#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:02:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180909 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/50/2105038.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2105038_Fobs loop_ _publ_author_name 'Joseph, Sumy' 'Sathishkumar, Ranganathan' 'Mahapatra, Sudarshan' 'Desiraju, Gautam R.' _publ_section_title ; Crystal packing and melting temperatures of small oxalate esters: the role of C---H···O hydrogen bonding ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 525 _journal_page_last 534 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 118.225 _cell_angle_gamma 90.000 _cell_length_a 11.1000 _cell_length_b 10.6350 _cell_length_c 11.2430 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.8279 _cod_data_source_file og5050DtBO125sup18.hkl _cod_data_source_block DtBO125 #BEGIN Tags that were not found in dictionaries: _shelx_title ' DATAM in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 96.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2024.70 1798.15 47.19 o 3 0 0 1281.31 1246.51 41.23 o 4 0 0 486.51 454.92 8.42 o 5 0 0 59.57 60.21 3.04 o 6 0 0 1073.57 1126.22 35.77 o 7 0 0 560.45 611.74 9.11 o 8 0 0 347.15 376.41 7.38 o 9 0 0 5.48 8.27 1.37 o 10 0 0 437.72 465.85 31.92 o 11 0 0 15.26 17.66 2.38 o 1 1 0 1660.16 1455.69 17.63 o 2 1 0 197.81 179.79 6.84 o 3 1 0 562.94 550.99 10.16 o 4 1 0 3.74 4.00 0.40 o 5 1 0 81.91 83.26 1.32 o 6 1 0 48.74 43.09 2.11 o 7 1 0 455.26 456.91 6.05 o 8 1 0 0.73 0.92 0.40 o 9 1 0 8.24 5.45 0.64 o 10 1 0 21.84 23.30 2.07 o 11 1 0 24.07 20.11 1.90 o 0 2 0 4.55 3.40 0.63 o 1 2 0 9337.69 8731.61 109.54 o 2 2 0 471.09 409.42 9.42 o 3 2 0 2.03 3.28 0.37 o 4 2 0 714.77 757.48 14.39 o 5 2 0 248.25 232.41 4.68 o 6 2 0 3.39 2.30 0.46 o 7 2 0 2.29 2.12 0.33 o 8 2 0 11.98 8.81 0.86 o 9 2 0 50.87 45.52 2.13 o 10 2 0 48.06 43.26 2.49 o 11 2 0 0.04 2.31 0.77 o 1 3 0 982.36 1059.88 23.62 o 2 3 0 27.33 27.99 1.51 o 3 3 0 982.56 973.45 25.27 o 4 3 0 291.38 269.91 6.31 o 5 3 0 282.81 260.40 4.67 o 6 3 0 2.43 3.86 0.66 o 7 3 0 23.93 22.87 1.38 o 8 3 0 155.41 165.68 3.35 o 9 3 0 118.43 129.24 5.76 o 10 3 0 6.33 4.93 0.64 o 11 3 0 1.15 1.16 0.82 o 0 4 0 198.31 219.66 7.87 o 1 4 0 563.60 540.15 11.51 o 2 4 0 431.09 401.42 8.59 o 3 4 0 1957.95 2047.79 62.26 o 4 4 0 217.67 211.12 6.09 o 5 4 0 195.48 210.15 6.77 o 6 4 0 28.95 30.59 2.56 o 7 4 0 210.42 211.26 9.11 o 8 4 0 172.90 157.75 5.16 o 9 4 0 302.80 294.67 12.85 o 10 4 0 157.50 180.62 8.96 o 11 4 0 1.23 2.81 0.70 o 1 5 0 101.69 107.62 2.97 o 2 5 0 510.15 519.61 10.52 o 3 5 0 39.28 38.97 2.08 o 4 5 0 199.21 205.81 3.93 o 5 5 0 99.24 104.01 2.49 o 6 5 0 163.94 174.26 8.02 o 7 5 0 499.74 483.34 19.78 o 8 5 0 360.94 385.55 14.53 o 9 5 0 5.50 4.97 0.74 o 10 5 0 8.08 5.35 1.44 o 0 6 0 257.35 303.75 15.95 o 1 6 0 102.17 104.52 1.74 o 2 6 0 116.39 105.85 2.68 o 3 6 0 145.86 136.39 3.81 o 4 6 0 124.57 130.16 2.99 o 5 6 0 9.71 8.11 0.85 o 6 6 0 203.64 213.30 8.90 o 7 6 0 2.13 1.52 1.07 o 8 6 0 9.35 7.58 1.16 o 9 6 0 74.73 75.64 4.79 o 10 6 0 7.98 6.13 1.12 o 1 7 0 17.89 18.93 1.32 o 2 7 0 382.69 415.74 8.10 o 3 7 0 86.48 80.03 3.03 o 4 7 0 94.82 76.86 3.71 o 5 7 0 0.28 1.44 1.31 o 6 7 0 1.06 1.41 1.09 o 7 7 0 3.54 3.87 1.09 o 8 7 0 121.54 120.88 8.15 o 9 7 0 57.12 64.90 5.49 o 0 8 0 20.51 19.85 2.40 o 1 8 0 164.87 177.00 3.39 o 2 8 0 429.89 423.86 11.96 o 3 8 0 116.83 112.16 4.67 o 4 8 0 133.11 133.38 6.16 o 5 8 0 52.19 47.70 3.87 o 6 8 0 292.72 309.90 14.36 o 7 8 0 2.50 3.85 0.74 o 8 8 0 7.39 7.04 1.06 o 9 8 0 20.92 23.10 3.42 o 1 9 0 552.94 583.17 14.55 o 2 9 0 51.83 53.40 2.54 o 3 9 0 248.06 240.75 6.82 o 4 9 0 232.51 217.11 12.78 o 5 9 0 277.90 264.22 19.03 o 6 9 0 31.14 30.03 2.92 o 7 9 0 0.01 0.62 0.95 o 8 9 0 17.74 19.48 2.80 o 0 10 0 14.83 12.28 1.26 o 1 10 0 201.92 192.09 3.95 o 2 10 0 99.41 98.79 5.49 o 3 10 0 136.97 134.44 5.60 o 4 10 0 118.44 122.99 6.08 o 5 10 0 18.97 19.35 1.90 o 6 10 0 4.19 5.48 0.95 o 7 10 0 16.00 15.93 1.99 o 1 11 0 31.93 30.27 1.78 o 2 11 0 46.35 44.23 4.23 o 3 11 0 41.25 36.21 3.39 o 4 11 0 0.69 1.03 1.00 o 5 11 0 0.31 2.20 0.96 o 6 11 0 36.20 43.99 3.59 o 0 12 0 36.76 32.00 3.55 o 1 12 0 137.67 141.90 5.52 o 2 12 0 140.73 161.44 5.29 o 3 12 0 19.80 19.89 2.01 o 4 12 0 70.82 78.69 6.52 o -12 1 1 33.51 36.38 3.59 o -11 1 1 31.56 27.27 2.98 o -10 1 1 295.22 288.72 8.05 o -9 1 1 87.23 74.94 2.41 o -8 1 1 116.42 109.22 3.52 o -7 1 1 28.20 28.60 1.49 o -6 1 1 566.34 593.77 7.94 o -5 1 1 1444.08 1506.63 27.65 o -4 1 1 181.36 173.92 2.70 o -3 1 1 163.11 169.58 3.18 o -2 1 1 2410.16 2315.17 48.23 o -1 1 1 71.62 53.89 0.72 o 0 1 1 5672.89 4947.99 87.91 o 1 1 1 227.31 198.30 4.97 o 2 1 1 701.21 636.76 19.35 o 3 1 1 791.21 760.52 15.09 o 4 1 1 1736.09 1812.35 36.33 o 5 1 1 38.48 38.30 1.67 o 6 1 1 8.25 13.02 1.05 o 7 1 1 45.52 50.00 2.57 o 8 1 1 17.88 15.22 1.45 o 9 1 1 28.56 28.03 1.52 o 10 1 1 137.42 134.26 3.54 o 11 1 1 6.85 10.02 1.13 o -12 2 1 60.47 60.46 7.03 o -11 2 1 32.76 28.28 1.77 o -10 2 1 78.24 78.60 4.73 o -9 2 1 6.00 5.53 0.68 o -8 2 1 23.03 21.32 1.60 o -7 2 1 460.79 477.05 8.27 o -6 2 1 7.55 5.27 0.50 o -5 2 1 287.52 305.75 7.30 o -4 2 1 727.36 764.35 17.10 o -3 2 1 2.60 3.78 0.45 o -2 2 1 2794.50 2651.39 49.35 o -1 2 1 400.40 354.01 8.60 o 0 2 1 4684.70 4305.97 138.71 o 1 2 1 1702.88 1485.76 36.14 o 2 2 1 274.22 282.99 7.71 o 3 2 1 4502.97 4526.86 120.17 o 4 2 1 10.61 13.68 1.03 o 5 2 1 817.27 867.67 18.05 o 6 2 1 126.32 110.60 2.99 o 7 2 1 1.01 2.95 0.72 o 8 2 1 59.70 57.96 3.18 o 9 2 1 178.21 181.48 5.76 o 10 2 1 100.00 101.69 4.29 o 11 2 1 6.85 7.42 1.06 o -11 3 1 18.81 18.30 1.97 o -10 3 1 16.09 13.55 1.29 o -9 3 1 121.64 107.53 4.40 o -8 3 1 73.97 73.20 3.64 o -7 3 1 343.76 334.93 4.88 o -6 3 1 104.20 100.43 1.53 o -5 3 1 535.05 511.39 13.07 o -4 3 1 200.10 195.02 5.56 o -3 3 1 331.86 312.35 6.20 o -2 3 1 0.67 1.13 0.40 o -1 3 1 0.51 2.59 0.79 o 0 3 1 37.14 34.83 1.42 o 1 3 1 62.68 70.26 1.42 o 2 3 1 88.00 84.58 2.39 o 3 3 1 378.50 348.29 7.28 o 4 3 1 9.67 9.86 0.86 o 5 3 1 177.96 157.81 4.94 o 6 3 1 137.59 129.59 2.94 o 7 3 1 73.84 75.23 2.98 o 8 3 1 177.19 175.50 5.33 o 9 3 1 27.83 23.32 1.77 o 10 3 1 54.96 54.98 3.35 o -11 4 1 9.05 8.55 1.27 o -10 4 1 57.75 65.19 5.16 o -9 4 1 12.83 11.96 1.31 o -8 4 1 53.40 49.26 3.68 o -7 4 1 376.04 371.67 10.14 o -6 4 1 411.12 404.30 11.43 o -5 4 1 685.41 725.06 20.07 o -4 4 1 26.80 28.75 1.59 o -3 4 1 18.69 18.01 1.14 o -2 4 1 641.78 662.21 14.28 o -1 4 1 22.58 20.20 1.05 o 0 4 1 182.02 180.49 4.56 o 1 4 1 894.81 825.01 23.01 o 2 4 1 1141.79 1143.29 29.16 o 3 4 1 1773.63 1928.54 51.98 o 4 4 1 10.99 7.21 0.71 o 5 4 1 376.51 384.64 11.27 o 6 4 1 95.90 89.55 3.34 o 7 4 1 12.72 8.62 0.87 o 8 4 1 307.08 317.50 9.29 o 9 4 1 0.16 0.32 0.89 o 10 4 1 0.01 2.07 0.78 o -11 5 1 30.60 29.27 2.76 o -10 5 1 5.11 3.82 0.93 o -9 5 1 365.88 395.85 20.06 o -8 5 1 5.47 9.20 1.32 o -7 5 1 35.83 36.02 2.99 o -6 5 1 415.50 405.75 13.82 o -5 5 1 281.54 283.30 10.73 o -4 5 1 61.27 57.98 2.64 o -3 5 1 46.06 40.60 2.53 o -2 5 1 723.96 765.32 13.43 o -1 5 1 390.77 413.84 13.02 o 0 5 1 0.00 1.23 0.49 o 1 5 1 392.59 416.78 11.76 o 2 5 1 205.19 199.40 6.13 o 3 5 1 49.58 58.10 2.55 o 4 5 1 3.60 2.07 0.33 o 5 5 1 11.50 8.86 0.93 o 6 5 1 145.56 142.86 3.11 o 7 5 1 708.46 726.35 32.85 o 8 5 1 76.73 74.98 4.82 o 9 5 1 12.45 14.27 1.92 o 10 5 1 1.50 1.61 1.04 o -10 6 1 24.70 26.25 3.23 o -9 6 1 7.17 9.06 1.15 o -8 6 1 656.78 718.96 36.63 o -7 6 1 0.81 1.87 1.06 o -6 6 1 739.28 711.46 22.43 o -5 6 1 210.90 203.06 8.05 o -4 6 1 1249.20 1419.78 54.02 o -3 6 1 0.01 0.27 0.42 o -2 6 1 507.66 497.31 9.32 o -1 6 1 261.29 269.04 6.10 o 0 6 1 802.48 767.10 17.64 o 1 6 1 106.34 109.53 2.69 o 2 6 1 502.81 570.56 16.50 o 3 6 1 13.49 13.33 0.87 o 4 6 1 707.13 700.18 21.10 o 5 6 1 16.03 14.93 1.34 o 6 6 1 917.36 938.56 32.61 o 7 6 1 54.51 57.04 4.30 o 8 6 1 76.84 73.08 5.75 o 9 6 1 41.39 40.92 3.90 o -10 7 1 0.02 0.81 0.96 o -9 7 1 7.73 9.40 1.18 o -8 7 1 76.02 77.72 4.32 o -7 7 1 131.60 134.59 7.29 o -6 7 1 71.07 72.74 4.36 o -5 7 1 21.89 19.11 1.46 o -4 7 1 301.21 290.14 11.32 o -3 7 1 0.11 1.11 1.05 o -2 7 1 92.82 109.10 2.02 o -1 7 1 87.53 96.74 2.63 o 0 7 1 29.53 30.11 1.88 o 1 7 1 68.49 71.40 1.64 o 2 7 1 28.92 23.55 1.63 o 3 7 1 38.58 33.86 2.48 o 4 7 1 51.99 57.12 3.08 o 5 7 1 96.76 103.98 2.40 o 6 7 1 0.24 -0.68 0.88 o 7 7 1 3.08 4.36 1.00 o 8 7 1 154.55 152.90 13.05 o 9 7 1 11.33 13.17 1.49 o -9 8 1 100.73 103.82 7.11 o -8 8 1 0.02 -0.48 0.92 o -7 8 1 267.09 269.15 14.08 o -6 8 1 54.32 55.09 5.31 o -5 8 1 132.32 133.82 6.01 o -4 8 1 37.28 34.03 3.06 o -3 8 1 241.04 231.44 8.87 o -2 8 1 60.30 62.17 2.26 o -1 8 1 204.88 216.27 4.83 o 0 8 1 87.76 79.05 3.03 o 1 8 1 70.81 61.89 1.96 o 2 8 1 28.44 29.71 1.64 o 3 8 1 0.23 1.59 0.64 o 4 8 1 129.81 131.37 3.49 o 5 8 1 215.69 214.18 10.95 o 6 8 1 17.77 19.23 2.18 o 7 8 1 93.31 92.05 6.30 o 8 8 1 18.54 21.56 2.30 o -8 9 1 1.40 2.70 0.98 o -7 9 1 32.14 37.90 2.76 o -6 9 1 148.30 143.91 7.82 o -5 9 1 108.14 98.52 7.70 o -4 9 1 34.74 32.63 2.85 o -3 9 1 43.60 49.31 2.28 o -2 9 1 19.42 17.88 1.21 o -1 9 1 0.59 0.71 0.68 o 0 9 1 32.36 33.21 1.59 o 1 9 1 295.68 301.79 5.42 o 2 9 1 26.14 27.76 1.48 o 3 9 1 239.74 247.19 6.30 o 4 9 1 0.06 0.18 0.70 o 5 9 1 51.98 55.02 4.04 o 6 9 1 5.30 5.20 0.97 o 7 9 1 28.48 33.48 2.85 o -7 10 1 0.67 0.99 0.81 o -6 10 1 1.10 2.13 1.77 o -5 10 1 93.99 85.32 6.52 o -4 10 1 27.95 27.93 2.26 o -3 10 1 1.97 1.57 0.58 o -2 10 1 8.64 6.61 0.88 o -1 10 1 963.78 1032.28 25.58 o 0 10 1 34.82 33.12 2.59 o 1 10 1 24.66 24.42 1.94 o 2 10 1 52.78 49.14 3.84 o 3 10 1 55.86 53.10 3.90 o 4 10 1 15.36 13.88 1.41 o 5 10 1 22.06 17.07 1.50 o 6 10 1 13.34 13.72 1.68 o -6 11 1 1.35 1.45 0.69 o -5 11 1 15.67 16.41 1.69 o -4 11 1 0.60 1.83 0.58 o -3 11 1 42.33 45.86 3.51 o -2 11 1 46.77 50.62 2.67 o -1 11 1 0.07 0.76 0.58 o 0 11 1 24.07 19.50 1.35 o 1 11 1 61.23 62.75 3.20 o 2 11 1 0.05 0.54 0.63 o 3 11 1 28.52 28.09 1.76 o 4 11 1 3.73 4.27 1.01 o 5 11 1 158.69 171.28 9.00 o -4 12 1 8.90 5.70 0.89 o -3 12 1 0.11 0.80 0.67 o -2 12 1 0.06 0.22 0.74 o -1 12 1 29.89 26.23 1.80 o 0 12 1 11.90 11.43 1.04 o 1 12 1 2.35 2.97 0.60 o 2 12 1 0.94 1.48 0.66 o 3 12 1 0.38 1.70 0.63 o -12 0 2 205.90 213.42 10.10 o -11 0 2 13.13 14.14 2.42 o -10 0 2 29.13 24.60 2.90 o -9 0 2 4.22 3.29 0.89 o -8 0 2 298.45 317.05 6.18 o -7 0 2 1.93 2.21 0.73 o -6 0 2 0.17 0.44 0.47 o -5 0 2 1381.49 1442.90 13.46 o -4 0 2 2613.80 2597.07 11.92 o -3 0 2 1212.88 1174.34 6.14 o -1 0 2 106.51 113.65 3.53 o 0 0 2 1510.76 1288.44 48.47 o 1 0 2 276.46 277.97 10.31 o 2 0 2 4507.25 4091.99 31.22 o 3 0 2 76.05 72.37 5.61 o 4 0 2 1970.75 2038.95 93.88 o 5 0 2 376.51 356.11 14.39 o 6 0 2 1342.63 1446.11 48.61 o 7 0 2 4.16 3.62 0.88 o 8 0 2 615.72 630.90 15.99 o 9 0 2 8.45 8.49 3.18 o 10 0 2 1.96 1.82 1.68 o -12 1 2 59.73 60.26 5.60 o -11 1 2 247.35 257.62 6.41 o -10 1 2 3.36 4.42 0.54 o -9 1 2 9.74 11.23 0.96 o -8 1 2 34.91 31.59 1.45 o -7 1 2 406.19 398.39 6.04 o -6 1 2 189.37 196.92 3.94 o -5 1 2 395.31 381.67 6.37 o -4 1 2 380.44 383.80 3.59 o -3 1 2 2104.93 2125.24 43.24 o -2 1 2 87.68 90.63 0.93 o -1 1 2 463.93 451.76 9.33 o 0 1 2 435.40 414.48 7.98 o 1 1 2 532.79 510.04 7.63 o 2 1 2 762.36 745.72 18.67 o 3 1 2 196.68 195.98 7.22 o 4 1 2 337.42 344.43 10.45 o 5 1 2 417.65 383.89 10.97 o 6 1 2 54.58 42.10 3.06 o 7 1 2 90.71 82.17 4.09 o 8 1 2 0.79 0.60 0.81 o 9 1 2 66.28 77.50 3.96 o 10 1 2 33.67 32.99 3.29 o -12 2 2 22.22 20.73 1.74 o -11 2 2 27.25 26.69 2.30 o -10 2 2 102.52 104.16 5.01 o -9 2 2 0.03 0.72 0.59 o -8 2 2 9.32 7.44 0.71 o -7 2 2 0.30 0.94 0.46 o -6 2 2 81.78 80.01 3.36 o -5 2 2 0.63 2.00 0.67 o -4 2 2 398.19 392.83 8.51 o -3 2 2 39.55 41.70 1.66 o -2 2 2 505.57 497.17 11.18 o -1 2 2 7050.00 6691.47 146.56 o 0 2 2 36.85 31.94 1.78 o 1 2 2 1535.06 1541.23 18.93 o 2 2 2 2323.65 2337.10 41.36 o 3 2 2 283.35 291.11 5.79 o 4 2 2 259.95 295.62 7.32 o 5 2 2 76.27 77.35 2.26 o 6 2 2 54.02 53.72 2.02 o 7 2 2 265.91 257.37 5.82 o 8 2 2 309.04 303.24 9.24 o 9 2 2 49.59 41.02 2.39 o 10 2 2 61.55 66.33 4.19 o -12 3 2 17.01 15.84 1.65 o -11 3 2 79.70 87.83 3.69 o -10 3 2 51.35 47.18 2.56 o -9 3 2 89.64 88.32 4.00 o -8 3 2 172.73 152.04 5.97 o -7 3 2 15.06 16.07 1.28 o -6 3 2 20.36 18.55 1.47 o -5 3 2 794.44 796.18 21.46 o -4 3 2 1.75 1.05 0.49 o -3 3 2 288.22 290.88 8.02 o -2 3 2 1811.87 1812.82 46.52 o -1 3 2 21.91 18.85 1.06 o 0 3 2 152.03 143.47 3.24 o 1 3 2 2086.23 2117.80 44.68 o 2 3 2 9.29 9.93 0.76 o 3 3 2 2071.73 2178.73 55.44 o 4 3 2 0.92 1.85 0.42 o 5 3 2 3.68 7.47 0.79 o 6 3 2 297.16 290.97 9.67 o 7 3 2 387.11 404.92 12.04 o 8 3 2 13.49 15.34 1.23 o 9 3 2 46.88 40.09 2.82 o 10 3 2 44.57 47.60 4.55 o -12 4 2 149.17 168.19 8.64 o -11 4 2 42.17 41.14 3.87 o -10 4 2 92.79 89.89 8.48 o -9 4 2 224.14 236.93 10.69 o -8 4 2 2.03 1.04 0.46 o -7 4 2 0.44 0.61 0.41 o -6 4 2 654.95 659.03 18.92 o -5 4 2 186.56 193.13 5.69 o -4 4 2 597.12 571.35 14.86 o -3 4 2 1254.47 1331.80 30.07 o -2 4 2 0.96 0.86 0.38 o -1 4 2 1156.45 1137.68 22.79 o 0 4 2 0.39 0.10 0.59 o 1 4 2 2370.90 2465.05 54.28 o 2 4 2 1414.68 1516.94 41.82 o 3 4 2 1319.61 1420.53 39.35 o 4 4 2 0.20 1.65 0.49 o 5 4 2 545.02 560.49 16.61 o 6 4 2 160.61 161.97 4.70 o 7 4 2 756.27 752.21 25.34 o 8 4 2 91.96 87.63 6.86 o 9 4 2 11.94 8.95 0.99 o 10 4 2 10.02 7.51 1.26 o -11 5 2 35.42 33.23 3.19 o -10 5 2 222.81 247.04 14.08 o -9 5 2 226.69 253.86 13.68 o -8 5 2 34.49 31.76 2.39 o -7 5 2 400.33 400.10 17.48 o -6 5 2 120.54 128.31 4.61 o -5 5 2 9.05 10.35 0.87 o -4 5 2 314.02 345.17 12.54 o -3 5 2 7.33 8.14 0.61 o -2 5 2 300.38 305.45 6.92 o -1 5 2 677.13 695.79 15.58 o 0 5 2 457.31 489.26 14.39 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