#------------------------------------------------------------------------------ #$Date: 2011-03-09 10:38:09 +0200 (Wed, 09 Mar 2011) $ #$Revision: 14261 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2104890.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104890_Fobs loop_ _publ_author_name 'Smeets, Stef' 'Parois, Pascal' 'B\"urgi, Hans-Beat' 'Lutz, Martin' _publ_section_title ; Temperature-dependent analysis of thermal motion, disorder and structures of tris(ethylenediamine)zinc(II) sulfate and tris(ethylenediamine)copper(II) sulfate ; _journal_coeditor_code BK5101 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 53 _journal_page_last 62 _journal_volume 67 _journal_year 2011 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 8.9664 _cell_length_b 8.9664 _cell_length_c 9.5996 _exptl_crystal_F_000 358.00 _reflns_d_resolution_high 0.7005 _[local]_cod_data_source_file bk51012esup12.hkl _[local]_cod_data_source_block 2e #BEGIN Tags that were not found in dictionaries: _shelx_title ' m107a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' 'x, x-y, -z+1/2' '-x+y, y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' '-x, -x+y, z-1/2' 'x-y, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3829.01 3741.33 40.39 o -1 2 0 5339.19 5330.38 43.28 o 0 2 0 5548.23 5440.87 37.52 o -1 3 0 368.99 388.02 2.09 o 0 3 0 1037.23 1041.62 8.30 o -2 4 0 3258.12 3340.01 19.94 o -1 4 0 577.06 556.62 3.32 o 0 4 0 1139.93 1195.59 9.73 o -2 5 0 14.08 10.83 0.43 o -1 5 0 3007.51 2958.00 14.40 o 0 5 0 1626.15 1659.52 13.34 o -3 6 0 1000.15 969.31 7.41 o -2 6 0 523.52 510.86 3.31 o -1 6 0 1007.10 1037.85 6.04 o 0 6 0 3251.60 3438.35 24.71 o -3 7 0 673.93 679.72 4.25 o -2 7 0 996.95 1056.08 6.27 o -1 7 0 130.18 139.96 1.81 o 0 7 0 0.89 0.93 0.93 o -4 8 0 1382.78 1419.08 10.84 o -3 8 0 90.04 89.49 1.42 o -2 8 0 406.28 419.01 3.36 o -1 8 0 668.66 720.11 4.95 o 0 8 0 280.56 302.45 4.11 o -4 9 0 105.50 95.50 1.58 o -3 9 0 641.29 668.49 4.88 o -2 9 0 208.93 218.18 2.55 o -1 9 0 170.98 164.87 2.22 o 0 9 0 324.93 330.89 4.90 o -5 10 0 861.06 849.95 9.20 o -4 10 0 156.12 143.54 2.42 o -3 10 0 176.77 166.82 2.42 o -2 10 0 394.45 385.41 3.71 o -1 10 0 75.80 73.95 1.96 o 0 10 0 85.33 73.60 2.82 o -5 11 0 126.88 117.98 2.67 o -4 11 0 219.05 220.17 3.31 o -3 11 0 25.69 23.16 1.68 o -2 11 0 15.83 16.14 1.59 o -1 11 0 256.06 263.88 3.69 o 0 11 0 86.50 83.23 5.35 o -6 12 0 169.00 171.27 4.72 o -5 12 0 95.94 92.54 2.74 o -4 12 0 18.22 19.55 1.83 o -3 12 0 196.07 198.26 3.62 o 0 1 1 1022.57 873.50 3.02 o 0 2 1 1517.28 1652.79 6.41 o 1 2 1 3.75 3.60 0.19 o -1 3 1 2927.60 2910.91 12.27 o 0 3 1 171.25 177.54 1.21 o 1 3 1 413.69 402.74 2.25 o 2 3 1 309.56 305.72 2.07 o -1 4 1 1424.06 1449.48 7.03 o 0 4 1 460.98 449.36 2.55 o 1 4 1 0.10 0.24 0.36 o 2 4 1 376.58 353.81 2.50 o 3 4 1 299.02 292.59 2.38 o -2 5 1 412.00 434.99 2.90 o -1 5 1 135.06 154.17 1.37 o 0 5 1 1818.23 1797.02 9.58 o 1 5 1 412.36 403.72 2.91 o 2 5 1 186.11 197.49 2.19 o 3 5 1 49.03 47.62 1.09 o 4 5 1 56.01 60.80 1.41 o -2 6 1 14.15 18.59 0.68 o -1 6 1 498.09 486.63 3.21 o 0 6 1 4.63 4.92 0.63 o 1 6 1 9.97 7.27 0.72 o 2 6 1 4.58 3.55 0.76 o 3 6 1 44.39 39.79 1.27 o 4 6 1 29.86 33.37 1.75 o 5 6 1 102.63 109.10 2.69 o -3 7 1 33.22 35.66 0.82 o -2 7 1 85.07 86.30 1.34 o -1 7 1 54.23 46.43 1.16 o 0 7 1 74.17 55.50 1.30 o 1 7 1 32.55 28.81 1.14 o 2 7 1 63.59 62.15 1.57 o 3 7 1 23.44 26.83 1.37 o 4 7 1 3.43 1.38 1.40 o 5 7 1 1.07 2.28 1.61 o -3 8 1 36.62 36.04 0.96 o -2 8 1 19.61 16.65 0.82 o -1 8 1 67.46 58.56 1.37 o 0 8 1 1.45 1.17 0.83 o 1 8 1 33.47 29.62 1.33 o 2 8 1 5.83 2.31 1.12 o 3 8 1 17.50 18.57 1.59 o 4 8 1 24.08 23.72 1.98 o -4 9 1 51.71 50.48 1.54 o -3 9 1 0.29 0.91 0.81 o -2 9 1 200.85 211.61 2.49 o -1 9 1 102.22 98.32 1.90 o 0 9 1 19.79 24.20 1.36 o 1 9 1 47.54 49.71 1.78 o 2 9 1 12.60 15.69 1.61 o 3 9 1 1.35 -0.40 1.71 o -4 10 1 74.36 85.33 1.82 o -3 10 1 15.11 16.37 1.22 o -2 10 1 1.23 0.48 1.04 o -1 10 1 8.09 14.10 1.41 o 0 10 1 40.31 45.55 1.86 o 1 10 1 0.53 -0.46 1.37 o -5 11 1 71.23 77.44 2.28 o -4 11 1 16.10 13.96 1.47 o -3 11 1 7.02 9.27 1.37 o -2 11 1 16.04 14.31 1.55 o -1 11 1 2.26 2.47 1.57 o 0 11 1 44.32 43.02 2.19 o -5 12 1 1.09 -0.64 1.67 o -4 12 1 10.07 9.63 1.82 o -3 12 1 0.01 3.13 1.67 o 0 0 2 18547.00 14457.68 124.31 o 0 1 2 1320.70 1356.32 5.21 o 1 1 2 1691.62 1709.72 10.23 o -1 2 2 10402.90 9429.72 76.90 o 0 2 2 2416.18 2408.18 9.95 o 1 2 2 296.51 288.39 1.71 o 2 2 2 1198.62 1174.94 8.29 o -1 3 2 2550.26 2504.87 11.12 o 0 3 2 2622.07 2479.92 10.60 o 1 3 2 195.34 172.23 1.23 o 2 3 2 425.19 400.02 2.38 o 3 3 2 2841.55 2825.62 20.32 o -2 4 2 9743.52 9433.40 60.26 o -1 4 2 1133.46 1079.95 5.28 o 0 4 2 781.63 776.38 3.90 o 1 4 2 1956.66 1953.94 9.34 o 2 4 2 423.02 429.45 2.85 o 3 4 2 783.26 788.46 4.94 o 4 4 2 1295.61 1310.21 10.76 o -2 5 2 74.97 60.78 0.86 o -1 5 2 1784.33 1666.73 8.38 o 0 5 2 716.20 718.84 4.14 o 1 5 2 673.09 695.10 4.64 o 2 5 2 1204.63 1237.40 6.93 o 3 5 2 252.65 251.01 2.37 o 4 5 2 33.78 32.98 1.32 o 5 5 2 481.78 509.99 7.64 o -3 6 2 1001.45 984.21 7.37 o -2 6 2 859.16 875.58 5.02 o -1 6 2 317.67 329.19 2.90 o 0 6 2 1858.39 1972.02 11.00 o 1 6 2 79.21 76.79 1.44 o 2 6 2 147.45 151.98 2.03 o 3 6 2 434.10 457.00 4.56 o 4 6 2 191.29 182.92 3.17 o 5 6 2 103.78 104.40 2.69 o 6 6 2 180.39 190.76 5.22 o -3 7 2 254.91 262.88 2.39 o -2 7 2 1123.81 1181.27 6.83 o -1 7 2 330.65 330.93 2.78 o 0 7 2 124.63 119.97 1.87 o 1 7 2 473.35 502.16 4.69 o 2 7 2 163.15 155.41 2.47 o 3 7 2 59.21 63.46 1.91 o 4 7 2 311.75 320.63 4.75 o 5 7 2 74.90 70.93 2.61 o -4 8 2 1068.21 1110.40 9.14 o -3 8 2 221.13 221.01 2.31 o -2 8 2 453.13 448.77 3.53 o -1 8 2 1191.97 1237.52 7.85 o 0 8 2 144.11 149.19 2.33 o 1 8 2 212.35 215.91 2.90 o 2 8 2 352.79 355.11 4.13 o 3 8 2 57.21 54.47 2.27 o 4 8 2 44.40 41.30 2.18 o -4 9 2 148.85 134.15 2.04 o -3 9 2 761.56 769.33 5.32 o -2 9 2 213.80 231.52 2.72 o -1 9 2 111.98 105.12 2.10 o 0 9 2 297.94 309.07 3.73 o 1 9 2 46.73 44.28 1.75 o 2 9 2 57.58 56.38 2.15 o 3 9 2 227.09 239.01 4.15 o -5 10 2 531.54 527.47 6.24 o -4 10 2 48.63 48.09 1.65 o -3 10 2 201.99 190.52 2.75 o -2 10 2 327.88 323.99 4.01 o -1 10 2 100.45 95.06 2.58 o 0 10 2 56.98 52.42 1.94 o 1 10 2 240.08 248.67 3.81 o -5 11 2 98.52 90.96 2.41 o -4 11 2 171.89 165.35 2.82 o -3 11 2 34.13 29.38 1.66 o -2 11 2 2.30 1.20 1.55 o -1 11 2 161.76 168.12 3.29 o -6 12 2 185.97 203.63 7.23 o -5 12 2 40.65 37.56 2.43 o -4 12 2 39.18 38.35 2.49 o -3 12 2 151.28 137.88 3.54 o 0 1 3 10.82 9.92 0.21 o 0 2 3 1113.81 1185.58 6.00 o 1 2 3 183.33 187.94 1.55 o -1 3 3 2516.19 2700.33 12.26 o 0 3 3 76.03 83.29 0.78 o 1 3 3 242.90 263.49 1.66 o 2 3 3 266.11 277.21 1.96 o -1 4 3 693.21 773.85 4.32 o 0 4 3 10.06 8.86 0.37 o 1 4 3 6.40 6.37 0.36 o 2 4 3 347.17 359.54 2.41 o 3 4 3 434.66 440.90 3.11 o -2 5 3 331.77 380.36 2.58 o -1 5 3 7.94 13.08 0.53 o 0 5 3 11.20 14.94 0.54 o 1 5 3 38.69 44.08 0.79 o 2 5 3 0.06 0.06 0.44 o 3 5 3 83.18 79.70 1.60 o 4 5 3 34.92 35.59 1.36 o -2 6 3 2.34 2.48 0.48 o -1 6 3 41.90 39.89 0.92 o 0 6 3 1.72 2.69 0.54 o 1 6 3 54.95 47.02 1.17 o 2 6 3 76.79 74.54 1.71 o 3 6 3 34.67 41.69 1.51 o 4 6 3 11.32 11.02 1.41 o 5 6 3 18.63 17.38 2.11 o -3 7 3 109.29 117.42 1.57 o -2 7 3 14.60 11.36 0.85 o -1 7 3 164.59 161.87 1.99 o 0 7 3 68.52 64.24 1.57 o 1 7 3 15.58 12.98 1.08 o 2 7 3 27.12 25.96 1.35 o 3 7 3 32.24 34.33 1.58 o 4 7 3 1.09 1.38 1.44 o 5 7 3 21.79 22.29 2.00 o -3 8 3 34.99 37.60 1.15 o -2 8 3 190.09 179.12 2.29 o -1 8 3 0.39 0.05 0.88 o 0 8 3 108.86 113.65 2.55 o 1 8 3 12.85 14.56 1.25 o 2 8 3 0.65 1.89 1.25 o 3 8 3 21.60 21.71 1.81 o 4 8 3 25.11 26.30 2.12 o -4 9 3 38.65 36.46 1.39 o -3 9 3 0.51 2.12 1.04 o -2 9 3 122.07 142.19 2.41 o -1 9 3 68.31 67.30 1.98 o 0 9 3 1.46 1.94 1.23 o 1 9 3 27.94 25.94 1.66 o 2 9 3 14.74 14.86 1.67 o 3 9 3 0.04 2.79 2.05 o -4 10 3 32.68 36.11 1.73 o -3 10 3 27.92 33.52 1.64 o -2 10 3 7.96 5.21 1.71 o -1 10 3 1.62 3.22 1.42 o 0 10 3 10.36 12.16 1.58 o 1 10 3 0.10 -0.93 1.50 o -5 11 3 10.72 12.67 1.71 o -4 11 3 4.72 5.57 1.51 o -3 11 3 17.47 17.65 1.80 o -2 11 3 23.60 24.70 1.88 o -1 11 3 1.33 0.87 1.69 o -5 12 3 21.96 20.42 2.34 o -4 12 3 8.52 8.01 2.04 o -3 12 3 2.17 3.62 1.90 o 0 0 4 794.38 903.14 9.07 o 0 1 4 439.01 433.00 2.24 o 1 1 4 3683.28 3638.88 26.81 o -1 2 4 3875.41 3757.55 22.39 o 0 2 4 398.44 377.73 2.38 o 1 2 4 1321.60 1305.20 7.71 o 2 2 4 3250.98 3130.77 23.67 o -1 3 4 1106.23 1067.32 5.29 o 0 3 4 3943.11 3769.89 18.04 o 1 3 4 720.90 712.19 4.93 o 2 3 4 813.80 785.33 4.65 o 3 3 4 2163.28 2162.02 14.33 o -2 4 4 3193.05 3035.25 20.19 o -1 4 4 618.59 560.60 3.40 o 0 4 4 345.98 313.77 2.02 o 1 4 4 1422.96 1462.53 7.22 o 2 4 4 444.82 461.24 2.78 o 3 4 4 242.20 255.50 2.41 o 4 4 4 659.81 661.99 6.42 o -2 5 4 803.55 762.76 4.49 o -1 5 4 1257.80 1194.77 6.48 o 0 5 4 164.93 153.03 1.56 o 1 5 4 120.26 127.30 1.46 o 2 5 4 1228.11 1261.12 7.57 o 3 5 4 323.92 308.89 3.14 o 4 5 4 98.10 99.69 1.97 o 5 5 4 183.58 188.24 4.51 o -3 6 4 2421.19 2456.84 18.09 o -2 6 4 471.01 480.85 3.44 o -1 6 4 190.10 198.82 1.99 o 0 6 4 631.03 667.76 4.49 o 1 6 4 268.58 261.05 2.81 o 2 6 4 111.30 116.96 2.07 o 3 6 4 494.53 498.82 4.69 o 4 6 4 61.60 53.95 1.96 o 5 6 4 61.00 68.83 2.96 o 6 6 4 177.59 167.16 6.16 o -3 7 4 189.25 200.32 2.38 o -2 7 4 1211.86 1224.92 7.52 o -1 7 4 296.69 290.48 2.75 o 0 7 4 492.24 500.03 4.41 o 1 7 4 670.05 690.75 5.79 o 2 7 4 123.93 109.64 2.21 o 3 7 4 41.86 48.70 1.76 o 4 7 4 279.75 280.92 4.56 o 5 7 4 26.77 23.07 2.60 o -4 8 4 714.76 768.55 7.32 o -3 8 4 355.44 365.92 3.47 o -2 8 4 141.88 134.31 2.07 o -1 8 4 807.03 836.21 6.70 o 0 8 4 53.01 46.81 1.60 o 1 8 4 106.16 114.58 2.36 o 2 8 4 253.36 275.20 3.64 o 3 8 4 82.05 77.89 3.50 o 4 8 4 67.37 62.06 4.13 o -4 9 4 118.33 113.38 2.25 o -3 9 4 476.50 491.15 4.76 o -2 9 4 93.89 99.15 2.17 o -1 9 4 86.57 82.14 2.08 o 0 9 4 290.72 287.15 3.64 o 1 9 4 70.45 62.53 2.08 o 2 9 4 50.43 51.23 2.29 o -5 10 4 214.54 210.74 4.44 o -4 10 4 58.03 60.61 2.00 o -3 10 4 76.36 65.63 2.24 o -2 10 4 272.05 275.34 4.06 o -1 10 4 54.94 50.76 2.01 o 0 10 4 32.33 32.33 2.19 o 1 10 4 135.93 135.32 3.26 o -5 11 4 40.31 39.41 2.13 o -4 11 4 237.24 230.30 3.87 o -3 11 4 77.33 69.90 2.48 o -2 11 4 50.71 45.14 2.87 o -1 11 4 116.21 116.10 3.22 o -6 12 4 188.14 200.94 5.95 o -5 12 4 19.64 19.75 2.09 o -4 12 4 67.68 60.31 2.69 o 0 1 5 240.30 212.99 1.34 o 0 2 5 1974.90 2071.29 10.29 o 1 2 5 586.79 606.03 4.22 o -1 3 5 32.22 40.90 0.73 o 0 3 5 23.29 20.40 0.60 o 1 3 5 183.25 186.98 1.63 o 2 3 5 92.07 79.87 1.41 o -1 4 5 45.32 50.00 0.78 o 0 4 5 121.91 125.65 1.38 o 1 4 5 0.00 0.93 0.44 o 2 4 5 65.07 64.63 1.26 o 3 4 5 34.44 34.66 1.02 o -2 5 5 169.35 179.59 1.71 o -1 5 5 70.72 66.37 0.99 o 0 5 5 37.60 28.69 0.94 o 1 5 5 22.45 23.98 0.91 o 2 5 5 62.85 63.29 1.44 o 3 5 5 121.90 120.71 2.11 o 4 5 5 36.52 39.66 1.50 o -2 6 5 417.45 423.03 3.35 o -1 6 5 6.54 6.55 0.63 o 0 6 5 1.73 2.44 0.61 o 1 6 5 138.25 137.23 2.20 o 2 6 5 236.47 245.87 2.96 o 3 6 5 18.44 10.78 1.27 o 4 6 5 34.68 31.76 2.30 o 5 6 5 1.09 -0.12 2.05 o -3 7 5 154.06 153.45 1.98 o -2 7 5 45.52 39.78 1.14 o -1 7 5 99.75 99.44 1.67 o 0 7 5 64.07 72.30 1.71 o 1 7 5 21.94 16.51 1.37 o 2 7 5 30.86 27.02 1.70 o 3 7 5 24.25 24.80 1.64 o 4 7 5 0.29 2.41 2.15 o -3 8 5 49.89 49.59 1.46 o -2 8 5 112.08 106.34 1.97 o -1 8 5 18.86 18.97 1.21 o 0 8 5 132.70 141.19 2.48 o 1 8 5 28.19 31.14 1.80 o 2 8 5 2.59 0.70 1.40 o 3 8 5 9.34 6.30 2.36 o -4 9 5 49.13 43.81 1.62 o -3 9 5 0.35 0.23 1.21 o -2 9 5 2.31 1.93 1.19 o -1 9 5 10.65 10.54 1.33 o 0 9 5 8.31 6.87 1.55 o 1 9 5 8.34 6.00 1.63 o 2 9 5 11.71 6.27 2.21 o -4 10 5 8.73 8.32 1.44 o -3 10 5 42.55 42.04 2.00 o -2 10 5 0.14 -0.01 1.37 o -1 10 5 25.20 21.25 2.02 o 0 10 5 4.76 -0.10 1.78 o -5 11 5 3.02 1.25 1.66 o -4 11 5 12.00 10.29 1.73 o -3 11 5 38.65 39.43 2.13 o -2 11 5 17.07 13.98 1.99 o 0 0 6 75.21 73.70 1.78 o 0 1 6 610.07 631.31 3.17 o 1 1 6 3464.15 3570.10 25.33 o -1 2 6 1322.42 1360.59 8.50 o 0 2 6 155.85 156.92 1.48 o 1 2 6 859.11 879.25 5.48 o 2 2 6 2305.40 2300.81 18.25 o -1 3 6 183.35 182.78 1.55 o 0 3 6 2656.37 2691.76 13.78 o 1 3 6 892.70 912.75 5.97 o 2 3 6 669.25 670.75 4.85 o 3 3 6 753.84 783.00 7.87 o -2 4 6 279.38 283.64 2.95 o -1 4 6 350.34 334.11 2.68 o 0 4 6 257.27 271.72 2.35 o 1 4 6 1612.15 1680.52 10.01 o 2 4 6 198.16 194.69 2.45 o 3 4 6 43.94 46.02 1.37 o 4 4 6 293.69 295.63 4.54 o -2 5 6 909.95 912.39 5.51 o -1 5 6 1490.52 1544.09 9.16 o 0 5 6 145.33 145.66 2.03 o 1 5 6 92.65 93.50 1.55 o 2 5 6 805.42 847.31 6.09 o 3 5 6 126.65 119.39 2.33 o 4 5 6 253.83 253.28 3.88 o 5 5 6 209.36 220.07 6.17 o -3 6 6 1626.31 1689.65 14.17 o -2 6 6 98.86 94.59 1.50 o -1 6 6 245.03 247.06 2.78 o 0 6 6 406.21 425.52 3.94 o 1 6 6 359.12 351.91 3.55 o 2 6 6 118.29 125.27 2.22 o 3 6 6 499.34 514.49 5.71 o 4 6 6 31.14 27.06 2.28 o 5 6 6 26.99 22.52 2.63 o -3 7 6 166.24 173.35 2.25 o -2 7 6 829.08 850.98 6.00 o -1 7 6 180.97 181.94 2.53 o 0 7 6 292.45 294.11 3.79 o 1 7 6 546.10 565.07 5.64 o 2 7 6 63.04 56.26 2.23 o 3 7 6 63.00 70.04 2.94 o 4 7 6 191.02 199.80 5.20 o -4 8 6 449.56 475.25 7.40 o -3 8 6 155.48 156.34 2.47 o -2 8 6 39.06 38.46 1.58 o -1 8 6 261.72 261.77 3.79 o 0 8 6 76.56 74.51 2.33 o 1 8 6 31.19 36.31 1.94 o 2 8 6 210.71 222.42 4.09 o 3 8 6 59.13 54.90 3.09 o -4 9 6 162.75 164.53 2.94 o -3 9 6 304.47 312.09 4.07 o -2 9 6 24.81 25.42 1.67 o -1 9 6 54.36 46.63 2.11 o 0 9 6 322.60 322.75 4.66 o 1 9 6 78.54 72.89 3.01 o -5 10 6 215.14 219.87 5.08 o -4 10 6 104.84 105.73 2.74 o -3 10 6 26.08 18.94 1.79 o -2 10 6 230.10 233.55 4.20 o -1 10 6 31.41 28.80 2.21 o -5 11 6 16.85 14.11 1.92 o -4 11 6 261.84 270.89 4.84 o -3 11 6 81.64 80.40 2.96 o 0 1 7 414.87 369.62 2.14 o 0 2 7 443.81 415.15 2.93 o 1 2 7 93.00 89.50 1.43 o -1 3 7 28.02 30.46 0.69 o 0 3 7 80.80 79.34 1.18 o 1 3 7 74.46 65.61 1.34 o 2 3 7 48.41 44.00 1.24 o -1 4 7 22.05 18.37 0.84 o 0 4 7 459.53 466.15 3.63 o 1 4 7 2.80 2.15 0.74 o 2 4 7 74.91 68.46 1.52 o 3 4 7 6.65 4.43 0.99 o -2 5 7 66.18 59.16 1.28 o -1 5 7 33.87 32.37 1.22 o 0 5 7 50.47 49.42 1.34 o 1 5 7 79.23 72.83 1.64 o 2 5 7 21.54 20.40 1.16 o 3 5 7 66.82 68.78 2.08 o 4 5 7 49.11 52.15 2.22 o -2 6 7 402.28 395.69 3.85 o -1 6 7 79.08 77.98 1.64 o 0 6 7 0.86 1.63 0.75 o 1 6 7 80.10 77.71 2.00 o 2 6 7 73.06 71.95 2.13 o 3 6 7 48.22 47.98 2.16 o 4 6 7 44.14 43.55 2.73 o -3 7 7 26.43 27.83 1.18 o -2 7 7 6.99 4.63 1.02 o -1 7 7 35.37 37.34 1.48 o 0 7 7 45.80 48.30 1.84 o 1 7 7 0.00 -0.46 1.47 o 2 7 7 10.33 11.78 1.81 o 3 7 7 18.46 12.14 2.51 o -3 8 7 71.13 73.88 1.88 o -2 8 7 20.32 19.07 1.44 o -1 8 7 0.98 1.04 1.31 o 0 8 7 20.87 21.77 1.70 o 1 8 7 26.93 25.31 2.15 o 2 8 7 0.00 -0.30 1.95 o -4 9 7 44.04 44.40 1.78 o -3 9 7 4.88 3.77 1.64 o -2 9 7 5.26 4.35 1.57 o -1 9 7 4.32 2.46 1.59 o 0 9 7 14.42 9.06 2.05 o -4 10 7 16.20 13.89 2.11 o -3 10 7 22.83 17.69 1.99 o -2 10 7 3.52 1.74 1.85 o 0 0 8 2104.81 2290.99 26.13 o 0 1 8 589.48 612.70 3.61 o 1 1 8 1522.83 1576.76 11.79 o -1 2 8 1230.98 1299.27 10.21 o 0 2 8 199.49 212.96 2.07 o 1 2 8 181.61 181.48 2.40 o 2 2 8 609.58 640.94 7.50 o -1 3 8 142.36 144.99 1.97 o 0 3 8 1139.99 1183.50 7.30 o 1 3 8 341.91 341.28 3.17 o 2 3 8 366.99 365.06 3.42 o 3 3 8 490.60 513.75 6.36 o -2 4 8 295.19 322.38 4.39 o -1 4 8 271.07 275.71 2.94 o 0 4 8 211.32 220.84 2.46 o 1 4 8 1142.50 1143.89 7.42 o 2 4 8 76.66 75.10 1.73 o 3 4 8 52.50 48.29 1.53 o 4 4 8 241.42 251.73 5.12 o -2 5 8 299.14 301.86 3.39 o -1 5 8 1081.82 1138.02 8.01 o 0 5 8 172.64 177.06 2.45 o 1 5 8 191.59 196.47 2.76 o 2 5 8 419.83 427.10 4.17 o 3 5 8 45.08 47.30 1.82 o 4 5 8 160.89 153.17 3.27 o 5 5 8 255.28 250.85 7.88 o -3 6 8 387.87 399.16 5.43 o -2 6 8 53.87 55.15 1.66 o -1 6 8 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