#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104888.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104888_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9513 _cell_length_b 8.9513 _cell_length_c 9.5876 _exptl_crystal_F_000 358.00 _reflns_d_resolution_high 0.7005 _[local]_cod_data_source_file bk51012csup10.hkl _[local]_cod_data_source_block 2c #BEGIN Tags that were not found in dictionaries: _shelx_title ' m107c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3812.35 3847.65 25.16 o -1 2 0 5375.90 5481.26 26.87 o 0 2 0 5590.40 5627.67 30.16 o -1 3 0 371.81 384.81 2.02 o 0 3 0 1032.20 1035.42 7.72 o -2 4 0 3289.51 3374.97 18.15 o -1 4 0 592.90 578.07 3.32 o 0 4 0 1148.17 1212.61 9.28 o -2 5 0 13.27 9.61 0.50 o -1 5 0 3120.79 3080.96 13.62 o 0 5 0 1710.59 1755.28 13.11 o -3 6 0 1054.57 1016.46 7.99 o -2 6 0 547.12 526.36 3.39 o -1 6 0 1074.77 1097.42 6.09 o 0 6 0 3465.26 3635.54 23.89 o -3 7 0 735.55 735.57 4.48 o -2 7 0 1063.68 1121.60 6.38 o -1 7 0 134.06 145.41 1.99 o 0 7 0 1.02 0.95 1.03 o -4 8 0 1528.08 1546.66 11.18 o -3 8 0 99.78 98.29 1.57 o -2 8 0 453.86 471.69 3.77 o -1 8 0 753.65 803.02 5.40 o 0 8 0 320.89 339.26 4.64 o -4 9 0 114.75 106.10 1.82 o -3 9 0 718.51 739.42 5.36 o -2 9 0 240.15 244.07 2.92 o -1 9 0 196.82 185.03 2.55 o 0 9 0 375.20 399.64 5.80 o -5 10 0 993.21 1002.53 9.61 o -4 10 0 177.09 164.99 2.82 o -3 10 0 205.30 199.79 2.89 o -2 10 0 455.94 450.16 4.30 o -1 10 0 93.14 90.89 2.34 o 0 10 0 102.02 94.18 3.41 o -5 11 0 148.32 145.06 3.23 o -4 11 0 251.15 252.38 3.83 o -3 11 0 29.89 30.39 2.04 o -2 11 0 17.24 20.37 1.82 o -1 11 0 317.75 324.34 4.42 o 0 11 0 109.40 105.17 4.53 o -6 12 0 199.51 197.60 5.44 o -5 12 0 120.36 114.90 3.28 o -4 12 0 21.31 20.96 2.39 o -3 12 0 248.27 246.25 4.32 o 0 1 1 1025.97 872.53 2.75 o 0 2 1 1509.13 1655.87 5.84 o 1 2 1 3.73 3.61 0.21 o -1 3 1 2954.49 2987.59 11.58 o 0 3 1 186.95 198.75 1.26 o 1 3 1 433.93 423.25 2.31 o 2 3 1 327.98 321.73 2.18 o -1 4 1 1464.34 1494.41 6.73 o 0 4 1 484.42 465.04 2.96 o 1 4 1 0.27 0.55 0.40 o 2 4 1 399.73 382.48 2.69 o 3 4 1 322.11 319.28 2.62 o -2 5 1 415.45 439.20 2.96 o -1 5 1 142.41 161.42 1.49 o 0 5 1 1934.31 1906.91 9.46 o 1 5 1 438.66 428.62 3.10 o 2 5 1 205.84 210.41 2.39 o 3 5 1 51.69 49.03 1.41 o 4 5 1 62.78 68.41 1.62 o -2 6 1 17.43 22.64 0.80 o -1 6 1 532.01 521.39 3.39 o 0 6 1 5.42 5.64 0.71 o 1 6 1 9.82 7.18 0.78 o 2 6 1 5.36 4.80 0.86 o 3 6 1 51.55 49.80 1.50 o 4 6 1 35.59 40.43 2.05 o 5 6 1 124.19 128.39 3.11 o -3 7 1 33.83 38.23 0.91 o -2 7 1 92.64 96.35 1.54 o -1 7 1 57.03 47.94 1.27 o 0 7 1 82.04 59.39 1.48 o 1 7 1 35.69 29.81 1.30 o 2 7 1 75.37 76.31 1.87 o 3 7 1 24.43 26.37 1.56 o 4 7 1 4.74 4.70 1.71 o 5 7 1 1.10 0.26 1.80 o -3 8 1 36.89 38.77 1.31 o -2 8 1 21.29 19.20 0.95 o -1 8 1 79.33 68.56 1.60 o 0 8 1 1.67 1.03 0.90 o 1 8 1 37.27 36.58 1.59 o 2 8 1 7.33 5.64 1.31 o 3 8 1 20.58 18.95 1.76 o 4 8 1 31.54 40.33 2.45 o -4 9 1 57.54 59.51 1.61 o -3 9 1 0.30 0.11 0.90 o -2 9 1 233.01 241.85 2.87 o -1 9 1 115.40 110.70 2.19 o 0 9 1 24.67 24.30 1.52 o 1 9 1 54.10 57.69 2.10 o 2 9 1 14.48 16.61 1.81 o 3 9 1 1.95 -0.03 1.91 o -4 10 1 87.52 97.40 2.12 o -3 10 1 16.45 18.09 1.39 o -2 10 1 1.47 0.47 1.18 o -1 10 1 8.49 13.65 1.55 o 0 10 1 49.38 56.07 2.18 o 1 10 1 0.66 2.87 1.60 o -5 11 1 90.00 97.32 2.84 o -4 11 1 21.03 22.63 1.84 o -3 11 1 8.63 11.77 1.58 o -2 11 1 19.80 27.79 2.05 o -1 11 1 2.93 3.57 1.78 o 0 11 1 57.56 61.50 2.68 o -5 12 1 1.41 -0.87 1.91 o -4 12 1 13.02 13.92 2.17 o -3 12 1 0.01 -1.67 1.94 o 0 0 2 18608.18 15761.30 158.93 o 0 1 2 1333.15 1365.16 4.78 o 1 1 2 1710.06 1723.50 9.33 o -1 2 2 10550.55 9817.75 63.03 o 0 2 2 2455.75 2467.73 9.37 o 1 2 2 295.11 282.53 1.67 o 2 2 2 1187.59 1175.44 7.75 o -1 3 2 2593.10 2560.86 10.28 o 0 3 2 2669.88 2526.15 9.81 o 1 3 2 203.66 182.91 1.32 o 2 3 2 435.31 408.69 2.41 o 3 3 2 2993.73 2964.46 19.55 o -2 4 2 10135.84 9948.93 56.51 o -1 4 2 1181.16 1120.91 5.14 o 0 4 2 794.59 785.75 3.77 o 1 4 2 2021.95 2008.85 8.88 o 2 4 2 443.72 442.51 2.95 o 3 4 2 845.20 837.25 5.11 o 4 4 2 1411.14 1430.16 13.15 o -2 5 2 76.57 61.23 0.94 o -1 5 2 1861.66 1760.40 8.22 o 0 5 2 751.92 752.15 4.18 o 1 5 2 710.25 729.61 4.77 o 2 5 2 1284.93 1315.89 7.03 o 3 5 2 277.81 281.86 2.67 o 4 5 2 35.45 34.01 1.49 o 5 5 2 560.26 578.54 8.58 o -3 6 2 1070.41 1053.24 7.96 o -2 6 2 916.45 931.17 5.15 o -1 6 2 342.83 343.82 3.15 o 0 6 2 1988.67 2093.54 10.92 o 1 6 2 79.00 81.22 1.61 o 2 6 2 162.78 173.30 2.46 o 3 6 2 488.61 511.78 4.93 o 4 6 2 222.24 214.44 3.68 o 5 6 2 123.40 125.56 3.20 o 6 6 2 216.13 222.36 9.65 o -3 7 2 278.74 290.07 2.68 o -2 7 2 1219.98 1273.03 7.03 o -1 7 2 363.48 357.17 3.04 o 0 7 2 134.87 130.89 2.06 o 1 7 2 527.45 559.55 4.75 o 2 7 2 189.82 176.42 2.86 o 3 7 2 67.23 72.05 2.20 o 4 7 2 371.79 368.35 5.10 o 5 7 2 95.21 91.96 3.41 o -4 8 2 1185.86 1242.60 9.78 o -3 8 2 242.08 240.17 2.58 o -2 8 2 507.06 510.98 3.94 o -1 8 2 1334.16 1385.25 8.38 o 0 8 2 162.41 167.70 2.66 o 1 8 2 248.54 252.07 3.36 o 2 8 2 412.83 422.19 4.82 o 3 8 2 69.55 64.74 2.74 o 4 8 2 53.48 53.87 2.60 o -4 9 2 165.96 152.49 2.36 o -3 9 2 853.22 871.29 5.89 o -2 9 2 240.68 261.85 3.13 o -1 9 2 126.91 121.46 2.43 o 0 9 2 344.51 355.15 4.28 o 1 9 2 57.13 57.28 2.16 o 2 9 2 68.98 66.60 2.51 o 3 9 2 289.21 308.80 5.07 o -5 10 2 602.74 596.22 7.04 o -4 10 2 53.83 52.28 1.89 o -3 10 2 237.43 220.93 3.19 o -2 10 2 383.05 384.01 4.36 o -1 10 2 118.11 109.70 2.71 o 0 10 2 69.12 67.50 2.32 o 1 10 2 295.75 305.08 4.53 o -5 11 2 116.68 111.71 2.88 o -4 11 2 197.55 192.61 3.61 o -3 11 2 39.60 34.35 1.98 o -2 11 2 2.18 3.55 1.80 o -1 11 2 201.24 201.11 3.86 o -6 12 2 228.04 238.17 6.41 o -5 12 2 48.37 42.85 2.69 o -4 12 2 48.63 48.13 2.91 o -3 12 2 186.45 187.11 4.39 o 0 1 3 10.85 10.44 0.23 o 0 2 3 1138.15 1204.76 5.66 o 1 2 3 182.81 186.56 1.55 o -1 3 3 2557.10 2727.20 11.20 o 0 3 3 79.37 86.39 0.84 o 1 3 3 251.81 270.94 1.84 o 2 3 3 280.54 297.44 2.11 o -1 4 3 710.85 784.06 4.19 o 0 4 3 8.72 6.66 0.40 o 1 4 3 7.01 7.83 0.43 o 2 4 3 375.42 389.71 2.59 o 3 4 3 475.29 481.84 3.36 o -2 5 3 341.15 384.06 2.60 o -1 5 3 6.69 11.26 0.56 o 0 5 3 11.42 15.19 0.59 o 1 5 3 41.03 46.15 0.89 o 2 5 3 0.04 0.72 0.50 o 3 5 3 94.80 88.88 1.76 o 4 5 3 39.53 39.97 1.58 o -2 6 3 2.58 1.58 0.54 o -1 6 3 45.51 42.58 1.01 o 0 6 3 1.89 2.71 0.58 o 1 6 3 61.30 53.38 1.35 o 2 6 3 87.40 86.57 2.01 o 3 6 3 40.77 50.85 1.80 o 4 6 3 13.66 16.78 1.63 o 5 6 3 21.19 22.05 1.91 o -3 7 3 115.91 124.86 1.75 o -2 7 3 17.76 13.31 0.79 o -1 7 3 182.47 178.84 2.24 o 0 7 3 76.46 72.51 1.78 o 1 7 3 19.10 14.20 1.20 o 2 7 3 30.96 27.52 1.78 o 3 7 3 37.37 39.77 1.85 o 4 7 3 1.34 1.61 1.62 o 5 7 3 25.30 20.93 2.32 o -3 8 3 37.17 36.22 1.26 o -2 8 3 211.17 208.61 2.66 o -1 8 3 0.21 1.03 1.01 o 0 8 3 123.06 121.92 2.51 o 1 8 3 15.09 14.76 1.39 o 2 8 3 0.81 1.25 1.38 o 3 8 3 25.21 22.24 2.07 o 4 8 3 31.17 26.03 2.29 o -4 9 3 43.06 43.65 1.65 o -3 9 3 0.60 3.53 1.22 o -2 9 3 138.75 162.42 2.78 o -1 9 3 78.61 78.73 2.23 o 0 9 3 1.71 2.29 1.39 o 1 9 3 33.59 33.23 1.95 o 2 9 3 17.34 12.69 2.03 o -4 10 3 37.09 39.18 1.95 o -3 10 3 35.73 37.57 1.89 o -2 10 3 10.00 4.16 1.52 o -1 10 3 1.91 2.17 1.58 o 0 10 3 12.07 10.73 1.80 o 1 10 3 0.10 1.80 1.75 o -5 11 3 13.62 14.11 2.38 o -4 11 3 6.05 7.04 1.75 o -3 11 3 21.97 24.23 2.39 o -2 11 3 30.18 30.54 2.28 o -1 11 3 1.70 1.75 1.99 o -5 12 3 29.51 33.18 3.18 o -4 12 3 9.58 6.61 2.23 o 0 0 4 877.50 981.59 10.61 o 0 1 4 446.71 444.05 2.15 o 1 1 4 3752.71 3732.29 24.93 o -1 2 4 3966.98 3864.39 20.77 o 0 2 4 406.59 390.13 2.41 o 1 2 4 1363.21 1347.90 7.49 o 2 2 4 3415.45 3305.15 22.86 o -1 3 4 1131.87 1092.70 5.06 o 0 3 4 4125.78 3943.93 17.07 o 1 3 4 764.61 754.14 4.48 o 2 3 4 868.99 839.33 4.77 o 3 3 4 2314.99 2280.95 13.95 o -2 4 4 3354.63 3221.56 19.41 o -1 4 4 649.91 590.95 3.47 o 0 4 4 364.75 326.81 2.09 o 1 4 4 1509.32 1537.60 7.08 o 2 4 4 478.25 497.90 2.91 o 3 4 4 260.51 269.44 2.62 o 4 4 4 715.20 710.31 6.81 o -2 5 4 862.80 824.40 4.63 o -1 5 4 1324.71 1270.67 6.47 o 0 5 4 171.46 160.68 1.70 o 1 5 4 125.17 126.31 1.65 o 2 5 4 1347.87 1379.37 7.86 o 3 5 4 358.16 346.96 3.54 o 4 5 4 111.08 110.32 2.25 o 5 5 4 209.81 209.42 6.08 o -3 6 4 2597.46 2649.57 17.94 o -2 6 4 509.12 516.50 3.67 o -1 6 4 201.62 204.58 2.14 o 0 6 4 681.09 711.73 4.69 o 1 6 4 296.86 279.21 3.07 o 2 6 4 120.89 130.89 2.38 o 3 6 4 560.42 558.58 5.25 o 4 6 4 71.84 62.49 2.96 o 5 6 4 74.56 74.77 3.01 o 6 6 4 223.51 223.40 7.49 o -3 7 4 199.30 210.55 2.32 o -2 7 4 1328.08 1339.69 10.59 o -1 7 4 333.81 316.28 3.03 o 0 7 4 559.56 555.46 4.85 o 1 7 4 747.16 773.39 6.35 o 2 7 4 141.79 126.16 2.58 o 3 7 4 47.06 57.29 2.02 o 4 7 4 344.47 356.32 5.49 o 5 7 4 33.22 32.75 3.15 o -4 8 4 798.16 856.09 7.91 o -3 8 4 393.03 406.00 3.85 o -2 8 4 157.92 144.17 2.34 o -1 8 4 898.71 917.47 7.12 o 0 8 4 58.71 54.50 1.83 o 1 8 4 123.89 134.23 2.75 o 2 8 4 300.36 316.07 4.20 o 3 8 4 100.29 92.39 3.25 o 4 8 4 85.13 83.52 3.87 o -4 9 4 137.35 130.31 2.62 o -3 9 4 543.95 551.71 5.31 o -2 9 4 105.03 115.51 2.54 o -1 9 4 99.41 94.19 2.43 o 0 9 4 343.52 341.92 4.23 o 1 9 4 84.03 76.77 2.46 o 2 9 4 64.03 67.28 2.89 o -5 10 4 242.55 245.37 5.19 o -4 10 4 69.43 73.70 2.83 o -3 10 4 89.80 74.61 2.54 o -2 10 4 328.92 329.48 4.77 o -1 10 4 61.73 58.68 2.34 o 0 10 4 40.01 37.11 2.56 o 1 10 4 167.00 171.65 4.58 o -5 11 4 48.04 45.18 2.69 o -4 11 4 287.80 277.99 6.37 o -3 11 4 95.23 88.61 2.96 o -2 11 4 63.06 54.99 2.62 o -1 11 4 142.91 140.41 3.84 o -6 12 4 239.36 246.71 7.10 o -5 12 4 22.25 22.73 3.26 o -4 12 4 86.32 72.32 3.30 o 0 1 5 256.35 228.80 1.45 o 0 2 5 2070.14 2167.97 9.87 o 1 2 5 599.24 611.51 4.24 o -1 3 5 30.95 38.16 0.65 o 0 3 5 28.26 25.45 0.73 o 1 3 5 186.38 182.42 1.66 o 2 3 5 89.73 76.90 1.53 o -1 4 5 45.88 50.76 0.82 o 0 4 5 126.37 132.40 1.53 o 1 4 5 0.01 0.30 0.50 o 2 4 5 68.40 69.11 1.43 o 3 4 5 35.33 36.19 1.14 o -2 5 5 185.91 193.83 1.81 o -1 5 5 81.32 73.53 1.10 o 0 5 5 46.27 36.61 1.11 o 1 5 5 23.71 27.24 1.04 o 2 5 5 73.62 73.21 1.60 o 3 5 5 143.24 146.16 2.52 o 4 5 5 42.84 39.63 1.73 o -2 6 5 462.78 464.29 3.65 o -1 6 5 6.96 6.82 0.70 o 0 6 5 2.08 1.67 0.82 o 1 6 5 157.69 157.21 2.43 o 2 6 5 273.37 288.67 3.45 o 3 6 5 22.38 12.50 1.45 o 4 6 5 41.68 41.12 2.71 o 5 6 5 1.59 4.78 2.51 o -3 7 5 168.29 172.76 2.26 o -2 7 5 54.75 44.69 1.44 o -1 7 5 113.63 111.68 1.92 o 0 7 5 71.31 77.84 1.89 o 1 7 5 26.50 22.45 1.33 o 2 7 5 33.49 35.85 1.94 o 3 7 5 30.45 31.28 1.94 o 4 7 5 0.56 5.03 2.46 o -3 8 5 57.97 56.90 1.68 o -2 8 5 123.77 115.06 2.24 o -1 8 5 22.76 23.48 1.39 o 0 8 5 155.71 166.38 2.89 o 1 8 5 34.52 42.58 2.15 o 2 8 5 3.21 3.84 1.65 o 3 8 5 11.18 8.72 2.66 o -4 9 5 56.64 52.41 1.90 o -3 9 5 0.29 -0.35 1.24 o -2 9 5 2.12 1.73 1.34 o -1 9 5 12.34 11.06 1.48 o 0 9 5 11.16 6.99 1.75 o 1 9 5 10.97 9.54 1.90 o 2 9 5 14.57 8.37 2.48 o -4 10 5 8.83 6.57 1.59 o -3 10 5 54.55 52.35 2.34 o -2 10 5 0.20 1.20 1.48 o -1 10 5 32.68 31.14 2.49 o 0 10 5 5.41 5.68 2.19 o -5 11 5 3.00 1.95 1.98 o -4 11 5 16.18 15.17 2.15 o -3 11 5 48.52 44.83 2.42 o -2 11 5 21.18 19.75 2.31 o 0 0 6 61.33 58.60 1.73 o 0 1 6 634.27 657.31 3.17 o 1 1 6 3625.40 3746.02 24.30 o -1 2 6 1370.57 1415.04 8.23 o 0 2 6 155.92 157.32 1.56 o 1 2 6 915.67 931.16 5.64 o 2 2 6 2488.86 2471.23 18.25 o -1 3 6 189.48 185.32 1.45 o 0 3 6 2850.70 2899.82 15.20 o 1 3 6 959.49 976.58 6.20 o 2 3 6 751.98 747.53 5.29 o 3 3 6 831.35 840.08 8.35 o -2 4 6 275.12 273.25 2.96 o -1 4 6 369.65 355.87 2.87 o 0 4 6 280.82 292.76 2.57 o 1 4 6 1779.69 1830.58 9.85 o 2 4 6 218.28 211.81 2.76 o 3 4 6 46.86 49.89 1.56 o 4 4 6 328.56 332.93 5.16 o -2 5 6 1004.24 999.55 5.77 o -1 5 6 1610.36 1669.63 9.33 o 0 5 6 153.62 149.14 2.21 o 1 5 6 100.17 102.46 1.92 o 2 5 6 915.80 959.11 6.71 o 3 5 6 143.41 130.68 2.64 o 4 5 6 304.87 300.08 4.57 o 5 5 6 243.14 245.41 7.04 o -3 6 6 1754.90 1809.81 14.27 o -2 6 6 103.37 101.97 1.81 o -1 6 6 264.53 271.15 3.12 o 0 6 6 445.47 455.58 4.24 o 1 6 6 417.83 409.07 4.09 o 2 6 6 131.75 139.26 2.53 o 3 6 6 581.37 587.66 6.48 o 4 6 6 36.60 34.73 2.64 o 5 6 6 32.71 28.40 3.01 o -3 7 6 176.69 183.96 2.49 o -2 7 6 926.19 939.74 6.42 o -1 7 6 207.16 207.20 3.01 o 0 7 6 343.94 342.97 4.30 o 1 7 6 625.23 645.86 6.24 o 2 7 6 70.95 58.18 2.59 o 3 7 6 74.22 72.94 3.48 o 4 7 6 239.62 239.66 5.43 o -4 8 6 512.06 537.20 6.55 o -3 8 6 177.05 186.95 2.91 o -2 8 6 42.75 39.64 1.56 o -1 8 6 296.03 298.55 4.37 o 0 8 6 90.83 87.20 2.71 o 1 8 6 35.25 39.06 2.22 o 2 8 6 254.96 279.15 4.92 o 3 8 6 73.04 58.09 3.44 o -4 9 6 197.84 197.55 3.50 o -3 9 6 360.23 368.52 5.96 o -2 9 6 28.24 24.75 1.84 o -1 9 6 63.66 57.65 2.95 o 0 9 6 397.47 386.13 5.44 o 1 9 6 95.91 89.12 3.46 o -5 10 6 256.48 265.00 6.06 o -4 10 6 131.19 130.92 3.33 o -3 10 6 29.94 21.73 2.04 o -2 10 6 283.99 274.91 4.93 o -1 10 6 37.03 37.39 2.60 o -5 11 6 19.63 17.45 2.19 o -4 11 6 330.95 344.78 5.90 o -3 11 6 104.45 108.27 4.09 o 0 1 7 443.36 404.88 2.32 o 0 2 7 481.08 450.05 3.14 o 1 2 7 93.20 94.34 1.62 o -1 3 7 32.24 34.09 0.79 o 0 3 7 95.81 92.64 1.39 o 1 3 7 74.71 69.01 1.50 o 2 3 7 48.18 40.89 1.35 o -1 4 7 22.96 21.58 0.96 o 0 4 7 517.44 519.14 3.98 o 1 4 7 3.17 1.93 0.84 o 2 4 7 80.99 78.75 1.79 o 3 4 7 9.57 6.86 1.15 o -2 5 7 75.38 66.04 1.46 o -1 5 7 37.17 37.64 1.38 o 0 5 7 50.53 52.20 1.47 o 1 5 7 87.15 76.57 1.85 o 2 5 7 27.49 27.39 1.39 o 3 5 7 78.78 78.92 2.32 o 4 5 7 59.21 59.31 2.55 o -2 6 7 465.36 459.19 4.39 o -1 6 7 88.41 86.37 1.86 o 0 6 7 0.91 0.94 0.86 o 1 6 7 91.54 90.45 2.34 o 2 6 7 84.29 82.49 2.38 o 3 6 7 61.56 59.87 3.19 o 4 6 7 53.53 53.67 3.16 o -3 7 7 28.89 29.30 1.32 o -2 7 7 8.65 4.70 1.12 o -1 7 7 41.00 41.69 1.70 o 0 7 7 51.36 59.35 2.17 o 1 7 7 0.01 -1.60 1.60 o 2 7 7 10.88 10.94 2.07 o 3 7 7 23.46 22.72 2.70 o -3 8 7 85.37 86.30 2.19 o -2 8 7 22.41 20.94 1.61 o -1 8 7 1.70 0.94 1.48 o 0 8 7 25.40 24.93 1.96 o 1 8 7 32.62 28.88 2.50 o 2 8 7 0.00 -1.42 2.18 o -4 9 7 51.61 47.33 2.47 o -3 9 7 6.79 8.07 1.89 o -2 9 7 8.05 6.62 1.80 o -1 9 7 4.88 5.17 1.78 o 0 9 7 19.62 22.92 2.50 o -4 10 7 18.40 14.05 2.05 o -3 10 7 26.93 18.36 2.53 o -2 10 7 4.86 1.40 2.15 o 0 0 8 2268.70 2403.59 24.80 o 0 1 8 642.49 653.39 3.77 o 1 1 8 1666.12 1716.23 11.96 o -1 2 8 1338.90 1403.69 9.79 o 0 2 8 210.83 223.90 2.25 o 1 2 8 200.89 199.08 2.38 o 2 2 8 664.98 703.20 7.13 o -1 3 8 157.40 160.77 2.23 o 0 3 8 1257.48 1295.63 8.19 o 1 3 8 374.68 372.96 3.53 o 2 3 8 422.16 414.60 3.90 o 3 3 8 557.97 583.96 7.15 o -2 4 8 305.87 335.48 4.67 o -1 4 8 294.31 298.98 3.24 o 0 4 8 237.18 243.24 2.88 o 1 4 8 1292.09 1296.51 9.19 o 2 4 8 85.30 79.53 1.94 o 3 4 8 58.47 53.91 1.83 o 4 4 8 284.25 281.76 5.28 o -2 5 8 336.21 331.99 3.76 o -1 5 8 1211.73 1270.71 8.56 o 0 5 8 190.44 196.01 2.75 o 1 5 8 219.84 211.55 3.12 o 2 5 8 487.51 496.26 4.81 o 3 5 8 52.89 52.21 2.06 o 4 5 8 200.90 191.52 3.86 o 5 5 8 316.02 320.84 11.56 o -3 6 8 424.49 449.38 6.43 o -2 6 8 56.40 54.97 1.82 o -1 6 8 191.81 187.87 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