#------------------------------------------------------------------------------ #$Date: 2011-11-08 16:24:06 +0200 (Tue, 08 Nov 2011) $ #$Revision: 29951 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/49/2104983.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104983_Fobs loop_ _publ_author_name 'Cole, Jacqueline M.' 'Chan, Michael C. W.' 'Gibson, Vernon C.' 'Howard, Judith A. K.' _publ_section_title ; Effects of the [OC~6~F~5~] moiety upon structural geometry: crystal structures of half-sandwich tantalum(V) aryloxide complexes from reaction of Cp*Ta(N^t^Bu)(CH~2~R)~2~ with pentafluorophenol ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 416 _journal_page_last 424 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.760 _cell_angle_gamma 90.000 _cell_length_a 9.0830 _cell_length_b 16.2160 _cell_length_c 16.8720 _exptl_crystal_F_000 1080.00 _reflns_d_resolution_high 0.6196 _[local]_cod_data_source_file zb5019combinedsup3.hkl _[local]_cod_data_source_block combined #BEGIN Tags that were not found in dictionaries: _shelx_title ' withoutcos in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 379.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 39021.82 38812.32 87.60 o 2 0 0 3211.89 3342.01 86.46 o 3 0 0 58745.18 57509.69 285.39 o 4 0 0 36142.84 35677.96 267.02 o 5 0 0 186.67 386.38 96.40 o 6 0 0 14367.46 14116.33 231.06 o 7 0 0 44325.78 43401.01 413.93 o 8 0 0 5118.12 4996.18 201.22 o 9 0 0 1911.09 1769.71 154.55 o 10 0 0 12712.97 12631.24 281.56 o 11 0 0 6051.78 5886.78 242.54 o 12 0 0 87.40 74.22 183.63 o 13 0 0 3869.46 4147.67 258.61 o 14 0 0 3156.94 3332.83 267.79 o 1 1 0 67603.48 67286.63 216.34 o 2 1 0 16974.87 17082.81 222.27 o 3 1 0 7852.45 7264.44 102.53 o 4 1 0 19148.90 19412.38 146.06 o 5 1 0 32558.16 31690.46 205.55 o 6 1 0 21865.16 21473.43 193.12 o 7 1 0 2993.66 2931.76 115.43 o 8 1 0 17945.28 17905.07 219.20 o 9 1 0 11945.36 11701.16 196.25 o 10 1 0 238.42 174.35 105.97 o 11 1 0 5614.04 5568.04 167.91 o 12 1 0 7097.84 6907.99 237.95 o 13 1 0 1794.72 1978.71 165.82 o 14 1 0 430.06 569.03 155.54 o 0 2 0 144024.08 134454.75 291.51 o 1 2 0 33669.16 35512.68 113.38 o 2 2 0 3219.94 3568.49 100.99 o 3 2 0 50760.97 51060.55 287.68 o 4 2 0 46720.25 46182.19 315.23 o 5 2 0 12.34 18.36 96.40 o 6 2 0 20835.73 20594.54 275.44 o 7 2 0 28539.80 28600.67 352.72 o 8 2 0 2235.30 2326.71 174.45 o 9 2 0 1044.27 967.10 149.20 o 10 2 0 9223.37 9232.61 249.43 o 11 2 0 7042.65 6895.96 255.55 o 12 2 0 15.60 -100.99 186.69 o 13 2 0 3548.62 3743.70 257.84 o 14 2 0 3238.31 3094.11 275.44 o 1 3 0 12545.27 13362.88 121.27 o 2 3 0 66136.79 67113.38 304.51 o 3 3 0 9835.41 10224.96 156.85 o 4 3 0 12830.67 12550.14 188.22 o 5 3 0 53815.01 53037.60 387.15 o 6 3 0 18971.89 18407.84 270.85 o 7 3 0 1433.60 1403.98 150.73 o 8 3 0 10911.16 11244.86 266.26 o 9 3 0 10968.28 10733.00 247.90 o 10 3 0 553.97 789.60 150.73 o 11 3 0 4617.67 4407.81 231.06 o 12 3 0 7430.18 7436.13 286.15 o 13 3 0 1690.08 1840.86 228.00 o 14 3 0 258.25 394.03 220.35 o 0 4 0 63092.33 65547.20 300.69 o 1 4 0 13158.35 14284.80 306.05 o 2 4 0 20496.43 21391.02 200.46 o 3 4 0 29968.71 30248.72 256.31 o 4 4 0 25763.29 26053.61 267.02 o 5 4 0 333.23 201.99 106.35 o 6 4 0 12857.86 13098.73 242.54 o 7 4 0 18374.51 18507.31 306.81 o 8 4 0 5251.67 4934.98 213.47 o 9 4 0 1283.73 1368.02 159.91 o 10 4 0 11225.23 10932.69 277.74 o 11 4 0 6861.62 7322.13 255.55 o 12 4 0 0.86 374.14 191.28 o 13 4 0 3220.30 2934.97 254.02 o 14 4 0 3053.10 3410.11 273.15 o 1 5 0 36570.07 37657.57 319.43 o 2 5 0 31194.44 30449.18 254.02 o 3 5 0 449.89 335.12 101.76 o 4 5 0 2403.61 2175.98 127.01 o 5 5 0 28659.01 28143.90 314.46 o 6 5 0 16933.87 17826.36 281.56 o 7 5 0 13.38 171.39 141.55 o 8 5 0 8629.13 8260.92 254.78 o 9 5 0 9715.62 9903.62 246.37 o 10 5 0 182.76 342.01 152.26 o 11 5 0 3761.23 3951.04 225.71 o 12 5 0 5235.92 5215.77 266.26 o 13 5 0 1469.74 1633.52 227.24 o 14 5 0 411.50 410.10 231.06 o 0 6 0 49740.39 52177.62 333.59 o 1 6 0 13261.64 13265.13 123.50 o 2 6 0 14715.32 16203.55 210.41 o 3 6 0 36750.69 38009.26 322.11 o 4 6 0 30195.72 30909.78 312.17 o 5 6 0 1551.07 1474.37 134.66 o 6 6 0 16183.86 15474.40 280.80 o 7 6 0 25255.44 25016.12 364.19 o 8 6 0 2868.05 2995.42 189.75 o 9 6 0 1764.72 1859.99 169.85 o 10 6 0 10116.57 10572.33 275.44 o 11 6 0 6433.80 6637.35 263.96 o 12 6 0 88.79 216.53 197.40 o 13 6 0 3254.08 3316.00 259.37 o 14 6 0 3806.40 3505.75 289.98 o 1 7 0 14823.98 15427.85 289.21 o 2 7 0 32585.63 32479.79 304.51 o 3 7 0 9258.97 10099.49 196.63 o 4 7 0 2662.66 2737.57 139.25 o 5 7 0 24560.55 24674.11 319.82 o 6 7 0 15037.42 14918.93 286.15 o 7 7 0 1582.66 1375.67 173.68 o 8 7 0 8851.21 8504.23 228.77 o 9 7 0 5296.24 5539.41 214.23 o 10 7 0 428.19 387.91 172.15 o 11 7 0 2539.69 2531.76 216.53 o 12 7 0 3710.82 3768.94 246.37 o 13 7 0 1083.65 1364.96 228.77 o 0 8 0 42805.15 42572.39 357.31 o 1 8 0 8289.94 8029.85 203.90 o 2 8 0 4541.74 4844.69 157.61 o 3 8 0 31961.96 33061.27 337.41 o 4 8 0 21232.61 21922.00 300.69 o 5 8 0 65.59 195.87 129.30 o 6 8 0 13728.05 14052.82 291.51 o 7 8 0 18559.78 18423.14 338.18 o 8 8 0 2138.54 2095.64 170.62 o 9 8 0 1116.51 977.81 169.09 o 10 8 0 10144.06 10488.93 290.74 o 11 8 0 4910.76 4801.08 254.78 o 12 8 0 2.26 -120.12 199.69 o 13 8 0 3064.12 3189.75 270.85 o 1 9 0 34184.77 33955.22 610.18 o 2 9 0 34319.30 34567.79 352.72 o 3 9 0 7740.75 7930.39 201.99 o 4 9 0 6596.01 6486.62 204.29 o 5 9 0 17578.42 16966.37 298.39 o 6 9 0 7409.79 7352.73 244.07 o 7 9 0 580.79 404.74 169.85 o 8 9 0 9173.07 8963.29 244.84 o 9 9 0 10215.41 10055.87 275.44 o 10 9 0 574.51 391.74 189.75 o 11 9 0 2801.37 3061.98 227.24 o 12 9 0 3090.18 3645.00 254.02 o 13 9 0 293.11 345.07 230.30 o 0 10 0 33858.32 34163.81 365.72 o 1 10 0 6543.57 6383.35 125.22 o 2 10 0 2094.90 2352.72 149.20 o 3 10 0 19964.89 20953.37 309.87 o 4 10 0 14188.08 14283.89 276.21 o 5 10 0 16.40 -24.48 144.61 o 6 10 0 8363.19 8429.24 262.43 o 7 10 0 10104.00 10398.65 244.84 o 8 10 0 2000.60 2388.68 175.21 o 9 10 0 1049.70 1456.01 172.92 o 10 10 0 6739.01 6911.26 266.26 o 11 10 0 3046.17 2660.30 237.95 o 12 10 0 10.26 -18.36 211.17 o 13 10 0 2425.87 2452.19 264.73 o 1 11 0 12447.28 12521.28 165.41 o 2 11 0 16078.30 15671.04 280.03 o 3 11 0 4914.94 4912.02 201.22 o 4 11 0 2723.95 2578.43 182.10 o 5 11 0 13128.54 13127.80 298.39 o 6 11 0 5294.48 5128.55 229.53 o 7 11 0 2299.34 2297.63 180.57 o 8 11 0 8590.28 8609.81 262.43 o 9 11 0 4983.46 4995.42 237.95 o 10 11 0 369.09 410.87 186.69 o 11 11 0 938.69 957.16 212.70 o 12 11 0 2430.49 2626.63 259.37 o 13 11 0 341.52 457.54 238.72 o 0 12 0 28202.69 28379.56 374.14 o 1 12 0 6588.03 6527.23 345.45 o 2 12 0 2353.28 2590.67 175.21 o 3 12 0 17466.16 17562.39 326.70 o 4 12 0 12982.16 12493.52 296.86 o 5 12 0 1700.61 1336.65 184.39 o 6 12 0 6269.04 6447.60 219.59 o 7 12 0 9608.95 9286.94 257.08 o 8 12 0 721.14 606.73 167.56 o 9 12 0 729.84 656.47 179.80 o 10 12 0 3715.42 3844.69 246.37 o 11 12 0 2083.65 2446.06 231.83 o 12 12 0 13.14 121.65 214.23 o 1 13 0 9606.30 9633.73 174.83 o 2 13 0 5800.31 5917.38 232.59 o 3 13 0 732.72 687.84 164.50 o 4 13 0 1970.49 2354.25 188.22 o 5 13 0 4941.86 4934.21 234.12 o 6 13 0 3522.49 3371.85 201.22 o 7 13 0 944.68 720.74 166.79 o 8 13 0 5363.69 4977.06 232.59 o 9 13 0 3942.33 3847.75 231.83 o 10 13 0 223.29 149.96 198.16 o 11 13 0 1126.11 1116.30 228.00 o 12 13 0 1720.99 1291.51 255.55 o 0 14 0 18332.76 18563.93 346.60 o 1 14 0 3078.13 3136.70 130.87 o 2 14 0 1988.34 2192.05 192.04 o 3 14 0 12460.31 12550.90 309.87 o 4 14 0 8742.07 8625.11 270.85 o 5 14 0 701.87 869.17 151.49 o 6 14 0 2188.72 2211.18 179.80 o 7 14 0 4410.65 4436.12 221.12 o 8 14 0 1027.28 1055.86 188.22 o 9 14 0 238.14 324.41 185.92 o 10 14 0 3659.16 3514.93 250.96 o 11 14 0 1240.85 1205.05 228.00 o 12 14 0 6.56 122.42 232.59 o 1 15 0 4160.50 4179.61 143.54 o 2 15 0 5194.74 5545.54 237.95 o 3 15 0 1896.25 1823.26 201.22 o 4 15 0 3387.96 3436.12 191.28 o 5 15 0 7050.42 6599.10 240.25 o 6 15 0 2299.55 2178.28 192.81 o 7 15 0 517.76 114.77 173.68 o 8 15 0 3303.07 2810.26 229.53 o 9 15 0 2686.53 2602.15 231.06 o 10 15 0 288.07 450.65 202.75 o 11 15 0 1146.96 1566.19 237.18 o 0 16 0 4600.09 5086.47 202.75 o 1 16 0 2086.66 2071.77 124.35 o 2 16 0 175.12 3.83 147.67 o 3 16 0 6364.93 5911.26 228.00 o 4 16 0 5740.91 5548.60 226.47 o 5 16 0 221.24 165.26 165.26 o 6 16 0 2187.28 2278.51 202.75 o 7 16 0 2805.08 3103.30 209.64 o 8 16 0 233.93 108.65 194.34 o 9 16 0 130.20 -11.48 198.93 o 10 16 0 1623.05 1980.11 243.31 o 11 16 0 958.23 837.03 244.07 o 1 17 0 3368.14 3084.84 140.04 o 2 17 0 3150.57 3053.56 196.63 o 3 17 0 519.61 586.08 156.85 o 4 17 0 1095.62 1033.67 178.27 o 5 17 0 3781.50 3629.69 222.65 o 6 17 0 2090.35 2305.28 201.99 o 7 17 0 103.32 -180.57 186.69 o 8 17 0 2356.43 2436.12 233.36 o 9 17 0 1067.01 947.97 216.53 o 10 17 0 132.65 319.82 220.35 o 0 18 0 7942.94 7739.88 259.37 o 1 18 0 1523.27 1373.65 262.82 o 2 18 0 1122.80 1189.75 172.92 o 3 18 0 2084.11 2033.67 192.04 o 4 18 0 1763.01 1983.17 195.87 o 5 18 0 109.47 55.09 179.80 o 6 18 0 1143.36 1169.09 198.16 o 7 18 0 2810.33 2980.88 238.72 o 8 18 0 541.01 693.19 208.88 o 9 18 0 213.12 202.75 215.00 o 10 18 0 1148.21 912.78 251.72 o 1 19 0 2123.21 1807.66 138.45 o 2 19 0 740.20 478.96 179.80 o 3 19 0 287.41 100.23 179.04 o 4 19 0 204.17 308.34 171.39 o 5 19 0 1279.91 1190.52 205.05 o 6 19 0 745.13 908.95 204.29 o 7 19 0 1.91 -82.63 200.46 o 8 19 0 815.31 681.72 221.88 o 9 19 0 334.90 65.80 221.88 o 0 20 0 2271.05 2236.42 213.47 o 1 20 0 717.63 676.61 132.47 o 2 20 0 10.89 62.74 166.03 o 3 20 0 1165.29 1335.89 198.16 o 4 20 0 1185.66 1446.06 201.22 o 5 20 0 24.17 -73.45 189.75 o 6 20 0 1208.64 1140.78 220.35 o 7 20 0 1387.20 1768.94 228.77 o 8 20 0 106.81 -218.82 218.82 o 9 20 0 66.49 144.61 211.94 o 1 21 0 501.86 663.45 144.22 o 2 21 0 1214.57 995.41 200.46 o 3 21 0 688.97 604.44 201.99 o 4 21 0 395.30 373.37 192.04 o 5 21 0 908.13 742.92 208.88 o 6 21 0 503.74 389.44 221.12 o 7 21 0 30.33 245.60 205.82 o 8 21 0 179.00 629.69 210.41 o 0 22 0 908.02 993.12 205.05 o 1 22 0 213.77 113.96 139.85 o 2 22 0 23.86 -81.10 190.51 o 3 22 0 562.37 705.43 198.16 o 4 22 0 113.39 71.92 189.75 o 5 22 0 36.22 -74.98 199.69 o 6 22 0 510.85 736.80 218.82 o 7 22 0 467.06 216.53 233.36 o 1 23 0 912.54 1127.54 144.14 o 2 23 0 530.39 192.04 208.88 o 3 23 0 50.42 125.48 192.04 o 4 23 0 124.45 584.55 200.46 o 5 23 0 402.25 351.19 210.41 o 6 23 0 335.10 803.37 204.29 o 0 24 0 914.72 1365.73 219.59 o 1 24 0 141.25 249.04 207.73 o 2 24 0 88.54 -149.96 206.58 o 3 24 0 209.43 -78.81 209.64 o 4 24 0 121.92 -220.35 220.35 o 5 24 0 8.40 -224.94 224.94 o 1 25 0 51.83 -92.67 151.47 o 2 25 0 48.38 -13.77 211.17 o 3 25 0 0.64 34.43 213.47 o 4 25 0 10.42 -84.16 220.35 o 0 26 0 174.17 -149.20 223.41 o 1 26 0 116.74 368.06 251.34 o -14 1 1 20.35 -5.76 201.22 o -13 1 1 68.31 140.72 141.46 o -12 1 1 77.13 37.95 179.04 o -11 1 1 122.60 291.15 112.79 o -10 1 1 0.99 8.03 108.26 o -9 1 1 74.13 -19.66 92.49 o -8 1 1 0.67 36.92 95.72 o -7 1 1 104.00 68.33 87.64 o -6 1 1 460.79 455.05 80.31 o -5 1 1 1212.47 1360.55 73.85 o -4 1 1 2909.66 3215.82 136.96 o -3 1 1 259.21 305.95 53.83 o -2 1 1 148.59 218.65 50.04 o -1 1 1 8.36 45.20 26.43 o 1 1 1 26.82 63.69 33.43 o 2 1 1 10.07 27.33 52.50 o 3 1 1 1057.34 1065.69 61.90 o 4 1 1 938.19 947.10 69.39 o 5 1 1 9.36 57.20 65.44 o 6 1 1 313.30 262.28 81.42 o 7 1 1 154.23 81.39 93.01 o 8 1 1 21.01 69.47 182.10 o 9 1 1 38.60 138.31 107.50 o 10 1 1 0.92 45.04 100.61 o 11 1 1 5.21 89.50 135.81 o 12 1 1 14.42 83.52 125.64 o 13 1 1 13.55 198.05 144.97 o 14 1 1 18.60 16.28 154.97 o -14 2 1 20.88 221.88 217.29 o -13 2 1 4.29 -201.99 201.99 o -12 2 1 211.06 308.34 179.80 o -11 2 1 174.98 153.79 162.20 o -10 2 1 10.70 84.16 143.84 o -9 2 1 14.96 -130.83 130.83 o -8 2 1 207.51 161.44 139.25 o -7 2 1 6.37 269.32 123.18 o -6 2 1 94.80 73.45 105.59 o -5 2 1 2106.28 2182.87 121.65 o -4 2 1 523.39 586.08 91.05 o -3 2 1 184.84 243.31 78.04 o -2 2 1 410.29 443.77 79.57 o -1 2 1 115.02 115.05 43.57 o 0 2 1 161.89 182.81 47.28 o 1 2 1 119.38 20.21 49.61 o 2 2 1 271.66 269.32 87.99 o 3 2 1 739.02 829.38 91.81 o 4 2 1 861.29 872.23 104.82 o 5 2 1 1134.11 1372.61 110.18 o 6 2 1 596.22 338.18 128.54 o 7 2 1 177.47 306.81 134.66 o 8 2 1 89.68 197.40 141.55 o 9 2 1 164.53 164.50 133.89 o 10 2 1 140.73 216.53 147.67 o 11 2 1 25.32 22.95 167.56 o 12 2 1 98.21 241.01 185.16 o 13 2 1 140.82 127.77 213.47 o 14 2 1 5.29 -223.41 223.41 o -14 3 1 46.56 338.94 214.23 o -13 3 1 45.86 109.41 201.99 o -12 3 1 345.59 499.62 190.51 o -11 3 1 270.31 284.62 166.79 o -10 3 1 258.08 88.75 153.79 o -9 3 1 310.92 332.82 136.96 o -8 3 1 74.19 244.84 138.49 o -7 3 1 1637.53 1749.05 146.90 o -6 3 1 323.48 423.11 114.77 o -5 3 1 271.29 287.68 101.76 o -4 3 1 1023.84 889.06 102.53 o -3 3 1 1162.87 1202.76 89.52 o -2 3 1 3024.09 3247.14 100.99 o -1 3 1 225.82 240.34 53.90 o 0 3 1 2732.17 2889.25 68.94 o 1 3 1 1904.42 2071.10 65.20 o 2 3 1 36.04 -45.14 90.28 o 3 3 1 200.08 157.61 87.99 o 4 3 1 1199.98 1299.93 111.71 o 5 3 1 5.25 -107.88 107.88 o 6 3 1 2.13 -74.98 120.89 o 7 3 1 1290.33 1015.30 153.02 o 8 3 1 489.75 730.68 149.20 o 9 3 1 48.25 248.66 131.60 o 10 3 1 52.44 336.65 143.08 o 11 3 1 578.34 566.18 179.80 o 12 3 1 44.09 98.70 184.39 o 13 3 1 6.18 117.83 202.75 o 14 3 1 84.24 -228.77 228.77 o -14 4 1 113.79 336.65 230.30 o -13 4 1 25.72 144.61 200.46 o -12 4 1 409.44 706.96 189.75 o -11 4 1 951.87 1188.22 180.57 o -10 4 1 167.74 533.28 148.43 o -9 4 1 336.66 263.20 143.08 o -8 4 1 1825.98 2035.96 166.79 o -7 4 1 153.87 306.81 135.42 o -6 4 1 826.95 654.94 125.48 o -5 4 1 1483.36 1325.17 120.12 o -4 4 1 652.61 513.39 103.29 o -3 4 1 1294.68 1353.48 101.76 o -2 4 1 2583.98 2631.99 104.06 o -1 4 1 3071.14 3219.29 75.36 o 0 4 1 464.56 427.52 70.60 o 1 4 1 619.31 669.16 65.40 o 2 4 1 1934.55 1957.92 107.88 o 3 4 1 147.81 166.03 94.11 o 4 4 1 562.70 465.19 105.59 o 5 4 1 388.75 285.39 109.41 o 6 4 1 812.99 921.96 133.13 o 7 4 1 257.65 417.75 138.49 o 8 4 1 94.28 451.42 136.19 o 9 4 1 254.98 220.35 146.14 o 10 4 1 284.95 315.99 153.79 o 11 4 1 243.21 488.14 178.27 o 12 4 1 132.98 16.07 188.22 o 13 4 1 77.59 506.50 201.99 o 14 4 1 8.30 -59.68 233.36 o -14 5 1 147.86 -163.73 239.48 o -13 5 1 90.35 264.73 209.64 o -12 5 1 6.52 120.12 182.86 o -11 5 1 250.25 398.62 174.45 o -10 5 1 426.86 426.17 156.85 o -9 5 1 549.10 285.39 149.96 o -8 5 1 14.57 -151.49 151.49 o -7 5 1 1605.35 1537.11 159.14 o -6 5 1 601.64 424.64 132.36 o -5 5 1 4.40 240.25 100.99 o -4 5 1 2222.26 1993.12 120.89 o -3 5 1 2798.24 2919.67 117.83 o -2 5 1 88.85 -78.04 88.75 o -1 5 1 542.93 608.71 61.55 o 0 5 1 5790.03 6044.17 96.84 o 1 5 1 123.68 70.88 148.43 o 2 5 1 58.87 67.33 93.34 o 3 5 1 1287.75 1304.52 113.24 o 4 5 1 4830.56 4771.24 153.02 o 5 5 1 194.96 422.34 110.18 o 6 5 1 10.08 273.15 123.18 o 7 5 1 2266.97 2257.08 170.62 o 8 5 1 873.42 897.48 159.91 o 9 5 1 139.95 70.39 141.55 o 10 5 1 672.27 799.54 162.20 o 11 5 1 1035.18 801.84 191.28 o 12 5 1 105.24 102.53 188.98 o 13 5 1 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