#------------------------------------------------------------------------------ #$Date: 2012-01-03 14:54:16 +0200 (Tue, 03 Jan 2012) $ #$Revision: 31968 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/49/2104994.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2104994_Fobs loop_ _publ_author_name 'Siegler, Maxime A.' 'Hao, Xiang' 'Parkin, Sean' 'Brock, Carolyn Pratt' _publ_section_title ; [Ni(H~2~O)~6~](NO~3~)~2~·(15-crown-5)·2H~2~O: three phase transitions and an intermediate modulated phase stable over a range of ca 40K ; _journal_coeditor_code HW5018 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 486 _journal_page_last 498 _journal_volume 67 _journal_year 2011 _space_group_IT_number 12 _symmetry_space_group_name_Hall '-I 2y' _symmetry_space_group_name_H-M 'I 1 2/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.480 _cell_angle_gamma 90.000 _cell_length_a 12.3700 _cell_length_b 12.5700 _cell_length_c 8.1140 _exptl_crystal_F_000 580.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file hw5018294K_Isup2.hkl _[local]_cod_data_source_block 294K_I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k02180 in I2/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 181.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5381.91 5129.85 100.79 o 4 0 0 1118.65 1041.51 23.11 o 6 0 0 9756.06 10345.83 223.63 o 8 0 0 1955.36 2065.18 41.99 o 10 0 0 273.86 274.03 9.45 o 12 0 0 76.26 62.99 16.80 o 14 0 0 6.72 0.00 18.90 o 1 1 0 7578.00 6945.43 86.40 o 3 1 0 1175.82 1100.91 15.95 o 5 1 0 714.61 623.49 9.09 o 7 1 0 945.89 867.82 14.35 o 9 1 0 1088.68 1131.71 23.17 o 11 1 0 168.64 172.93 13.30 o 13 1 0 94.94 95.83 14.11 o 15 1 0 45.06 66.20 18.25 o 0 2 0 12487.79 13854.13 241.27 o 2 2 0 54.21 43.07 1.48 o 4 2 0 2581.86 2508.83 34.63 o 6 2 0 2026.86 2270.98 48.82 o 8 2 0 917.35 953.55 17.07 o 10 2 0 324.90 340.99 10.00 o 12 2 0 134.80 180.38 16.40 o 14 2 0 21.78 39.60 12.60 o 1 3 0 71.09 82.18 2.10 o 3 3 0 11531.58 11572.53 137.38 o 5 3 0 5520.41 5477.79 125.46 o 7 3 0 436.28 436.93 17.32 o 9 3 0 350.67 349.28 9.09 o 11 3 0 527.56 542.43 23.63 o 13 3 0 167.05 173.51 18.38 o 15 3 0 39.83 45.41 21.36 o 0 4 0 696.55 779.99 13.60 o 2 4 0 9705.00 9658.59 120.03 o 4 4 0 7668.81 7913.22 90.73 o 6 4 0 1149.19 1080.35 15.95 o 8 4 0 683.56 701.58 14.35 o 10 4 0 168.19 158.16 8.51 o 12 4 0 138.76 135.30 15.10 o 14 4 0 58.79 50.35 18.16 o 1 5 0 360.59 372.56 5.53 o 3 5 0 626.69 708.17 10.40 o 5 5 0 2412.62 2557.94 47.78 o 7 5 0 276.65 294.72 18.37 o 9 5 0 8.39 12.28 4.78 o 11 5 0 373.79 360.22 19.61 o 13 5 0 123.54 129.45 14.09 o 0 6 0 1685.19 1968.64 44.09 o 2 6 0 6565.85 6806.63 154.86 o 4 6 0 1946.94 2039.38 27.83 o 6 6 0 617.43 635.89 27.81 o 8 6 0 445.98 440.50 13.11 o 10 6 0 156.64 156.66 9.84 o 12 6 0 59.27 63.01 13.01 o 14 6 0 35.96 26.23 18.92 o 1 7 0 1881.80 1845.48 24.05 o 3 7 0 470.02 419.49 7.77 o 5 7 0 1233.81 1291.73 23.45 o 7 7 0 356.19 376.13 11.81 o 9 7 0 110.77 93.44 8.07 o 11 7 0 267.84 274.03 16.31 o 13 7 0 30.48 33.27 18.25 o 0 8 0 1372.79 1386.19 72.96 o 2 8 0 756.58 788.29 12.11 o 4 8 0 73.69 76.64 5.20 o 6 8 0 206.31 183.73 8.32 o 8 8 0 379.03 350.14 33.08 o 10 8 0 251.80 270.13 15.85 o 12 8 0 4.64 9.07 14.76 o 1 9 0 812.47 846.55 16.27 o 3 9 0 64.84 59.23 4.03 o 5 9 0 137.89 160.58 9.97 o 7 9 0 292.32 275.65 12.36 o 9 9 0 257.56 248.42 25.20 o 11 9 0 44.82 59.59 18.52 o 13 9 0 14.69 27.78 19.26 o 0 10 0 1682.88 1925.89 67.71 o 2 10 0 200.87 205.05 13.12 o 4 10 0 40.16 38.22 15.22 o 6 10 0 405.88 418.08 15.54 o 8 10 0 197.74 198.80 13.79 o 10 10 0 60.22 110.70 21.07 o 12 10 0 11.20 -14.57 18.83 o 1 11 0 91.92 103.37 12.60 o 3 11 0 102.80 98.26 8.82 o 5 11 0 154.83 169.23 12.62 o 7 11 0 69.96 74.13 10.59 o 9 11 0 31.73 23.20 14.70 o 11 11 0 15.87 6.13 23.88 o 0 12 0 252.29 238.69 33.07 o 2 12 0 132.14 141.97 12.07 o 4 12 0 243.78 253.10 15.59 o 6 12 0 148.35 126.43 13.72 o 8 12 0 7.13 15.58 17.32 o 10 12 0 15.90 36.34 25.05 o 1 13 0 58.60 56.39 17.32 o 3 13 0 305.25 292.26 15.75 o 5 13 0 140.81 154.72 23.10 o 7 13 0 11.41 1.55 25.20 o 9 13 0 17.25 33.30 20.16 o 0 14 0 3.30 10.09 20.92 o 2 14 0 25.75 18.05 33.07 o 4 14 0 43.02 46.92 21.00 o 6 14 0 16.56 21.93 26.77 o 8 14 0 14.26 21.64 27.17 o 1 15 0 7.78 -15.38 18.83 o 3 15 0 14.46 25.53 18.52 o 5 15 0 12.64 14.04 26.77 o 0 16 0 53.78 23.66 31.18 o 2 16 0 36.69 58.34 40.95 o -15 0 1 62.81 62.99 24.15 o -13 0 1 73.75 98.69 15.75 o -11 0 1 643.87 608.95 29.40 o -9 0 1 2996.07 3673.66 120.72 o -7 0 1 3570.13 3871.03 73.51 o -5 0 1 596.35 550.14 11.56 o -3 0 1 21553.81 21857.04 395.81 o -1 0 1 1692.89 1537.06 27.28 o 1 0 1 381.54 318.12 5.25 o 3 0 1 1738.88 1878.30 40.96 o 5 0 1 42.76 31.50 4.20 o 7 0 1 211.10 211.03 10.50 o 9 0 1 1110.14 1241.01 35.69 o 11 0 1 21.77 30.45 8.40 o 13 0 1 1.14 -4.20 15.75 o 15 0 1 57.42 107.09 30.45 o -14 1 1 72.61 84.72 24.67 o -12 1 1 76.09 81.04 11.49 o -10 1 1 915.29 937.33 21.37 o -8 1 1 782.43 750.72 13.37 o -6 1 1 510.69 685.72 11.06 o -4 1 1 483.80 488.45 6.80 o -2 1 1 179.21 180.61 2.97 o 0 1 1 190.05 208.42 2.97 o 2 1 1 16238.24 15974.51 257.22 o 4 1 1 2039.07 2344.62 58.28 o 6 1 1 754.37 776.44 13.60 o 8 1 1 2116.55 2202.22 40.42 o 10 1 1 401.08 388.66 19.42 o 12 1 1 64.45 67.81 12.85 o 14 1 1 39.00 22.29 24.67 o -15 2 1 65.49 70.26 25.72 o -13 2 1 121.88 146.13 17.63 o -11 2 1 291.19 302.81 15.21 o -9 2 1 978.14 1044.44 33.08 o -7 2 1 3051.42 2969.45 41.08 o -5 2 1 352.71 371.51 5.53 o -3 2 1 8945.77 9331.46 143.30 o -1 2 1 10537.68 10031.37 116.60 o 1 2 1 2098.99 1948.66 26.74 o 3 2 1 15.28 18.90 1.75 o 5 2 1 578.87 506.71 9.09 o 7 2 1 92.45 86.49 4.27 o 9 2 1 56.71 47.12 5.25 o 11 2 1 4.08 6.78 7.77 o 13 2 1 40.89 38.71 15.26 o 15 2 1 35.44 30.26 16.88 o -14 3 1 183.31 191.57 19.58 o -12 3 1 165.72 160.27 14.88 o -10 3 1 65.45 58.09 7.77 o -8 3 1 524.50 486.67 9.85 o -6 3 1 4435.79 4672.34 58.89 o -4 3 1 2430.26 2590.05 40.43 o -2 3 1 4471.36 4605.42 51.41 o 0 3 1 6961.07 7219.77 138.06 o 2 3 1 5411.86 5482.05 70.12 o 4 3 1 3135.52 3405.37 40.96 o 6 3 1 1170.79 1375.27 19.67 o 8 3 1 234.39 232.32 7.31 o 10 3 1 205.37 165.43 13.12 o 12 3 1 154.65 173.23 16.11 o 14 3 1 69.75 77.72 43.57 o -15 4 1 49.42 47.53 18.63 o -13 4 1 206.11 238.88 17.43 o -11 4 1 369.33 367.55 23.62 o -9 4 1 310.16 302.62 15.22 o -7 4 1 481.92 465.88 10.00 o -5 4 1 4701.25 4920.12 65.81 o -3 4 1 5659.56 5797.10 215.77 o -1 4 1 233.33 202.63 3.28 o 1 4 1 6.76 4.72 1.48 o 3 4 1 1307.46 1363.22 16.87 o 5 4 1 1962.67 1921.02 23.67 o 7 4 1 94.94 94.80 4.78 o 9 4 1 24.45 16.34 3.65 o 11 4 1 44.55 44.10 9.31 o 13 4 1 169.27 185.91 19.41 o -14 5 1 150.38 124.49 20.33 o -12 5 1 211.92 193.13 20.47 o -10 5 1 72.80 65.49 7.02 o -8 5 1 202.89 217.62 10.50 o -6 5 1 670.80 692.44 12.62 o -4 5 1 613.85 653.04 9.65 o -2 5 1 384.89 423.87 9.98 o 0 5 1 1696.40 1941.12 24.12 o 2 5 1 21.12 24.33 2.23 o 4 5 1 6006.35 6000.91 74.53 o 6 5 1 7.48 10.40 3.65 o 8 5 1 68.46 74.82 5.40 o 10 5 1 371.43 368.09 20.48 o 12 5 1 129.23 102.95 13.99 o 14 5 1 41.74 9.05 24.15 o -13 6 1 95.56 117.69 18.09 o -11 6 1 342.65 308.00 15.40 o -9 6 1 695.13 676.30 18.38 o -7 6 1 161.77 162.96 11.02 o -5 6 1 2825.63 2920.10 42.30 o -3 6 1 3039.75 3110.87 39.01 o -1 6 1 902.02 836.00 11.06 o 1 6 1 1137.56 1051.83 27.81 o 3 6 1 1249.53 1328.03 30.98 o 5 6 1 478.92 414.38 21.01 o 7 6 1 444.01 468.38 14.17 o 9 6 1 51.38 59.10 6.20 o 11 6 1 41.78 36.36 11.60 o 13 6 1 89.02 82.18 18.16 o -14 7 1 51.37 48.17 18.83 o -12 7 1 69.82 51.51 17.15 o -10 7 1 113.57 95.83 8.82 o -8 7 1 785.32 878.95 22.20 o -6 7 1 329.46 298.90 14.70 o -4 7 1 165.43 147.33 9.45 o -2 7 1 1466.91 1483.31 19.58 o 0 7 1 1351.77 1284.82 17.03 o 2 7 1 812.60 871.81 13.60 o 4 7 1 799.57 814.97 15.95 o 6 7 1 55.62 50.17 7.87 o 8 7 1 521.74 555.80 16.50 o 10 7 1 208.50 199.91 13.30 o 12 7 1 39.19 49.33 14.93 o -13 8 1 26.27 55.13 17.15 o -11 8 1 83.91 87.09 21.46 o -9 8 1 339.73 295.70 13.30 o -7 8 1 237.59 227.47 22.57 o -5 8 1 108.33 95.65 5.94 o -3 8 1 120.30 134.13 8.93 o -1 8 1 852.28 966.71 24.14 o 1 8 1 716.57 781.47 12.55 o 3 8 1 6.22 5.95 3.28 o 5 8 1 5.45 -1.57 5.94 o 7 8 1 383.32 431.92 40.41 o 9 8 1 62.58 67.27 16.80 o 11 8 1 15.18 0.78 10.65 o 13 8 1 14.64 36.17 24.20 o -12 9 1 28.64 31.08 19.39 o -10 9 1 79.70 58.91 16.80 o -8 9 1 334.24 300.27 19.42 o -6 9 1 180.43 157.07 8.07 o -4 9 1 250.21 233.75 8.07 o -2 9 1 437.22 422.78 12.09 o 0 9 1 1108.07 1084.08 19.95 o 2 9 1 880.25 887.36 17.64 o 4 9 1 44.78 37.96 5.53 o 6 9 1 110.28 110.40 9.08 o 8 9 1 279.31 256.30 14.76 o 10 9 1 82.05 84.66 12.98 o 12 9 1 17.18 -1.46 40.94 o -11 10 1 52.12 38.97 19.26 o -9 10 1 176.36 151.33 25.72 o -7 10 1 244.58 223.53 23.62 o -5 10 1 203.69 205.45 11.26 o -3 10 1 791.54 882.47 19.16 o -1 10 1 894.82 914.78 19.42 o 1 10 1 533.59 512.13 13.30 o 3 10 1 454.20 440.11 18.91 o 5 10 1 142.58 126.53 11.14 o 7 10 1 130.68 104.10 17.85 o 9 10 1 79.56 69.56 16.27 o 11 10 1 21.43 27.50 40.42 o -10 11 1 39.45 73.18 24.00 o -8 11 1 74.94 69.48 10.84 o -6 11 1 53.42 63.46 8.51 o -4 11 1 179.30 180.31 10.08 o -2 11 1 26.99 20.84 23.10 o 0 11 1 43.21 42.46 8.54 o 2 11 1 277.35 269.59 12.23 o 4 11 1 35.92 54.88 12.07 o 6 11 1 67.91 54.39 9.18 o 8 11 1 78.86 63.99 13.12 o 10 11 1 25.61 35.84 20.91 o -9 12 1 32.45 13.83 38.32 o -7 12 1 87.58 79.23 12.98 o -5 12 1 31.68 17.85 10.84 o -3 12 1 105.12 78.82 11.06 o -1 12 1 28.53 17.12 9.57 o 1 12 1 1.20 -10.71 12.60 o 3 12 1 86.66 63.99 9.57 o 5 12 1 98.86 87.95 11.14 o 7 12 1 39.65 24.24 12.36 o 9 12 1 15.97 16.66 18.25 o -8 13 1 23.66 8.93 24.67 o -6 13 1 117.39 126.56 18.52 o -4 13 1 125.56 137.23 15.75 o -2 13 1 49.73 44.50 24.67 o 0 13 1 58.89 49.23 13.36 o 2 13 1 95.24 117.26 30.45 o 4 13 1 103.57 98.19 14.11 o 6 13 1 95.61 127.61 19.66 o 8 13 1 15.12 8.72 24.17 o -7 14 1 21.04 41.47 16.33 o -5 14 1 67.14 59.07 18.37 o -3 14 1 85.04 45.15 16.80 o -1 14 1 55.51 57.50 16.27 o 1 14 1 24.26 18.95 15.38 o 3 14 1 60.80 59.58 13.59 o 5 14 1 69.52 70.80 33.07 o 7 14 1 6.41 10.89 23.90 o -6 15 1 15.49 18.59 18.06 o -4 15 1 35.47 15.58 18.66 o -2 15 1 34.19 36.79 23.62 o 0 15 1 27.99 25.60 17.34 o 2 15 1 27.54 26.78 17.15 o 4 15 1 32.09 32.74 17.29 o -3 16 1 24.83 16.83 26.73 o -1 16 1 24.94 20.58 22.12 o 1 16 1 25.73 32.03 22.56 o -16 0 2 44.52 39.90 37.80 o -14 0 2 94.74 101.84 22.05 o -12 0 2 35.33 32.55 13.65 o -10 0 2 604.44 567.99 25.20 o -8 0 2 1798.53 1613.71 33.61 o -6 0 2 1082.96 1069.86 20.99 o -4 0 2 360.88 368.53 7.35 o -2 0 2 9406.01 7376.68 109.20 o 0 0 2 10990.90 7334.69 228.86 o 2 0 2 721.24 693.98 12.62 o 4 0 2 70.05 71.39 4.20 o 6 0 2 5.19 5.25 3.15 o 8 0 2 843.98 874.57 27.28 o 10 0 2 126.19 121.79 15.75 o 12 0 2 60.02 57.75 25.20 o 14 0 2 38.70 44.10 31.50 o -15 1 2 39.30 37.22 16.87 o -13 1 2 59.35 62.99 18.37 o -11 1 2 55.03 50.05 8.82 o -9 1 2 574.41 593.06 15.21 o -7 1 2 1483.07 1681.60 25.96 o -5 1 2 13.01 14.66 2.62 o -3 1 2 3553.45 3256.86 39.36 o -1 1 2 33064.87 31594.50 1025.77 o 1 1 2 379.16 319.64 4.78 o 3 1 2 356.90 292.09 12.07 o 5 1 2 1369.48 1417.78 22.44 o 7 1 2 850.65 814.35 23.76 o 9 1 2 428.70 407.32 15.23 o 11 1 2 160.28 156.63 18.37 o 13 1 2 6.51 16.65 12.60 o -14 2 2 91.51 79.37 17.96 o -12 2 2 203.07 196.89 12.62 o -10 2 2 404.28 361.68 24.15 o -8 2 2 71.78 59.33 5.20 o -6 2 2 61.36 74.02 2.97 o -4 2 2 353.55 336.01 8.93 o -2 2 2 2212.98 2321.32 108.67 o 0 2 2 5868.24 5105.43 274.54 o 2 2 2 29.43 30.13 1.75 o 4 2 2 146.98 112.93 4.46 o 6 2 2 4.63 2.77 7.35 o 8 2 2 196.89 231.20 10.00 o 10 2 2 183.90 191.40 12.60 o 12 2 2 130.26 164.35 17.09 o 14 2 2 42.56 37.80 16.88 o -15 3 2 37.64 65.39 18.43 o -13 3 2 146.73 125.85 14.35 o -11 3 2 227.02 203.21 12.60 o -9 3 2 325.01 424.04 12.11 o -7 3 2 167.68 210.31 7.35 o -5 3 2 2132.35 2117.98 40.43 o -3 3 2 1045.34 1156.14 18.91 o -1 3 2 43.67 40.61 2.63 o 1 3 2 936.99 986.29 30.45 o 3 3 2 3526.26 3557.43 42.51 o 5 3 2 1966.76 1977.31 33.76 o 7 3 2 890.34 836.88 26.77 o 9 3 2 270.90 311.64 12.10 o 11 3 2 170.43 166.75 16.27 o 13 3 2 59.03 102.83 16.40 o -14 4 2 69.75 84.91 23.62 o -12 4 2 416.69 440.29 38.84 o -10 4 2 113.28 86.75 7.77 o -8 4 2 6.90 3.99 4.20 o -6 4 2 1868.30 1900.52 29.26 o -4 4 2 2802.03 2630.91 35.95 o -2 4 2 134.78 141.81 3.15 o 0 4 2 31.73 36.93 4.72 o 2 4 2 175.77 191.31 7.87 o 4 4 2 1294.44 1444.96 19.39 o 6 4 2 610.14 558.21 14.05 o 8 4 2 36.79 33.12 5.53 o 10 4 2 152.56 121.73 10.75 o 12 4 2 212.99 205.81 20.16 o 14 4 2 43.11 56.69 21.36 o -15 5 2 28.08 23.17 20.00 o -13 5 2 84.72 74.96 19.39 o -11 5 2 97.88 98.53 10.23 o -9 5 2 90.95 91.30 7.87 o -7 5 2 72.33 59.84 4.20 o -5 5 2 803.33 859.33 29.39 o -3 5 2 1244.96 1266.87 41.47 o -1 5 2 59.07 69.71 3.28 o 1 5 2 1558.43 1482.56 24.14 o 3 5 2 361.76 432.82 11.56 o 5 5 2 333.00 371.44 8.32 o 7 5 2 431.05 454.26 14.84 o 9 5 2 49.75 46.58 7.56 o 11 5 2 72.37 57.86 10.65 o 13 5 2 77.92 87.28 17.09 o -14 6 2 26.74 68.79 22.12 o -12 6 2 258.12 259.66 19.16 o -10 6 2 59.67 56.66 9.18 o -8 6 2 69.93 85.57 5.53 o -6 6 2 1323.15 1240.27 25.73 o -4 6 2 797.78 806.32 12.55 o -2 6 2 477.45 462.98 7.77 o 0 6 2 1320.89 1343.97 17.63 o 2 6 2 11.01 15.06 2.52 o 4 6 2 678.94 765.74 14.56 o 6 6 2 530.46 571.45 15.84 o 8 6 2 27.39 9.71 7.87 o 10 6 2 190.83 201.16 12.98 o 12 6 2 111.51 126.89 17.15 o -13 7 2 12.84 24.94 16.80 o -11 7 2 169.92 195.49 15.21 o -9 7 2 271.74 269.93 19.42 o -7 7 2 147.70 143.54 7.35 o -5 7 2 286.56 272.98 13.65 o -3 7 2 1231.26 1205.50 22.69 o -1 7 2 642.60 628.36 17.85 o 1 7 2 1698.37 1632.14 30.98 o 3 7 2 519.74 536.38 32.55 o 5 7 2 287.18 306.14 10.48 o 7 7 2 324.28 338.28 12.60 o 9 7 2 270.26 292.37 15.54 o 11 7 2 41.24 37.88 15.22 o 13 7 2 18.73 28.66 18.43 o -14 8 2 12.82 20.07 27.17 o -12 8 2 47.59 43.40 17.09 o -10 8 2 189.85 211.21 17.15 o -8 8 2 192.72 190.27 13.65 o -6 8 2 79.32 73.31 8.93 o -4 8 2 8.64 13.58 2.70 o -2 8 2 300.54 304.52 8.07 o 0 8 2 273.36 256.39 7.35 o 2 8 2 18.99 13.21 4.27 o 4 8 2 168.54 176.14 16.27 o 6 8 2 53.84 49.33 11.02 o 8 8 2 112.12 119.97 12.85 o 10 8 2 149.34 139.86 13.72 o 12 8 2 12.67 -3.57 22.05 o -13 9 2 2.85 10.68 21.44 o -11 9 2 57.21 43.89 16.69 o -9 9 2 251.05 224.88 14.15 o -7 9 2 237.55 218.12 12.04 o -5 9 2 5.39 2.83 4.78 o -3 9 2 47.98 44.63 8.93 o -1 9 2 934.60 1050.93 32.55 o 1 9 2 594.58 555.30 12.55 o 3 9 2 33.38 34.18 5.04 o 5 9 2 110.46 129.08 11.06 o 7 9 2 276.49 265.63 14.15 o 9 9 2 205.70 208.18 30.97 o 11 9 2 10.58 22.54 46.72 o -12 10 2 10.94 0.23 21.00 o -10 10 2 57.74 39.32 21.52 o -8 10 2 212.05 192.87 13.50 o -6 10 2 152.52 138.44 15.22 o -4 10 2 27.53 27.94 7.87 o -2 10 2 235.89 244.60 8.82 o 0 10 2 306.69 330.12 10.49 o 2 10 2 132.57 152.94 8.54 o 4 10 2 88.13 93.38 10.70 o 6 10 2 94.80 99.04 11.26 o 8 10 2 143.13 160.60 22.57 o 10 10 2 27.41 37.22 18.90 o -11 11 2 15.92 9.67 22.39 o -9 11 2 12.55 9.06 11.75 o -7 11 2 170.06 161.78 15.75 o -5 11 2 107.74 95.24 10.50 o -3 11 2 3.58 10.12 7.29 o -1 11 2 275.08 272.71 24.15 o 1 11 2 88.21 82.36 7.77 o 3 11 2 20.73 11.26 7.77 o 5 11 2 152.78 142.41 13.36 o 7 11 2 57.33 66.67 18.90 o 9 11 2 16.74 5.85 12.60 o -10 12 2 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