#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:21 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180908 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/49/2104993.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104993_Fobs loop_ _publ_author_name 'Kamiya, Natsumi' 'Iwama, Wataru' 'Kudo, Tomokazu' 'Nasuno, Tomomi' 'Fujiyama, Shinjiro' 'Nishi, Koji' 'Yokomori, Yoshinobu' _publ_section_title ; Determining the structure of a benzene7.2-silicalite-1 zeolite using a single-crystal X-ray method ; _journal_coeditor_code DK5001 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 508 _journal_page_last 515 _journal_volume 67 _journal_year 2011 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.9200 _cell_length_b 19.8800 _cell_length_c 13.3860 _exptl_crystal_F_000 3181.00 _reflns_d_resolution_high 0.8295 _cod_data_source_file dk5001Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pnma in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 939.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 59696.45 29975.75 30956.87 o 4 0 0 35266.88 32866.96 590.16 o 6 0 0 59038.36 58984.13 1014.90 o 8 0 0 161434.70 161237.25 3108.43 o 10 0 0 378268.03 430752.34 9643.39 o 12 0 0 1969.18 2088.50 120.30 o 14 0 0 23222.97 21120.95 615.55 o 16 0 0 60715.68 55645.08 1009.94 o 18 0 0 9300.09 9634.75 410.29 o 20 0 0 37527.62 39936.42 825.00 o 22 0 0 330.72 69.68 184.51 o 24 0 0 1948.03 2058.73 359.97 o 2 1 0 11745.42 6535.85 2079.13 o 4 1 0 9459.14 10403.14 115.53 o 6 1 0 8850.63 8449.65 127.61 o 8 1 0 115.68 72.95 41.67 o 10 1 0 1641.76 2726.97 179.66 o 12 1 0 180.99 136.64 60.77 o 14 1 0 3118.20 2991.61 155.17 o 16 1 0 3119.32 3019.04 173.64 o 18 1 0 4191.90 4017.23 222.96 o 20 1 0 109.20 133.12 115.11 o 22 1 0 9.63 -71.94 111.72 o 0 2 0 235463.91 49941.36 52623.91 o 2 2 0 2331.98 1801.31 62.93 o 4 2 0 1049.03 726.65 46.08 o 6 2 0 855.78 1270.98 62.58 o 8 2 0 19454.58 18528.37 210.53 o 10 2 0 12457.14 12885.59 199.27 o 12 2 0 144.40 152.67 61.00 o 14 2 0 5161.36 4761.44 188.48 o 16 2 0 4153.26 4610.76 207.38 o 18 2 0 1443.40 1411.29 145.56 o 20 2 0 10.72 -54.07 105.48 o 22 2 0 3123.28 2821.16 232.55 o 2 3 0 18470.46 15817.98 179.08 o 4 3 0 37834.78 38728.09 240.29 o 6 3 0 44710.53 41775.77 278.74 o 8 3 0 7757.46 6797.30 136.88 o 10 3 0 1198.79 1194.07 81.81 o 12 3 0 49008.67 48325.78 709.88 o 14 3 0 9863.10 10172.96 252.64 o 16 3 0 33452.83 31851.82 458.83 o 18 3 0 5252.07 5082.76 248.71 o 20 3 0 214.80 58.07 124.55 o 22 3 0 2032.01 2089.47 209.40 o 0 4 0 47383.69 34270.48 586.65 o 2 4 0 31288.66 27676.61 275.94 o 4 4 0 3678.58 4172.87 79.42 o 6 4 0 31.72 -7.13 30.64 o 8 4 0 53.49 44.70 42.62 o 10 4 0 9045.80 8174.19 169.19 o 12 4 0 135.93 192.73 64.40 o 14 4 0 514.84 432.25 84.68 o 16 4 0 3222.76 3412.99 219.89 o 18 4 0 67.35 -87.89 87.89 o 20 4 0 195.29 281.02 129.42 o 22 4 0 175.78 186.18 130.38 o 2 5 0 23341.94 27439.75 392.57 o 4 5 0 3738.68 3669.57 85.17 o 6 5 0 38877.12 35582.66 334.76 o 8 5 0 154.22 0.23 34.25 o 10 5 0 1239.01 1104.82 81.61 o 12 5 0 6799.46 6877.66 176.47 o 14 5 0 8797.24 8622.00 237.39 o 16 5 0 69144.03 66440.75 1069.34 o 18 5 0 22344.72 24565.05 498.50 o 20 5 0 1736.89 1965.59 198.27 o 22 5 0 440.92 302.95 158.27 o 0 6 0 59931.91 54560.03 929.42 o 2 6 0 8095.06 6566.11 104.99 o 4 6 0 5583.37 5475.64 109.32 o 6 6 0 3216.33 2988.48 81.67 o 8 6 0 9607.37 8795.41 136.37 o 10 6 0 4280.86 4025.66 132.58 o 12 6 0 1875.67 1778.27 108.21 o 14 6 0 56.05 104.66 80.39 o 16 6 0 2297.50 2500.70 187.49 o 18 6 0 2714.97 2733.46 206.84 o 20 6 0 696.31 716.11 151.67 o 22 6 0 379.71 328.71 145.42 o 2 7 0 8.59 -5.75 34.69 o 4 7 0 30604.13 27727.00 322.04 o 6 7 0 320.34 257.43 42.70 o 8 7 0 1837.13 2046.45 81.93 o 10 7 0 4892.22 4951.40 143.94 o 12 7 0 23562.46 22771.47 354.67 o 14 7 0 10950.38 10819.96 270.07 o 16 7 0 479.06 284.81 115.55 o 18 7 0 3733.05 3827.11 233.93 o 20 7 0 2356.70 2074.07 208.61 o 22 7 0 1286.62 1217.41 186.36 o 0 8 0 102155.77 87661.56 1689.17 o 2 8 0 16624.96 14963.24 192.25 o 4 8 0 1605.07 1296.81 65.57 o 6 8 0 299.57 255.44 46.08 o 8 8 0 50269.14 51413.71 329.49 o 10 8 0 2216.43 2051.62 124.30 o 12 8 0 3270.37 3413.50 166.89 o 14 8 0 1344.23 1273.89 131.98 o 16 8 0 0.59 24.50 98.53 o 18 8 0 9106.89 9060.99 328.18 o 20 8 0 30532.44 31555.38 685.75 o 22 8 0 5057.32 5742.48 313.57 o 2 9 0 15.00 38.46 39.67 o 4 9 0 139.81 178.25 47.29 o 6 9 0 232.68 224.05 45.82 o 8 9 0 1990.11 1938.62 102.33 o 10 9 0 58.57 88.89 72.09 o 12 9 0 2.10 19.47 76.98 o 14 9 0 186.22 174.38 95.13 o 16 9 0 79.75 31.12 86.33 o 18 9 0 71.67 29.50 112.66 o 20 9 0 75.09 145.21 133.82 o 22 9 0 195.07 76.45 127.42 o 0 10 0 750513.31 787350.06 8761.42 o 2 10 0 11542.57 12104.00 177.79 o 4 10 0 1763.92 1688.44 82.27 o 6 10 0 4887.12 4863.39 116.97 o 8 10 0 1768.11 1688.44 102.21 o 10 10 0 44860.88 45890.47 631.77 o 12 10 0 1877.92 1651.16 136.33 o 14 10 0 4547.68 4404.11 207.72 o 16 10 0 8750.95 8255.93 274.45 o 18 10 0 3.20 34.03 114.42 o 20 10 0 4289.46 4457.51 274.99 o 2 11 0 1444.13 1405.74 80.86 o 4 11 0 5263.79 5253.53 131.60 o 6 11 0 930.55 955.23 92.76 o 8 11 0 1401.57 1520.56 105.76 o 10 11 0 956.78 1007.00 114.57 o 12 11 0 1744.86 1797.70 142.91 o 14 11 0 464.01 596.43 118.04 o 16 11 0 221.36 348.73 113.30 o 18 11 0 5.77 -21.21 113.76 o 20 11 0 33.28 23.78 125.16 o 0 12 0 613.66 749.07 99.89 o 2 12 0 1860.06 2251.84 110.18 o 4 12 0 3301.63 3462.96 119.55 o 6 12 0 14.31 61.31 62.05 o 8 12 0 29218.48 27666.02 481.28 o 10 12 0 11.90 17.88 80.12 o 12 12 0 254.53 254.06 100.63 o 14 12 0 3738.93 3931.56 204.40 o 16 12 0 3750.53 3904.68 215.35 o 18 12 0 3368.12 3322.26 239.07 o 20 12 0 6604.16 6306.47 319.50 o 2 13 0 5380.54 5414.83 148.38 o 4 13 0 107356.99 105738.05 649.43 o 6 13 0 42587.13 39621.56 471.27 o 8 13 0 22676.46 21701.70 348.13 o 10 13 0 8401.12 8295.23 251.62 o 12 13 0 119977.11 119889.22 1501.23 o 14 13 0 36686.39 36301.74 537.37 o 16 13 0 43752.14 40127.55 593.18 o 18 13 0 526.37 614.38 152.40 o 20 13 0 3032.03 2936.73 287.90 o 0 14 0 320.25 472.70 106.05 o 2 14 0 30.36 6.43 58.49 o 4 14 0 16.08 29.31 67.64 o 6 14 0 1012.70 925.56 101.44 o 8 14 0 2094.65 2318.15 135.71 o 10 14 0 269.78 145.60 98.19 o 12 14 0 0.38 11.58 92.64 o 14 14 0 716.99 604.43 126.69 o 16 14 0 90.38 44.80 119.61 o 18 14 0 150.65 299.14 156.94 o 2 15 0 392.07 306.59 80.51 o 4 15 0 16118.87 15699.33 283.90 o 6 15 0 1352.86 1131.21 111.87 o 8 15 0 6445.61 5886.66 221.85 o 10 15 0 2268.15 2099.57 178.35 o 12 15 0 2516.48 2363.22 192.91 o 14 15 0 1.76 -13.40 111.22 o 16 15 0 3496.11 3144.50 235.79 o 18 15 0 6096.04 5689.31 344.42 o 0 16 0 124637.55 124778.09 1330.77 o 2 16 0 4035.83 4093.75 185.99 o 4 16 0 7100.23 6525.55 228.91 o 6 16 0 1017.53 1063.39 126.93 o 8 16 0 6960.52 6496.72 265.20 o 10 16 0 10574.97 10599.39 334.70 o 12 16 0 209.12 337.40 142.55 o 14 16 0 0.73 50.54 115.55 o 16 16 0 875.16 893.37 169.89 o 2 17 0 1513.02 1490.35 153.74 o 4 17 0 1797.32 1892.78 168.29 o 6 17 0 2096.76 1945.42 152.14 o 8 17 0 587.77 631.65 133.01 o 10 17 0 434.90 315.23 125.35 o 12 17 0 9287.51 9501.06 342.69 o 14 17 0 2037.48 2116.51 230.12 o 16 17 0 167.14 220.58 142.34 o 0 18 0 55453.75 55562.30 1492.25 o 2 18 0 4153.72 4161.81 255.28 o 4 18 0 4223.37 4352.17 230.95 o 6 18 0 177.43 133.94 107.43 o 8 18 0 5304.25 5122.17 290.21 o 10 18 0 3480.27 3439.61 261.47 o 12 18 0 645.89 730.43 177.77 o 14 18 0 755.46 576.11 171.38 o 2 19 0 126.26 53.00 108.78 o 4 19 0 455.19 648.22 134.24 o 6 19 0 393.45 431.55 128.09 o 8 19 0 645.22 587.16 159.81 o 10 19 0 133.68 113.11 138.52 o 12 19 0 349.92 219.33 149.05 o 14 19 0 87.18 27.33 139.37 o 0 20 0 18836.34 21244.62 1057.05 o 2 20 0 1070.30 1152.21 177.91 o 4 20 0 400.16 514.93 152.77 o 6 20 0 1796.46 2028.30 191.81 o 8 20 0 10882.21 10083.29 406.83 o 10 20 0 200.26 283.02 148.72 o 12 20 0 438.57 311.83 159.41 o 2 21 0 1236.38 1343.22 198.26 o 4 21 0 1729.47 1845.33 215.30 o 6 21 0 5640.10 5658.36 373.98 o 8 21 0 10795.60 10779.56 427.57 o 10 21 0 45.05 -3.58 135.17 o 0 22 0 465.89 436.93 215.97 o 2 22 0 436.36 438.02 156.91 o 4 22 0 22.84 129.91 135.95 o 6 22 0 33.66 178.90 168.76 o 8 22 0 1445.76 1493.49 218.55 o 2 23 0 173.77 150.20 138.44 o 4 23 0 8725.61 8917.71 409.79 o 6 23 0 1300.20 1340.43 256.09 o 1 0 1 50341.79 23617.88 10393.69 o 2 0 1 450.80 59.35 31.18 o 3 0 1 30991.46 28466.59 351.27 o 4 0 1 1443.70 1608.51 56.18 o 5 0 1 882067.13 887551.56 13626.67 o 6 0 1 706.90 793.51 47.76 o 7 0 1 9148.47 7188.46 121.57 o 8 0 1 1008.99 663.82 50.65 o 9 0 1 11259.42 12499.22 158.95 o 10 0 1 19491.51 20085.77 343.82 o 11 0 1 1814.19 2049.69 86.65 o 12 0 1 4065.94 4044.91 108.64 o 13 0 1 9473.88 10058.81 240.78 o 14 0 1 5979.38 5630.18 201.65 o 15 0 1 21922.53 19203.46 393.57 o 16 0 1 129493.16 118489.71 2138.51 o 17 0 1 320.20 456.22 109.93 o 18 0 1 25785.55 24927.82 474.77 o 19 0 1 4609.96 5011.51 251.24 o 20 0 1 5853.28 5650.01 276.65 o 21 0 1 4736.13 5237.28 309.83 o 22 0 1 276.80 208.55 146.27 o 23 0 1 1080.15 930.46 195.20 o 0 1 1 102787.52 37943.46 22535.60 o 1 1 1 20016.61 8124.84 2320.84 o 2 1 1 4218.05 2352.65 451.71 o 3 1 1 2441.98 2349.47 36.66 o 4 1 1 1747.46 2075.54 43.31 o 5 1 1 37.80 21.35 38.91 o 6 1 1 1077.09 1227.88 39.00 o 7 1 1 749.18 778.94 34.26 o 8 1 1 9880.41 9365.12 88.44 o 9 1 1 145.38 143.25 27.05 o 10 1 1 5486.41 5705.58 87.71 o 11 1 1 3577.52 4135.99 71.93 o 12 1 1 1893.89 1913.69 72.69 o 13 1 1 6183.78 5844.33 142.13 o 14 1 1 356.39 352.86 67.45 o 15 1 1 15.11 89.73 58.82 o 16 1 1 4583.24 4878.83 149.85 o 17 1 1 31.97 59.46 68.35 o 18 1 1 1608.35 1654.10 108.08 o 19 1 1 1234.64 1517.70 112.54 o 20 1 1 58.89 75.79 82.05 o 21 1 1 8.58 54.88 83.55 o 22 1 1 33.36 58.82 87.22 o 23 1 1 155.33 183.85 105.12 o 1 2 1 1383.83 1216.78 121.45 o 2 2 1 404.34 208.08 16.15 o 3 2 1 808.70 1468.14 34.38 o 4 2 1 45452.41 49088.68 406.71 o 5 2 1 17937.74 18545.48 134.29 o 6 2 1 10917.65 10890.22 86.36 o 7 2 1 2734.21 2284.16 48.55 o 8 2 1 719.65 839.80 44.59 o 9 2 1 14.62 14.77 31.06 o 10 2 1 7206.04 7540.56 113.08 o 11 2 1 50.72 69.30 38.13 o 12 2 1 7776.03 8245.29 129.28 o 13 2 1 3128.05 3451.40 97.47 o 14 2 1 4355.03 4408.16 135.12 o 15 2 1 420.54 425.97 76.22 o 16 2 1 3492.75 3370.58 133.05 o 17 2 1 7.11 75.51 67.40 o 18 2 1 5465.86 5280.22 170.38 o 19 2 1 195.28 287.77 84.90 o 20 2 1 1352.94 1372.08 122.86 o 21 2 1 255.41 127.16 93.92 o 22 2 1 326.76 373.00 99.71 o 23 2 1 70.07 149.07 99.90 o 0 3 1 35592.26 23946.91 162.80 o 1 3 1 25838.51 21824.08 106.85 o 2 3 1 1914.43 1430.57 36.61 o 3 3 1 9822.50 10126.31 85.08 o 4 3 1 8566.05 8943.08 98.13 o 5 3 1 589.50 719.75 32.73 o 6 3 1 11.75 13.44 22.71 o 7 3 1 15668.82 15616.13 138.24 o 8 3 1 89.20 299.38 37.15 o 9 3 1 7306.52 7003.64 108.95 o 10 3 1 1418.95 1492.53 63.18 o 11 3 1 51501.84 52571.23 496.26 o 12 3 1 12402.70 11714.74 152.98 o 13 3 1 21679.64 20439.24 223.85 o 14 3 1 1806.31 1836.90 93.25 o 15 3 1 2.15 14.93 57.32 o 16 3 1 497.69 567.52 83.31 o 17 3 1 5384.24 5313.18 175.31 o 18 3 1 278.71 307.40 83.50 o 19 3 1 858.93 892.91 108.39 o 20 3 1 2144.31 2129.55 140.67 o 21 3 1 616.25 534.59 104.66 o 22 3 1 1556.81 1554.32 147.42 o 23 3 1 910.76 874.44 123.69 o 1 4 1 18445.88 17030.91 93.76 o 2 4 1 225.55 131.62 23.73 o 3 4 1 5266.02 6306.54 73.49 o 4 4 1 381.60 453.38 30.86 o 5 4 1 4367.81 3889.77 58.00 o 6 4 1 16.59 47.39 23.73 o 7 4 1 498.19 444.40 33.88 o 8 4 1 282.12 355.32 33.23 o 9 4 1 65.18 98.60 35.54 o 10 4 1 0.05 -15.01 33.45 o 11 4 1 314.99 287.23 46.84 o 12 4 1 31.00 27.77 40.88 o 13 4 1 68.10 62.32 46.06 o 14 4 1 199.53 160.15 51.88 o 15 4 1 202.74 183.90 68.86 o 16 4 1 4782.29 4555.53 164.58 o 17 4 1 1035.23 1105.01 105.54 o 18 4 1 26.71 40.42 77.02 o 19 4 1 10.06 -35.59 75.03 o 20 4 1 225.02 208.25 88.21 o 21 4 1 47.97 -26.76 79.87 o 22 4 1 30.87 -0.31 87.04 o 23 4 1 2.90 -39.98 87.02 o 0 5 1 796346.63 816941.75 5844.79 o 1 5 1 111312.82 121551.52 635.71 o 2 5 1 296.28 193.11 25.24 o 3 5 1 8544.67 9220.62 89.08 o 4 5 1 4743.79 4514.39 69.05 o 5 5 1 171.23 160.81 27.70 o 6 5 1 5564.69 5308.32 69.80 o 7 5 1 4322.11 3877.74 68.11 o 8 5 1 2724.49 1094.47 43.66 o 9 5 1 631.12 1011.33 46.99 o 10 5 1 26946.44 27518.67 210.82 o 11 5 1 48802.49 47018.83 442.78 o 12 5 1 9385.56 9164.95 141.44 o 13 5 1 49781.20 48464.72 376.64 o 14 5 1 1787.22 1861.65 89.72 o 15 5 1 56.50 45.90 69.28 o 16 5 1 23628.37 22392.87 317.34 o 17 5 1 584.13 681.77 95.15 o 18 5 1 3873.20 4380.77 170.41 o 19 5 1 2063.01 2440.78 150.92 o 20 5 1 1058.53 1237.38 131.16 o 21 5 1 578.38 657.34 111.36 o 22 5 1 908.60 774.63 120.11 o 23 5 1 2447.49 2739.52 183.23 o 1 6 1 11909.98 10303.54 97.93 o 2 6 1 904.23 669.30 33.15 o 3 6 1 7615.21 7604.31 92.99 o 4 6 1 175.30 203.01 29.81 o 5 6 1 5682.95 5779.72 82.15 o 6 6 1 3.39 3.80 26.37 o 7 6 1 359.92 397.13 36.28 o 8 6 1 418.01 495.12 36.90 o 9 6 1 830.36 985.55 44.97 o 10 6 1 939.84 1080.98 58.74 o 11 6 1 194.00 201.79 44.81 o 12 6 1 472.28 499.00 58.91 o 13 6 1 3182.64 3439.33 110.27 o 14 6 1 3.93 27.14 54.85 o 15 6 1 493.63 531.43 80.46 o 16 6 1 1912.36 1822.49 120.39 o 17 6 1 1723.89 1770.78 122.53 o 18 6 1 2063.32 2125.64 133.84 o 19 6 1 44.60 14.26 74.40 o 20 6 1 322.43 382.82 100.89 o 21 6 1 216.63 253.11 98.50 o 22 6 1 9.95 -33.24 82.88 o 23 6 1 287.50 314.88 105.44 o 0 7 1 9427.08 6690.07 114.21 o 1 7 1 1081.49 1282.24 43.20 o 2 7 1 1720.01 1439.64 45.88 o 3 7 1 84.77 97.90 25.81 o 4 7 1 867.35 833.18 41.90 o 5 7 1 511.22 452.77 36.68 o 6 7 1 272.90 285.14 35.66 o 7 7 1 3539.08 3439.61 75.61 o 8 7 1 4440.80 4030.48 86.31 o 9 7 1 3212.93 3063.17 69.61 o 10 7 1 1710.68 1668.60 75.50 o 11 7 1 1015.07 1026.41 67.88 o 12 7 1 3962.71 4032.69 122.53 o 13 7 1 35.79 62.69 54.93 o 14 7 1 6590.70 6743.65 159.99 o 15 7 1 3.42 5.12 59.61 o 16 7 1 4934.49 5169.28 172.85 o 17 7 1 1380.30 1394.89 115.93 o 18 7 1 390.25 339.89 87.60 o 19 7 1 491.33 547.49 100.96 o 20 7 1 1214.49 1317.94 130.40 o 21 7 1 1333.95 1384.37 140.56 o 22 7 1 7226.03 7723.88 260.18 o 1 8 1 4686.39 3997.99 70.35 o 2 8 1 324.97 339.20 32.06 o 3 8 1 5164.32 6152.48 84.13 o 4 8 1 10679.92 7497.41 98.85 o 5 8 1 7440.99 5011.83 86.34 o 6 8 1 937.77 1246.17 52.79 o 7 8 1 19019.92 18119.76 157.59 o 8 8 1 981.65 996.06 52.79 o 9 8 1 496.33 566.32 47.22 o 10 8 1 1453.96 1418.66 72.52 o 11 8 1 291.63 286.63 58.16 o 12 8 1 20077.86 19843.73 242.54 o 13 8 1 22167.98 22184.50 263.77 o 14 8 1 207.06 137.74 65.28 o 15 8 1 15120.84 14465.33 231.84 o 16 8 1 20770.61 19646.33 307.96 o 17 8 1 513.39 434.77 92.98 o 18 8 1 2553.85 2569.69 145.72 o 19 8 1 5449.28 5821.63 204.57 o 20 8 1 551.81 513.24 107.23 o 21 8 1 0.15 -15.65 80.43 o 22 8 1 2587.22 2602.43 178.11 o 0 9 1 4410.40 4869.13 113.46 o 1 9 1 6760.51 6539.24 90.10 o 2 9 1 263.55 290.26 33.90 o 3 9 1 1078.37 1154.21 47.43 o 4 9 1 0.82 -16.16 28.98 o 5 9 1 3.27 4.74 32.82 o 6 9 1 0.99 22.84 33.13 o 7 9 1 830.60 835.61 51.43 o 8 9 1 1589.63 1535.88 63.39 o 9 9 1 1080.41 1112.23 62.06 o 10 9 1 2.30 41.55 49.79 o 11 9 1 1794.24 1614.58 89.22 o 12 9 1 229.78 223.89 62.45 o 13 9 1 995.95 920.70 84.36 o 14 9 1 145.69 199.99 68.09 o 15 9 1 48.54 70.34 64.37 o 16 9 1 90.86 164.98 67.07 o 17 9 1 1.85 -41.83 69.33 o 18 9 1 138.40 203.35 85.73 o 19 9 1 3.26 -21.63 80.33 o 20 9 1 163.38 247.75 93.34 o 21 9 1 25.96 65.70 89.09 o 22 9 1 106.68 210.63 100.05 o 1 10 1 6510.66 7388.62 101.80 o 2 10 1 91.04 155.17 33.63 o 3 10 1 1574.40 1540.98 55.15 o 4 10 1 2199.96 2623.77 67.47 o 5 10 1 38800.32 41027.24 282.06 o 6 10 1 633.82 863.21 54.64 o 7 10 1 2923.62 2672.69 78.49 o 8 10 1 1069.63 1045.26 63.24 o 9 10 1 349.92 319.11 51.20 o 10 10 1 1195.65 1104.39 79.60 o 11 10 1 306.75 235.40 62.46 o 12 10 1 100.67 66.71 60.22 o 13 10 1 10.99 -1.62 59.89 o 14 10 1 2586.42 2354.90 115.58 o 15 10 1 5729.68 5354.15 159.01 o 16 10 1 30585.43 28089.58 334.22 o 17 10 1 89.08 11.15 76.92 o 18 10 1 765.57 720.79 107.17 o 19 10 1 698.96 684.65 113.22 o 20 10 1 526.33 493.90 104.11 o 21 10 1 265.70 331.49 104.54 o 0 11 1 9679.56 10397.50 173.83 o 1 11 1 1.19 20.12 32.93 o 2 11 1 1.05 5.68 32.94 o 3 11 1 21.72 18.66 33.09 o 4 11 1 89.72 70.15 34.64 o 5 11 1 6.73 17.46 37.52 o 6 11 1 1257.75 1217.62 61.13 o 7 11 1 140.48 207.97 48.52 o 8 11 1 1307.34 1352.66 71.44 o 9 11 1 1022.16 958.52 77.12 o 10 11 1 702.74 699.72 75.76 o 11 11 1 1251.55 1151.32 86.73 o 12 11 1 194.55 156.75 68.12 o 13 11 1 259.27 326.56 72.68 o 14 11 1 1026.27 947.26 91.43 o 15 11 1 26.30 64.74 63.21 o 16 11 1 814.21 843.83 93.62 o 17 11 1 391.52 412.19 93.60 o 18 11 1 197.25 59.51 86.26 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