#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/49/2104940.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104940_Fobs loop_ _publ_author_name 'Gagor, Anna' 'Wa\'skowska, Alicja' 'Czapla, Zbigniew' 'Dacko, Slawomir' _publ_section_title ; Structural phase transitions in tetra(isopropylammonium) decachlorotricadmate(II), [(CH~3~)~2~CHNH~3~]~4~Cd~3~Cl~10~, crystal with a two-dimensional cadmium(II) halide network ; _journal_coeditor_code KD5047 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 122 _journal_page_last 129 _journal_volume 67 _journal_year 2011 _space_group_IT_number 64 _symmetry_space_group_name_Hall '-C 2ac 2' _symmetry_space_group_name_H-M 'C m c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.4634 _cell_length_b 22.0476 _cell_length_c 19.6139 _exptl_crystal_F_000 1816.00 _reflns_d_resolution_high 0.7158 _[local]_cod_data_source_file kd5047Cmcesup2.hkl _[local]_cod_data_source_block Cmce #BEGIN Tags that were not found in dictionaries: _shelx_title ' cmce in Cmce' _shelx_refln_list_code 4 _shelx_f_calc_maximum 602.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 362589.59 355870.53 2881.43 o 6 0 0 17443.42 17050.50 244.74 o 8 0 0 18438.85 17937.33 400.05 o 10 0 0 774.69 641.84 147.77 o 2 2 0 18693.88 19479.67 139.62 o 4 2 0 131069.19 132336.80 687.03 o 6 2 0 8868.54 8630.64 133.49 o 8 2 0 9859.83 10025.63 201.54 o 10 2 0 596.36 354.46 117.93 o 0 4 0 15760.31 16476.86 201.68 o 2 4 0 14998.53 16221.89 148.04 o 4 4 0 4450.47 4205.46 63.26 o 6 4 0 2837.27 2741.64 87.59 o 8 4 0 361.78 709.26 94.34 o 10 4 0 155.27 255.58 116.85 o 0 6 0 80479.96 85466.13 557.94 o 2 6 0 12018.29 13167.56 118.98 o 4 6 0 17852.54 17489.88 130.90 o 6 6 0 786.94 753.45 69.63 o 8 6 0 1471.27 1364.19 117.30 o 0 8 0 162211.31 159224.00 2124.34 o 2 8 0 2296.95 2461.55 52.85 o 4 8 0 53021.98 51250.05 383.05 o 6 8 0 129.12 128.80 66.14 o 8 8 0 2785.33 2786.53 137.04 o 0 10 0 18961.44 17661.01 193.04 o 2 10 0 609.34 613.33 45.58 o 4 10 0 2897.82 2995.56 83.80 o 6 10 0 157.55 173.74 70.63 o 8 10 0 89.42 209.68 112.28 o 0 12 0 32082.18 31385.74 300.88 o 2 12 0 11192.94 11359.77 120.19 o 4 12 0 12368.82 12278.55 158.35 o 6 12 0 1597.42 1577.27 124.41 o 8 12 0 1473.62 1625.78 150.54 o 0 14 0 29429.69 28973.67 701.32 o 2 14 0 4729.25 4829.44 93.59 o 4 14 0 18149.88 17958.34 305.05 o 6 14 0 1788.80 1554.28 167.37 o 8 14 0 2909.44 3153.01 186.11 o 0 16 0 28080.70 28934.72 931.48 o 2 16 0 11382.98 11702.11 204.23 o 4 16 0 13575.35 13646.49 495.75 o 6 16 0 2141.29 2118.84 179.93 o 8 16 0 1644.78 1511.27 185.98 o 0 18 0 5154.45 5823.58 270.59 o 2 18 0 5200.20 5577.34 162.81 o 4 18 0 1557.69 1679.60 132.95 o 6 18 0 764.58 939.87 149.81 o 8 18 0 130.93 235.83 136.76 o 0 20 0 1904.25 2174.26 166.65 o 2 20 0 48.90 92.21 96.80 o 4 20 0 620.45 565.23 101.28 o 6 20 0 24.40 51.52 139.75 o 0 22 0 11.99 86.89 165.46 o 2 22 0 138.42 122.81 94.74 o 4 22 0 138.63 -14.53 322.94 o 6 22 0 0.27 -89.23 138.96 o 0 24 0 43.76 49.00 151.04 o 2 24 0 93.05 -55.25 141.07 o 4 24 0 0.28 -71.28 125.08 o 6 24 0 0.07 -185.44 235.74 o 0 26 0 464.99 579.94 220.36 o 2 26 0 28.98 61.75 115.09 o 4 26 0 204.83 197.62 208.44 o 4 28 0 467.49 67.93 215.20 o 3 1 1 70549.65 71661.92 207.08 o 5 1 1 36075.30 35757.18 198.81 o 7 1 1 6773.01 6824.84 106.13 o 9 1 1 2596.46 2652.15 100.75 o 2 2 1 6397.60 6435.30 69.66 o 4 2 1 35924.97 36314.13 182.60 o 6 2 1 1937.04 2001.95 53.45 o 8 2 1 1939.66 1994.95 83.20 o 10 2 1 103.58 61.97 87.53 o 1 3 1 78372.64 84463.75 435.60 o 3 3 1 34258.75 34502.96 129.79 o 5 3 1 11088.44 11198.76 87.44 o 7 3 1 3751.05 3723.40 84.68 o 9 3 1 761.80 822.49 79.38 o 0 4 1 35604.14 37380.33 209.92 o 2 4 1 9139.88 9823.59 68.10 o 4 4 1 22883.21 22054.21 104.32 o 6 4 1 630.31 662.89 46.13 o 8 4 1 2473.09 2754.99 93.12 o 10 4 1 139.24 261.36 96.20 o 1 5 1 6146.57 6552.87 74.07 o 3 5 1 6016.70 5900.93 51.14 o 5 5 1 248.13 285.98 32.70 o 7 5 1 1070.64 987.25 60.26 o 9 5 1 5.37 -55.94 72.03 o 0 6 1 61842.90 63461.33 847.27 o 2 6 1 17.91 21.88 18.67 o 4 6 1 11208.21 10731.20 73.76 o 6 6 1 53.80 43.71 41.31 o 8 6 1 565.77 592.92 69.01 o 10 6 1 16.46 -140.00 182.16 o 1 7 1 4774.42 4874.88 59.51 o 3 7 1 368.19 355.10 19.60 o 5 7 1 827.25 736.71 42.20 o 7 7 1 22.81 33.49 54.08 o 9 7 1 63.74 113.79 80.98 o 0 8 1 650.63 754.29 113.45 o 2 8 1 6117.61 6149.53 55.63 o 4 8 1 1756.26 1707.20 39.70 o 6 8 1 1027.56 1043.75 61.41 o 8 8 1 222.65 289.70 72.40 o 10 8 1 28.10 -347.16 347.16 o 1 9 1 2354.06 2401.25 45.08 o 3 9 1 875.44 878.41 26.67 o 5 9 1 6.33 1.16 38.53 o 7 9 1 2.67 47.86 61.57 o 9 9 1 18.21 -17.03 91.15 o 0 10 1 99530.52 98427.41 424.96 o 2 10 1 41343.79 39229.74 219.34 o 4 10 1 24020.66 23134.69 156.99 o 6 10 1 3544.00 3593.88 97.48 o 8 10 1 1688.16 1759.71 102.42 o 1 11 1 11302.95 11360.92 87.00 o 3 11 1 2625.49 2661.48 43.91 o 5 11 1 3216.02 3152.42 78.54 o 7 11 1 87.71 73.68 70.86 o 9 11 1 371.48 376.71 92.90 o 0 12 1 17615.80 17946.63 151.70 o 2 12 1 2876.36 2873.51 48.97 o 4 12 1 7681.54 7491.87 102.72 o 6 12 1 823.74 915.81 68.01 o 8 12 1 823.40 794.76 90.15 o 1 13 1 11497.13 11302.42 120.89 o 3 13 1 5906.86 5761.84 74.77 o 5 13 1 5686.01 5355.02 104.25 o 7 13 1 745.51 814.52 88.14 o 9 13 1 704.45 703.43 94.09 o 0 14 1 410.65 461.92 47.92 o 2 14 1 528.29 545.25 34.51 o 4 14 1 113.72 98.71 49.81 o 6 14 1 11.71 93.47 77.33 o 8 14 1 21.71 105.14 97.57 o 1 15 1 18932.23 18625.45 213.81 o 3 15 1 11148.27 10948.44 115.41 o 5 15 1 4562.27 4119.79 114.51 o 7 15 1 1394.63 1378.20 107.46 o 9 15 1 363.27 490.40 316.87 o 0 16 1 2342.65 2559.13 96.20 o 2 16 1 3361.77 3524.67 72.72 o 4 16 1 1486.10 1562.41 80.59 o 6 16 1 652.61 645.06 99.32 o 8 16 1 271.11 297.15 107.62 o 1 17 1 6896.60 6997.08 111.31 o 3 17 1 5758.45 5671.96 133.40 o 5 17 1 1195.85 1193.68 79.35 o 7 17 1 1032.16 986.86 125.15 o 0 18 1 16200.82 16390.02 293.27 o 2 18 1 12671.04 12989.62 190.29 o 4 18 1 5636.62 5344.49 129.98 o 6 18 1 1370.24 1234.68 115.51 o 8 18 1 453.37 510.05 164.24 o 1 19 1 296.88 247.80 64.53 o 3 19 1 610.62 582.60 75.12 o 5 19 1 18.15 34.02 66.77 o 7 19 1 218.62 170.50 109.54 o 0 20 1 1225.00 1333.63 119.20 o 2 20 1 1304.14 1404.01 86.77 o 4 20 1 708.62 600.34 75.41 o 6 20 1 297.35 373.49 105.34 o 1 21 1 3.18 -27.63 66.01 o 3 21 1 25.22 61.55 84.67 o 5 21 1 0.62 46.63 73.09 o 7 21 1 9.66 -53.77 102.22 o 0 22 1 340.02 391.60 100.31 o 2 22 1 107.44 167.15 69.85 o 4 22 1 99.05 132.67 77.51 o 6 22 1 8.96 -32.22 103.22 o 1 23 1 53.85 48.08 75.33 o 3 23 1 0.46 5.32 87.60 o 5 23 1 19.26 30.04 75.20 o 0 24 1 580.60 668.48 138.61 o 2 24 1 436.00 452.46 75.82 o 4 24 1 377.99 342.86 88.70 o 6 24 1 114.48 -105.18 130.65 o 1 25 1 30.34 26.13 86.16 o 3 25 1 3.24 2155.57 1333.07 o 5 25 1 65.84 201.56 147.54 o 0 26 1 980.92 1083.19 164.41 o 2 26 1 920.46 885.19 96.80 o 4 26 1 449.97 423.34 162.56 o 1 27 1 273.14 281.68 118.72 o 3 27 1 140.46 198.08 207.38 o 4 28 1 33.59 364.52 315.01 o 2 0 2 10098.33 11254.59 110.80 o 4 0 2 2219.79 2018.24 55.60 o 6 0 2 409.54 359.96 56.72 o 8 0 2 737.18 706.24 89.02 o 10 0 2 11.92 70.25 107.64 o 3 1 2 8267.51 9157.92 57.00 o 5 1 2 3739.28 3731.72 55.82 o 7 1 2 593.18 547.14 50.86 o 9 1 2 277.49 189.05 71.28 o 0 2 2 18753.64 20049.96 165.47 o 2 2 2 9392.97 9934.06 88.11 o 4 2 2 7595.24 7262.91 58.15 o 6 2 2 453.27 447.88 40.96 o 8 2 2 817.78 883.13 68.41 o 10 2 2 12.27 -46.35 69.21 o 1 3 2 141543.27 142064.94 3797.49 o 3 3 2 32867.05 31741.96 148.42 o 5 3 2 13093.81 13060.09 102.05 o 7 3 2 2181.27 2097.73 68.17 o 9 3 2 982.34 977.53 80.95 o 0 4 2 27985.16 28721.51 704.48 o 2 4 2 65570.12 70591.16 383.01 o 4 4 2 5832.32 5972.39 53.33 o 6 4 2 6473.30 6306.38 86.17 o 8 4 2 714.97 760.97 66.99 o 10 4 2 319.70 237.67 101.51 o 1 5 2 4658.19 4018.06 62.08 o 3 5 2 11296.43 11458.80 65.04 o 5 5 2 5622.21 5662.50 73.95 o 7 5 2 1716.82 1679.62 71.46 o 9 5 2 552.71 496.80 89.66 o 0 6 2 5338.95 5200.55 167.21 o 2 6 2 72830.03 71169.55 345.82 o 4 6 2 4169.71 4224.51 51.75 o 6 6 2 12923.46 12856.61 133.45 o 8 6 2 618.77 603.83 70.13 o 10 6 2 785.25 732.45 182.37 o 1 7 2 328.31 354.87 31.24 o 3 7 2 122.41 181.49 22.38 o 5 7 2 208.86 232.21 38.14 o 7 7 2 17.38 100.19 50.91 o 9 7 2 32.39 67.77 78.81 o 0 8 2 49447.02 49950.52 522.02 o 2 8 2 75000.09 73489.20 316.20 o 4 8 2 13429.70 12936.26 93.56 o 6 8 2 11858.93 11729.10 130.45 o 8 8 2 775.34 756.13 81.57 o 1 9 2 44207.18 43332.16 288.13 o 3 9 2 17033.39 17446.79 111.62 o 5 9 2 9556.92 9516.00 110.06 o 7 9 2 1096.10 1139.92 78.22 o 9 9 2 645.43 628.75 88.24 o 0 10 2 20631.37 20243.24 195.04 o 2 10 2 3820.93 3514.40 49.84 o 4 10 2 8848.65 8632.04 82.45 o 6 10 2 2090.83 2407.88 85.58 o 8 10 2 666.62 723.22 79.23 o 1 11 2 17237.40 17126.56 142.00 o 3 11 2 12815.75 12773.86 103.48 o 5 11 2 7037.56 6598.86 104.63 o 7 11 2 1751.43 1774.10 86.91 o 9 11 2 603.49 736.55 99.14 o 0 12 2 12495.53 11364.33 160.98 o 2 12 2 3220.54 3239.66 54.60 o 4 12 2 4853.59 4608.65 80.04 o 6 12 2 86.33 69.15 57.81 o 8 12 2 468.96 506.49 88.82 o 1 13 2 554.27 594.54 34.19 o 3 13 2 1206.84 1149.96 44.60 o 5 13 2 360.72 396.85 50.50 o 7 13 2 519.84 585.91 92.71 o 9 13 2 48.75 215.49 108.83 o 0 14 2 12448.21 12954.71 163.73 o 2 14 2 955.65 989.77 43.76 o 4 14 2 3644.94 3506.80 86.62 o 6 14 2 351.66 392.21 85.54 o 8 14 2 290.79 335.95 94.89 o 1 15 2 877.81 857.27 47.03 o 3 15 2 251.40 205.54 40.04 o 5 15 2 981.70 872.22 65.68 o 7 15 2 26.83 38.20 81.00 o 0 16 2 392.92 299.82 60.57 o 2 16 2 318.71 299.63 41.67 o 4 16 2 331.21 407.73 67.64 o 6 16 2 39.17 155.90 91.82 o 8 16 2 101.52 53.84 95.20 o 1 17 2 14756.48 15303.75 164.40 o 3 17 2 7637.75 7559.31 114.34 o 5 17 2 3901.46 3526.04 111.84 o 7 17 2 702.24 645.85 123.05 o 0 18 2 51.83 -22.82 84.72 o 2 18 2 1915.79 1825.06 71.90 o 4 18 2 115.18 166.52 64.79 o 6 18 2 420.14 440.96 106.85 o 8 18 2 42.47 170.06 130.51 o 1 19 2 3667.90 3710.35 94.76 o 3 19 2 3106.72 3276.77 126.08 o 5 19 2 1379.56 1449.00 87.53 o 7 19 2 573.69 752.49 115.89 o 0 20 2 938.91 863.51 111.72 o 2 20 2 6501.02 6675.45 130.19 o 4 20 2 323.99 321.35 66.36 o 6 20 2 1157.31 1149.02 125.38 o 1 21 2 33.09 39.85 64.76 o 3 21 2 80.12 114.74 74.64 o 5 21 2 0.15 -69.54 69.54 o 7 21 2 54.67 -62.89 100.59 o 0 22 2 130.76 45.34 96.87 o 2 22 2 2075.29 2247.00 101.79 o 4 22 2 125.59 123.31 77.58 o 6 22 2 619.17 694.49 124.34 o 1 23 2 484.89 431.55 80.50 o 3 23 2 224.21 152.66 93.84 o 5 23 2 239.34 239.63 81.48 o 0 24 2 483.50 524.00 128.83 o 2 24 2 670.82 716.13 90.41 o 4 24 2 199.11 276.79 92.19 o 6 24 2 144.05 290.73 196.75 o 1 25 2 1488.72 1477.44 96.28 o 3 25 2 1071.22 1067.06 119.19 o 5 25 2 504.48 150.99 168.86 o 0 26 2 175.70 335.36 136.14 o 2 26 2 16.85 83.50 83.90 o 4 26 2 81.53 286.11 158.25 o 1 27 2 940.19 1039.66 146.57 o 3 27 2 569.78 705.21 289.20 o 4 28 2 0.49 600.77 264.57 o 3 29 2 0.07 512.70 252.18 o 1 1 3 17265.15 19611.68 187.63 o 3 1 3 21421.23 21561.95 82.31 o 5 1 3 3778.92 3659.31 57.72 o 7 1 3 1999.83 2089.41 67.58 o 9 1 3 84.29 119.28 63.92 o 0 2 3 1713.37 1701.91 63.15 o 2 2 3 13751.67 15427.27 84.20 o 4 2 3 1696.89 1747.38 37.97 o 6 2 3 1107.27 1026.02 49.73 o 8 2 3 344.39 363.68 62.59 o 10 2 3 41.62 37.89 81.51 o 1 3 3 8229.12 9097.83 98.94 o 3 3 3 3771.53 3853.02 49.28 o 5 3 3 1478.58 1480.42 45.28 o 7 3 3 317.76 333.24 48.67 o 9 3 3 108.71 133.59 66.16 o 0 4 3 804.07 896.76 49.53 o 2 4 3 11928.01 12045.74 69.26 o 4 4 3 1402.58 1276.58 33.43 o 6 4 3 1343.05 1429.99 51.56 o 8 4 3 442.93 460.60 63.99 o 10 4 3 61.60 -64.50 109.54 o 1 5 3 39636.87 39468.21 197.28 o 3 5 3 42783.67 43642.75 235.22 o 5 5 3 16421.70 16238.05 119.14 o 7 5 3 6957.34 7257.09 126.25 o 9 5 3 1120.29 1152.80 99.01 o 0 6 3 6448.02 6631.62 120.60 o 2 6 3 847.00 898.08 29.25 o 4 6 3 765.85 708.13 29.39 o 6 6 3 263.05 292.33 48.27 o 8 6 3 5.51 47.66 61.51 o 10 6 3 24.61 212.63 215.69 o 1 7 3 198711.81 190854.28 951.40 o 3 7 3 106925.23 105136.23 354.26 o 5 7 3 33988.98 33279.14 240.65 o 7 7 3 12669.19 12993.99 158.56 o 9 7 3 2207.40 2301.31 122.89 o 0 8 3 58741.23 60849.84 540.51 o 2 8 3 141.93 120.94 26.43 o 4 8 3 8455.14 8067.11 76.45 o 6 8 3 139.12 125.48 51.35 o 8 8 3 308.48 391.24 73.26 o 1 9 3 112163.35 105382.02 693.58 o 3 9 3 67296.43 64854.29 281.18 o 5 9 3 23258.99 22785.55 168.97 o 7 9 3 6608.39 6510.99 131.77 o 9 9 3 1437.29 1488.50 102.96 o 0 10 3 17789.03 18082.90 398.45 o 2 10 3 5027.56 4921.79 63.16 o 4 10 3 7445.24 7419.30 86.62 o 6 10 3 528.41 551.57 65.06 o 8 10 3 703.72 784.69 81.79 o 1 11 3 6682.83 6604.29 73.36 o 3 11 3 3353.37 3340.41 55.94 o 5 11 3 2413.56 2434.01 77.55 o 7 11 3 574.57 572.72 70.32 o 9 11 3 339.36 400.04 89.21 o 0 12 3 5249.12 5131.30 117.70 o 2 12 3 169.10 137.88 32.77 o 4 12 3 1728.98 1732.83 58.09 o 6 12 3 198.67 254.70 66.02 o 8 12 3 211.92 265.92 89.58 o 1 13 3 197.98 198.42 31.93 o 3 13 3 186.82 195.26 33.10 o 5 13 3 20.36 21.63 46.00 o 7 13 3 133.45 91.24 66.63 o 9 13 3 1.38 215.50 173.27 o 0 14 3 5819.78 6158.03 139.03 o 2 14 3 28.87 21.35 33.76 o 4 14 3 1123.16 1120.75 56.47 o 6 14 3 1.61 37.97 58.16 o 8 14 3 11.10 7.08 90.74 o 1 15 3 5610.75 5901.34 99.45 o 3 15 3 3405.92 3175.20 70.86 o 5 15 3 1340.02 1192.16 66.03 o 7 15 3 304.44 296.44 85.36 o 0 16 3 8673.36 9039.85 153.88 o 2 16 3 450.49 456.83 43.79 o 4 16 3 3753.90 3721.28 96.66 o 6 16 3 49.96 34.98 86.90 o 8 16 3 254.52 210.28 102.82 o 1 17 3 1826.50 1801.71 67.87 o 3 17 3 388.76 415.47 53.36 o 5 17 3 205.21 206.44 66.85 o 7 17 3 0.03 -12.99 104.95 o 0 18 3 6571.33 6879.42 195.49 o 2 18 3 70.23 108.88 48.89 o 4 18 3 2235.44 2218.01 97.50 o 6 18 3 57.52 33.90 101.34 o 8 18 3 198.14 223.16 216.04 o 1 19 3 4696.06 4859.85 98.15 o 3 19 3 2813.47 2763.44 110.78 o 5 19 3 777.89 797.68 78.07 o 7 19 3 452.31 353.84 111.59 o 0 20 3 719.78 867.77 110.92 o 2 20 3 24.32 -29.33 58.95 o 4 20 3 308.51 360.22 77.27 o 6 20 3 0.17 21.97 115.22 o 1 21 3 3329.27 3581.56 115.42 o 3 21 3 2432.26 2519.47 119.39 o 5 21 3 1250.65 1319.94 97.99 o 7 21 3 496.53 342.68 125.05 o 0 22 3 286.47 381.11 102.28 o 2 22 3 14.30 20.91 63.04 o 4 22 3 133.35 136.85 76.81 o 6 22 3 2.37 -178.26 178.26 o 1 23 3 1355.11 1482.35 101.71 o 3 23 3 902.10 892.01 113.05 o 5 23 3 729.75 679.60 91.36 o 0 24 3 930.43 986.26 131.18 o 2 24 3 1.73 28.59 80.56 o 4 24 3 352.51 405.01 97.46 o 6 24 3 2.13 -63.73 170.77 o 1 25 3 617.85 792.60 108.45 o 3 25 3 274.64 305.33 100.50 o 5 25 3 170.93 -179.62 179.62 o 0 26 3 212.35 286.12 135.11 o 2 26 3 0.63 73.18 111.41 o 4 26 3 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