.62 351.93 5.10 o -5 10 2 647.43 667.31 8.63 o -4 10 2 56.17 54.57 1.76 o -3 10 2 257.01 232.24 3.03 o -2 10 2 412.44 409.88 4.25 o -1 10 2 128.69 121.85 2.98 o 0 10 2 77.22 74.46 2.40 o 1 10 2 325.26 332.53 4.43 o -5 11 2 126.53 123.06 2.73 o -4 11 2 210.59 206.79 3.63 o -3 11 2 42.72 39.41 1.88 o -2 11 2 1.96 -1.56 1.56 o -1 11 2 221.80 226.02 3.65 o -6 12 2 256.32 264.25 7.13 o -5 12 2 53.45 48.97 2.53 o -4 12 2 54.69 52.24 2.70 o -3 12 2 206.59 197.74 4.15 o 0 1 3 11.58 11.35 0.22 o 0 2 3 1153.12 1217.86 5.81 o 1 2 3 185.14 188.30 1.50 o -1 3 3 2568.23 2719.87 12.02 o 0 3 3 80.29 89.00 0.81 o 1 3 3 257.02 275.68 1.71 o 2 3 3 292.43 305.87 2.09 o -1 4 3 713.94 781.67 4.28 o 0 4 3 7.94 5.99 0.35 o 1 4 3 7.84 7.97 0.40 o 2 4 3 397.67 406.85 2.60 o 3 4 3 499.23 506.06 3.40 o -2 5 3 346.65 384.54 2.56 o -1 5 3 6.62 11.44 0.51 o 0 5 3 11.41 14.53 0.55 o 1 5 3 41.53 47.02 0.81 o 2 5 3 0.01 0.05 0.44 o 3 5 3 99.65 93.47 1.59 o 4 5 3 39.37 40.59 1.44 o -2 6 3 2.77 3.26 0.52 o -1 6 3 47.32 44.32 0.95 o 0 6 3 2.33 3.67 0.55 o 1 6 3 65.72 58.74 1.46 o 2 6 3 90.93 88.91 2.02 o 3 6 3 43.80 52.24 1.66 o 4 6 3 14.00 14.38 1.56 o 5 6 3 22.67 27.25 2.22 o -3 7 3 120.06 128.92 1.65 o -2 7 3 19.49 16.13 0.75 o -1 7 3 194.51 189.51 2.18 o 0 7 3 80.00 74.38 1.68 o 1 7 3 21.45 17.46 1.14 o 2 7 3 31.58 29.21 1.51 o 3 7 3 40.25 45.39 1.74 o 4 7 3 1.40 1.51 1.56 o 5 7 3 29.05 25.58 2.09 o -3 8 3 38.22 38.67 1.17 o -2 8 3 224.54 214.48 2.52 o -1 8 3 0.18 -0.23 0.91 o 0 8 3 129.58 129.82 2.37 o 1 8 3 15.83 15.25 1.29 o 2 8 3 0.76 -0.73 1.24 o 3 8 3 28.26 29.89 2.01 o 4 8 3 36.04 35.60 2.58 o -4 9 3 45.14 41.33 1.47 o -3 9 3 0.64 0.58 1.20 o -2 9 3 148.73 175.80 2.66 o -1 9 3 84.19 83.83 2.12 o 0 9 3 1.69 1.22 1.22 o 1 9 3 36.33 35.42 1.82 o 2 9 3 19.59 19.35 1.80 o -4 10 3 38.76 44.04 2.16 o -3 10 3 39.04 39.93 1.73 o -2 10 3 11.39 6.12 1.43 o -1 10 3 1.88 5.16 1.51 o 0 10 3 12.87 12.96 1.67 o 1 10 3 0.08 -1.00 1.54 o -5 11 3 14.98 14.76 1.77 o -4 11 3 7.16 7.55 1.56 o -3 11 3 24.09 25.45 1.93 o -2 11 3 33.33 31.87 2.10 o -1 11 3 1.86 -0.30 1.72 o -5 12 3 33.78 32.31 2.44 o -4 12 3 9.95 8.23 2.05 o 0 0 4 905.24 1027.92 9.89 o 0 1 4 452.83 448.00 2.20 o 1 1 4 3809.96 3775.21 26.80 o -1 2 4 3996.35 3903.48 22.45 o 0 2 4 409.47 390.32 2.40 o 1 2 4 1385.66 1370.69 7.82 o 2 2 4 3483.97 3396.05 24.68 o -1 3 4 1141.61 1106.70 5.35 o 0 3 4 4192.62 4046.23 18.68 o 1 3 4 780.52 771.66 4.60 o 2 3 4 889.41 869.65 5.09 o 3 3 4 2364.77 2369.06 15.16 o -2 4 4 3413.18 3310.55 21.97 o -1 4 4 655.06 604.89 3.61 o 0 4 4 369.95 336.93 2.11 o 1 4 4 1538.36 1576.97 7.54 o 2 4 4 496.07 517.98 2.99 o 3 4 4 268.37 277.72 2.53 o 4 4 4 749.19 748.85 6.96 o -2 5 4 897.14 861.93 4.87 o -1 5 4 1359.12 1300.96 6.84 o 0 5 4 176.12 166.27 1.65 o 1 5 4 124.64 129.19 1.52 o 2 5 4 1415.13 1442.09 8.26 o 3 5 4 379.24 363.51 3.50 o 4 5 4 119.08 119.42 2.15 o 5 5 4 221.37 223.99 7.22 o -3 6 4 2693.05 2738.16 21.18 o -2 6 4 528.39 535.89 3.69 o -1 6 4 208.49 211.94 2.07 o 0 6 4 708.41 743.15 4.82 o 1 6 4 314.67 300.31 3.04 o 2 6 4 126.51 134.14 2.34 o 3 6 4 601.81 600.52 5.29 o 4 6 4 76.43 66.33 2.14 o 5 6 4 82.66 84.40 2.84 o 6 6 4 247.74 250.42 7.25 o -3 7 4 206.84 217.32 2.42 o -2 7 4 1390.84 1413.07 8.24 o -1 7 4 350.51 339.99 3.03 o 0 7 4 597.31 589.67 4.90 o 1 7 4 795.15 810.31 6.42 o 2 7 4 152.57 138.29 2.49 o 3 7 4 50.67 59.65 1.91 o 4 7 4 380.10 397.16 5.50 o 5 7 4 36.06 29.70 2.85 o -4 8 4 839.37 897.17 8.12 o -3 8 4 412.53 431.76 3.83 o -2 8 4 166.33 152.50 2.24 o -1 8 4 951.46 978.64 7.33 o 0 8 4 63.06 63.00 1.78 o 1 8 4 133.81 143.25 2.63 o 2 8 4 324.04 344.35 4.14 o 3 8 4 109.21 99.05 3.38 o -4 9 4 144.92 135.25 2.46 o -3 9 4 579.47 582.68 5.30 o -2 9 4 112.28 124.93 2.42 o -1 9 4 106.75 99.81 2.28 o 0 9 4 369.94 366.74 4.14 o 1 9 4 90.68 82.94 2.33 o 2 9 4 71.09 72.00 2.55 o -5 10 4 254.76 259.05 4.98 o -4 10 4 75.47 83.09 2.38 o -3 10 4 97.33 82.66 2.51 o -2 10 4 359.29 360.44 4.69 o -1 10 4 65.15 56.67 2.23 o 0 10 4 42.70 39.71 2.26 o 1 10 4 183.95 174.78 3.84 o -5 11 4 52.99 46.00 2.25 o -4 11 4 316.42 307.93 4.47 o -3 11 4 105.13 95.95 2.77 o -2 11 4 69.08 60.89 2.49 o -1 11 4 157.81 154.72 3.67 o -6 12 4 269.37 282.08 7.05 o -5 12 4 23.64 26.33 2.27 o 0 1 5 269.47 238.94 1.45 o 0 2 5 2108.10 2222.96 10.65 o 1 2 5 603.76 607.62 4.15 o -1 3 5 30.33 37.09 0.60 o 0 3 5 32.34 27.82 0.68 o 1 3 5 187.65 187.29 1.66 o 2 3 5 89.50 77.22 1.40 o -1 4 5 46.69 51.43 0.77 o 0 4 5 131.57 132.92 1.59 o 1 4 5 0.01 0.56 0.45 o 2 4 5 71.23 69.59 1.31 o 3 4 5 35.42 36.95 1.05 o -2 5 5 194.41 201.05 1.83 o -1 5 5 83.58 78.61 1.06 o 0 5 5 50.44 39.21 1.10 o 1 5 5 25.57 25.71 0.99 o 2 5 5 77.21 79.17 1.71 o 3 5 5 155.51 159.01 2.43 o 4 5 5 43.90 45.73 1.67 o -2 6 5 484.01 484.27 3.66 o -1 6 5 7.53 6.83 0.64 o 0 6 5 2.48 2.07 0.62 o 1 6 5 169.29 169.60 2.35 o 2 6 5 291.33 311.10 3.38 o 3 6 5 24.36 15.35 1.35 o 4 6 5 44.84 39.70 2.48 o 5 6 5 1.90 -1.75 2.12 o -3 7 5 174.61 180.70 2.17 o -2 7 5 59.38 50.90 1.26 o -1 7 5 119.03 120.62 1.83 o 0 7 5 74.31 80.76 1.77 o 1 7 5 28.65 22.12 1.22 o 2 7 5 34.48 27.73 1.64 o 3 7 5 33.63 36.68 1.85 o 4 7 5 0.67 0.85 2.18 o -3 8 5 61.55 61.12 1.59 o -2 8 5 128.86 120.10 2.11 o -1 8 5 24.56 24.17 1.31 o 0 8 5 169.41 179.05 3.66 o 1 8 5 37.69 40.41 1.95 o 2 8 5 3.44 2.02 1.51 o 3 8 5 11.61 5.74 2.39 o -4 9 5 58.97 54.11 1.75 o -3 9 5 0.34 -0.92 1.18 o -2 9 5 2.14 3.78 1.23 o -1 9 5 13.13 14.58 1.42 o 0 9 5 12.70 8.35 1.59 o 1 9 5 11.58 11.50 1.78 o 2 9 5 16.18 13.24 2.30 o -4 10 5 9.25 9.09 1.47 o -3 10 5 61.99 55.85 2.16 o -2 10 5 0.42 1.15 1.45 o -1 10 5 36.40 33.84 2.27 o 0 10 5 5.60 4.31 1.92 o -5 11 5 3.10 0.06 1.77 o -4 11 5 17.82 14.38 1.81 o -3 11 5 54.41 53.14 2.35 o -2 11 5 23.59 22.97 2.27 o 0 0 6 56.91 53.02 1.55 o 0 1 6 645.54 664.20 3.34 o 1 1 6 3692.40 3805.73 26.02 o -1 2 6 1385.66 1426.58 8.64 o 0 2 6 154.72 156.47 1.47 o 1 2 6 943.02 950.65 5.72 o 2 2 6 2564.72 2572.11 19.58 o -1 3 6 193.74 189.19 1.45 o 0 3 6 2943.23 2985.75 14.70 o 1 3 6 980.19 1004.87 6.30 o 2 3 6 791.01 791.72 5.39 o 3 3 6 857.48 877.52 8.42 o -2 4 6 278.25 278.08 2.90 o -1 4 6 375.18 365.40 2.83 o 0 4 6 297.35 306.64 2.53 o 1 4 6 1856.99 1900.98 10.41 o 2 4 6 226.15 221.62 2.62 o 3 4 6 49.29 52.31 1.43 o 4 4 6 350.98 358.58 5.01 o -2 5 6 1056.05 1051.93 6.10 o -1 5 6 1674.38 1742.39 9.96 o 0 5 6 156.35 159.76 2.12 o 1 5 6 104.97 104.18 1.63 o 2 5 6 973.17 1021.06 6.86 o 3 5 6 150.97 138.11 2.47 o 4 5 6 334.00 327.83 4.45 o 5 5 6 260.21 259.32 6.76 o -3 6 6 1818.00 1876.68 15.21 o -2 6 6 104.96 101.42 1.57 o -1 6 6 276.00 276.37 2.97 o 0 6 6 462.26 475.65 4.56 o 1 6 6 444.10 438.55 4.07 o 2 6 6 139.57 145.24 2.38 o 3 6 6 632.56 637.65 6.87 o 4 6 6 39.75 35.35 2.48 o 5 6 6 35.85 34.79 2.81 o -3 7 6 185.65 191.07 2.38 o -2 7 6 975.71 977.87 6.57 o -1 7 6 218.43 216.69 2.87 o 0 7 6 367.20 362.44 4.17 o 1 7 6 668.67 696.50 6.33 o 2 7 6 76.33 64.91 2.35 o 3 7 6 80.25 78.51 2.92 o 4 7 6 262.87 276.12 5.42 o -4 8 6 544.15 576.76 7.61 o -3 8 6 186.87 192.37 2.84 o -2 8 6 42.52 40.37 1.49 o -1 8 6 311.22 317.86 4.21 o 0 8 6 101.10 99.60 2.62 o 1 8 6 38.49 42.82 2.08 o 2 8 6 276.65 291.28 4.65 o 3 8 6 79.99 73.05 3.43 o -4 9 6 214.46 212.85 3.35 o -3 9 6 389.95 397.39 4.69 o -2 9 6 30.80 33.57 1.90 o -1 9 6 69.98 65.59 2.64 o 0 9 6 439.61 445.96 5.51 o 1 9 6 104.54 100.52 3.29 o -5 10 6 275.20 280.20 6.18 o -4 10 6 146.34 145.94 3.21 o -3 10 6 31.87 27.05 2.37 o -2 10 6 313.23 306.69 4.80 o -1 10 6 39.58 38.71 2.41 o -5 11 6 21.50 19.67 2.29 o -4 11 6 370.35 381.27 5.80 o -3 11 6 116.82 118.06 3.44 o 0 1 7 460.41 420.55 2.34 o 0 2 7 495.12 470.22 3.16 o 1 2 7 92.07 91.57 1.45 o -1 3 7 32.70 32.67 0.72 o 0 3 7 105.48 99.66 1.33 o 1 3 7 74.20 70.05 1.39 o 2 3 7 48.08 41.06 1.22 o -1 4 7 23.61 23.23 0.91 o 0 4 7 549.48 560.42 4.08 o 1 4 7 2.93 1.39 0.75 o 2 4 7 83.88 77.52 1.61 o 3 4 7 11.23 9.58 1.07 o -2 5 7 79.46 69.80 1.37 o -1 5 7 36.69 36.73 1.25 o 0 5 7 50.72 49.92 1.33 o 1 5 7 93.29 84.09 1.74 o 2 5 7 30.39 27.97 1.25 o 3 5 7 85.17 84.77 2.18 o 4 5 7 65.00 63.35 2.40 o -2 6 7 494.67 488.24 4.38 o -1 6 7 95.33 97.82 1.81 o 0 6 7 0.96 1.22 0.79 o 1 6 7 96.22 95.69 2.18 o 2 6 7 89.90 91.78 2.26 o 3 6 7 67.15 63.66 2.37 o 4 6 7 60.08 58.06 2.99 o -3 7 7 29.97 29.61 1.20 o -2 7 7 9.37 6.50 1.04 o -1 7 7 42.91 44.34 1.58 o 0 7 7 53.96 61.29 1.99 o 1 7 7 0.01 -1.04 1.46 o 2 7 7 11.55 10.42 1.94 o 3 7 7 26.78 25.66 2.58 o -3 8 7 94.47 95.11 2.33 o -2 8 7 23.27 20.73 1.49 o -1 8 7 1.97 1.74 1.35 o 0 8 7 28.89 32.98 1.96 o 1 8 7 36.15 33.30 2.29 o 2 8 7 0.01 2.29 2.03 o -4 9 7 55.38 50.60 1.87 o -3 9 7 7.71 6.60 1.67 o -2 9 7 9.48 6.49 1.73 o -1 9 7 5.27 4.22 1.63 o 0 9 7 21.92 15.20 2.17 o -4 10 7 20.61 18.94 1.96 o -3 10 7 29.86 22.41 2.26 o -2 10 7 6.18 3.19 2.27 o 0 0 8 2322.62 2488.60 26.66 o 0 1 8 661.88 674.40 3.81 o 1 1 8 1718.39 1759.84 12.58 o -1 2 8 1386.46 1432.63 10.11 o 0 2 8 215.03 220.64 2.11 o 1 2 8 210.87 205.76 2.24 o 2 2 8 695.30 724.91 7.05 o -1 3 8 166.71 167.85 2.13 o 0 3 8 1317.34 1344.95 7.91 o 1 3 8 386.59 388.03 3.42 o 2 3 8 452.68 446.67 3.85 o 3 3 8 596.23 620.30 7.07 o -2 4 8 316.14 345.66 5.44 o -1 4 8 304.70 314.35 3.19 o 0 4 8 253.59 261.72 2.70 o 1 4 8 1368.41 1363.84 8.34 o 2 4 8 89.33 83.01 1.79 o 3 4 8 62.88 61.04 1.68 o 4 4 8 306.68 316.92 5.17 o -2 5 8 353.55 357.93 3.73 o -1 5 8 1273.71 1330.13 8.91 o 0 5 8 197.12 211.74 2.70 o 1 5 8 237.18 235.07 3.03 o 2 5 8 520.49 523.99 4.73 o 3 5 8 56.25 51.83 1.88 o 4 5 8 220.66 215.00 3.75 o 5 5 8 348.56 354.00 9.35 o -3 6 8 438.87 451.13 5.86 o -2 6 8 57.80 59.05 1.70 o -1 6 8 203.22 197.36 2.76 o 0 6 8 570.70 582.47 5.56 o 1 6 8 198.72 203.09 3.24 o 2 6 8 79.57 76.11 2.26 o 3 6 8 353.21 359.90 5.22 o 4 6 8 83.80 79.25 3.89 o -3 7 8 115.68 115.57 2.32 o -2 7 8 588.05 607.32 5.60 o -1 7 8 164.87 169.20 2.85 o 0 7 8 110.42 112.17 2.96 o 1 7 8 294.37 307.19 5.47 o 2 7 8 34.58 29.13 2.87 o 3 7 8 73.12 64.06 3.32 o -4 8 8 368.67 377.08 6.59 o -3 8 8 48.14 44.97 1.93 o -2 8 8 85.27 90.09 2.55 o -1 8 8 226.43 225.51 4.89 o 0 8 8 136.82 133.45 3.43 o 1 8 8 28.65 24.35 2.43 o -4 9 8 226.14 226.32 3.88 o -3 9 8 380.74 372.90 5.33 o -2 9 8 40.45 39.45 2.04 o -1 9 8 36.24 33.66 2.76 o -5 10 8 326.24 332.27 10.23 o -4 10 8 86.25 74.83 3.23 o -3 10 8 39.92 43.18 2.82 o 0 1 9 179.62 177.06 1.90 o 0 2 9 53.95 46.21 1.19 o 1 2 9 2.30 2.79 0.80 o -1 3 9 80.16 78.83 1.60 o 0 3 9 19.09 16.33 1.06 o 1 3 9 18.22 19.89 1.12 o 2 3 9 59.39 63.63 1.62 o -1 4 9 89.48 86.43 1.77 o 0 4 9 215.69 206.70 2.78 o 1 4 9 8.18 10.97 1.25 o 2 4 9 141.35 141.87 2.41 o 3 4 9 24.09 25.84 1.56 o -2 5 9 55.00 50.56 1.57 o -1 5 9 6.74 6.18 1.32 o 0 5 9 129.30 135.77 2.63 o 1 5 9 84.66 78.70 1.94 o 2 5 9 0.03 -0.43 1.24 o 3 5 9 18.07 19.42 1.71 o 4 5 9 33.60 30.44 2.56 o -2 6 9 41.38 43.18 1.61 o -1 6 9 132.02 138.24 2.79 o 0 6 9 0.46 -0.29 1.33 o 1 6 9 37.32 44.05 2.20 o 2 6 9 2.46 3.80 1.63 o 3 6 9 1.18 0.06 1.98 o -3 7 9 2.11 1.04 1.27 o -2 7 9 0.17 -0.38 1.14 o -1 7 9 36.61 37.78 1.96 o 0 7 9 29.81 27.07 2.12 o 1 7 9 1.46 0.99 1.82 o 2 7 9 1.63 1.13 2.02 o -3 8 9 55.84 55.26 2.52 o -2 8 9 19.44 20.03 2.05 o -1 8 9 0.44 -0.87 1.83 o 0 8 9 3.48 1.16 2.08 o -4 9 9 15.89 10.79 2.02 o -3 9 9 12.76 8.33 2.15 o -2 9 9 8.38 3.81 2.15 o 0 0 10 1404.79 1421.53 20.33 o 0 1 10 247.46 239.47 2.61 o 1 1 10 637.69 620.23 7.56 o -1 2 10 1140.86 1132.32 11.01 o 0 2 10 240.77 243.66 2.83 o 1 2 10 100.62 89.01 2.03 o 2 2 10 367.31 365.27 5.74 o -1 3 10 298.47 297.03 3.25 o 0 3 10 620.28 607.69 5.20 o 1 3 10 69.67 68.45 1.89 o 2 3 10 137.31 122.06 2.41 o 3 3 10 597.43 599.80 7.77 o -2 4 10 1052.70 1111.16 11.55 o -1 4 10 199.50 205.78 2.71 o 0 4 10 165.90 157.39 2.93 o 1 4 10 450.10 432.83 4.45 o 2 4 10 101.94 106.80 2.39 o 3 4 10 122.42 116.43 2.52 o 4 4 10 365.81 392.95 8.25 o -2 5 10 78.19 78.43 2.15 o -1 5 10 501.16 509.79 5.18 o 0 5 10 117.48 120.89 2.96 o 1 5 10 179.15 167.68 2.99 o 2 5 10 332.79 332.29 4.44 o 3 5 10 71.83 73.76 2.58 o -3 6 10 227.43 240.75 5.11 o -2 6 10 139.28 145.10 2.97 o -1 6 10 71.49 68.29 2.26 o 0 6 10 474.63 501.89 5.49 o 1 6 10 47.09 43.23 2.39 o 2 6 10 50.94 47.40 2.55 o -3 7 10 71.39 70.88 2.38 o -2 7 10 356.93 355.00 5.05 o -1 7 10 99.92 95.25 2.89 o 0 7 10 65.00 60.20 2.99 o 1 7 10 182.92 190.81 4.11 o -4 8 10 277.98 263.32 5.90 o -3 8 10 57.37 53.47 2.99 o -2 8 10 107.49 102.74 3.61 o -1 8 10 310.50 305.51 5.22 o 0 1 11 21.53 25.25 1.10 o 0 2 11 14.91 15.12 1.29 o 1 2 11 44.42 53.66 1.81 o -1 3 11 190.89 194.80 3.09 o 0 3 11 9.38 10.01 1.38 o 1 3 11 33.52 44.73 1.82 o 2 3 11 53.87 55.46 2.04 o -1 4 11 87.14 98.15 2.73 o 0 4 11 2.22 2.35 1.36 o 1 4 11 0.15 -0.50 1.36 o 2 4 11 33.26 33.68 1.90 o 3 4 11 108.99 104.57 2.74 o -2 5 11 44.82 48.22 2.20 o -1 5 11 13.34 7.69 1.73 o 0 5 11 28.17 32.19 1.99 o 1 5 11 24.91 27.62 2.04 o 2 5 11 2.82 3.46 1.79 o -2 6 11 2.07 1.18 1.71 o -1 6 11 28.70 26.20 2.15 o 0 6 11 0.64 2.21 1.72 o 1 6 11 21.82 14.80 2.29 o -3 7 11 24.02 19.22 2.11 o -2 7 11 0.15 0.39 1.86 o -1 7 11 23.74 21.73 2.39 o 0 0 12 436.33 459.85 9.76 o 0 1 12 55.58 50.56 2.21 o 1 1 12 372.05 351.97 7.56 o -1 2 12 418.83 400.14 7.85 o 0 2 12 170.03 171.75 3.07 o 1 2 12 141.48 134.13 2.69 o 2 2 12 564.99 569.94 8.02 o -1 3 12 173.41 162.03 3.34 o 0 3 12 353.69 342.33 4.90 o 1 3 12 50.82 49.75 2.03 o 2 3 12 25.38 23.72 1.85 o 3 3 12 292.59 310.91 6.18 o -2 4 12 791.13 810.95 12.37 o -1 4 12 67.97 71.36 3.18 o 0 4 12 104.50 103.64 3.07 o 1 4 12 156.71 149.84 3.32 o 2 4 12 109.12 116.21 3.85 o -2 5 12 45.08 46.86 2.71 o -1 5 12 205.40 204.30 4.27 o 0 5 12 65.19 68.56 2.82 o -3 6 12 349.38 343.78 8.18 o -2 6 12 129.68 124.11 3.46 o 0 1 13 19.13 21.52 2.08 o 0 2 13 6.35 3.83 1.64 o 1 2 13 115.72 116.71 2.92 o -1 3 13 38.45 39.82 2.62 o 0 3 13 10.81 9.03 1.94 o