#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/48/2104889.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104889_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9572 _cell_length_b 8.9572 _cell_length_c 9.5926 _exptl_crystal_F_000 358.00 _reflns_d_resolution_high 0.7010 _[local]_cod_data_source_file bk51012dsup11.hkl _[local]_cod_data_source_block 2d #BEGIN Tags that were not found in dictionaries: _shelx_title ' m107b' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3819.53 3775.90 32.40 o -1 2 0 5360.78 5398.03 35.06 o 0 2 0 5557.56 5540.88 38.69 o -1 3 0 373.05 384.23 2.13 o 0 3 0 1036.54 1024.10 7.75 o -2 4 0 3281.36 3364.05 18.76 o -1 4 0 584.46 568.02 3.27 o 0 4 0 1151.42 1210.94 9.36 o -2 5 0 14.09 9.55 0.42 o -1 5 0 3074.81 3004.84 13.71 o 0 5 0 1666.96 1710.37 12.99 o -3 6 0 1025.63 997.65 7.63 o -2 6 0 534.47 521.42 3.28 o -1 6 0 1047.17 1079.23 6.00 o 0 6 0 3372.91 3546.18 23.84 o -3 7 0 706.62 709.30 4.24 o -2 7 0 1031.26 1090.10 6.20 o -1 7 0 132.40 143.84 1.90 o 0 7 0 0.97 1.14 0.95 o -4 8 0 1457.50 1496.64 10.76 o -3 8 0 94.90 92.53 1.51 o -2 8 0 432.84 445.76 3.46 o -1 8 0 713.74 761.96 5.03 o 0 8 0 302.65 322.26 4.24 o -4 9 0 109.31 101.71 1.65 o -3 9 0 680.53 705.09 4.95 o -2 9 0 225.17 233.35 2.64 o -1 9 0 184.91 170.93 2.28 o 0 9 0 350.69 356.15 5.12 o -5 10 0 931.49 932.40 8.86 o -4 10 0 168.13 157.40 2.56 o -3 10 0 191.11 187.99 2.59 o -2 10 0 427.06 417.35 3.87 o -1 10 0 84.70 79.66 2.05 o 0 10 0 94.78 83.94 3.03 o -5 11 0 138.00 131.07 2.81 o -4 11 0 235.06 227.94 3.42 o -3 11 0 27.62 28.77 1.80 o -2 11 0 16.71 18.05 1.63 o -1 11 0 289.53 292.57 3.90 o 0 11 0 99.31 102.28 4.69 o -6 12 0 187.42 184.00 4.95 o -5 12 0 109.85 107.59 2.96 o -4 12 0 19.76 18.48 1.90 o -3 12 0 222.96 220.86 3.84 o 0 1 1 1023.74 881.49 2.83 o 0 2 1 1507.80 1656.43 5.98 o 1 2 1 3.65 3.69 0.19 o -1 3 1 2940.27 2958.78 11.90 o 0 3 1 180.08 188.69 1.33 o 1 3 1 423.43 410.62 2.19 o 2 3 1 316.89 311.74 2.13 o -1 4 1 1446.80 1479.50 6.75 o 0 4 1 473.71 456.63 2.69 o 1 4 1 0.26 0.63 0.36 o 2 4 1 385.72 369.01 2.51 o 3 4 1 310.39 308.26 2.41 o -2 5 1 414.50 432.40 2.83 o -1 5 1 138.80 157.39 1.39 o 0 5 1 1880.62 1852.21 9.30 o 1 5 1 426.99 416.05 2.93 o 2 5 1 197.23 204.93 2.14 o 3 5 1 50.76 47.82 1.11 o 4 5 1 61.02 64.61 1.46 o -2 6 1 16.18 19.35 0.71 o -1 6 1 518.73 502.18 3.22 o 0 6 1 5.41 5.38 0.65 o 1 6 1 9.73 6.78 0.74 o 2 6 1 4.93 5.09 0.79 o 3 6 1 48.52 48.85 1.46 o 4 6 1 33.46 38.33 1.87 o 5 6 1 115.49 116.53 2.80 o -3 7 1 33.52 37.65 0.83 o -2 7 1 89.24 90.55 1.39 o -1 7 1 56.52 48.05 1.19 o 0 7 1 79.43 55.99 1.33 o 1 7 1 33.60 26.20 1.14 o 2 7 1 70.72 73.43 1.71 o 3 7 1 23.45 22.76 1.34 o 4 7 1 3.97 0.60 1.45 o 5 7 1 1.04 3.09 1.68 o -3 8 1 37.21 38.28 1.00 o -2 8 1 20.83 18.16 0.85 o -1 8 1 74.72 64.46 1.45 o 0 8 1 1.57 2.43 0.86 o 1 8 1 35.07 30.87 1.37 o 2 8 1 6.91 4.81 1.15 o 3 8 1 18.82 20.90 1.66 o 4 8 1 28.09 28.23 2.08 o -4 9 1 54.83 56.28 1.45 o -3 9 1 0.34 1.67 0.84 o -2 9 1 220.21 227.59 2.62 o -1 9 1 109.06 102.61 1.97 o 0 9 1 22.70 24.89 1.50 o 1 9 1 51.26 50.69 1.84 o 2 9 1 13.59 14.59 1.63 o 3 9 1 1.65 -1.74 1.74 o -4 10 1 80.44 89.36 1.90 o -3 10 1 16.08 20.07 1.31 o -2 10 1 1.39 -1.01 1.01 o -1 10 1 8.19 14.40 1.42 o 0 10 1 45.17 50.31 1.92 o 1 10 1 0.54 0.49 1.42 o -5 11 1 81.61 89.52 2.47 o -4 11 1 18.51 20.14 1.61 o -3 11 1 7.74 10.88 1.40 o -2 11 1 17.91 19.15 1.61 o -1 11 1 2.67 2.26 1.59 o 0 11 1 51.22 52.97 2.36 o -5 12 1 1.24 0.72 1.75 o -4 12 1 11.14 9.25 1.73 o -3 12 1 0.01 2.72 1.73 o 0 0 2 18546.40 15372.08 156.10 o 0 1 2 1327.69 1361.62 4.85 o 1 1 2 1701.61 1726.75 9.53 o -1 2 2 10489.13 9702.27 80.25 o 0 2 2 2438.85 2444.02 9.52 o 1 2 2 295.70 286.10 1.64 o 2 2 2 1190.93 1185.72 7.84 o -1 3 2 2565.21 2534.04 10.45 o 0 3 2 2645.88 2505.75 9.95 o 1 3 2 202.81 175.68 1.22 o 2 3 2 431.83 405.54 2.33 o 3 3 2 2928.51 2907.88 19.42 o -2 4 2 9959.89 9697.44 57.41 o -1 4 2 1156.16 1099.02 5.09 o 0 4 2 788.43 781.24 3.74 o 1 4 2 2000.24 1988.50 8.89 o 2 4 2 434.58 435.10 2.79 o 3 4 2 817.42 820.83 4.88 o 4 4 2 1355.21 1370.67 10.62 o -2 5 2 75.94 60.78 0.87 o -1 5 2 1818.95 1724.77 8.19 o 0 5 2 733.36 738.49 4.08 o 1 5 2 691.39 720.22 4.61 o 2 5 2 1246.93 1272.33 7.37 o 3 5 2 269.33 264.84 2.41 o 4 5 2 34.09 34.00 1.35 o 5 5 2 527.01 539.48 9.44 o -3 6 2 1038.46 1014.01 7.28 o -2 6 2 885.42 902.85 4.95 o -1 6 2 333.81 343.45 2.74 o 0 6 2 1926.36 2047.15 10.75 o 1 6 2 78.94 81.05 1.49 o 2 6 2 153.33 158.54 2.19 o 3 6 2 461.97 488.03 4.53 o 4 6 2 207.26 197.37 3.51 o 5 6 2 114.26 116.51 2.87 o 6 6 2 197.29 201.90 5.38 o -3 7 2 267.69 281.94 2.49 o -2 7 2 1172.53 1224.56 6.76 o -1 7 2 348.90 339.37 2.82 o 0 7 2 128.79 124.07 1.87 o 1 7 2 502.08 536.52 4.41 o 2 7 2 177.24 161.28 2.53 o 3 7 2 63.10 68.43 1.98 o 4 7 2 342.56 354.24 4.71 o 5 7 2 85.84 85.79 2.76 o -4 8 2 1129.40 1179.58 9.18 o -3 8 2 228.70 228.87 2.37 o -2 8 2 485.94 483.78 3.67 o -1 8 2 1269.17 1300.95 7.86 o 0 8 2 154.47 161.18 2.44 o 1 8 2 233.28 239.16 3.07 o 2 8 2 382.17 389.50 4.53 o 3 8 2 62.81 56.73 2.35 o 4 8 2 48.95 46.89 2.30 o -4 9 2 158.27 143.16 2.13 o -3 9 2 811.00 823.52 5.46 o -2 9 2 228.87 245.41 2.83 o -1 9 2 118.35 113.60 2.20 o 0 9 2 322.44 327.46 3.86 o 1 9 2 52.14 48.81 1.85 o 2 9 2 64.28 62.19 2.27 o 3 9 2 260.53 283.48 4.59 o -5 10 2 564.77 558.80 6.46 o -4 10 2 51.42 54.17 1.76 o -3 10 2 221.80 203.83 2.89 o -2 10 2 360.65 360.05 3.94 o -1 10 2 109.82 105.56 2.46 o 0 10 2 63.79 62.29 2.27 o 1 10 2 268.64 280.61 4.07 o -5 11 2 107.71 104.27 2.58 o -4 11 2 185.71 183.03 3.23 o -3 11 2 37.69 32.79 1.74 o -2 11 2 2.16 0.16 1.58 o -1 11 2 182.71 188.77 3.43 o -6 12 2 210.22 214.79 5.73 o -5 12 2 44.72 34.57 2.33 o -4 12 2 44.56 44.56 2.62 o -3 12 2 169.11 157.86 3.77 o 0 1 3 10.90 10.04 0.21 o 0 2 3 1125.61 1198.77 5.68 o 1 2 3 181.22 186.34 1.47 o -1 3 3 2543.73 2732.28 11.54 o 0 3 3 76.35 85.22 0.79 o 1 3 3 246.44 270.83 1.65 o 2 3 3 272.62 286.35 1.96 o -1 4 3 699.40 775.98 4.14 o 0 4 3 9.55 7.91 0.43 o 1 4 3 6.75 6.58 0.37 o 2 4 3 366.47 374.91 2.42 o 3 4 3 456.76 458.59 3.11 o -2 5 3 341.47 384.55 2.53 o -1 5 3 7.30 11.49 0.52 o 0 5 3 11.51 14.48 0.54 o 1 5 3 39.03 44.88 0.81 o 2 5 3 0.02 0.26 0.45 o 3 5 3 88.74 83.09 1.52 o 4 5 3 37.51 37.92 1.42 o -2 6 3 2.44 2.59 0.50 o -1 6 3 44.24 41.29 0.93 o 0 6 3 1.92 2.57 0.55 o 1 6 3 57.98 52.06 1.25 o 2 6 3 82.36 81.10 1.80 o 3 6 3 38.44 46.48 1.60 o 4 6 3 13.09 16.14 1.49 o 5 6 3 19.88 20.41 1.75 o -3 7 3 114.08 123.14 1.64 o -2 7 3 16.60 12.98 0.72 o -1 7 3 174.44 170.97 2.06 o 0 7 3 71.93 67.54 1.60 o 1 7 3 18.28 13.30 1.09 o 2 7 3 28.83 28.80 1.49 o 3 7 3 34.20 34.03 1.70 o 4 7 3 1.19 1.03 1.47 o 5 7 3 23.28 24.66 2.12 o -3 8 3 36.38 37.46 1.17 o -2 8 3 200.37 191.78 2.40 o -1 8 3 0.23 -0.92 0.92 o 0 8 3 116.07 111.39 2.24 o 1 8 3 14.06 15.84 1.29 o 2 8 3 0.72 0.44 1.24 o 3 8 3 23.68 22.83 1.97 o 4 8 3 29.34 31.59 2.39 o -4 9 3 40.50 37.45 1.44 o -3 9 3 0.68 1.12 1.03 o -2 9 3 130.63 151.99 2.50 o -1 9 3 73.33 79.27 2.09 o 0 9 3 1.52 1.50 1.30 o 1 9 3 30.91 28.82 1.71 o 2 9 3 16.39 19.97 1.82 o -4 10 3 34.33 37.95 1.79 o -3 10 3 32.63 32.96 1.68 o -2 10 3 9.45 6.05 1.78 o -1 10 3 1.69 4.85 1.53 o 0 10 3 11.23 9.01 1.53 o 1 10 3 0.09 0.24 1.55 o -5 11 3 11.83 10.86 1.70 o -4 11 3 5.63 4.91 1.53 o -3 11 3 20.09 22.16 1.91 o -2 11 3 27.19 27.62 1.99 o -1 11 3 1.44 1.37 1.77 o -5 12 3 26.18 23.56 2.89 o -4 12 3 8.93 5.27 2.04 o 0 0 4 847.52 937.71 8.82 o 0 1 4 442.50 443.34 2.12 o 1 1 4 3718.72 3675.05 25.12 o -1 2 4 3928.79 3836.59 21.09 o 0 2 4 403.32 383.09 2.33 o 1 2 4 1346.36 1319.93 7.33 o 2 2 4 3330.72 3213.50 22.62 o -1 3 4 1116.55 1084.18 5.06 o 0 3 4 4036.78 3873.57 17.19 o 1 3 4 742.83 727.46 4.28 o 2 3 4 840.20 823.97 4.62 o 3 3 4 2247.86 2235.10 13.82 o -2 4 4 3270.40 3144.83 19.47 o -1 4 4 633.53 575.53 3.36 o 0 4 4 354.40 321.87 2.00 o 1 4 4 1466.27 1501.13 6.94 o 2 4 4 462.06 477.75 2.75 o 3 4 4 251.96 260.82 2.41 o 4 4 4 685.10 689.46 6.43 o -2 5 4 831.70 800.60 4.49 o -1 5 4 1286.21 1225.52 6.75 o 0 5 4 168.67 155.75 1.58 o 1 5 4 121.59 123.12 1.44 o 2 5 4 1291.36 1329.73 7.51 o 3 5 4 345.44 330.26 3.23 o 4 5 4 104.84 103.98 2.02 o 5 5 4 199.00 196.71 6.16 o -3 6 4 2513.08 2558.22 18.97 o -2 6 4 491.40 499.14 3.47 o -1 6 4 194.96 201.95 2.01 o 0 6 4 654.15 683.47 4.46 o 1 6 4 283.34 264.61 2.81 o 2 6 4 114.54 126.10 2.17 o 3 6 4 529.98 526.71 4.79 o 4 6 4 66.00 57.50 2.26 o 5 6 4 68.20 68.67 2.37 o 6 6 4 197.97 205.04 6.75 o -3 7 4 193.47 205.97 2.17 o -2 7 4 1270.58 1270.46 8.35 o -1 7 4 317.38 306.43 2.83 o 0 7 4 530.37 530.90 4.72 o 1 7 4 714.74 729.08 5.86 o 2 7 4 134.15 118.24 2.33 o 3 7 4 44.92 56.84 1.88 o 4 7 4 314.02 328.05 4.97 o 5 7 4 29.93 29.97 2.88 o -4 8 4 763.06 807.67 7.41 o -3 8 4 374.43 389.98 3.58 o -2 8 4 150.51 140.18 2.15 o -1 8 4 854.96 879.18 6.69 o 0 8 4 55.91 48.70 1.65 o 1 8 4 116.23 129.86 2.72 o 2 8 4 276.57 292.84 3.79 o 3 8 4 91.02 80.72 2.89 o 4 8 4 76.50 71.01 3.46 o -4 9 4 129.46 125.13 2.37 o -3 9 4 513.29 522.35 4.90 o -2 9 4 99.87 106.13 2.28 o -1 9 4 92.78 91.02 2.20 o 0 9 4 319.48 322.38 5.13 o 1 9 4 78.19 70.69 2.48 o 2 9 4 57.75 58.16 2.38 o -5 10 4 228.09 229.15 4.68 o -4 10 4 63.80 70.16 2.15 o -3 10 4 83.97 74.69 2.35 o -2 10 4 303.22 298.94 4.25 o -1 10 4 58.27 54.28 2.09 o 0 10 4 36.36 35.01 2.26 o 1 10 4 150.49 163.53 3.57 o -5 11 4 44.35 42.37 2.19 o -4 11 4 263.87 259.20 4.11 o -3 11 4 87.64 85.94 2.69 o -2 11 4 56.51 50.26 2.47 o -1 11 4 129.79 122.64 3.37 o -6 12 4 213.67 221.77 6.31 o -5 12 4 20.42 16.46 2.24 o -4 12 4 77.98 74.96 2.93 o 0 1 5 248.52 221.30 1.35 o 0 2 5 2020.82 2117.93 9.81 o 1 2 5 593.76 604.13 4.06 o -1 3 5 31.58 39.25 0.62 o 0 3 5 25.77 22.47 0.73 o 1 3 5 185.09 184.53 1.70 o 2 3 5 91.05 77.48 1.41 o -1 4 5 45.28 50.84 0.83 o 0 4 5 124.91 127.92 1.40 o 1 4 5 0.00 0.00 0.44 o 2 4 5 68.69 66.71 1.29 o 3 4 5 35.29 36.66 1.15 o -2 5 5 179.14 187.86 1.75 o -1 5 5 75.93 69.72 1.00 o 0 5 5 41.62 30.84 0.99 o 1 5 5 22.77 26.17 0.96 o 2 5 5 67.76 68.56 1.59 o 3 5 5 131.67 132.00 2.21 o 4 5 5 39.02 40.46 1.52 o -2 6 5 441.80 442.86 3.41 o -1 6 5 6.93 6.69 0.64 o 0 6 5 2.11 1.20 0.61 o 1 6 5 148.97 145.85 2.20 o 2 6 5 255.90 272.83 3.12 o 3 6 5 20.33 13.59 1.33 o 4 6 5 38.65 32.97 2.35 o 5 6 5 1.40 -2.07 2.07 o -3 7 5 162.12 163.10 2.24 o -2 7 5 51.04 44.16 1.21 o -1 7 5 106.60 106.61 1.74 o 0 7 5 66.69 78.86 1.76 o 1 7 5 24.67 20.84 1.47 o 2 7 5 31.55 30.72 1.71 o 3 7 5 27.31 32.53 1.80 o 4 7 5 0.44 1.21 2.21 o -3 8 5 53.97 53.05 1.53 o -2 8 5 117.07 109.38 2.03 o -1 8 5 21.07 21.13 1.40 o 0 8 5 144.93 153.44 2.60 o 1 8 5 32.06 37.65 2.38 o 2 8 5 3.17 4.32 1.63 o 3 8 5 10.55 5.23 2.33 o -4 9 5 53.35 46.41 1.79 o -3 9 5 0.32 0.06 1.16 o -2 9 5 2.07 3.04 1.20 o -1 9 5 11.17 12.37 1.49 o 0 9 5 10.02 5.62 1.60 o 1 9 5 9.55 6.76 1.70 o 2 9 5 13.42 13.45 2.36 o -4 10 5 8.74 9.70 1.50 o -3 10 5 48.70 46.81 2.08 o -2 10 5 0.16 1.41 1.38 o -1 10 5 29.18 26.58 2.14 o 0 10 5 5.26 3.54 1.95 o -5 11 5 2.97 0.41 1.68 o -4 11 5 13.80 10.43 1.81 o -3 11 5 43.86 45.61 2.44 o -2 11 5 19.33 16.08 2.05 o 0 0 6 68.12 65.18 1.70 o 0 1 6 620.84 645.37 3.09 o 1 1 6 3544.87 3682.84 24.40 o -1 2 6 1342.97 1387.66 8.13 o 0 2 6 155.46 156.13 1.67 o 1 2 6 889.78 907.09 5.43 o 2 2 6 2394.73 2387.49 17.73 o -1 3 6 187.13 184.75 1.40 o 0 3 6 2753.12 2802.29 13.36 o 1 3 6 922.34 936.48 5.86 o 2 3 6 707.81 712.73 4.93 o 3 3 6 791.58 807.22 7.84 o -2 4 6 275.53 281.10 2.86 o -1 4 6 358.16 341.05 2.68 o 0 4 6 268.97 280.92 2.36 o 1 4 6 1690.30 1755.25 9.85 o 2 4 6 208.71 205.15 2.53 o 3 4 6 45.12 48.93 1.40 o 4 4 6 310.32 317.07 4.69 o -2 5 6 957.21 961.46 5.54 o -1 5 6 1550.54 1604.79 9.02 o 0 5 6 150.09 150.96 2.08 o 1 5 6 95.72 96.18 1.58 o 2 5 6 862.43 898.89 6.16 o 3 5 6 135.08 121.73 2.74 o 4 5 6 281.39 278.90 4.08 o 5 5 6 227.08 236.63 6.56 o -3 6 6 1685.34 1757.51 13.94 o -2 6 6 101.20 99.91 1.56 o -1 6 6 253.91 257.18 2.84 o 0 6 6 426.40 437.67 3.96 o 1 6 6 389.35 379.72 3.71 o 2 6 6 125.63 126.70 2.24 o 3 6 6 542.05 543.81 5.83 o 4 6 6 33.50 31.03 2.97 o 5 6 6 29.84 26.50 2.70 o -3 7 6 170.80 175.84 2.30 o -2 7 6 879.30 883.26 6.01 o -1 7 6 195.02 193.69 2.63 o 0 7 6 320.74 322.01 3.89 o 1 7 6 588.98 610.97 5.93 o 2 7 6 66.92 57.81 2.29 o 3 7 6 69.35 69.44 2.98 o 4 7 6 216.21 213.54 4.83 o -4 8 6 483.34 504.51 6.06 o -3 8 6 167.73 171.85 2.62 o -2 8 6 40.41 36.39 1.51 o -1 8 6 278.69 283.66 3.97 o 0 8 6 83.29 78.37 2.41 o 1 8 6 33.08 40.07 2.05 o 2 8 6 232.56 247.31 4.31 o 3 8 6 66.30 54.29 3.15 o -4 9 6 180.60 179.65 3.09 o -3 9 6 333.19 344.14 4.29 o -2 9 6 26.44 23.49 1.66 o -1 9 6 59.86 57.27 2.31 o 0 9 6 361.20 364.30 4.94 o 1 9 6 87.89 79.63 3.12 o -5 10 6 237.41 235.51 6.06 o -4 10 6 118.70 116.69 2.90 o -3 10 6 27.76 22.16 1.88 o -2 10 6 255.82 248.38 4.36 o -1 10 6 33.86 32.02 2.32 o -5 11 6 18.45 16.16 2.01 o -4 11 6 296.33 301.47 5.16 o -3 11 6 92.63 95.97 3.17 o 0 1 7 428.87 386.55 2.15 o 0 2 7 460.17 434.90 2.95 o 1 2 7 93.65 91.43 1.46 o -1 3 7 30.06 31.93 0.74 o 0 3 7 88.05 87.13 1.25 o 1 3 7 74.51 66.78 1.38 o 2 3 7 48.46 43.77 1.26 o -1 4 7 23.00 20.49 0.89 o 0 4 7 488.43 488.96 3.89 o 1 4 7 2.98 1.16 0.76 o 2 4 7 77.85 73.65 1.60 o 3 4 7 8.01 6.74 1.06 o -2 5 7 70.72 63.23 1.33 o -1 5 7 35.40 33.82 1.22 o 0 5 7 50.55 52.23 1.61 o 1 5 7 83.61 75.13 1.68 o 2 5 7 24.73 23.07 1.22 o 3 5 7 72.81 67.79 2.03 o 4 5 7 53.88 52.88 2.27 o -2 6 7 433.98 429.07 4.02 o -1 6 7 84.26 85.04 1.72 o 0 6 7 0.87 0.60 0.76 o 1 6 7 86.38 86.43 2.11 o 2 6 7 78.72 77.11 2.16 o 3 6 7 55.10 57.59 2.30 o 4 6 7 48.53 47.00 2.78 o -3 7 7 27.42 25.96 1.17 o -2 7 7 7.75 4.95 0.96 o -1 7 7 38.14 40.83 1.56 o 0 7 7 48.62 49.85 1.87 o 1 7 7 0.00 0.05 1.47 o 2 7 7 10.48 10.08 1.85 o 3 7 7 21.31 22.17 2.42 o -3 8 7 78.28 80.25 2.68 o -2 8 7 21.44 20.91 1.50 o -1 8 7 1.39 1.15 1.34 o 0 8 7 23.28 23.99 1.77 o 1 8 7 30.18 29.44 2.26 o 2 8 7 0.00 -2.01 2.01 o -4 9 7 48.04 44.00 1.78 o -3 9 7 5.57 6.25 1.68 o 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